#------------------------------------------------------------------------------
#$Date: 2016-03-24 02:47:15 +0200 (Thu, 24 Mar 2016) $
#$Revision: 179596 $
#$URL: svn://www.crystallography.net/cod/cif/4/50/60/4506090.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4506090
loop_
_publ_author_name
'Zhu, Yan'
'Luo, Feng'
'Song, Yu-mei'
'Feng, Xue-feng'
'Luo, Ming-biao'
'Liao, Zhen-wei'
'Sun, Gong-ming'
'Tian, Xiao-zhao'
'Yuan, Zi-Jun'
_publ_section_title
;
 The First One-Pot Synthesis of Multinuclear 3d-4f Metal--Organic
 Compounds Involving a Polytopic N,O-Donor Ligand Formed in Situ
;
_journal_issue                   5
_journal_name_full               'Crystal Growth & Design'
_journal_page_first              2158
_journal_paper_doi               10.1021/cg3002509
_journal_volume                  12
_journal_year                    2012
_chemical_formula_sum            'C120 H86 Co4 Dy2 N12 O14'
_chemical_formula_weight         2480.73
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           176
_symmetry_cell_setting           hexagonal
_symmetry_space_group_name_Hall  '-P 6c'
_symmetry_space_group_name_H-M   'P 63/m'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                120.00
_cell_formula_units_Z            1
_cell_length_a                   13.3921(2)
_cell_length_b                   13.3921(2)
_cell_length_c                   18.3790(5)
_cell_measurement_reflns_used    5102
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      27.17
_cell_measurement_theta_min      2.83
_cell_volume                     2854.63(10)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0345
_diffrn_reflns_av_sigmaI/netI    0.0199
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       -15
_diffrn_reflns_limit_k_max       9
_diffrn_reflns_limit_k_min       -14
_diffrn_reflns_limit_l_max       21
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_number            14294
_diffrn_reflns_theta_full        24.99
_diffrn_reflns_theta_max         24.99
_diffrn_reflns_theta_min         1.76
_exptl_absorpt_coefficient_mu    1.925
_exptl_absorpt_correction_T_max  0.6446
_exptl_absorpt_correction_T_min  0.5958
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    1.443
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             1242
_exptl_crystal_size_max          0.30
_exptl_crystal_size_mid          0.30
_exptl_crystal_size_min          0.25
_platon_squeeze_details
;
;
_refine_diff_density_max         0.966
_refine_diff_density_min         -1.634
_refine_diff_density_rms         0.068
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.105
_refine_ls_hydrogen_treatment    refU
_refine_ls_matrix_type           full
_refine_ls_number_parameters     127
_refine_ls_number_reflns         1734
_refine_ls_number_restraints     1
_refine_ls_restrained_S_all      1.105
_refine_ls_R_factor_all          0.0457
_refine_ls_R_factor_gt           0.0398
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0467P)²+3.8749P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1048
_refine_ls_wR_factor_ref         0.1090
_reflns_number_gt                1497
_reflns_number_total             1734
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            cg3002509_si_002.cif
_cod_data_source_block           2
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Hexagonal' changed to 'hexagonal'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.1 from
2010-06-29.

'_refine_ls_hydrogen_treatment' value 'refu' changed to
'refU' according to
/home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 
;
_cod_original_sg_symbol_H-M      P6(3)/m
_cod_database_code               4506090
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-y, x-y, z'
'-x+y, -x, z'
'-x, -y, z+1/2'
'y, -x+y, z+1/2'
'x-y, x, z+1/2'
'-x, -y, -z'
'y, -x+y, -z'
'x-y, x, -z'
'x, y, -z-1/2'
'-y, x-y, -z-1/2'
'-x+y, -x, -z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
C1 C 0.8382(4) 0.1692(4) 0.1808(2) 0.0558(11) Uani 1 1 d .
C2 C 0.7990(3) 0.2311(3) 0.1408(2) 0.0481(9) Uani 1 1 d .
C3 C 0.8521(3) 0.2801(4) 0.0728(2) 0.0540(10) Uani 1 1 d .
C4 C 0.9467(4) 0.2705(4) 0.0468(3) 0.0675(13) Uani 1 1 d .
C5 C 0.7769(6) 0.1067(6) 0.2500 0.0594(15) Uani 1 2 d S
C6 C 0.9330(5) 0.1616(6) 0.1535(3) 0.0802(16) Uani 1 1 d .
H6 H 0.9604 0.1217 0.1806 0.096 Uiso 1 1 calc R
C7 C 0.7488(8) -0.0191(6) 0.2500 0.087(2) Uani 1 2 d S
H7A H 0.8173 -0.0223 0.2608 0.131 Uiso 0.50 1 calc PR
H7B H 0.7202 -0.0525 0.2030 0.131 Uiso 0.50 1 calc PR
H7C H 0.6912 -0.0615 0.2862 0.131 Uiso 0.50 1 calc PR
C8 C 0.9862(5) 0.2103(6) 0.0893(3) 0.0880(18) Uani 1 1 d .
H8 H 1.0486 0.2035 0.0737 0.106 Uiso 1 1 calc R
C9 C 0.8514(5) 0.3775(4) -0.0307(3) 0.0779(15) Uani 1 1 d .
H9 H 0.8203 0.4140 -0.0579 0.093 Uiso 1 1 calc R
C10 C 0.9459(5) 0.3710(5) -0.0593(3) 0.0877(17) Uani 1 1 d .
H10 H 0.9773 0.4041 -0.1041 0.105 Uiso 1 1 calc R
C11 C 0.9898(5) 0.3166(5) -0.0212(3) 0.0851(16) Uani 1 1 d .
H11 H 1.0501 0.3097 -0.0408 0.102 Uiso 1 1 calc R
Co1 Co 0.6667 0.3333 0.08551(5) 0.0476(3) Uani 1 3 d S
Dy1 Dy 0.6667 0.3333 0.2500 0.0602(2) Uani 1 6 d S
N1 N 0.8058(3) 0.3338(3) 0.03312(18) 0.0592(9) Uani 1 1 d .
O1 O 0.7102(2) 0.2418(2) 0.16152(12) 0.0462(6) Uani 1 1 d .
O2 O 0.5917(8) 0.4851(8) 0.2500 0.037(2) Uani 0.33 2 d SPD
H1 H 0.5545 0.5214 0.2500 0.044 Uiso 0.33 2 d SPRD
H5 H 0.696(5) 0.100(5) 0.2500 0.047(15) Uiso 1 2 d S
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1892 4.4098 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
C2 C1 C6 118.3(4) . .
C2 C1 C5 120.6(4) . .
C6 C1 C5 121.0(5) . .
O1 C2 C1 122.7(4) . .
O1 C2 C3 118.1(4) . .
C1 C2 C3 119.2(4) . .
N1 C3 C4 121.9(4) . .
N1 C3 C2 117.1(4) . .
C4 C3 C2 121.0(4) . .
C11 C4 C8 124.5(5) . .
C11 C4 C3 117.0(5) . .
C8 C4 C3 118.4(4) . .
C1 C5 C1 113.8(6) 10_556 .
C1 C5 C7 112.0(3) 10_556 .
C1 C5 C7 112.0(3) . .
C1 C5 H5 107.3(15) 10_556 .
C1 C5 H5 107.3(15) . .
C7 C5 H5 104(3) . .
C8 C6 C1 123.1(5) . .
C8 C6 H6 118.5 . .
C1 C6 H6 118.5 . .
C5 C7 H7A 109.5 . .
C5 C7 H7B 109.5 . .
H7A C7 H7B 109.5 . .
C5 C7 H7C 109.5 . .
H7A C7 H7C 109.5 . .
H7B C7 H7C 109.5 . .
C6 C8 C4 120.0(5) . .
C6 C8 H8 120.0 . .
C4 C8 H8 120.0 . .
N1 C9 C10 122.3(5) . .
N1 C9 H9 118.8 . .
C10 C9 H9 118.8 . .
C11 C10 C9 119.3(5) . .
C11 C10 H10 120.4 . .
C9 C10 H10 120.4 . .
C10 C11 C4 121.1(5) . .
C10 C11 H11 119.5 . .
C4 C11 H11 119.5 . .
N1 Co1 N1 100.54(13) . 3_665
N1 Co1 N1 100.54(13) . 2_655
N1 Co1 N1 100.54(13) 3_665 2_655
N1 Co1 O1 78.68(12) . .
N1 Co1 O1 99.55(12) 3_665 .
N1 Co1 O1 159.68(13) 2_655 .
N1 Co1 O1 99.55(12) . 2_655
N1 Co1 O1 159.68(13) 3_665 2_655
N1 Co1 O1 78.68(12) 2_655 2_655
O1 Co1 O1 81.42(10) . 2_655
N1 Co1 O1 159.68(13) . 3_665
N1 Co1 O1 78.68(12) 3_665 3_665
N1 Co1 O1 99.55(12) 2_655 3_665
O1 Co1 O1 81.42(10) . 3_665
O1 Co1 O1 81.42(10) 2_655 3_665
N1 Co1 Dy1 117.37(10) . .
N1 Co1 Dy1 117.37(10) 3_665 .
N1 Co1 Dy1 117.37(10) 2_655 .
O1 Co1 Dy1 48.86(7) . .
O1 Co1 Dy1 48.86(7) 2_655 .
O1 Co1 Dy1 48.86(7) 3_665 .
O1 Dy1 O1 90.95(12) . 10_556
O1 Dy1 O1 138.95(5) . 11_656
O1 Dy1 O1 74.79(10) 10_556 11_656
O1 Dy1 O1 74.79(10) . 2_655
O1 Dy1 O1 138.95(5) 10_556 2_655
O1 Dy1 O1 90.95(13) 11_656 2_655
O1 Dy1 O1 74.79(10) . 3_665
O1 Dy1 O1 138.95(5) 10_556 3_665
O1 Dy1 O1 138.95(5) 11_656 3_665
O1 Dy1 O1 74.79(10) 2_655 3_665
O1 Dy1 O1 138.95(5) . 12_666
O1 Dy1 O1 74.79(10) 10_556 12_666
O1 Dy1 O1 74.79(10) 11_656 12_666
O1 Dy1 O1 138.95(5) 2_655 12_666
O1 Dy1 O1 90.95(13) 3_665 12_666
O1 Dy1 O2 69.83(15) . 3_665
O1 Dy1 O2 69.83(15) 10_556 3_665
O1 Dy1 O2 69.13(15) 11_656 3_665
O1 Dy1 O2 69.13(15) 2_655 3_665
O1 Dy1 O2 134.52(6) 3_665 3_665
O1 Dy1 O2 134.52(6) 12_666 3_665
O1 Dy1 O2 69.13(15) . 2_655
O1 Dy1 O2 69.13(15) 10_556 2_655
O1 Dy1 O2 134.52(6) 11_656 2_655
O1 Dy1 O2 134.52(6) 2_655 2_655
O1 Dy1 O2 69.83(15) 3_665 2_655
O1 Dy1 O2 69.83(15) 12_666 2_655
O2 Dy1 O2 120.0 3_665 2_655
O1 Dy1 O2 134.52(6) . .
O1 Dy1 O2 134.52(6) 10_556 .
O1 Dy1 O2 69.83(15) 11_656 .
O1 Dy1 O2 69.83(15) 2_655 .
O1 Dy1 O2 69.13(15) 3_665 .
O1 Dy1 O2 69.13(15) 12_666 .
O2 Dy1 O2 120.000(2) 3_665 .
O2 Dy1 O2 120.000(2) 2_655 .
O1 Dy1 Co1 44.52(6) . .
O1 Dy1 Co1 135.48(6) 10_556 .
O1 Dy1 Co1 135.48(6) 11_656 .
O1 Dy1 Co1 44.52(6) 2_655 .
O1 Dy1 Co1 44.52(6) 3_665 .
O1 Dy1 Co1 135.48(6) 12_666 .
O2 Dy1 Co1 90.0 3_665 .
O2 Dy1 Co1 90.0 2_655 .
O2 Dy1 Co1 90.0 . .
O1 Dy1 Co1 135.48(6) . 10_556
O1 Dy1 Co1 44.52(6) 10_556 10_556
O1 Dy1 Co1 44.52(6) 11_656 10_556
O1 Dy1 Co1 135.48(6) 2_655 10_556
O1 Dy1 Co1 135.48(6) 3_665 10_556
O1 Dy1 Co1 44.52(6) 12_666 10_556
O2 Dy1 Co1 90.0 3_665 10_556
O2 Dy1 Co1 90.0 2_655 10_556
O2 Dy1 Co1 90.0 . 10_556
Co1 Dy1 Co1 180.0 . 10_556
C9 N1 C3 118.4(4) . .
C9 N1 Co1 128.7(4) . .
C3 N1 Co1 112.9(2) . .
C2 O1 Co1 113.2(2) . .
C2 O1 Dy1 138.5(2) . .
Co1 O1 Dy1 86.61(10) . .
Dy1 O2 H1 168.5 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
C1 C2 1.393(6) .
C1 C6 1.415(6) .
C1 C5 1.518(6) .
C2 O1 1.323(5) .
C2 C3 1.426(6) .
C3 N1 1.370(6) .
C3 C4 1.419(6) .
C4 C11 1.387(7) .
C4 C8 1.402(8) .
C5 C1 1.518(6) 10_556
C5 C7 1.532(9) .
C5 H5 1.04(6) .
C6 C8 1.364(8) .
C6 H6 0.9300 .
C7 H7A 0.9600 .
C7 H7B 0.9600 .
C7 H7C 0.9600 .
C8 H8 0.9300 .
C9 N1 1.317(5) .
C9 C10 1.413(8) .
C9 H9 0.9300 .
C10 C11 1.339(8) .
C10 H10 0.9300 .
C11 H11 0.9300 .
Co1 N1 2.094(4) .
Co1 N1 2.094(4) 3_665
Co1 N1 2.094(4) 2_655
Co1 O1 2.124(3) .
Co1 O1 2.124(3) 2_655
Co1 O1 2.124(3) 3_665
Co1 Dy1 3.0231(8) .
Dy1 O1 2.281(2) .
Dy1 O1 2.281(2) 10_556
Dy1 O1 2.281(2) 11_656
Dy1 O1 2.281(2) 2_655
Dy1 O1 2.281(2) 3_665
Dy1 O1 2.281(2) 12_666
Dy1 O2 2.680(9) 3_665
Dy1 O2 2.680(9) 2_655
Dy1 O2 2.680(9) .
Dy1 Co1 3.0231(8) 10_556
O2 H1 0.8519 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
C6 C1 C2 O1 179.2(4) . .
C5 C1 C2 O1 2.0(6) . .
C6 C1 C2 C3 2.7(6) . .
C5 C1 C2 C3 -174.5(4) . .
O1 C2 C3 N1 -0.8(5) . .
C1 C2 C3 N1 175.8(4) . .
O1 C2 C3 C4 -179.2(4) . .
C1 C2 C3 C4 -2.5(6) . .
N1 C3 C4 C11 -0.9(7) . .
C2 C3 C4 C11 177.4(4) . .
N1 C3 C4 C8 -177.5(5) . .
C2 C3 C4 C8 0.8(7) . .
C2 C1 C5 C1 -102.4(5) . 10_556
C6 C1 C5 C1 80.5(7) . 10_556
C2 C1 C5 C7 129.4(5) . .
C6 C1 C5 C7 -47.7(7) . .
C2 C1 C6 C8 -1.3(8) . .
C5 C1 C6 C8 175.8(5) . .
C1 C6 C8 C4 -0.4(9) . .
C11 C4 C8 C6 -175.7(6) . .
C3 C4 C8 C6 0.7(8) . .
N1 C9 C10 C11 1.3(9) . .
C9 C10 C11 C4 -2.4(9) . .
C8 C4 C11 C10 178.5(6) . .
C3 C4 C11 C10 2.2(8) . .
N1 Co1 Dy1 O1 -41.78(14) . .
N1 Co1 Dy1 O1 78.22(14) 3_665 .
N1 Co1 Dy1 O1 -161.78(14) 2_655 .
O1 Co1 Dy1 O1 -120.0 2_655 .
O1 Co1 Dy1 O1 120.0 3_665 .
N1 Co1 Dy1 O1 -41.78(14) . 10_556
N1 Co1 Dy1 O1 78.22(14) 3_665 10_556
N1 Co1 Dy1 O1 -161.78(14) 2_655 10_556
O1 Co1 Dy1 O1 0.0 . 10_556
O1 Co1 Dy1 O1 -120.0 2_655 10_556
O1 Co1 Dy1 O1 120.0 3_665 10_556
N1 Co1 Dy1 O1 78.22(14) . 11_656
N1 Co1 Dy1 O1 -161.78(14) 3_665 11_656
N1 Co1 Dy1 O1 -41.78(14) 2_655 11_656
O1 Co1 Dy1 O1 120.0 . 11_656
O1 Co1 Dy1 O1 0.0 2_655 11_656
O1 Co1 Dy1 O1 -120.0 3_665 11_656
N1 Co1 Dy1 O1 78.22(14) . 2_655
N1 Co1 Dy1 O1 -161.78(14) 3_665 2_655
N1 Co1 Dy1 O1 -41.78(14) 2_655 2_655
O1 Co1 Dy1 O1 120.0 . 2_655
O1 Co1 Dy1 O1 -120.0 3_665 2_655
N1 Co1 Dy1 O1 -161.78(14) . 3_665
N1 Co1 Dy1 O1 -41.78(14) 3_665 3_665
N1 Co1 Dy1 O1 78.22(14) 2_655 3_665
O1 Co1 Dy1 O1 -120.0 . 3_665
O1 Co1 Dy1 O1 120.0 2_655 3_665
N1 Co1 Dy1 O1 -161.78(14) . 12_666
N1 Co1 Dy1 O1 -41.78(14) 3_665 12_666
N1 Co1 Dy1 O1 78.22(14) 2_655 12_666
O1 Co1 Dy1 O1 -120.0 . 12_666
O1 Co1 Dy1 O1 120.0 2_655 12_666
O1 Co1 Dy1 O1 0.0 3_665 12_666
N1 Co1 Dy1 O2 18.8(2) . 3_665
N1 Co1 Dy1 O2 138.8(2) 3_665 3_665
N1 Co1 Dy1 O2 -101.2(2) 2_655 3_665
O1 Co1 Dy1 O2 60.5(2) . 3_665
O1 Co1 Dy1 O2 -59.5(2) 2_655 3_665
O1 Co1 Dy1 O2 -179.5(2) 3_665 3_665
N1 Co1 Dy1 O2 -101.2(2) . 2_655
N1 Co1 Dy1 O2 18.8(2) 3_665 2_655
N1 Co1 Dy1 O2 138.8(2) 2_655 2_655
O1 Co1 Dy1 O2 -59.5(2) . 2_655
O1 Co1 Dy1 O2 -179.5(2) 2_655 2_655
O1 Co1 Dy1 O2 60.5(2) 3_665 2_655
N1 Co1 Dy1 O2 138.8(2) . .
N1 Co1 Dy1 O2 -101.2(2) 3_665 .
N1 Co1 Dy1 O2 18.8(2) 2_655 .
O1 Co1 Dy1 O2 -179.5(2) . .
O1 Co1 Dy1 O2 60.5(2) 2_655 .
O1 Co1 Dy1 O2 -59.5(2) 3_665 .
N1 Co1 Dy1 Co1 -90(26) . 10_556
N1 Co1 Dy1 Co1 30(26) 3_665 10_556
N1 Co1 Dy1 Co1 150(41) 2_655 10_556
O1 Co1 Dy1 Co1 -48(26) . 10_556
O1 Co1 Dy1 Co1 -168(26) 2_655 10_556
O1 Co1 Dy1 Co1 72(41) 3_665 10_556
C10 C9 N1 C3 0.0(7) . .
C10 C9 N1 Co1 -179.9(4) . .
C4 C3 N1 C9 -0.1(6) . .
C2 C3 N1 C9 -178.5(4) . .
C4 C3 N1 Co1 179.7(3) . .
C2 C3 N1 Co1 1.4(5) . .
N1 Co1 N1 C9 81.0(4) 3_665 .
N1 Co1 N1 C9 -22.0(4) 2_655 .
O1 Co1 N1 C9 178.7(4) . .
O1 Co1 N1 C9 -102.1(4) 2_655 .
O1 Co1 N1 C9 166.8(4) 3_665 .
Dy1 Co1 N1 C9 -150.5(4) . .
N1 Co1 N1 C3 -98.8(3) 3_665 .
N1 Co1 N1 C3 158.2(3) 2_655 .
O1 Co1 N1 C3 -1.1(3) . .
O1 Co1 N1 C3 78.1(3) 2_655 .
O1 Co1 N1 C3 -13.0(5) 3_665 .
Dy1 Co1 N1 C3 29.7(3) . .
C1 C2 O1 Co1 -176.7(3) . .
C3 C2 O1 Co1 -0.1(4) . .
C1 C2 O1 Dy1 70.5(5) . .
C3 C2 O1 Dy1 -112.9(4) . .
N1 Co1 O1 C2 0.7(2) . .
N1 Co1 O1 C2 99.6(3) 3_665 .
N1 Co1 O1 C2 -89.1(4) 2_655 .
O1 Co1 O1 C2 -101.0(3) 2_655 .
O1 Co1 O1 C2 176.5(3) 3_665 .
Dy1 Co1 O1 C2 -142.2(3) . .
N1 Co1 O1 Dy1 142.89(12) . .
N1 Co1 O1 Dy1 -118.17(12) 3_665 .
N1 Co1 O1 Dy1 53.1(4) 2_655 .
O1 Co1 O1 Dy1 41.27(4) 2_655 .
O1 Co1 O1 Dy1 -41.27(4) 3_665 .
O1 Dy1 O1 C2 -58.1(4) 10_556 .
O1 Dy1 O1 C2 9.5(4) 11_656 .
O1 Dy1 O1 C2 82.9(4) 2_655 .
O1 Dy1 O1 C2 160.9(4) 3_665 .
O1 Dy1 O1 C2 -125.7(4) 12_666 .
O2 Dy1 O1 C2 10.0(4) 3_665 .
O2 Dy1 O1 C2 -125.3(4) 2_655 .
O2 Dy1 O1 C2 122.7(4) . .
Co1 Dy1 O1 C2 121.9(4) . .
Co1 Dy1 O1 C2 -58.1(4) 10_556 .
O1 Dy1 O1 Co1 180.0 10_556 .
O1 Dy1 O1 Co1 -112.37(2) 11_656 .
O1 Dy1 O1 Co1 -39.00(3) 2_655 .
O1 Dy1 O1 Co1 39.00(3) 3_665 .
O1 Dy1 O1 Co1 112.37(2) 12_666 .
O2 Dy1 O1 Co1 -111.94(19) 3_665 .
O2 Dy1 O1 Co1 112.81(19) 2_655 .
O2 Dy1 O1 Co1 0.8(3) . .
Co1 Dy1 O1 Co1 180.0 10_556 .
loop_
_platon_squeeze_void_nr
_platon_squeeze_void_average_x
_platon_squeeze_void_average_y
_platon_squeeze_void_average_z
_platon_squeeze_void_volume
_platon_squeeze_void_count_electrons
_platon_squeeze_void_content
1 0.000 0.000 0.000 26 1 ' '
2 0.000 0.000 0.500 25 1 ' '
3 0.333 0.667 0.250 255 67 ' '
4 0.667 0.333 0.750 255 68 ' '
