#------------------------------------------------------------------------------
#$Date: 2018-08-11 17:03:44 +0300 (Sat, 11 Aug 2018) $
#$Revision: 209571 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/00/02/7000262.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7000262
loop_
_publ_author_name
'Hitchcock, Peter B.'
'Lappert, Michael F.'
'Protchenko, Andrey V.'
'Uiterweerd, Patrick G. H.'
_publ_section_title
;
 Synthesis and structures of halides and pseudohalides of
 bis[2,6-bis(dimethylamino)phenyl]tin(IV)
;
_journal_coden_ASTM              DTARAF
_journal_issue                   2
_journal_name_full               'Dalton Transactions'
_journal_page_first              353
_journal_page_last               361
_journal_paper_doi               10.1039/b813353k
_journal_year                    2009
_chemical_compound_source        'synthesis as described'
_chemical_formula_moiety         'C20 H30 I2 N4 Sn'
_chemical_formula_sum            'C20 H30 I2 N4 Sn'
_chemical_formula_weight         698.97
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      14
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_conform_dict_location
ftp://ftp.iucr.org/cifdics/cif_core_2.1beta5.dic
_audit_conform_dict_name         cif_core.dic
_audit_conform_dict_version      2.1beta5
_audit_creation_date             1999-10-19T09:59:22-00:00
_audit_creation_method           'WinGX routine CIF_UPDATE'
_cell_angle_alpha                90
_cell_angle_beta                 90.824(1)
_cell_angle_gamma                90
_cell_formula_units_Z            8
_cell_length_a                   16.4333(2)
_cell_length_b                   15.0037(2)
_cell_length_c                   20.1333(3)
_cell_measurement_reflns_used    28119
_cell_measurement_temperature    173(2)
_cell_measurement_theta_max      30.034
_cell_measurement_theta_min      4.246
_cell_measurement_wavelength     0.71073
_cell_volume                     4963.56(12)
_computing_cell_refinement       'HKL Scalepack (Otwinowski & Minor 1997)'
_computing_data_reduction
'HKL Denzo and Scalepack (Otwinowski & Minor 1997)'
_computing_molecular_graphics    'Ortep-3 for Windows (Farrugia, 1997)'
_computing_publication_material  'WinGX publication routines (Farrugia, 1999)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      173(2)
_diffrn_measured_fraction_theta_full 0.983
_diffrn_measured_fraction_theta_max 0.983
_diffrn_measurement_device       KappaCCD
_diffrn_measurement_method       CCD
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.045
_diffrn_reflns_av_sigmaI/netI    0.0352
_diffrn_reflns_limit_h_max       22
_diffrn_reflns_limit_h_min       -23
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_k_min       -20
_diffrn_reflns_limit_l_max       28
_diffrn_reflns_limit_l_min       -28
_diffrn_reflns_number            44805
_diffrn_reflns_theta_full        30.04
_diffrn_reflns_theta_max         30.04
_diffrn_reflns_theta_min         4.25
_exptl_absorpt_coefficient_mu    3.529
_exptl_absorpt_correction_T_max  0.4234
_exptl_absorpt_correction_T_min  0.3635
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
[c.f. r.h. blessing, acta cryst. (1995), a51, 33-38]
;
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.871
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             2672
_exptl_crystal_size_max          0.3
_exptl_crystal_size_mid          0.3
_exptl_crystal_size_min          0.2
_refine_diff_density_max         1.939
_refine_diff_density_min         -1.615
_refine_diff_density_rms         0.1
_refine_ls_extinction_coef       0.00049(4)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.027
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     488
_refine_ls_number_reflns         14287
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.027
_refine_ls_R_factor_all          0.039
_refine_ls_R_factor_gt           0.0299
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0120P)²+9.5660P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0624
_refine_ls_wR_factor_ref         0.0664
_reflns_number_gt                12199
_reflns_number_total             14287
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            B813353K.txt
_cod_data_source_block           (6)-oct1899
_cod_original_sg_symbol_H-M      P2(1)/c
_cod_database_code               7000262
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Sn Sn 0.316188(11) 0.175446(12) 0.240555(9) 0.02192(5) Uani 1 1 d . . .
I1 I 0.348032(13) 0.103868(15) 0.116114(10) 0.03819(6) Uani 1 1 d . . .
I2 I 0.305596(15) 0.010685(14) 0.297245(12) 0.04259(6) Uani 1 1 d . . .
N1 N 0.30802(15) 0.34090(17) 0.17479(12) 0.0299(5) Uani 1 1 d . . .
N2 N 0.11210(16) 0.15009(19) 0.28179(13) 0.0352(6) Uani 1 1 d . . .
N3 N 0.29943(14) 0.24684(16) 0.36703(11) 0.0266(5) Uani 1 1 d . . .
N4 N 0.52255(15) 0.22964(17) 0.21507(13) 0.0311(5) Uani 1 1 d . . .
C1 C 0.20673(16) 0.24959(19) 0.22632(13) 0.0245(5) Uani 1 1 d . . .
C2 C 0.22569(17) 0.33175(19) 0.19826(14) 0.0271(5) Uani 1 1 d . . .
C3 C 0.1682(2) 0.3999(2) 0.19536(16) 0.0377(7) Uani 1 1 d . . .
H3 H 0.181 0.4558 0.1761 0.045 Uiso 1 1 calc R . .
C4 C 0.0926(2) 0.3845(3) 0.22089(19) 0.0459(8) Uani 1 1 d . . .
H4 H 0.0533 0.4309 0.2198 0.055 Uiso 1 1 calc R . .
C5 C 0.0719(2) 0.3027(3) 0.24842(17) 0.0411(8) Uani 1 1 d . . .
H5 H 0.0187 0.2938 0.2651 0.049 Uiso 1 1 calc R . .
C6 C 0.12868(17) 0.2336(2) 0.25172(14) 0.0303(6) Uani 1 1 d . . .
C7 C 0.3104(2) 0.3414(3) 0.10155(16) 0.0452(8) Uani 1 1 d . . .
H7A H 0.3669 0.3476 0.0872 0.068 Uiso 1 1 calc R . .
H7B H 0.2782 0.3915 0.0844 0.068 Uiso 1 1 calc R . .
H7C H 0.2878 0.2854 0.0843 0.068 Uiso 1 1 calc R . .
C8 C 0.3502(2) 0.4194(2) 0.20160(19) 0.0436(8) Uani 1 1 d . . .
H8A H 0.4054 0.422 0.184 0.065 Uiso 1 1 calc R . .
H8B H 0.3529 0.4155 0.2502 0.065 Uiso 1 1 calc R . .
H8C H 0.3204 0.4734 0.1885 0.065 Uiso 1 1 calc R . .
C9 C 0.0446(3) 0.1481(3) 0.3280(2) 0.0591(11) Uani 1 1 d . . .
H9A H 0.0384 0.0877 0.3457 0.089 Uiso 1 1 calc R . .
H9B H -0.0057 0.1658 0.3048 0.089 Uiso 1 1 calc R . .
H9C H 0.0556 0.1896 0.3647 0.089 Uiso 1 1 calc R . .
C10 C 0.1049(2) 0.0764(2) 0.23439(19) 0.0463(8) Uani 1 1 d . . .
H10A H 0.0935 0.021 0.2584 0.07 Uiso 1 1 calc R . .
H10B H 0.156 0.0701 0.2103 0.07 Uiso 1 1 calc R . .
H10C H 0.0605 0.0887 0.2028 0.07 Uiso 1 1 calc R . .
C11 C 0.41105(16) 0.24517(17) 0.29177(13) 0.0224(5) Uani 1 1 d . . .
C12 C 0.37715(16) 0.28348(18) 0.34806(13) 0.0247(5) Uani 1 1 d . . .
C13 C 0.41575(19) 0.3536(2) 0.38131(15) 0.0323(6) Uani 1 1 d . . .
H13 H 0.3929 0.3789 0.4201 0.039 Uiso 1 1 calc R . .
C14 C 0.4881(2) 0.3855(2) 0.35645(16) 0.0346(7) Uani 1 1 d . . .
H14 H 0.5135 0.4354 0.377 0.042 Uiso 1 1 calc R . .
C15 C 0.52435(18) 0.3458(2) 0.30191(15) 0.0317(6) Uani 1 1 d . . .
H15 H 0.5746 0.3683 0.2863 0.038 Uiso 1 1 calc R . .
C16 C 0.48780(16) 0.27322(19) 0.26985(14) 0.0265(5) Uani 1 1 d . . .
C17 C 0.23786(19) 0.3144(2) 0.38169(17) 0.0389(7) Uani 1 1 d . . .
H17A H 0.187 0.285 0.394 0.058 Uiso 1 1 calc R . .
H17B H 0.2283 0.3515 0.3423 0.058 Uiso 1 1 calc R . .
H17C H 0.2571 0.3518 0.4186 0.058 Uiso 1 1 calc R . .
C18 C 0.3089(2) 0.1857(2) 0.42388(16) 0.0403(8) Uani 1 1 d . . .
H18A H 0.2555 0.1618 0.4358 0.06 Uiso 1 1 calc R . .
H18B H 0.3323 0.2181 0.4619 0.06 Uiso 1 1 calc R . .
H18C H 0.3451 0.1366 0.4118 0.06 Uiso 1 1 calc R . .
C19 C 0.5918(2) 0.2742(3) 0.18478(18) 0.0479(9) Uani 1 1 d . . .
H19A H 0.6113 0.2383 0.1476 0.072 Uiso 1 1 calc R . .
H19B H 0.6356 0.281 0.2179 0.072 Uiso 1 1 calc R . .
H19C H 0.575 0.333 0.1686 0.072 Uiso 1 1 calc R . .
C20 C 0.5377(2) 0.1348(2) 0.22404(18) 0.0404(7) Uani 1 1 d . . .
H20A H 0.5618 0.1104 0.1837 0.061 Uiso 1 1 calc R . .
H20B H 0.4863 0.1042 0.2327 0.061 Uiso 1 1 calc R . .
H20C H 0.5752 0.126 0.2617 0.061 Uiso 1 1 calc R . .
Sn1B Sn 0.177787(11) -0.206246(12) 0.481418(9) 0.02251(5) Uani 1 1 d . . .
I1B I 0.130873(15) -0.170546(17) 0.352629(11) 0.04461(6) Uani 1 1 d . . .
I2B I 0.161459(15) -0.032390(14) 0.521066(14) 0.04643(7) Uani 1 1 d . . .
N1B N 0.20982(18) -0.37443(18) 0.43012(16) 0.0420(7) Uani 1 1 d . . .
N2B N 0.37877(16) -0.14049(19) 0.52261(13) 0.0356(6) Uani 1 1 d . . .
N3B N 0.20674(15) -0.25750(19) 0.61252(12) 0.0330(5) Uani 1 1 d . . .
N4B N -0.02566(15) -0.28168(17) 0.46433(13) 0.0301(5) Uani 1 1 d . . .
C1B C 0.29796(17) -0.26074(19) 0.47462(13) 0.0259(5) Uani 1 1 d . . .
C2B C 0.29076(19) -0.3475(2) 0.45134(16) 0.0336(6) Uani 1 1 d . . .
C3B C 0.3575(2) -0.4049(2) 0.4513(2) 0.0493(10) Uani 1 1 d . . .
H3B H 0.3523 -0.4643 0.4355 0.059 Uiso 1 1 calc R . .
C4B C 0.4311(2) -0.3732(3) 0.4748(2) 0.0522(10) Uani 1 1 d . . .
H4B H 0.4771 -0.4116 0.4756 0.063 Uiso 1 1 calc R . .
C5B C 0.4394(2) -0.2867(3) 0.49728(19) 0.0439(8) Uani 1 1 d . . .
H5B H 0.4911 -0.2664 0.5124 0.053 Uiso 1 1 calc R . .
C6B C 0.37311(18) -0.2286(2) 0.49817(14) 0.0312(6) Uani 1 1 d . . .
C7B C 0.2068(3) -0.3961(3) 0.3589(2) 0.0695(13) Uani 1 1 d . . .
H7B1 H 0.1514 -0.414 0.3462 0.104 Uiso 1 1 calc R . .
H7B2 H 0.2445 -0.4451 0.3499 0.104 Uiso 1 1 calc R . .
H7B3 H 0.2226 -0.3436 0.3331 0.104 Uiso 1 1 calc R . .
C8B C 0.1779(3) -0.4492(2) 0.4696(3) 0.0620(13) Uani 1 1 d . . .
H8B1 H 0.1232 -0.4647 0.4534 0.093 Uiso 1 1 calc R . .
H8B2 H 0.1755 -0.4316 0.5164 0.093 Uiso 1 1 calc R . .
H8B3 H 0.2139 -0.5009 0.4652 0.093 Uiso 1 1 calc R . .
C9B C 0.4474(3) -0.1219(3) 0.5674(2) 0.0626(12) Uani 1 1 d . . .
H9B1 H 0.4455 -0.0594 0.5814 0.094 Uiso 1 1 calc R . .
H9B2 H 0.4985 -0.1333 0.5444 0.094 Uiso 1 1 calc R . .
H9B3 H 0.4441 -0.1606 0.6065 0.094 Uiso 1 1 calc R . .
C10B C 0.3733(2) -0.0729(2) 0.47094(18) 0.0433(8) Uani 1 1 d . . .
H10D H 0.3776 -0.0136 0.4911 0.065 Uiso 1 1 calc R . .
H10E H 0.321 -0.0783 0.4473 0.065 Uiso 1 1 calc R . .
H10F H 0.4177 -0.0812 0.4396 0.065 Uiso 1 1 calc R . .
C11B C 0.09146(16) -0.27660(18) 0.53980(13) 0.0239(5) Uani 1 1 d . . .
C12B C 0.12982(17) -0.3017(2) 0.59833(14) 0.0282(6) Uani 1 1 d . . .
C13B C 0.0969(2) -0.3670(2) 0.63961(16) 0.0378(7) Uani 1 1 d . . .
H13B H 0.1238 -0.3845 0.6796 0.045 Uiso 1 1 calc R . .
C14B C 0.0235(2) -0.4055(2) 0.62006(17) 0.0389(7) Uani 1 1 d . . .
H14B H 0.001 -0.4517 0.6463 0.047 Uiso 1 1 calc R . .
C15B C -0.01758(19) -0.3779(2) 0.56311(16) 0.0332(6) Uani 1 1 d . . .
H15B H -0.0684 -0.4045 0.5517 0.04 Uiso 1 1 calc R . .
C16B C 0.01445(17) -0.31170(18) 0.52212(14) 0.0254(5) Uani 1 1 d . . .
C17B C 0.2730(2) -0.3187(3) 0.6314(2) 0.0539(10) Uani 1 1 d . . .
H17D H 0.3229 -0.2845 0.6401 0.081 Uiso 1 1 calc R . .
H17E H 0.2823 -0.3609 0.5951 0.081 Uiso 1 1 calc R . .
H17F H 0.2581 -0.3515 0.6715 0.081 Uiso 1 1 calc R . .
C18B C 0.1979(2) -0.1883(3) 0.66352(17) 0.0472(9) Uani 1 1 d . . .
H18D H 0.2507 -0.1597 0.6719 0.071 Uiso 1 1 calc R . .
H18E H 0.1785 -0.2154 0.7047 0.071 Uiso 1 1 calc R . .
H18F H 0.1586 -0.1435 0.648 0.071 Uiso 1 1 calc R . .
C19B C -0.0942(2) -0.3356(3) 0.43998(19) 0.0473(9) Uani 1 1 d . . .
H19D H -0.1172 -0.3084 0.3996 0.071 Uiso 1 1 calc R . .
H19E H -0.136 -0.3385 0.4741 0.071 Uiso 1 1 calc R . .
H19F H -0.0751 -0.3959 0.4299 0.071 Uiso 1 1 calc R . .
C20B C -0.0478(2) -0.1873(2) 0.46441(18) 0.0388(7) Uani 1 1 d . . .
H20D H -0.0754 -0.1723 0.4224 0.058 Uiso 1 1 calc R . .
H20E H 0.0014 -0.1509 0.4695 0.058 Uiso 1 1 calc R . .
H20F H -0.0845 -0.1753 0.5014 0.058 Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0 0 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
I I -0.4742 1.8119 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sn Sn -0.6537 1.4246 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C1 Sn C11 114.77(10) . . ?
C1 Sn I2 118.05(8) . . ?
C11 Sn I2 107.03(7) . . ?
C1 Sn I1 104.46(7) . . ?
C11 Sn I1 118.65(7) . . ?
I2 Sn I1 92.345(9) . . ?
C2 N1 C8 113.3(3) . . ?
C2 N1 C7 111.5(3) . . ?
C8 N1 C7 110.1(3) . . ?
C6 N2 C9 116.2(3) . . ?
C6 N2 C10 113.7(3) . . ?
C9 N2 C10 110.2(3) . . ?
C12 N3 C17 113.9(2) . . ?
C12 N3 C18 111.0(2) . . ?
C17 N3 C18 109.8(3) . . ?
C16 N4 C20 115.3(2) . . ?
C16 N4 C19 116.2(3) . . ?
C20 N4 C19 111.5(3) . . ?
C2 C1 C6 120.6(3) . . ?
C2 C1 Sn 108.86(19) . . ?
C6 C1 Sn 129.3(2) . . ?
C3 C2 C1 120.7(3) . . ?
C3 C2 N1 123.7(3) . . ?
C1 C2 N1 115.6(2) . . ?
C4 C3 C2 118.6(3) . . ?
C3 C4 C5 121.8(3) . . ?
C4 C5 C6 120.4(3) . . ?
C5 C6 C1 117.9(3) . . ?
C5 C6 N2 122.9(3) . . ?
C1 C6 N2 119.1(3) . . ?
C12 C11 C16 120.1(3) . . ?
C12 C11 Sn 107.32(18) . . ?
C16 C11 Sn 130.4(2) . . ?
C11 C12 C13 121.1(3) . . ?
C11 C12 N3 115.0(2) . . ?
C13 C12 N3 123.8(3) . . ?
C14 C13 C12 118.3(3) . . ?
C13 C14 C15 121.2(3) . . ?
C14 C15 C16 120.8(3) . . ?
C15 C16 C11 118.0(3) . . ?
C15 C16 N4 123.1(3) . . ?
C11 C16 N4 118.8(3) . . ?
C11B Sn1B C1B 117.82(10) . . ?
C11B Sn1B I2B 103.98(7) . . ?
C1B Sn1B I2B 118.39(8) . . ?
C11B Sn1B I1B 115.88(8) . . ?
C1B Sn1B I1B 105.10(7) . . ?
I2B Sn1B I1B 93.553(10) . . ?
C2B N1B C7B 111.5(3) . . ?
C2B N1B C8B 112.7(3) . . ?
C7B N1B C8B 110.5(3) . . ?
C6B N2B C10B 113.6(3) . . ?
C6B N2B C9B 116.1(3) . . ?
C10B N2B C9B 110.4(3) . . ?
C12B N3B C18B 111.5(2) . . ?
C12B N3B C17B 113.9(3) . . ?
C18B N3B C17B 110.0(3) . . ?
C16B N4B C20B 115.1(2) . . ?
C16B N4B C19B 116.7(3) . . ?
C20B N4B C19B 110.2(3) . . ?
C2B C1B C6B 120.5(3) . . ?
C2B C1B Sn1B 107.8(2) . . ?
C6B C1B Sn1B 130.9(2) . . ?
C1B C2B C3B 121.1(3) . . ?
C1B C2B N1B 115.8(3) . . ?
C3B C2B N1B 123.1(3) . . ?
C4B C3B C2B 118.2(3) . . ?
C3B C4B C5B 121.3(3) . . ?
C4B C5B C6B 121.2(3) . . ?
C5B C6B C1B 117.7(3) . . ?
C5B C6B N2B 122.8(3) . . ?
C1B C6B N2B 119.5(3) . . ?
C12B C11B C16B 120.7(2) . . ?
C12B C11B Sn1B 107.83(19) . . ?
C16B C11B Sn1B 130.2(2) . . ?
C11B C12B C13B 121.5(3) . . ?
C11B C12B N3B 115.4(2) . . ?
C13B C12B N3B 123.1(3) . . ?
C14B C13B C12B 117.7(3) . . ?
C15B C14B C13B 121.4(3) . . ?
C14B C15B C16B 121.1(3) . . ?
C15B C16B N4B 122.7(3) . . ?
C15B C16B C11B 117.4(3) . . ?
N4B C16B C11B 119.9(2) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Sn C1 2.131(3) . ?
Sn C11 2.131(3) . ?
Sn I2 2.7294(3) . ?
Sn I1 2.7824(3) . ?
N1 C2 1.446(4) . ?
N1 C8 1.466(4) . ?
N1 C7 1.476(4) . ?
N2 C6 1.420(4) . ?
N2 C9 1.459(4) . ?
N2 C10 1.464(4) . ?
N3 C12 1.447(3) . ?
N3 C17 1.465(4) . ?
N3 C18 1.473(4) . ?
N4 C16 1.410(4) . ?
N4 C20 1.455(4) . ?
N4 C19 1.461(4) . ?
C1 C2 1.393(4) . ?
C1 C6 1.408(4) . ?
C2 C3 1.393(4) . ?
C3 C4 1.370(5) . ?
C4 C5 1.391(5) . ?
C5 C6 1.396(4) . ?
C11 C12 1.394(4) . ?
C11 C16 1.407(4) . ?
C12 C13 1.395(4) . ?
C13 C14 1.382(4) . ?
C14 C15 1.391(4) . ?
C15 C16 1.397(4) . ?
Sn1B C11B 2.135(3) . ?
Sn1B C1B 2.144(3) . ?
Sn1B I2B 2.7422(3) . ?
Sn1B I1B 2.7472(3) . ?
N1B C2B 1.449(4) . ?
N1B C7B 1.471(5) . ?
N1B C8B 1.475(5) . ?
N2B C6B 1.414(4) . ?
N2B C10B 1.455(4) . ?
N2B C9B 1.461(5) . ?
N3B C12B 1.453(4) . ?
N3B C18B 1.469(4) . ?
N3B C17B 1.470(4) . ?
N4B C16B 1.403(4) . ?
N4B C20B 1.463(4) . ?
N4B C19B 1.465(4) . ?
C1B C2B 1.387(4) . ?
C1B C6B 1.402(4) . ?
C2B C3B 1.395(5) . ?
C3B C4B 1.378(6) . ?
C4B C5B 1.380(6) . ?
C5B C6B 1.395(4) . ?
C11B C12B 1.381(4) . ?
C11B C16B 1.412(4) . ?
C12B C13B 1.398(4) . ?
C13B C14B 1.389(5) . ?
C14B C15B 1.385(5) . ?
C15B C16B 1.399(4) . ?
