#------------------------------------------------------------------------------
#$Date: 2016-03-24 01:32:20 +0200 (Thu, 24 Mar 2016) $
#$Revision: 179534 $
#$URL: svn://www.crystallography.net/cod/cif/4/50/03/4500393.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4500393
loop_
_publ_author_name
'Mu, Yajuan'
'Fu, Junhong'
'Song, Yajing'
'Li, Zhen'
'Hou, Hongwei'
'Fan, Yaoting'
_publ_section_title
;
 Hydrothermal Syntheses of Metal--Organic Frameworks Constructed from
 Aromatic Polycarboxylate and
 4,4′-Bis(1,2,4-triazol-1-ylmethyl)biphenyl
;
_journal_issue                   6
_journal_name_full               'Crystal Growth & Design'
_journal_page_first              2183
_journal_paper_doi               10.1021/cg101494t
_journal_volume                  11
_journal_year                    2011
_chemical_formula_sum            'C26 H20 Cu N6 O4'
_chemical_formula_weight         544.02
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                93.68(3)
_cell_angle_beta                 105.18(3)
_cell_angle_gamma                92.97(3)
_cell_formula_units_Z            2
_cell_length_a                   8.2582(17)
_cell_length_b                   11.067(2)
_cell_length_c                   14.080(3)
_cell_measurement_reflns_used    3350
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      27.7534
_cell_measurement_theta_min      1.8486
_cell_volume                     1236.2(5)
_computing_cell_refinement       CrystalClear
_computing_data_collection       CrystalClear
_computing_data_reduction        CrystalClear
_computing_publication_material  'CrystalStructure 3.7.0'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.987
_diffrn_measured_fraction_theta_max 0.987
_diffrn_measurement_device_type  'Rigaku Saturn'
_diffrn_measurement_method       ω
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0476
_diffrn_reflns_av_sigmaI/netI    0.0544
_diffrn_reflns_limit_h_max       9
_diffrn_reflns_limit_h_min       -9
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       16
_diffrn_reflns_limit_l_min       -16
_diffrn_reflns_number            12230
_diffrn_reflns_theta_full        24.99
_diffrn_reflns_theta_max         24.99
_diffrn_reflns_theta_min         2.29
_exptl_absorpt_coefficient_mu    0.928
_exptl_absorpt_correction_T_max  0.8361
_exptl_absorpt_correction_T_min  0.7681
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'Jacobson, R. (1998) Private communication'
_exptl_crystal_colour            Blue
_exptl_crystal_density_diffrn    1.462
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Prism
_exptl_crystal_F_000             558
_exptl_crystal_size_max          0.30
_exptl_crystal_size_mid          0.28
_exptl_crystal_size_min          0.20
_refine_diff_density_max         0.534
_refine_diff_density_min         -0.354
_refine_diff_density_rms         0.064
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.160
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     337
_refine_ls_number_reflns         4286
_refine_ls_number_restraints     6
_refine_ls_restrained_S_all      1.174
_refine_ls_R_factor_all          0.1140
_refine_ls_R_factor_gt           0.0863
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0687P)²+1.3565P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1787
_refine_ls_wR_factor_ref         0.1960
_reflns_number_gt                3227
_reflns_number_total             4286
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            cg101494t_si_002.cif
_cod_data_source_block           complex_6
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_absorpt_correction_type' value 'Multi-scan' changed to
'multi-scan' according to
/home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 
;
_cod_original_cell_volume        1236.2(4)
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               4500393
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Cu1 Cu 0.5000 0.0000 1.0000 0.0618(4) Uani 1 2 d S
Cu2 Cu 0.5000 0.0000 0.5000 0.0786(4) Uani 1 2 d S
N1 N 0.4628(8) 0.1605(4) 0.9428(3) 0.0774(16) Uani 1 1 d .
N2 N 0.4556(12) 0.3606(6) 0.9334(6) 0.120(3) Uani 1 1 d .
N3 N 0.3550(8) 0.3014(5) 0.8504(4) 0.0782(16) Uani 1 1 d .
N4 N 0.2953(7) -0.0096(6) 0.3884(4) 0.0902(19) Uani 1 1 d .
N5 N 0.0351(9) -0.0656(8) 0.2907(7) 0.141(4) Uani 1 1 d .
N6 N 0.1430(7) -0.0374(6) 0.2355(5) 0.0890(19) Uani 1 1 d .
O1 O 0.2910(5) -0.0692(3) 0.9063(3) 0.0605(10) Uani 1 1 d .
O2 O 0.4833(5) -0.1047(4) 0.8268(3) 0.0638(10) Uani 1 1 d .
O3 O 0.3923(7) -0.1275(4) 0.5573(3) 0.0823(14) Uani 1 1 d .
O4 O 0.3141(6) 0.0229(4) 0.6444(3) 0.0720(12) Uani 1 1 d .
C1 C 0.5214(12) 0.2730(6) 0.9884(5) 0.107(3) Uani 1 1 d .
H1 H 0.5978 0.2865 1.0503 0.129 Uiso 1 1 calc R
C2 C 0.3603(9) 0.1821(5) 0.8568(5) 0.0686(17) Uani 1 1 d .
H2 H 0.3013 0.1230 0.8085 0.082 Uiso 1 1 calc R
C3 C 0.2495(10) 0.3666(7) 0.7719(5) 0.092(2) Uani 1 1 d .
H3A H 0.2129 0.4380 0.8017 0.110 Uiso 1 1 calc R
H3B H 0.1501 0.3146 0.7385 0.110 Uiso 1 1 calc R
C4 C 0.3393(8) 0.4059(6) 0.6956(5) 0.0694(17) Uani 1 1 d .
C5 C 0.3708(14) 0.5241(6) 0.6851(7) 0.139(4) Uani 1 1 d .
H5 H 0.3501 0.5824 0.7301 0.167 Uiso 1 1 calc R
C6 C 0.4341(14) 0.5611(6) 0.6080(6) 0.125(4) Uani 1 1 d .
H6 H 0.4513 0.6435 0.6015 0.150 Uiso 1 1 calc R
C7 C 0.4706(7) 0.4795(5) 0.5431(4) 0.0551(14) Uani 1 1 d .
C8 C 0.4522(11) 0.3613(6) 0.5589(5) 0.092(2) Uani 1 1 d .
H8 H 0.4843 0.3030 0.5182 0.110 Uiso 1 1 calc R
C9 C 0.3863(11) 0.3242(6) 0.6347(5) 0.093(2) Uani 1 1 d .
H9 H 0.3746 0.2419 0.6434 0.111 Uiso 1 1 calc R
C10 C 0.1343(11) -0.0446(9) 0.3831(8) 0.125(4) Uani 1 1 d .
H10 H 0.0953 -0.0535 0.4387 0.150 Uiso 1 1 calc R
C11 C 0.2934(10) -0.0041(6) 0.2931(6) 0.085(2) Uani 1 1 d .
H11 H 0.3859 0.0200 0.2710 0.102 Uiso 1 1 calc R
C12 C 0.0891(9) -0.0565(7) 0.1278(6) 0.089(2) Uani 1 1 d .
H12A H 0.1746 -0.0192 0.1009 0.107 Uiso 1 1 calc R
H12B H -0.0136 -0.0162 0.1037 0.107 Uiso 1 1 calc R
C13 C 0.0588(10) -0.1873(7) 0.0909(8) 0.095(3) Uani 1 1 d .
C14 C 0.1673(12) -0.2717(10) 0.1342(10) 0.149(4) Uani 1 1 d U
H14 H 0.2566 -0.2473 0.1888 0.179 Uiso 1 1 calc R
C15 C 0.1440(11) -0.3916(9) 0.0970(11) 0.174(6) Uani 1 1 d .
H15 H 0.2216 -0.4452 0.1263 0.209 Uiso 1 1 calc R
C16 C 0.0129(10) -0.4353(7) 0.0195(8) 0.103(3) Uani 1 1 d .
C17 C -0.0957(12) -0.3510(8) -0.0215(6) 0.101(3) Uani 1 1 d .
H17 H -0.1875 -0.3766 -0.0744 0.121 Uiso 1 1 calc R
C18 C -0.0742(12) -0.2297(8) 0.0128(6) 0.097(3) Uani 1 1 d .
H18 H -0.1510 -0.1762 -0.0175 0.116 Uiso 1 1 calc R
C19 C 0.2001(8) -0.1781(6) 0.6508(4) 0.0650(16) Uani 1 1 d .
C20 C 0.0828(12) -0.2520(8) 0.5798(5) 0.115(3) Uani 1 1 d .
H20 H 0.0801 -0.2488 0.5135 0.138 Uiso 1 1 calc R
C21 C -0.0319(13) -0.3316(10) 0.6065(9) 0.157(5) Uani 1 1 d .
H21 H -0.1061 -0.3847 0.5590 0.188 Uiso 1 1 calc R
C22 C -0.0338(12) -0.3306(10) 0.7051(8) 0.142(4) Uani 1 1 d .
H22 H -0.1131 -0.3802 0.7233 0.170 Uiso 1 1 calc R
C23 C 0.0798(9) -0.2574(7) 0.7747(6) 0.086(2) Uani 1 1 d .
H23 H 0.0774 -0.2574 0.8403 0.103 Uiso 1 1 calc R
C24 C 0.2016(7) -0.1812(5) 0.7494(4) 0.0579(14) Uani 1 1 d .
C25 C 0.3352(7) -0.1140(5) 0.8307(4) 0.0509(13) Uani 1 1 d .
C26 C 0.3097(8) -0.0859(5) 0.6170(4) 0.0633(15) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O1 Cu1 O1 180.00(17) 2_657 .
O1 Cu1 N1 89.7(2) 2_657 2_657
O1 Cu1 N1 90.3(2) . 2_657
O1 Cu1 N1 90.3(2) 2_657 .
O1 Cu1 N1 89.7(2) . .
N1 Cu1 N1 180.000(2) 2_657 .
O3 Cu2 O3 180.000(1) . 2_656
O3 Cu2 N4 91.7(2) . 2_656
O3 Cu2 N4 88.3(2) 2_656 2_656
O3 Cu2 N4 88.3(2) . .
O3 Cu2 N4 91.7(2) 2_656 .
N4 Cu2 N4 180.000(1) 2_656 .
C2 N1 C1 104.7(5) . .
C2 N1 Cu1 127.5(4) . .
C1 N1 Cu1 127.4(5) . .
C1 N2 N3 104.6(6) . .
C2 N3 N2 109.6(6) . .
C2 N3 C3 128.4(7) . .
N2 N3 C3 121.8(6) . .
C11 N4 C10 102.7(7) . .
C11 N4 Cu2 125.2(5) . .
C10 N4 Cu2 131.0(5) . .
C10 N5 N6 102.1(7) . .
C11 N6 N5 110.2(7) . .
C11 N6 C12 128.9(5) . .
N5 N6 C12 120.6(7) . .
C25 O1 Cu1 105.5(3) . .
C26 O3 Cu2 113.3(4) . .
N2 C1 N1 111.5(7) . .
N2 C1 H1 124.2 . .
N1 C1 H1 124.2 . .
N1 C2 N3 109.6(6) . .
N1 C2 H2 125.2 . .
N3 C2 H2 125.2 . .
N3 C3 C4 113.5(5) . .
N3 C3 H3A 108.9 . .
C4 C3 H3A 108.9 . .
N3 C3 H3B 108.9 . .
C4 C3 H3B 108.9 . .
H3A C3 H3B 107.7 . .
C5 C4 C9 117.3(6) . .
C5 C4 C3 121.1(6) . .
C9 C4 C3 121.6(6) . .
C4 C5 C6 121.5(7) . .
C4 C5 H5 119.3 . .
C6 C5 H5 119.3 . .
C7 C6 C5 121.1(6) . .
C7 C6 H6 119.5 . .
C5 C6 H6 119.5 . .
C6 C7 C8 117.1(5) . .
C6 C7 C7 120.6(6) . 2_666
C8 C7 C7 122.3(6) . 2_666
C7 C8 C9 121.7(6) . .
C7 C8 H8 119.1 . .
C9 C8 H8 119.1 . .
C4 C9 C8 120.9(6) . .
C4 C9 H9 119.6 . .
C8 C9 H9 119.6 . .
N5 C10 N4 114.2(7) . .
N5 C10 H10 122.9 . .
N4 C10 H10 122.9 . .
N6 C11 N4 110.7(6) . .
N6 C11 H11 124.7 . .
N4 C11 H11 124.7 . .
N6 C12 C13 113.2(6) . .
N6 C12 H12A 108.9 . .
C13 C12 H12A 108.9 . .
N6 C12 H12B 108.9 . .
C13 C12 H12B 108.9 . .
H12A C12 H12B 107.8 . .
C18 C13 C14 116.9(9) . .
C18 C13 C12 122.4(7) . .
C14 C13 C12 120.7(9) . .
C15 C14 C13 120.7(11) . .
C15 C14 H14 119.7 . .
C13 C14 H14 119.7 . .
C16 C15 C14 123.2(9) . .
C16 C15 H15 118.4 . .
C14 C15 H15 118.4 . .
C15 C16 C17 115.5(8) . .
C15 C16 C16 123.1(11) . 2_545
C17 C16 C16 121.5(12) . 2_545
C16 C17 C18 122.8(9) . .
C16 C17 H17 118.6 . .
C18 C17 H17 118.6 . .
C13 C18 C17 121.0(8) . .
C13 C18 H18 119.5 . .
C17 C18 H18 119.5 . .
C24 C19 C20 119.5(6) . .
C24 C19 C26 121.8(5) . .
C20 C19 C26 118.3(6) . .
C19 C20 C21 120.7(8) . .
C19 C20 H20 119.6 . .
C21 C20 H20 119.6 . .
C22 C21 C20 119.2(8) . .
C22 C21 H21 120.4 . .
C20 C21 H21 120.4 . .
C23 C22 C21 120.1(8) . .
C23 C22 H22 119.9 . .
C21 C22 H22 119.9 . .
C22 C23 C24 121.2(7) . .
C22 C23 H23 119.4 . .
C24 C23 H23 119.4 . .
C19 C24 C23 119.0(6) . .
C19 C24 C25 122.4(5) . .
C23 C24 C25 118.4(5) . .
O2 C25 O1 121.5(5) . .
O2 C25 C24 121.1(5) . .
O1 C25 C24 117.4(5) . .
O4 C26 O3 123.5(5) . .
O4 C26 C19 120.4(6) . .
O3 C26 C19 116.1(5) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Cu1 O1 1.961(4) 2_657
Cu1 O1 1.961(4) .
Cu1 N1 2.002(5) 2_657
Cu1 N1 2.002(5) .
Cu2 O3 1.956(4) .
Cu2 O3 1.956(4) 2_656
Cu2 N4 1.976(6) 2_656
Cu2 N4 1.976(6) .
N1 C2 1.327(8) .
N1 C1 1.367(8) .
N2 C1 1.329(10) .
N2 N3 1.349(9) .
N3 C2 1.331(7) .
N3 C3 1.471(8) .
N4 C11 1.343(8) .
N4 C10 1.347(9) .
N5 C10 1.342(12) .
N5 N6 1.365(7) .
N6 C11 1.313(9) .
N6 C12 1.462(9) .
O1 C25 1.291(6) .
O2 C25 1.238(6) .
O3 C26 1.291(7) .
O4 C26 1.236(7) .
C1 H1 0.9300 .
C2 H2 0.9300 .
C3 C4 1.528(8) .
C3 H3A 0.9700 .
C3 H3B 0.9700 .
C4 C5 1.345(9) .
C4 C9 1.348(9) .
C5 C6 1.397(9) .
C5 H5 0.9300 .
C6 C7 1.345(9) .
C6 H6 0.9300 .
C7 C8 1.349(8) .
C7 C7 1.506(10) 2_666
C8 C9 1.393(9) .
C8 H8 0.9300 .
C9 H9 0.9300 .
C10 H10 0.9300 .
C11 H11 0.9300 .
C12 C13 1.492(11) .
C12 H12A 0.9700 .
C12 H12B 0.9700 .
C13 C18 1.373(11) .
C13 C14 1.386(12) .
C14 C15 1.379(13) .
C14 H14 0.9300 .
C15 C16 1.363(14) .
C15 H15 0.9300 .
C16 C17 1.376(11) .
C16 C16 1.483(16) 2_545
C17 C18 1.383(11) .
C17 H17 0.9300 .
C18 H18 0.9300 .
C19 C24 1.388(7) .
C19 C20 1.383(9) .
C19 C26 1.509(8) .
C20 C21 1.399(12) .
C20 H20 0.9300 .
C21 C22 1.392(13) .
C21 H21 0.9300 .
C22 C23 1.354(11) .
C22 H22 0.9300 .
C23 C24 1.410(8) .
C23 H23 0.9300 .
C24 C25 1.492(8) .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
O1 Cu1 N1 C2 163.1(6) 2_657 .
O1 Cu1 N1 C2 -16.9(6) . .
N1 Cu1 N1 C2 -96(100) 2_657 .
O1 Cu1 N1 C1 -25.6(7) 2_657 .
O1 Cu1 N1 C1 154.4(7) . .
N1 Cu1 N1 C1 76(100) 2_657 .
C1 N2 N3 C2 0.6(9) . .
C1 N2 N3 C3 176.1(7) . .
O3 Cu2 N4 C11 -139.4(6) . .
O3 Cu2 N4 C11 40.6(6) 2_656 .
N4 Cu2 N4 C11 44(100) 2_656 .
O3 Cu2 N4 C10 26.4(8) . .
O3 Cu2 N4 C10 -153.6(8) 2_656 .
N4 Cu2 N4 C10 -150(100) 2_656 .
C10 N5 N6 C11 0.7(9) . .
C10 N5 N6 C12 175.3(7) . .
O1 Cu1 O1 C25 105(26) 2_657 .
N1 Cu1 O1 C25 -87.9(3) 2_657 .
N1 Cu1 O1 C25 92.1(3) . .
O3 Cu2 O3 C26 -58(100) 2_656 .
N4 Cu2 O3 C26 88.4(5) 2_656 .
N4 Cu2 O3 C26 -91.6(5) . .
N3 N2 C1 N1 -0.9(10) . .
C2 N1 C1 N2 0.9(10) . .
Cu1 N1 C1 N2 -172.0(6) . .
C1 N1 C2 N3 -0.5(8) . .
Cu1 N1 C2 N3 172.4(4) . .
N2 N3 C2 N1 0.0(8) . .
C3 N3 C2 N1 -175.2(6) . .
C2 N3 C3 C4 -97.2(8) . .
N2 N3 C3 C4 88.1(8) . .
N3 C3 C4 C5 -115.3(9) . .
N3 C3 C4 C9 66.4(10) . .
C9 C4 C5 C6 6.3(15) . .
C3 C4 C5 C6 -172.1(9) . .
C4 C5 C6 C7 -2.0(17) . .
C5 C6 C7 C8 -3.5(14) . .
C5 C6 C7 C7 176.5(9) . 2_666
C6 C7 C8 C9 4.7(12) . .
C7 C7 C8 C9 -175.3(8) 2_666 .
C5 C4 C9 C8 -5.1(13) . .
C3 C4 C9 C8 173.3(7) . .
C7 C8 C9 C4 -0.4(13) . .
N6 N5 C10 N4 -2.0(11) . .
C11 N4 C10 N5 2.5(10) . .
Cu2 N4 C10 N5 -165.7(6) . .
N5 N6 C11 N4 0.8(9) . .
C12 N6 C11 N4 -173.3(6) . .
C10 N4 C11 N6 -1.9(8) . .
Cu2 N4 C11 N6 167.1(5) . .
C11 N6 C12 C13 105.5(8) . .
N5 N6 C12 C13 -68.1(8) . .
N6 C12 C13 C18 139.5(7) . .
N6 C12 C13 C14 -41.5(10) . .
C18 C13 C14 C15 2.4(15) . .
C12 C13 C14 C15 -176.7(10) . .
C13 C14 C15 C16 -2.4(19) . .
C14 C15 C16 C17 1.0(17) . .
C14 C15 C16 C16 -179.1(11) . 2_545
C15 C16 C17 C18 0.3(12) . .
C16 C16 C17 C18 -179.6(8) 2_545 .
C14 C13 C18 C17 -1.1(12) . .
C12 C13 C18 C17 177.9(6) . .
C16 C17 C18 C13 -0.2(12) . .
C24 C19 C20 C21 -1.4(14) . .
C26 C19 C20 C21 -174.4(9) . .
C19 C20 C21 C22 3.9(18) . .
C20 C21 C22 C23 -3.2(19) . .
C21 C22 C23 C24 0.0(16) . .
C20 C19 C24 C23 -1.8(10) . .
C26 C19 C24 C23 171.0(6) . .
C20 C19 C24 C25 173.5(7) . .
C26 C19 C24 C25 -13.8(9) . .
C22 C23 C24 C19 2.6(12) . .
C22 C23 C24 C25 -172.9(8) . .
Cu1 O1 C25 O2 -2.2(6) . .
Cu1 O1 C25 C24 175.8(4) . .
C19 C24 C25 O2 -36.9(8) . .
C23 C24 C25 O2 138.4(6) . .
C19 C24 C25 O1 145.1(6) . .
C23 C24 C25 O1 -39.6(8) . .
Cu2 O3 C26 O4 -8.0(8) . .
Cu2 O3 C26 C19 170.2(4) . .
C24 C19 C26 O4 -48.7(9) . .
C20 C19 C26 O4 124.1(8) . .
C24 C19 C26 O3 132.9(6) . .
C20 C19 C26 O3 -54.2(9) . .
