#------------------------------------------------------------------------------
#$Date: 2016-03-25 09:10:57 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179716 $
#$URL: svn://www.crystallography.net/cod/cif/7/00/18/7001897.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7001897
loop_
_publ_author_name
'Petit, Sarah'
'Baril-Robert, François'
'Pilet, Guillaume'
'Reber, Christian'
'Luneau, Dominique'
_publ_section_title
;
 Luminescence spectroscopy of europium(III) and terbium(III) penta-,
 octa- and nonanuclear clusters with β-diketonate ligands
;
_journal_issue                   34
_journal_name_full               'Dalton Transactions'
_journal_page_first              6809
_journal_page_last               6815
_journal_paper_doi               10.1039/b822883c
_journal_year                    2009
_chemical_formula_moiety         'C150 H115 Eu5 O25'
_chemical_formula_sum            'C150 H115 Eu5 O25'
_chemical_formula_weight         3077.3
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_cell_angle_alpha                90
_cell_angle_beta                 101.051(2)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   22.0525(7)
_cell_length_b                   17.3193(7)
_cell_length_c                   35.4127(13)
_cell_measurement_reflns_used    14358
_cell_measurement_temperature    293
_cell_measurement_theta_max      24
_cell_measurement_theta_min      0
_cell_volume                     13274.5(8)
_computing_cell_refinement       'DENZO/SCALEPACK (Otwinowski & Minor, 1997)'
_computing_data_collection       'COLLECT (Nonius, 1997-2001).'
_computing_data_reduction        'DENZO/SCALEPACK (Otwinowski & Minor, 1997)'
_computing_molecular_graphics    'CAMERON (Watkin et al., 1996)'
_computing_publication_material  'CRYSTALS (Betteridge et al., 2003)'
_computing_structure_refinement  'CRYSTALS (Betteridge et al., 2003)'
_computing_structure_solution    'SIR92 (Altomare et al., 1994)'
_diffrn_ambient_temperature      293
_diffrn_measured_fraction_theta_full 0.978
_diffrn_measured_fraction_theta_max 0.964
_diffrn_measurement_device_type  'Nonius KappaCCD'
_diffrn_measurement_method       ω/2θ
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.051
_diffrn_reflns_limit_h_max       25
_diffrn_reflns_limit_h_min       -25
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       40
_diffrn_reflns_limit_l_min       -40
_diffrn_reflns_number            32579
_diffrn_reflns_theta_full        18.070
_diffrn_reflns_theta_max         24.093
_diffrn_reflns_theta_min         0.941
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    2.399
_exptl_absorpt_correction_T_max  0.9373
_exptl_absorpt_correction_T_min  0.9328
_exptl_absorpt_correction_type   none
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.540
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       cubic
_exptl_crystal_F_000             6120
_exptl_crystal_size_max          0.03
_exptl_crystal_size_mid          0.03
_exptl_crystal_size_min          0.03
_refine_diff_density_max         1.28
_refine_diff_density_min         -1.49
_refine_ls_extinction_method     None
_refine_ls_goodness_of_fit_ref   1.0834
_refine_ls_hydrogen_treatment    noref
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1621
_refine_ls_number_reflns         10326
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.1112
_refine_ls_R_factor_gt           0.0585
_refine_ls_shift/su_max          0.000740
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details
;
Method, part 1, Chebychev polynomial, (Watkin, 1994, Prince, 1982)
[weight] = 1.0/[A₀*T₀(x)+A₁*T₁(x) ... +Aₙ₋₁]*Tₙ₋₁(x)]
where Ai are the Chebychev coefficients listed below and x= Fcalc/Fmax
Method = Robust Weighting (Prince, 1982)
W = [weight] * [1-(deltaF/6*sigmaF)²]²
Ai are:
0.305 0.204 0.131
;
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_all         0.1141
_refine_ls_wR_factor_gt          0.0592
_refine_ls_wR_factor_ref         0.0569
_reflns_limit_h_max              24
_reflns_limit_h_min              -25
_reflns_limit_k_max              19
_reflns_limit_k_min              0
_reflns_limit_l_max              40
_reflns_limit_l_min              0
_reflns_number_gt                11062
_reflns_number_total             20307
_reflns_threshold_expression     I>2.0σ(I)
_cod_data_source_file            b822883c.txt
_cod_data_source_block           6
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      'P 1 21/c 1 '
_cod_database_code               7001897
loop_
_symmetry_equiv_pos_as_xyz
x,y,z
-x,-y,-z
-x,y+1/2,-z+1/2
x,-y+1/2,z+1/2
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_occupancy
_atom_site_adp_type
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
_oxford_atom_site_special_shape
_atom_site_attached_hydrogens
Eu1 Eu 0.23992(3) 0.90080(4) 0.17632(2) 0.0424 1.0000 Uani . . . . . . .
Eu2 Eu 0.22652(3) 0.70259(4) 0.06932(2) 0.0436 1.0000 Uani . . . . . . .
Eu3 Eu 0.29439(3) 0.89543(3) 0.08521(2) 0.0432 1.0000 Uani . . . . . . .
Eu4 Eu 0.18108(3) 0.70579(4) 0.16194(2) 0.0434 1.0000 Uani . . . . . . .
Eu5 Eu 0.35620(3) 0.73798(3) 0.16104(2) 0.0444 1.0000 Uani . . . . . . .
O1 O 0.2128(3) 0.8084(4) 0.1184(2) 0.0415 1.0000 Uani . . . . . . .
O11 O 0.2649(4) 0.6624(4) 0.1331(3) 0.0440 1.0000 Uani . . . . . . .
O12 O 0.2697(4) 0.7709(4) 0.1926(3) 0.0444 1.0000 Uani . . . . . . .
O13 O 0.3229(4) 0.7654(5) 0.0933(3) 0.0508 1.0000 Uani . . . . . . .
O14 O 0.3297(3) 0.8764(4) 0.1513(2) 0.0386 1.0000 Uani . . . . . . .
O21 O 0.2855(4) 0.7035(4) 0.0196(3) 0.0464 1.0000 Uani . . . . . . .
C22 C 0.2816(6) 0.7416(8) -0.0108(4) 0.0513 1.0000 Uani . . . . . . .
C23 C 0.2372(6) 0.8024(8) -0.0225(4) 0.0509 1.0000 Uani . . . . . . .
C24 C 0.2057(6) 0.8421(7) 0.0011(4) 0.0473 1.0000 Uani . . . . . . .
O25 O 0.2151(4) 0.8269(4) 0.0395(3) 0.0453 1.0000 Uani . . . . . . .
C26 C 0.3266(6) 0.7257(8) -0.0356(4) 0.0498 1.0000 Uani . . . . . . .
C27 C 0.3547(7) 0.6541(8) -0.0331(5) 0.0588 1.0000 Uani . . . . . . .
C28 C 0.4014(7) 0.6403(9) -0.0532(4) 0.0656 1.0000 Uani . . . . . . .
C29 C 0.4228(7) 0.6973(11) -0.0749(5) 0.0737 1.0000 Uani . . . . . . .
C30 C 0.3935(7) 0.7683(9) -0.0785(5) 0.0631 1.0000 Uani . . . . . . .
C31 C 0.3462(6) 0.7828(8) -0.0580(4) 0.0554 1.0000 Uani . . . . . . .
C32 C 0.1626(6) 0.9052(7) -0.0121(4) 0.0460 1.0000 Uani . . . . . . .
C33 C 0.1594(6) 0.9411(8) -0.0463(4) 0.0500 1.0000 Uani . . . . . . .
C34 C 0.1206(6) 1.0041(8) -0.0573(4) 0.0556 1.0000 Uani . . . . . . .
C35 C 0.0830(6) 1.0304(8) -0.0327(5) 0.0561 1.0000 Uani . . . . . . .
C36 C 0.0847(6) 0.9953(8) 0.0021(4) 0.0553 1.0000 Uani . . . . . . .
C37 C 0.1235(6) 0.9324(8) 0.0126(4) 0.0545 1.0000 Uani . . . . . . .
O38 O 0.3724(4) 0.8749(5) 0.0499(3) 0.0496 1.0000 Uani . . . . . . .
C39 C 0.3901(6) 0.9054(8) 0.0216(4) 0.0523 1.0000 Uani . . . . . . .
C40 C 0.3618(6) 0.9676(8) 0.0007(5) 0.0580 1.0000 Uani . . . . . . .
C41 C 0.3076(7) 1.0023(8) 0.0066(4) 0.0543 1.0000 Uani . . . . . . .
O42 O 0.2794(4) 0.9815(5) 0.0342(3) 0.0512 1.0000 Uani . . . . . . .
C43 C 0.4475(7) 0.8687(8) 0.0109(5) 0.0597 1.0000 Uani . . . . . . .
C44 C 0.4668(6) 0.7991(9) 0.0253(5) 0.0665 1.0000 Uani . . . . . . .
C45 C 0.5181(8) 0.7625(10) 0.0183(5) 0.0770 1.0000 Uani . . . . . . .
C46 C 0.5520(8) 0.7980(13) -0.0053(7) 0.0921 1.0000 Uani . . . . . . .
C47 C 0.5347(8) 0.8682(13) -0.0200(5) 0.0814 1.0000 Uani . . . . . . .
C48 C 0.4806(7) 0.9070(9) -0.0132(5) 0.0638 1.0000 Uani . . . . . . .
C49 C 0.2772(6) 1.0668(7) -0.0177(4) 0.0525 1.0000 Uani . . . . . . .
C50 C 0.2889(8) 1.0822(10) -0.0548(6) 0.0832 1.0000 Uani . . . . . . .
C51 C 0.2573(10) 1.1421(11) -0.0753(6) 0.0871 1.0000 Uani . . . . . . .
C52 C 0.2169(9) 1.1861(10) -0.0619(6) 0.0839 1.0000 Uani . . . . . . .
C53 C 0.2037(7) 1.1718(9) -0.0269(6) 0.0769 1.0000 Uani . . . . . . .
C54 C 0.2337(7) 1.1122(8) -0.0049(5) 0.0617 1.0000 Uani . . . . . . .
O55 O 0.2335(4) 0.5717(5) 0.0612(3) 0.0522 1.0000 Uani . . . . . . .
C56 C 0.2190(7) 0.5260(7) 0.0318(4) 0.0564 1.0000 Uani . . . . . . .
C57 C 0.1826(7) 0.5480(7) -0.0035(4) 0.0514 1.0000 Uani . . . . . . .
C58 C 0.1489(6) 0.6169(7) -0.0108(4) 0.0519 1.0000 Uani . . . . . . .
O59 O 0.1537(4) 0.6727(4) 0.0130(3) 0.0466 1.0000 Uani . . . . . . .
C60 C 0.1058(6) 0.6281(8) -0.0486(4) 0.0509 1.0000 Uani . . . . . . .
C61 C 0.0851(7) 0.7013(9) -0.0591(5) 0.0659 1.0000 Uani . . . . . . .
C62 C 0.0484(7) 0.7136(10) -0.0949(5) 0.0754 1.0000 Uani . . . . . . .
C63 C 0.0287(7) 0.6538(9) -0.1199(5) 0.0622 1.0000 Uani . . . . . . .
C64 C 0.0476(7) 0.5801(8) -0.1084(4) 0.0645 1.0000 Uani . . . . . . .
C65 C 0.0868(6) 0.5665(8) -0.0738(4) 0.0558 1.0000 Uani . . . . . . .
C66 C 0.2446(6) 0.4461(7) 0.0366(5) 0.0527 1.0000 Uani . . . . . . .
C67 C 0.2533(7) 0.4127(8) 0.0723(5) 0.0638 1.0000 Uani . . . . . . .
C68 C 0.2729(8) 0.3364(9) 0.0789(5) 0.0720 1.0000 Uani . . . . . . .
C69 C 0.2878(8) 0.2954(10) 0.0485(7) 0.0885 1.0000 Uani . . . . . . .
C70 C 0.2817(8) 0.3291(10) 0.0124(6) 0.0805 1.0000 Uani . . . . . . .
C72 C 0.2599(7) 0.4031(8) 0.0066(5) 0.0658 1.0000 Uani . . . . . . .
O73 O 0.1322(3) 0.6783(4) 0.0960(3) 0.0411 1.0000 Uani . . . . . . .
C74 C 0.0934(6) 0.6219(7) 0.0858(4) 0.0507 1.0000 Uani . . . . . . .
C75 C 0.0976(6) 0.5479(8) 0.1008(5) 0.0623 1.0000 Uani . . . . . . .
C76 C 0.1443(6) 0.5246(7) 0.1341(4) 0.0466 1.0000 Uani . . . . . . .
O77 O 0.1773(4) 0.5708(5) 0.1557(3) 0.0471 1.0000 Uani . . . . . . .
C78 C 0.0385(6) 0.6419(8) 0.0553(5) 0.0594 1.0000 Uani . . . . . . .
C79 C -0.0002(7) 0.5859(8) 0.0354(5) 0.0732 1.0000 Uani . . . . . . .
C80 C -0.0522(8) 0.6069(11) 0.0073(5) 0.0807 1.0000 Uani . . . . . . .
C82 C -0.0653(7) 0.6829(11) 0.0000(5) 0.0751 1.0000 Uani . . . . . . .
C83 C -0.0281(9) 0.7379(10) 0.0196(5) 0.0861 1.0000 Uani . . . . . . .
C84 C 0.0256(8) 0.7184(8) 0.0477(5) 0.0701 1.0000 Uani . . . . . . .
C85 C 0.1522(6) 0.4404(7) 0.1423(5) 0.0561 1.0000 Uani . . . . . . .
C86 C 0.1215(6) 0.3824(7) 0.1205(5) 0.0664 1.0000 Uani . . . . . . .
C87 C 0.1328(7) 0.3057(8) 0.1304(6) 0.0867 1.0000 Uani . . . . . . .
C88 C 0.1760(9) 0.2844(8) 0.1612(6) 0.0869 1.0000 Uani . . . . . . .
C89 C 0.2077(9) 0.3411(10) 0.1831(6) 0.0965 1.0000 Uani . . . . . . .
C90 C 0.1957(9) 0.4188(8) 0.1745(6) 0.0855 1.0000 Uani . . . . . . .
O91 O 0.1856(4) 0.6781(5) 0.2266(3) 0.0525 1.0000 Uani . . . . . . .
C92 C 0.1523(7) 0.6447(7) 0.2460(4) 0.0561 1.0000 Uani . . . . . . .
C93 C 0.0885(7) 0.6254(8) 0.2311(5) 0.0612 1.0000 Uani . . . . . . .
C94 C 0.0571(6) 0.6405(8) 0.1939(5) 0.0524 1.0000 Uani . . . . . . .
O95 O 0.0808(4) 0.6772(5) 0.1688(3) 0.0517 1.0000 Uani . . . . . . .
C96 C -0.0092(7) 0.6155(8) 0.1802(5) 0.0611 1.0000 Uani . . . . . . .
C97 C -0.0402(6) 0.6357(8) 0.1437(5) 0.0582 1.0000 Uani . . . . . . .
C98 C -0.1007(8) 0.6153(9) 0.1304(6) 0.0811 1.0000 Uani . . . . . . .
C99 C -0.1300(8) 0.5712(10) 0.1545(7) 0.0877 1.0000 Uani . . . . . . .
C100 C -0.1003(10) 0.5497(13) 0.1901(6) 0.0979 1.0000 Uani . . . . . . .
C101 C -0.0404(8) 0.5707(11) 0.2037(6) 0.0860 1.0000 Uani . . . . . . .
C102 C 0.1784(7) 0.6296(8) 0.2873(5) 0.0602 1.0000 Uani . . . . . . .
C103 C 0.2326(8) 0.6677(9) 0.3037(5) 0.0659 1.0000 Uani . . . . . . .
C104 C 0.2592(8) 0.6542(10) 0.3428(5) 0.0744 1.0000 Uani . . . . . . .
C105 C 0.2365(9) 0.5989(13) 0.3629(6) 0.0906 1.0000 Uani . . . . . . .
C106 C 0.1840(9) 0.5604(12) 0.3465(5) 0.0840 1.0000 Uani . . . . . . .
C107 C 0.1542(7) 0.5734(10) 0.3085(5) 0.0734 1.0000 Uani . . . . . . .
O108 O 0.3618(4) 0.6297(5) 0.2029(2) 0.0481 1.0000 Uani . . . . . . .
C109 C 0.3638(6) 0.5576(7) 0.1962(4) 0.0509 1.0000 Uani . . . . . . .
C110 C 0.3753(7) 0.5248(8) 0.1621(5) 0.0598 1.0000 Uani . . . . . . .
C111 C 0.3969(6) 0.5649(8) 0.1329(4) 0.0496 1.0000 Uani . . . . . . .
O112 O 0.4037(4) 0.6382(5) 0.1328(3) 0.0552 1.0000 Uani . . . . . . .
C113 C 0.3497(7) 0.5049(8) 0.2273(4) 0.0586 1.0000 Uani . . . . . . .
C114 C 0.3121(8) 0.5313(9) 0.2512(5) 0.0732 1.0000 Uani . . . . . . .
C115 C 0.2956(8) 0.4825(11) 0.2801(5) 0.0802 1.0000 Uani . . . . . . .
C116 C 0.3219(9) 0.4099(10) 0.2837(6) 0.0870 1.0000 Uani . . . . . . .
C117 C 0.3616(7) 0.3841(9) 0.2608(5) 0.0664 1.0000 Uani . . . . . . .
C118 C 0.3746(7) 0.4309(8) 0.2324(4) 0.0554 1.0000 Uani . . . . . . .
C119 C 0.4127(6) 0.5226(8) 0.0995(4) 0.0577 1.0000 Uani . . . . . . .
C120 C 0.4115(6) 0.4441(8) 0.0959(5) 0.0617 1.0000 Uani . . . . . . .
C121 C 0.4260(8) 0.4044(9) 0.0655(5) 0.0706 1.0000 Uani . . . . . . .
C122 C 0.4430(9) 0.4461(11) 0.0364(5) 0.0818 1.0000 Uani . . . . . . .
C123 C 0.4455(9) 0.5252(12) 0.0385(6) 0.0973 1.0000 Uani . . . . . . .
C124 C 0.4309(9) 0.5640(9) 0.0705(5) 0.0794 1.0000 Uani . . . . . . .
O125 O 0.4011(4) 0.7872(5) 0.2217(3) 0.0514 1.0000 Uani . . . . . . .
C126 C 0.4336(6) 0.8474(7) 0.2325(4) 0.0488 1.0000 Uani . . . . . . .
C127 C 0.4690(6) 0.8861(7) 0.2087(4) 0.0474 1.0000 Uani . . . . . . .
C128 C 0.4749(5) 0.8617(7) 0.1714(4) 0.0438 1.0000 Uani . . . . . . .
O129 O 0.4503(3) 0.8016(5) 0.1548(3) 0.0459 1.0000 Uani . . . . . . .
C130 C 0.4341(6) 0.8744(7) 0.2719(4) 0.0463 1.0000 Uani . . . . . . .
C131 C 0.4620(6) 0.9406(8) 0.2879(4) 0.0528 1.0000 Uani . . . . . . .
C132 C 0.4594(7) 0.9655(8) 0.3241(5) 0.0602 1.0000 Uani . . . . . . .
C133 C 0.4265(7) 0.9218(10) 0.3461(4) 0.0603 1.0000 Uani . . . . . . .
C134 C 0.3961(7) 0.8539(9) 0.3310(5) 0.0670 1.0000 Uani . . . . . . .
C135 C 0.4010(7) 0.8311(9) 0.2943(4) 0.0598 1.0000 Uani . . . . . . .
C136 C 0.5150(6) 0.9086(8) 0.1501(4) 0.0515 1.0000 Uani . . . . . . .
C137 C 0.5274(9) 0.8799(12) 0.1174(6) 0.1015 1.0000 Uani . . . . . . .
C138 C 0.5648(10) 0.9234(13) 0.0967(5) 0.1072 1.0000 Uani . . . . . . .
C139 C 0.5869(8) 0.9945(11) 0.1083(5) 0.0841 1.0000 Uani . . . . . . .
C140 C 0.5748(9) 1.0206(9) 0.1414(6) 0.0834 1.0000 Uani . . . . . . .
C141 C 0.5382(9) 0.9804(9) 0.1620(6) 0.0828 1.0000 Uani . . . . . . .
O142 O 0.2319(4) 0.8809(5) 0.2412(3) 0.0508 1.0000 Uani . . . . . . .
C143 C 0.1872(6) 0.8756(8) 0.2582(4) 0.0526 1.0000 Uani . . . . . . .
C144 C 0.1241(6) 0.8663(8) 0.2381(4) 0.0480 1.0000 Uani . . . . . . .
C145 C 0.1039(6) 0.8515(7) 0.1995(4) 0.0473 1.0000 Uani . . . . . . .
O146 O 0.1427(4) 0.8370(5) 0.1760(3) 0.0477 1.0000 Uani . . . . . . .
C147 C 0.2014(7) 0.8799(9) 0.3014(4) 0.0583 1.0000 Uani . . . . . . .
C148 C 0.2514(8) 0.9206(11) 0.3191(5) 0.0781 1.0000 Uani . . . . . . .
C149 C 0.2656(8) 0.9287(14) 0.3574(6) 0.0968 1.0000 Uani . . . . . . .
C150 C 0.2309(11) 0.8878(18) 0.3795(6) 0.1148 1.0000 Uani . . . . . . .
C151 C 0.1815(11) 0.8445(14) 0.3638(6) 0.1024 1.0000 Uani . . . . . . .
C152 C 0.1655(8) 0.8389(11) 0.3222(5) 0.0832 1.0000 Uani . . . . . . .
C153 C 0.0385(6) 0.8547(7) 0.1812(5) 0.0522 1.0000 Uani . . . . . . .
C154 C 0.0185(6) 0.8335(8) 0.1433(5) 0.0558 1.0000 Uani . . . . . . .
C155 C -0.0431(8) 0.8375(8) 0.1259(5) 0.0676 1.0000 Uani . . . . . . .
C156 C -0.0863(8) 0.8605(10) 0.1472(6) 0.0755 1.0000 Uani . . . . . . .
C157 C -0.0698(8) 0.8828(11) 0.1849(6) 0.0873 1.0000 Uani . . . . . . .
C158 C -0.0053(7) 0.8800(10) 0.2022(5) 0.0728 1.0000 Uani . . . . . . .
O159 O 0.3414(4) 1.0134(5) 0.1118(3) 0.0521 1.0000 Uani . . . . . . .
C160 C 0.3190(6) 1.0778(7) 0.1166(4) 0.0484 1.0000 Uani . . . . . . .
C161 C 0.2521(6) 1.0932(6) 0.1100(4) 0.0433 1.0000 Uani . . . . . . .
C162 C 0.2083(5) 1.0393(7) 0.1066(4) 0.0416 1.0000 Uani . . . . . . .
O163 O 0.2198(4) 0.9644(5) 0.1125(3) 0.0496 1.0000 Uani . . . . . . .
C164 C 0.3609(6) 1.1430(7) 0.1300(4) 0.0504 1.0000 Uani . . . . . . .
C165 C 0.4221(7) 1.1411(8) 0.1242(5) 0.0615 1.0000 Uani . . . . . . .
C166 C 0.4628(7) 1.2002(10) 0.1363(5) 0.0704 1.0000 Uani . . . . . . .
C167 C 0.4442(8) 1.2604(9) 0.1581(5) 0.0730 1.0000 Uani . . . . . . .
C168 C 0.3840(8) 1.2621(9) 0.1649(5) 0.0758 1.0000 Uani . . . . . . .
C169 C 0.3435(7) 1.2046(8) 0.1510(4) 0.0570 1.0000 Uani . . . . . . .
C170 C 0.1422(6) 1.0607(7) 0.0967(4) 0.0477 1.0000 Uani . . . . . . .
C171 C 0.1210(7) 1.1303(8) 0.0781(5) 0.0612 1.0000 Uani . . . . . . .
C172 C 0.0595(7) 1.1479(7) 0.0699(5) 0.0696 1.0000 Uani . . . . . . .
C173 C 0.0164(6) 1.0966(8) 0.0781(4) 0.0529 1.0000 Uani . . . . . . .
C174 C 0.0353(6) 1.0282(7) 0.0967(4) 0.0520 1.0000 Uani . . . . . . .
C175 C 0.0973(5) 1.0099(7) 0.1050(4) 0.0463 1.0000 Uani . . . . . . .
O176 O 0.1792(4) 1.0050(4) 0.1886(2) 0.0465 1.0000 Uani . . . . . . .
C177 C 0.1896(6) 1.0662(7) 0.2095(4) 0.0465 1.0000 Uani . . . . . . .
C178 C 0.2475(7) 1.0921(7) 0.2271(4) 0.0551 1.0000 Uani . . . . . . .
C179 C 0.3021(7) 1.0574(8) 0.2227(4) 0.0544 1.0000 Uani . . . . . . .
O180 O 0.3077(4) 0.9962(5) 0.2028(3) 0.0494 1.0000 Uani . . . . . . .
C182 C 0.1318(7) 1.1114(8) 0.2116(5) 0.0591 1.0000 Uani . . . . . . .
C183 C 0.0757(7) 1.0900(10) 0.1928(5) 0.0715 1.0000 Uani . . . . . . .
C184 C 0.0236(8) 1.1325(13) 0.1925(6) 0.0910 1.0000 Uani . . . . . . .
C185 C 0.0255(11) 1.1958(13) 0.2148(8) 0.1108 1.0000 Uani . . . . . . .
C186 C 0.0788(13) 1.2193(11) 0.2354(11) 0.1546 1.0000 Uani . . . . . . .
C187 C 0.1338(9) 1.1776(11) 0.2351(7) 0.1042 1.0000 Uani . . . . . . .
C188 C 0.3639(7) 1.0949(7) 0.2410(5) 0.0586 1.0000 Uani . . . . . . .
C189 C 0.4141(7) 1.0861(7) 0.2230(5) 0.0639 1.0000 Uani . . . . . . .
C190 C 0.4704(9) 1.1210(10) 0.2378(6) 0.0868 1.0000 Uani . . . . . . .
C191 C 0.4758(9) 1.1645(10) 0.2702(8) 0.0960 1.0000 Uani . . . . . . .
C192 C 0.4277(10) 1.1732(9) 0.2887(5) 0.0821 1.0000 Uani . . . . . . .
C193 C 0.3706(8) 1.1394(8) 0.2749(5) 0.0754 1.0000 Uani . . . . . . .
H231 H 0.2278 0.8169 -0.0507 0.0623 1.0000 Uiso . . . . . . .
H271 H 0.3407 0.6116 -0.0169 0.0692 1.0000 Uiso . . . . . . .
H281 H 0.4208 0.5869 -0.0526 0.0805 1.0000 Uiso . . . . . . .
H291 H 0.4595 0.6867 -0.0874 0.0861 1.0000 Uiso . . . . . . .
H301 H 0.4074 0.8099 -0.0958 0.0804 1.0000 Uiso . . . . . . .
H311 H 0.3257 0.8363 -0.0599 0.0686 1.0000 Uiso . . . . . . .
H331 H 0.1865 0.9210 -0.0645 0.0613 1.0000 Uiso . . . . . . .
H341 H 0.1193 1.0315 -0.0832 0.0655 1.0000 Uiso . . . . . . .
H351 H 0.0547 1.0754 -0.0406 0.0622 1.0000 Uiso . . . . . . .
H361 H 0.0572 1.0159 0.0198 0.0655 1.0000 Uiso . . . . . . .
H371 H 0.1245 0.9045 0.0381 0.0643 1.0000 Uiso . . . . . . .
H401 H 0.3817 0.9882 -0.0211 0.0730 1.0000 Uiso . . . . . . .
H441 H 0.4393 0.7711 0.0413 0.0810 1.0000 Uiso . . . . . . .
H451 H 0.5316 0.7103 0.0309 0.0957 1.0000 Uiso . . . . . . .
H461 H 0.5884 0.7728 -0.0136 0.1042 1.0000 Uiso . . . . . . .
H471 H 0.5610 0.8945 -0.0371 0.0976 1.0000 Uiso . . . . . . .
H481 H 0.4677 0.9587 -0.0251 0.0804 1.0000 Uiso . . . . . . .
H501 H 0.3197 1.0505 -0.0659 0.0965 1.0000 Uiso . . . . . . .
H511 H 0.2643 1.1522 -0.1025 0.1044 1.0000 Uiso . . . . . . .
H521 H 0.1971 1.2304 -0.0780 0.0920 1.0000 Uiso . . . . . . .
H531 H 0.1720 1.2044 -0.0171 0.0864 1.0000 Uiso . . . . . . .
H541 H 0.2238 1.1009 0.0217 0.0752 1.0000 Uiso . . . . . . .
H571 H 0.1798 0.5106 -0.0260 0.0611 1.0000 Uiso . . . . . . .
H611 H 0.0967 0.7468 -0.0406 0.0805 1.0000 Uiso . . . . . . .
H621 H 0.0353 0.7681 -0.1036 0.0855 1.0000 Uiso . . . . . . .
H631 H 0.0006 0.6642 -0.1466 0.0779 1.0000 Uiso . . . . . . .
H641 H 0.0321 0.5350 -0.1263 0.0762 1.0000 Uiso . . . . . . .
H651 H 0.1023 0.5119 -0.0663 0.0666 1.0000 Uiso . . . . . . .
H671 H 0.2451 0.4454 0.0949 0.0734 1.0000 Uiso . . . . . . .
H681 H 0.2755 0.3112 0.1053 0.0832 1.0000 Uiso . . . . . . .
H691 H 0.3033 0.2400 0.0526 0.1025 1.0000 Uiso . . . . . . .
H701 H 0.2935 0.2993 -0.0106 0.0982 1.0000 Uiso . . . . . . .
H721 H 0.2536 0.4271 -0.0205 0.0822 1.0000 Uiso . . . . . . .
H751 H 0.0661 0.5079 0.0890 0.0704 1.0000 Uiso . . . . . . .
H791 H 0.0092 0.5290 0.0411 0.0878 1.0000 Uiso . . . . . . .
H801 H -0.0785 0.5653 -0.0076 0.0963 1.0000 Uiso . . . . . . .
H821 H -0.1027 0.7004 -0.0204 0.0874 1.0000 Uiso . . . . . . .
H831 H -0.0390 0.7935 0.0145 0.0979 1.0000 Uiso . . . . . . .
H841 H 0.0541 0.7605 0.0605 0.0858 1.0000 Uiso . . . . . . .
H861 H 0.0878 0.3963 0.0978 0.0824 1.0000 Uiso . . . . . . .
H871 H 0.1101 0.2646 0.1127 0.0976 1.0000 Uiso . . . . . . .
H881 H 0.1843 0.2278 0.1679 0.1010 1.0000 Uiso . . . . . . .
H891 H 0.2423 0.3270 0.2061 0.1092 1.0000 Uiso . . . . . . .
H901 H 0.2186 0.4602 0.1915 0.0965 1.0000 Uiso . . . . . . .
H931 H 0.0636 0.5993 0.2491 0.0774 1.0000 Uiso . . . . . . .
H971 H -0.0159 0.6675 0.1271 0.0670 1.0000 Uiso . . . . . . .
H981 H -0.1229 0.6305 0.1028 0.0980 1.0000 Uiso . . . . . . .
H991 H -0.1755 0.5571 0.1453 0.1092 1.0000 Uiso . . . . . . .
H1001 H -0.1223 0.5146 0.2067 0.1109 1.0000 Uiso . . . . . . .
H1011 H -0.0171 0.5561 0.2306 0.0995 1.0000 Uiso . . . . . . .
H1031 H 0.2526 0.7045 0.2871 0.0755 1.0000 Uiso . . . . . . .
H1041 H 0.2951 0.6881 0.3562 0.0892 1.0000 Uiso . . . . . . .
H1051 H 0.2589 0.5860 0.3905 0.1091 1.0000 Uiso . . . . . . .
H1061 H 0.1655 0.5209 0.3631 0.0985 1.0000 Uiso . . . . . . .
H1071 H 0.1157 0.5439 0.2965 0.0933 1.0000 Uiso . . . . . . .
H1101 H 0.3687 0.4675 0.1586 0.0710 1.0000 Uiso . . . . . . .
H1141 H 0.2973 0.5868 0.2493 0.0858 1.0000 Uiso . . . . . . .
H1151 H 0.2641 0.5000 0.2962 0.0963 1.0000 Uiso . . . . . . .
H1161 H 0.3111 0.3740 0.3043 0.0974 1.0000 Uiso . . . . . . .
H1171 H 0.3811 0.3307 0.2651 0.0772 1.0000 Uiso . . . . . . .
H1181 H 0.4025 0.4124 0.2146 0.0633 1.0000 Uiso . . . . . . .
H1201 H 0.3991 0.4134 0.1178 0.0735 1.0000 Uiso . . . . . . .
H1211 H 0.4243 0.3453 0.0648 0.0821 1.0000 Uiso . . . . . . .
H1221 H 0.4520 0.4173 0.0130 0.0997 1.0000 Uiso . . . . . . .
H1231 H 0.4589 0.5570 0.0168 0.1108 1.0000 Uiso . . . . . . .
H1241 H 0.4345 0.6225 0.0723 0.0913 1.0000 Uiso . . . . . . .
H1271 H 0.4917 0.9348 0.2195 0.0560 1.0000 Uiso . . . . . . .
H1311 H 0.4856 0.9727 0.2714 0.0639 1.0000 Uiso . . . . . . .
H1321 H 0.4816 1.0145 0.3343 0.0714 1.0000 Uiso . . . . . . .
H1331 H 0.4257 0.9386 0.3736 0.0694 1.0000 Uiso . . . . . . .
H1341 H 0.3690 0.8238 0.3465 0.0837 1.0000 Uiso . . . . . . .
H1351 H 0.3793 0.7815 0.2835 0.0758 1.0000 Uiso . . . . . . .
H1371 H 0.5134 0.8256 0.1078 0.1270 1.0000 Uiso . . . . . . .
H1381 H 0.5772 0.8995 0.0728 0.1272 1.0000 Uiso . . . . . . .
H1391 H 0.6094 1.0279 0.0922 0.1088 1.0000 Uiso . . . . . . .
H1401 H 0.5932 1.0715 0.1512 0.0967 1.0000 Uiso . . . . . . .
H1411 H 0.5279 1.0042 0.1867 0.1031 1.0000 Uiso . . . . . . .
H1441 H 0.0902 0.8703 0.2538 0.0583 1.0000 Uiso . . . . . . .
H1481 H 0.2782 0.9477 0.3017 0.0963 1.0000 Uiso . . . . . . .
H1491 H 0.3012 0.9652 0.3701 0.1130 1.0000 Uiso . . . . . . .
H1501 H 0.2431 0.8896 0.4088 0.1307 1.0000 Uiso . . . . . . .
H1511 H 0.1562 0.8172 0.3813 0.1231 1.0000 Uiso . . . . . . .
H1521 H 0.1295 0.8055 0.3092 0.1064 1.0000 Uiso . . . . . . .
H1541 H 0.0505 0.8131 0.1285 0.0654 1.0000 Uiso . . . . . . .
H1551 H -0.0564 0.8225 0.0972 0.0832 1.0000 Uiso . . . . . . .
H1561 H -0.1316 0.8616 0.1339 0.0900 1.0000 Uiso . . . . . . .
H1571 H -0.1025 0.8984 0.2003 0.1105 1.0000 Uiso . . . . . . .
H1581 H 0.0093 0.8985 0.2298 0.0862 1.0000 Uiso . . . . . . .
H1611 H 0.2387 1.1487 0.1077 0.0483 1.0000 Uiso . . . . . . .
H1651 H 0.4361 1.0950 0.1101 0.0754 1.0000 Uiso . . . . . . .
H1661 H 0.5054 1.2012 0.1295 0.0866 1.0000 Uiso . . . . . . .
H1671 H 0.4742 1.3024 0.1692 0.0860 1.0000 Uiso . . . . . . .
H1681 H 0.3700 1.3070 0.1804 0.0849 1.0000 Uiso . . . . . . .
H1691 H 0.2997 1.2058 0.1564 0.0674 1.0000 Uiso . . . . . . .
H1711 H 0.1525 1.1673 0.0705 0.0751 1.0000 Uiso . . . . . . .
H1721 H 0.0458 1.1994 0.0576 0.0774 1.0000 Uiso . . . . . . .
H1731 H -0.0290 1.1099 0.0707 0.0608 1.0000 Uiso . . . . . . .
H1741 H 0.0037 0.9919 0.1046 0.0653 1.0000 Uiso . . . . . . .
H1751 H 0.1105 0.9584 0.1172 0.0583 1.0000 Uiso . . . . . . .
H1781 H 0.2502 1.1399 0.2441 0.0650 1.0000 Uiso . . . . . . .
H1891 H 0.4102 1.0535 0.1984 0.0721 1.0000 Uiso . . . . . . .
H1901 H 0.5081 1.1159 0.2242 0.0976 1.0000 Uiso . . . . . . .
H1911 H 0.5165 1.1905 0.2816 0.1011 1.0000 Uiso . . . . . . .
H1921 H 0.4322 1.2060 0.3134 0.0923 1.0000 Uiso . . . . . . .
H1931 H 0.3331 1.1461 0.2882 0.0871 1.0000 Uiso . . . . . . .
H1821 H 0.0722 1.0400 0.1778 0.0874 1.0000 Uiso . . . . . . .
H1822 H -0.0161 1.1161 0.1759 0.1105 1.0000 Uiso . . . . . . .
H1823 H -0.0141 1.2240 0.2158 0.1325 1.0000 Uiso . . . . . . .
H1824 H 0.0790 1.2670 0.2512 0.1886 1.0000 Uiso . . . . . . .
H1825 H 0.1732 1.1953 0.2517 0.1270 1.0000 Uiso . . . . . . .
H131 H 0.3556 0.7512 0.0779 0.0592 1.0000 Uiso . . . . . . .
H111 H 0.2717 0.6051 0.1354 0.0518 1.0000 Uiso . . . . . . .
H121 H 0.2796 0.7618 0.2214 0.0531 1.0000 Uiso . . . . . . .
H141 H 0.3650 0.9118 0.1625 0.0458 1.0000 Uiso . . . . . . .
H11 H 0.1706 0.8285 0.1059 0.0479 1.0000 Uiso . . . . . . .
loop_
_atom_type_symbol
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_Cromer_Mann_a1
_atom_type_scat_Cromer_Mann_b1
_atom_type_scat_Cromer_Mann_a2
_atom_type_scat_Cromer_Mann_b2
_atom_type_scat_Cromer_Mann_a3
_atom_type_scat_Cromer_Mann_b3
_atom_type_scat_Cromer_Mann_a4
_atom_type_scat_Cromer_Mann_b4
_atom_type_scat_Cromer_Mann_c
_atom_type_scat_source
C 0.0033 0.0016 2.3100 20.8439 1.0200 10.2075 1.5886 0.5687 0.8650 51.6512
0.2156 'International Tables Vol C 4.2.6.8 and 6.1.1.4'
H 0.0000 0.0000 0.4930 10.5109 0.3229 26.1257 0.1402 3.1424 0.0408 57.7998
0.0030 'International Tables Vol C 4.2.6.8 and 6.1.1.4'
Eu -0.1578 3.6682 24.6274 2.3879 19.0886 0.1942 13.7603 13.7546 2.9227 123.1740
2.5745 'International Tables Vol C 4.2.6.8 and 6.1.1.4'
O 0.0106 0.0060 3.0485 13.2771 2.2868 5.7011 1.5463 0.3239 0.8670 32.9089
0.2508 'International Tables Vol C 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_site_symmetry_1
_geom_angle_atom_site_label_2
_geom_angle_site_symmetry_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
O1 . Eu1 . O12 . 67.6(3) yes
O1 . Eu1 . O14 . 70.9(3) yes
O12 . Eu1 . O14 . 73.1(3) yes
O1 . Eu1 . O142 . 129.3(3) yes
O12 . Eu1 . O142 . 72.3(3) yes
O14 . Eu1 . O142 . 124.4(3) yes
O1 . Eu1 . O146 . 69.0(3) yes
O12 . Eu1 . O146 . 76.8(3) yes
O14 . Eu1 . O146 . 136.6(3) yes
O142 . Eu1 . O146 . 72.9(3) yes
O1 . Eu1 . O163 . 64.9(3) yes
O12 . Eu1 . O163 . 129.3(3) yes
O14 . Eu1 . O163 . 75.7(3) yes
O142 . Eu1 . O163 . 156.7(3) yes
O146 . Eu1 . O163 . 101.3(3) yes
O1 . Eu1 . O176 . 124.9(3) yes
O12 . Eu1 . O176 . 145.6(3) yes
O14 . Eu1 . O176 . 139.5(3) yes
O142 . Eu1 . O176 . 77.3(3) yes
O146 . Eu1 . O176 . 79.3(3) yes
O1 . Eu1 . O180 . 143.3(3) yes
O12 . Eu1 . O180 . 116.8(3) yes
O14 . Eu1 . O180 . 75.8(3) yes
O142 . Eu1 . O180 . 82.7(3) yes
O146 . Eu1 . O180 . 146.9(3) yes
O163 . Eu1 . O176 . 79.5(3) yes
O163 . Eu1 . O180 . 92.3(3) yes
O176 . Eu1 . O180 . 73.8(3) yes
O1 . Eu2 . O11 . 68.4(3) yes
O1 . Eu2 . O13 . 69.5(3) yes
O11 . Eu2 . O13 . 70.4(3) yes
O1 . Eu2 . O21 . 130.1(3) yes
O11 . Eu2 . O21 . 124.3(3) yes
O13 . Eu2 . O21 . 71.7(3) yes
O1 . Eu2 . O25 . 69.0(3) yes
O11 . Eu2 . O25 . 132.6(3) yes
O13 . Eu2 . O25 . 76.1(3) yes
O21 . Eu2 . O25 . 72.2(3) yes
O1 . Eu2 . O55 . 143.6(3) yes
O11 . Eu2 . O55 . 79.0(3) yes
O13 . Eu2 . O55 . 114.7(3) yes
O21 . Eu2 . O55 . 81.6(3) yes
O25 . Eu2 . O55 . 147.0(3) yes
O1 . Eu2 . O59 . 125.1(3) yes
O11 . Eu2 . O59 . 143.4(3) yes
O13 . Eu2 . O59 . 144.3(3) yes
O21 . Eu2 . O59 . 75.9(3) yes
O25 . Eu2 . O59 . 80.1(3) yes
O1 . Eu2 . O73 . 69.5(3) yes
O11 . Eu2 . O73 . 76.0(3) yes
O13 . Eu2 . O73 . 134.0(3) yes
O21 . Eu2 . O73 . 154.1(3) yes
O25 . Eu2 . O73 . 107.2(3) yes
O55 . Eu2 . O59 . 74.2(3) yes
O55 . Eu2 . O73 . 87.8(3) yes
O59 . Eu2 . O73 . 78.5(3) yes
O1 . Eu3 . O13 . 66.9(3) yes
O1 . Eu3 . O14 . 67.6(2) yes
O13 . Eu3 . O14 . 73.3(3) yes
O1 . Eu3 . O25 . 65.0(3) yes
O13 . Eu3 . O25 . 75.9(3) yes
O14 . Eu3 . O25 . 130.6(3) yes
O1 . Eu3 . O38 . 138.3(3) yes
O13 . Eu3 . O38 . 73.2(3) yes
O14 . Eu3 . O38 . 112.0(3) yes
O25 . Eu3 . O38 . 94.4(3) yes
O1 . Eu3 . O42 . 132.2(3) yes
O13 . Eu3 . O42 . 135.2(3) yes
O14 . Eu3 . O42 . 147.1(3) yes
O25 . Eu3 . O42 . 79.6(3) yes
O38 . Eu3 . O42 . 72.0(3) yes
O1 . Eu3 . O159 . 124.2(3) yes
O13 . Eu3 . O159 . 133.2(3) yes
O14 . Eu3 . O159 . 72.0(3) yes
O25 . Eu3 . O159 . 150.6(3) yes
O38 . Eu3 . O159 . 91.9(3) yes
O1 . Eu3 . O163 . 63.1(3) yes
O13 . Eu3 . O163 . 128.6(3) yes
O14 . Eu3 . O163 . 77.8(3) yes
O25 . Eu3 . O163 . 92.9(3) yes
O38 . Eu3 . O163 . 158.2(3) yes
O42 . Eu3 . O159 . 75.2(3) yes
O42 . Eu3 . O163 . 89.2(3) yes
O159 . Eu3 . O163 . 72.2(3) yes
O1 . Eu4 . O11 . 68.7(3) yes
O1 . Eu4 . O12 . 69.0(3) yes
O11 . Eu4 . O12 . 72.8(3) yes
O1 . Eu4 . O73 . 71.0(3) yes
O11 . Eu4 . O73 . 76.4(3) yes
O12 . Eu4 . O73 . 136.1(3) yes
O1 . Eu4 . O77 . 130.5(3) yes
O11 . Eu4 . O77 . 70.3(3) yes
O12 . Eu4 . O77 . 122.4(3) yes
O73 . Eu4 . O77 . 73.3(3) yes
O1 . Eu4 . O91 . 141.2(3) yes
O11 . Eu4 . O91 . 117.6(3) yes
O12 . Eu4 . O91 . 76.6(3) yes
O73 . Eu4 . O91 . 146.7(3) yes
O77 . Eu4 . O91 . 83.2(3) yes
O1 . Eu4 . O95 . 126.3(3) yes
O11 . Eu4 . O95 . 143.5(3) yes
O12 . Eu4 . O95 . 141.5(3) yes
O73 . Eu4 . O95 . 78.6(3) yes
O77 . Eu4 . O95 . 77.3(3) yes
O1 . Eu4 . O146 . 68.2(3) yes
O11 . Eu4 . O146 . 133.3(3) yes
O12 . Eu4 . O146 . 75.8(3) yes
O73 . Eu4 . O146 . 105.3(3) yes
O77 . Eu4 . O146 . 156.0(3) yes
O91 . Eu4 . O95 . 73.4(3) yes
O91 . Eu4 . O146 . 86.8(3) yes
O95 . Eu4 . O146 . 79.0(3) yes
O11 . Eu5 . O12 . 70.0(3) yes
O11 . Eu5 . O13 . 68.6(3) yes
O12 . Eu5 . O13 . 107.0(3) yes
O11 . Eu5 . O14 . 107.9(2) yes
O12 . Eu5 . O14 . 69.9(3) yes
O13 . Eu5 . O14 . 69.7(3) yes
O11 . Eu5 . O108 . 76.7(3) yes
O12 . Eu5 . O108 . 81.5(3) yes
O13 . Eu5 . O108 . 137.9(3) yes
O14 . Eu5 . O108 . 146.4(3) yes
O11 . Eu5 . O112 . 80.4(3) yes
O12 . Eu5 . O112 . 144.7(3) yes
O13 . Eu5 . O112 . 78.2(3) yes
O14 . Eu5 . O112 . 140.1(3) yes
O108 . Eu5 . O112 . 73.2(3) yes
O11 . Eu5 . O125 . 137.3(3) yes
O12 . Eu5 . O125 . 74.1(3) yes
O13 . Eu5 . O125 . 146.3(3) yes
O14 . Eu5 . O125 . 79.8(3) yes
O108 . Eu5 . O125 . 75.8(3) yes
O11 . Eu5 . O129 . 150.3(3) yes
O12 . Eu5 . O129 . 134.2(3) yes
O13 . Eu5 . O129 . 85.5(3) yes
O14 . Eu5 . O129 . 74.2(3) yes
O108 . Eu5 . O129 . 118.6(3) yes
O112 . Eu5 . O125 . 121.0(3) yes
O112 . Eu5 . O129 . 80.4(3) yes
O125 . Eu5 . O129 . 72.4(3) yes
Eu3 . O1 . Eu2 . 86.1(2) yes
Eu3 . O1 . Eu1 . 86.0(2) yes
Eu2 . O1 . Eu1 . 159.3(3) yes
Eu3 . O1 . Eu4 . 156.1(3) yes
Eu2 . O1 . Eu4 . 89.6(2) yes
Eu1 . O1 . Eu4 . 90.0(3) yes
Eu3 . O1 . H11 . 104.1 no
Eu2 . O1 . H11 . 99.6 no
Eu1 . O1 . H11 . 100.8 no
Eu4 . O1 . H11 . 99.8 no
Eu5 . O11 . Eu4 . 107.6(3) yes
Eu5 . O11 . Eu2 . 110.2(3) yes
Eu4 . O11 . Eu2 . 98.7(3) yes
Eu5 . O11 . H111 . 113.5 no
Eu4 . O11 . H111 . 113.1 no
Eu2 . O11 . H111 . 112.8 no
Eu5 . O12 . Eu1 . 108.1(3) yes
Eu5 . O12 . Eu4 . 109.2(3) yes
Eu1 . O12 . Eu4 . 100.1(3) yes
Eu5 . O12 . H121 . 112.7 no
Eu1 . O12 . H121 . 112.8 no
Eu4 . O12 . H121 . 113.1 no
Eu5 . O13 . Eu2 . 110.0(3) yes
Eu5 . O13 . Eu3 . 109.5(3) yes
Eu2 . O13 . Eu3 . 101.2(3) yes
Eu5 . O13 . H131 . 111.9 no
Eu2 . O13 . H131 . 111.9 no
Eu3 . O13 . H131 . 111.8 no
Eu5 . O14 . Eu1 . 108.3(3) yes
Eu5 . O14 . Eu3 . 107.5(3) yes
Eu1 . O14 . Eu3 . 102.0(3) yes
Eu5 . O14 . H141 . 112.9 no
Eu1 . O14 . H141 . 112.5 no
Eu3 . O14 . H141 . 113.0 no
Eu2 . O21 . C22 . 133.0(8) yes
O21 . C22 . C23 . 124.2(13) yes
O21 . C22 . C26 . 118.1(12) yes
C23 . C22 . C26 . 117.6(13) yes
C22 . C23 . C24 . 126.0(13) yes
C22 . C23 . H231 . 117.5 no
C24 . C23 . H231 . 116.5 no
C23 . C24 . O25 . 120.9(12) yes
C23 . C24 . C32 . 123.6(14) yes
O25 . C24 . C32 . 115.4(12) yes
C24 . O25 . Eu3 . 121.2(7) yes
C24 . O25 . Eu2 . 126.8(7) yes
Eu3 . O25 . Eu2 . 98.2(3) yes
C22 . C26 . C27 . 118.4(13) yes
C22 . C26 . C31 . 121.9(13) yes
C27 . C26 . C31 . 119.3(13) yes
C26 . C27 . C28 . 119.6(14) yes
C26 . C27 . H271 . 120.3 no
C28 . C27 . H271 . 120.1 no
C27 . C28 . C29 . 121.9(14) yes
C27 . C28 . H281 . 120.0 no
C29 . C28 . H281 . 118.1 no
C28 . C29 . C30 . 118.7(14) yes
C28 . C29 . H291 . 120.0 no
C30 . C29 . H291 . 121.3 no
C29 . C30 . C31 . 119.4(14) yes
C29 . C30 . H301 . 119.3 no
C31 . C30 . H301 . 121.3 no
C30 . C31 . C26 . 120.9(13) yes
C30 . C31 . H311 . 119.2 no
C26 . C31 . H311 . 119.9 no
C24 . C32 . C33 . 123.3(13) yes
C24 . C32 . C37 . 118.9(13) yes
C33 . C32 . C37 . 117.8(13) yes
C32 . C33 . C34 . 122.1(14) yes
C32 . C33 . H331 . 118.2 no
C34 . C33 . H331 . 119.6 no
C33 . C34 . C35 . 119.5(13) yes
C33 . C34 . H341 . 121.3 no
C35 . C34 . H341 . 119.2 no
C34 . C35 . C36 . 120.0(12) yes
C34 . C35 . H351 . 119.6 no
C36 . C35 . H351 . 120.3 no
C35 . C36 . C37 . 119.8(14) yes
C35 . C36 . H361 . 118.8 no
C37 . C36 . H361 . 121.4 no
C32 . C37 . C36 . 120.8(14) yes
C32 . C37 . H371 . 118.4 no
C36 . C37 . H371 . 120.8 no
Eu3 . O38 . C39 . 137.2(8) yes
O38 . C39 . C40 . 125.1(13) yes
O38 . C39 . C43 . 114.9(12) yes
C40 . C39 . C43 . 120.0(14) yes
C39 . C40 . C41 . 124.6(14) yes
C39 . C40 . H401 . 117.4 no
C41 . C40 . H401 . 118.0 no
C40 . C41 . O42 . 122.8(13) yes
C40 . C41 . C49 . 122.7(14) yes
O42 . C41 . C49 . 114.5(13) yes
C41 . O42 . Eu3 . 138.0(8) yes
C39 . C43 . C44 . 119.7(14) yes
C39 . C43 . C48 . 120.7(14) yes
C44 . C43 . C48 . 119.6(15) yes
C43 . C44 . C45 . 124.1(16) yes
C43 . C44 . H441 . 117.1 no
C45 . C44 . H441 . 118.7 no
C44 . C45 . C46 . 118.2(17) yes
C44 . C45 . H451 . 120.8 no
C46 . C45 . H451 . 120.9 no
C45 . C46 . C47 . 119.5(16) yes
C45 . C46 . H461 . 122.9 no
C47 . C46 . H461 . 117.5 no
C46 . C47 . C48 . 122.9(17) yes
C46 . C47 . H471 . 118.6 no
C48 . C47 . H471 . 118.5 no
C47 . C48 . C43 . 115.5(16) yes
C47 . C48 . H481 . 121.8 no
C43 . C48 . H481 . 122.7 no
C41 . C49 . C50 . 122.6(14) yes
C41 . C49 . C54 . 119.9(14) yes
C50 . C49 . C54 . 117.5(13) yes
C49 . C50 . C51 . 118.0(18) yes
C49 . C50 . H501 . 121.1 no
C51 . C50 . H501 . 120.9 no
C50 . C51 . C52 . 123.3(19) yes
C50 . C51 . H511 . 118.3 no
C52 . C51 . H511 . 118.3 no
C51 . C52 . C53 . 120.1(16) yes
C51 . C52 . H521 . 118.9 no
C53 . C52 . H521 . 121.0 no
C52 . C53 . C54 . 119.4(17) yes
C52 . C53 . H531 . 119.7 no
C54 . C53 . H531 . 120.9 no
C49 . C54 . C53 . 121.7(16) yes
C49 . C54 . H541 . 118.5 no
C53 . C54 . H541 . 119.8 no
Eu2 . O55 . C56 . 133.8(8) yes
O55 . C56 . C57 . 124.0(12) yes
O55 . C56 . C66 . 116.4(13) yes
C57 . C56 . C66 . 119.5(13) yes
C56 . C57 . C58 . 126.0(13) yes
C56 . C57 . H571 . 117.6 no
C58 . C57 . H571 . 116.4 no
C57 . C58 . O59 . 123.2(12) yes
C57 . C58 . C60 . 119.8(12) yes
O59 . C58 . C60 . 117.0(11) yes
C58 . O59 . Eu2 . 133.0(8) yes
C58 . C60 . C61 . 118.8(13) yes
C58 . C60 . C65 . 122.1(12) yes
C61 . C60 . C65 . 119.0(13) yes
C60 . C61 . C62 . 119.7(14) yes
C60 . C61 . H611 . 120.4 no
C62 . C61 . H611 . 119.9 no
C61 . C62 . C63 . 122.1(15) yes
C61 . C62 . H621 . 120.1 no
C63 . C62 . H621 . 117.8 no
C62 . C63 . C64 . 117.7(14) yes
C62 . C63 . H631 . 120.8 no
C64 . C63 . H631 . 121.5 no
C63 . C64 . C65 . 121.6(13) yes
C63 . C64 . H641 . 118.5 no
C65 . C64 . H641 . 119.9 no
C60 . C65 . C64 . 119.8(13) yes
C60 . C65 . H651 . 119.5 no
C64 . C65 . H651 . 120.7 no
C56 . C66 . C67 . 118.6(14) yes
C56 . C66 . C72 . 123.5(14) yes
C67 . C66 . C72 . 117.9(13) yes
C66 . C67 . C68 . 122.5(15) yes
C66 . C67 . H671 . 118.2 no
C68 . C67 . H671 . 119.4 no
C67 . C68 . C69 . 118.0(16) yes
C67 . C68 . H681 . 121.2 no
C69 . C68 . H681 . 120.8 no
C68 . C69 . C70 . 120.5(16) yes
C68 . C69 . H691 . 119.6 no
C70 . C69 . H691 . 119.9 no
C69 . C70 . C72 . 119.9(17) yes
C69 . C70 . H701 . 121.3 no
C72 . C70 . H701 . 118.8 no
C66 . C72 . C70 . 121.1(16) yes
C66 . C72 . H721 . 119.1 no
C70 . C72 . H721 . 119.8 no
Eu2 . O73 . Eu4 . 94.8(2) yes
Eu2 . O73 . C74 . 125.1(8) yes
Eu4 . O73 . C74 . 124.1(8) yes
O73 . C74 . C75 . 126.6(12) yes
O73 . C74 . C78 . 115.0(11) yes
C75 . C74 . C78 . 118.4(12) yes
C74 . C75 . C76 . 123.3(11) yes
C74 . C75 . H751 . 119.0 no
C76 . C75 . H751 . 117.7 no
C75 . C76 . O77 . 123.8(11) yes
C75 . C76 . C85 . 117.7(11) yes
O77 . C76 . C85 . 118.5(12) yes
C76 . O77 . Eu4 . 134.9(8) yes
C74 . C78 . C79 . 122.4(13) yes
C74 . C78 . C84 . 118.2(13) yes
C79 . C78 . C84 . 119.3(15) yes
C78 . C79 . C80 . 120.9(14) yes
C78 . C79 . H791 . 119.5 no
C80 . C79 . H791 . 119.6 no
C79 . C80 . C82 . 119.8(15) yes
C79 . C80 . H801 . 119.5 no
C82 . C80 . H801 . 120.7 no
C80 . C82 . C83 . 119.7(15) yes
C80 . C82 . H821 . 121.9 no
C83 . C82 . H821 . 118.4 no
C82 . C83 . C84 . 121.9(15) yes
C82 . C83 . H831 . 118.8 no
C84 . C83 . H831 . 119.3 no
C83 . C84 . C78 . 118.5(15) yes
C83 . C84 . H841 . 120.1 no
C78 . C84 . H841 . 121.4 no
C76 . C85 . C86 . 125.6(14) yes
C76 . C85 . C90 . 117.4(12) yes
C86 . C85 . C90 . 117.1(13) yes
C85 . C86 . C87 . 121.1(15) yes
C85 . C86 . H861 . 119.0 no
C87 . C86 . H861 . 119.8 no
C86 . C87 . C88 . 122.0(15) yes
C86 . C87 . H871 . 118.3 no
C88 . C87 . H871 . 119.6 no
C87 . C88 . C89 . 117.9(14) yes
C87 . C88 . H881 . 121.2 no
C89 . C88 . H881 . 120.9 no
C88 . C89 . C90 . 121.2(16) yes
C88 . C89 . H891 . 120.0 no
C90 . C89 . H891 . 118.8 no
C89 . C90 . C85 . 120.7(15) yes
C89 . C90 . H901 . 120.3 no
C85 . C90 . H901 . 119.0 no
Eu4 . O91 . C92 . 136.4(9) yes
O91 . C92 . C93 . 122.9(13) yes
O91 . C92 . C102 . 117.9(13) yes
C93 . C92 . C102 . 119.0(14) yes
C92 . C93 . C94 . 125.2(13) yes
C92 . C93 . H931 . 118.4 no
C94 . C93 . H931 . 116.4 no
C93 . C94 . O95 . 123.7(12) yes
C93 . C94 . C96 . 121.6(14) yes
O95 . C94 . C96 . 114.6(14) yes
C94 . O95 . Eu4 . 134.4(8) yes
C94 . C96 . C97 . 120.1(14) yes
C94 . C96 . C101 . 121.3(15) yes
C97 . C96 . C101 . 118.6(13) yes
C96 . C97 . C98 . 122.0(16) yes
C96 . C97 . H971 . 116.7 no
C98 . C97 . H971 . 121.4 no
C97 . C98 . C99 . 117.7(17) yes
C97 . C98 . H981 . 120.7 no
C99 . C98 . H981 . 121.5 no
C98 . C99 . C100 . 121.4(16) yes
C98 . C99 . H991 . 118.6 no
C100 . C99 . H991 . 119.9 no
C99 . C100 . C101 . 121.2(18) yes
C99 . C100 . H1001 . 119.9 no
C101 . C100 . H1001 . 118.8 no
C96 . C101 . C100 . 119.0(18) yes
C96 . C101 . H1011 . 118.0 no
C100 . C101 . H1011 . 123.0 no
C92 . C102 . C103 . 117.9(14) yes
C92 . C102 . C107 . 122.4(14) yes
C103 . C102 . C107 . 119.3(15) yes
C102 . C103 . C104 . 119.6(15) yes
C102 . C103 . H1031 . 118.9 no
C104 . C103 . H1031 . 121.5 no
C103 . C104 . C105 . 120.5(16) yes
C103 . C104 . H1041 . 119.7 no
C105 . C104 . H1041 . 119.7 no
C104 . C105 . C106 . 119.6(18) yes
C104 . C105 . H1051 . 119.7 no
C106 . C105 . H1051 . 120.7 no
C105 . C106 . C107 . 122.3(17) yes
C105 . C106 . H1061 . 118.4 no
C107 . C106 . H1061 . 119.3 no
C102 . C107 . C106 . 118.3(15) yes
C102 . C107 . H1071 . 120.1 no
C106 . C107 . H1071 . 121.7 no
Eu5 . O108 . C109 . 131.2(9) yes
O108 . C109 . C110 . 125.1(13) yes
O108 . C109 . C113 . 116.1(13) yes
C110 . C109 . C113 . 118.8(12) yes
C109 . C110 . C111 . 125.3(13) yes
C109 . C110 . H1101 . 117.4 no
C111 . C110 . H1101 . 117.2 no
C110 . C111 . O112 . 123.5(13) yes
C110 . C111 . C119 . 120.4(13) yes
O112 . C111 . C119 . 116.1(13) yes
C111 . O112 . Eu5 . 131.9(9) yes
C109 . C113 . C114 . 118.8(13) yes
C109 . C113 . C118 . 121.3(14) yes
C114 . C113 . C118 . 120.0(14) yes
C113 . C114 . C115 . 120.7(14) yes
C113 . C114 . H1141 . 120.1 no
C115 . C114 . H1141 . 119.1 no
C114 . C115 . C116 . 116.4(16) yes
C114 . C115 . H1151 . 121.1 no
C116 . C115 . H1151 . 122.4 no
C115 . C116 . C117 . 123.1(16) yes
C115 . C116 . H1161 . 117.9 no
C117 . C116 . H1161 . 119.0 no
C116 . C117 . C118 . 119.2(14) yes
C116 . C117 . H1171 . 120.5 no
C118 . C117 . H1171 . 120.3 no
C113 . C118 . C117 . 120.5(15) yes
C113 . C118 . H1181 . 118.8 no
C117 . C118 . H1181 . 120.7 no
C111 . C119 . C120 . 124.3(15) yes
C111 . C119 . C124 . 118.9(14) yes
C120 . C119 . C124 . 116.8(15) yes
C119 . C120 . C121 . 125.1(16) yes
C119 . C120 . H1201 . 116.7 no
C121 . C120 . H1201 . 118.3 no
C120 . C121 . C122 . 117.7(15) yes
C120 . C121 . H1211 . 120.8 no
C122 . C121 . H1211 . 121.5 no
C121 . C122 . C123 . 120.1(16) yes
C121 . C122 . H1221 . 118.6 no
C123 . C122 . H1221 . 121.2 no
C122 . C123 . C124 . 120.3(17) yes
C122 . C123 . H1231 . 120.5 no
C124 . C123 . H1231 . 119.2 no
C123 . C124 . C119 . 120.0(16) yes
C123 . C124 . H1241 . 119.7 no
C119 . C124 . H1241 . 120.3 no
Eu5 . O125 . C126 . 133.1(9) yes
O125 . C126 . C127 . 123.0(13) yes
O125 . C126 . C130 . 116.4(13) yes
C127 . C126 . C130 . 120.5(11) yes
C126 . C127 . C128 . 124.9(12) yes
C126 . C127 . H1271 . 117.1 no
C128 . C127 . H1271 . 118.0 no
C127 . C128 . O129 . 124.8(12) yes
C127 . C128 . C136 . 118.3(12) yes
O129 . C128 . C136 . 116.8(12) yes
C128 . O129 . Eu5 . 129.5(8) yes
C126 . C130 . C131 . 125.4(13) yes
C126 . C130 . C135 . 117.4(12) yes
C131 . C130 . C135 . 117.2(14) yes
C130 . C131 . C132 . 123.8(14) yes
C130 . C131 . H1311 . 117.2 no
C132 . C131 . H1311 . 119.0 no
C131 . C132 . C133 . 118.5(14) yes
C131 . C132 . H1321 . 119.8 no
C133 . C132 . H1321 . 121.7 no
C132 . C133 . C134 . 120.2(14) yes
C132 . C133 . H1331 . 119.3 no
C134 . C133 . H1331 . 120.5 no
C133 . C134 . C135 . 118.7(14) yes
C133 . C134 . H1341 . 120.3 no
C135 . C134 . H1341 . 121.0 no
C130 . C135 . C134 . 121.6(14) yes
C130 . C135 . H1351 . 119.8 no
C134 . C135 . H1351 . 118.5 no
C128 . C136 . C137 . 118.1(14) yes
C128 . C136 . C141 . 123.6(14) yes
C137 . C136 . C141 . 118.3(15) yes
C136 . C137 . C138 . 119.1(16) yes
C136 . C137 . H1371 . 121.9 no
C138 . C137 . H1371 . 118.8 no
C137 . C138 . C139 . 122.3(17) yes
C137 . C138 . H1381 . 119.0 no
C139 . C138 . H1381 . 118.7 no
C138 . C139 . C140 . 117.0(16) yes
C138 . C139 . H1391 . 122.5 no
C140 . C139 . H1391 . 120.4 no
C139 . C140 . C141 . 122.1(16) yes
C139 . C140 . H1401 . 117.8 no
C141 . C140 . H1401 . 120.1 no
C136 . C141 . C140 . 121.2(17) yes
C136 . C141 . H1411 . 119.2 no
C140 . C141 . H1411 . 119.6 no
Eu1 . O142 . C143 . 133.6(9) yes
O142 . C143 . C144 . 122.9(13) yes
O142 . C143 . C147 . 117.2(12) yes
C144 . C143 . C147 . 119.9(13) yes
C143 . C144 . C145 . 127.4(13) yes
C143 . C144 . H1441 . 117.5 no
C145 . C144 . H1441 . 115.1 no
C144 . C145 . O146 . 122.1(11) yes
C144 . C145 . C153 . 122.5(13) yes
O146 . C145 . C153 . 115.3(12) yes
C145 . O146 . Eu4 . 125.3(7) yes
C145 . O146 . Eu1 . 126.2(7) yes
Eu4 . O146 . Eu1 . 94.7(3) yes
C143 . C147 . C148 . 119.2(15) yes
C143 . C147 . C152 . 119.4(15) yes
C148 . C147 . C152 . 121.2(16) yes
C147 . C148 . C149 . 122.3(19) yes
C147 . C148 . H1481 . 117.6 no
C149 . C148 . H1481 . 120.1 no
C148 . C149 . C150 . 118.0(20) yes
C148 . C149 . H1491 . 120.7 no
C150 . C149 . H1491 . 121.3 no
C149 . C150 . C151 . 122.5(19) yes
C149 . C150 . H1501 . 119.3 no
C151 . C150 . H1501 . 118.1 no
C150 . C151 . C152 . 118.4(20) yes
C150 . C151 . H1511 . 119.5 no
C152 . C151 . H1511 . 122.0 no
C151 . C152 . C147 . 117.2(19) yes
C151 . C152 . H1521 . 120.9 no
C147 . C152 . H1521 . 121.9 no
C145 . C153 . C154 . 121.7(13) yes
C145 . C153 . C158 . 119.8(14) yes
C154 . C153 . C158 . 118.5(12) yes
C153 . C154 . C155 . 121.7(14) yes
C153 . C154 . H1541 . 118.0 no
C155 . C154 . H1541 . 120.3 no
C154 . C155 . C156 . 119.5(16) yes
C154 . C155 . H1551 . 119.8 no
C156 . C155 . H1551 . 120.7 no
C155 . C156 . C157 . 122.0(16) yes
C155 . C156 . H1561 . 118.2 no
C157 . C156 . H1561 . 119.8 no
C156 . C157 . C158 . 117.5(16) yes
C156 . C157 . H1571 . 120.8 no
C158 . C157 . H1571 . 121.6 no
C157 . C158 . C153 . 120.7(16) yes
C157 . C158 . H1581 . 120.1 no
C153 . C158 . H1581 . 119.1 no
Eu3 . O159 . C160 . 131.5(8) yes
O159 . C160 . C161 . 123.5(11) yes
O159 . C160 . C164 . 119.2(12) yes
C161 . C160 . C164 . 117.2(11) yes
C160 . C161 . C162 . 125.0(10) yes
C160 . C161 . H1611 . 117.2 no
C162 . C161 . H1611 . 117.8 no
C161 . C162 . O163 . 123.8(10) yes
C161 . C162 . C170 . 120.7(11) yes
O163 . C162 . C170 . 115.5(10) yes
C162 . O163 . Eu1 . 124.8(8) yes
C162 . O163 . Eu3 . 123.5(8) yes
Eu1 . O163 . Eu3 . 97.5(3) yes
C160 . C164 . C165 . 119.7(13) yes
C160 . C164 . C169 . 122.4(13) yes
C165 . C164 . C169 . 117.7(12) yes
C164 . C165 . C166 . 121.8(14) yes
C164 . C165 . H1651 . 118.6 no
C166 . C165 . H1651 . 119.6 no
C165 . C166 . C167 . 118.8(14) yes
C165 . C166 . H1661 . 121.3 no
C167 . C166 . H1661 . 119.9 no
C166 . C167 . C168 . 120.0(14) yes
C166 . C167 . H1671 . 120.7 no
C168 . C167 . H1671 . 119.3 no
C167 . C168 . C169 . 120.0(15) yes
C167 . C168 . H1681 . 120.0 no
C169 . C168 . H1681 . 119.9 no
C164 . C169 . C168 . 121.5(15) yes
C164 . C169 . H1691 . 118.8 no
C168 . C169 . H1691 . 119.7 no
C162 . C170 . C171 . 123.3(13) yes
C162 . C170 . C175 . 119.9(11) yes
C171 . C170 . C175 . 116.8(12) yes
C170 . C171 . C172 . 121.2(14) yes
C170 . C171 . H1711 . 118.7 no
C172 . C171 . H1711 . 120.1 no
C171 . C172 . C173 . 120.7(12) yes
C171 . C172 . H1721 . 119.5 no
C173 . C172 . H1721 . 119.8 no
C172 . C173 . C174 . 119.8(12) yes
C172 . C173 . H1731 . 119.4 no
C174 . C173 . H1731 . 120.7 no
C173 . C174 . C175 . 119.6(12) yes
C173 . C174 . H1741 . 120.2 no
C175 . C174 . H1741 . 120.2 no
C170 . C175 . C174 . 121.6(12) yes
C170 . C175 . H1751 . 119.3 no
C174 . C175 . H1751 . 119.0 no
Eu1 . O176 . C177 . 134.2(8) yes
O176 . C177 . C178 . 124.9(12) yes
O176 . C177 . C182 . 113.4(11) yes
C178 . C177 . C182 . 121.7(12) yes
C177 . C178 . C179 . 123.9(13) yes
C177 . C178 . H1781 . 118.2 no
C179 . C178 . H1781 . 117.8 no
C178 . C179 . O180 . 126.5(12) yes
C178 . C179 . C188 . 119.4(13) yes
O180 . C179 . C188 . 114.0(13) yes
C179 . O180 . Eu1 . 133.5(8) yes
C177 . C182 . C183 . 122.6(13) yes
C177 . C182 . C187 . 121.2(15) yes
C183 . C182 . C187 . 116.1(14) yes
C182 . C183 . C184 . 123.4(18) yes
C182 . C183 . H1821 . 118.0 no
C184 . C183 . H1821 . 118.6 no
C183 . C184 . C185 . 120.3(20) yes
C183 . C184 . H1822 . 119.7 no
C185 . C184 . H1822 . 120.0 no
C184 . C185 . C186 . 119.8(19) yes
C184 . C185 . H1823 . 119.0 no
C186 . C185 . H1823 . 121.1 no
C185 . C186 . C187 . 121(2) yes
C185 . C186 . H1824 . 118.1 no
C187 . C186 . H1824 . 121.2 no
C186 . C187 . C182 . 119.3(20) yes
C186 . C187 . H1825 . 119.3 no
C182 . C187 . H1825 . 121.4 no
C179 . C188 . C189 . 118.9(14) yes
C179 . C188 . C193 . 121.9(15) yes
C189 . C188 . C193 . 119.3(14) yes
C188 . C189 . C190 . 120.9(17) yes
C188 . C189 . H1891 . 120.4 no
C190 . C189 . H1891 . 118.8 no
C189 . C190 . C191 . 119(2) yes
C189 . C190 . H1901 . 121.5 no
C191 . C190 . H1901 . 119.4 no
C190 . C191 . C192 . 121.3(17) yes
C190 . C191 . H1911 . 120.7 no
C192 . C191 . H1911 . 118.0 no
C191 . C192 . C193 . 121.5(17) yes
C191 . C192 . H1921 . 120.9 no
C193 . C192 . H1921 . 117.7 no
C188 . C193 . C192 . 117.9(17) yes
C188 . C193 . H1931 . 119.2 no
C192 . C193 . H1931 . 122.9 no
loop_
_geom_bond_atom_site_label_1
_geom_bond_site_symmetry_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Eu1 . O1 . 2.580(8) yes
Eu1 . O12 . 2.384(8) yes
Eu1 . O14 . 2.357(8) yes
Eu1 . O142 . 2.364(9) yes
Eu1 . O146 . 2.410(8) yes
Eu1 . O163 . 2.478(9) yes
Eu1 . O176 . 2.337(8) yes
Eu1 . O180 . 2.304(8) yes
Eu2 . O1 . 2.583(8) yes
Eu2 . O11 . 2.361(9) yes
Eu2 . O13 . 2.395(8) yes
Eu2 . O21 . 2.382(9) yes
Eu2 . O25 . 2.391(8) yes
Eu2 . O55 . 2.294(8) yes
Eu2 . O59 . 2.365(8) yes
Eu2 . O73 . 2.480(8) yes
Eu3 . O1 . 2.774(8) yes
Eu3 . O13 . 2.341(8) yes
Eu3 . O14 . 2.343(8) yes
Eu3 . O25 . 2.451(8) yes
Eu3 . O38 . 2.340(9) yes
Eu3 . O42 . 2.318(10) yes
Eu3 . O159 . 2.401(9) yes
Eu3 . O163 . 2.381(9) yes
Eu4 . O1 . 2.538(8) yes
Eu4 . O11 . 2.397(8) yes
Eu4 . O12 . 2.337(8) yes
Eu4 . O73 . 2.425(8) yes
Eu4 . O77 . 2.348(8) yes
Eu4 . O91 . 2.323(9) yes
Eu4 . O95 . 2.325(8) yes
Eu4 . O146 . 2.508(8) yes
Eu5 . O11 . 2.446(8) yes
Eu5 . O12 . 2.456(8) yes
Eu5 . O13 . 2.418(9) yes
Eu5 . O14 . 2.476(7) yes
Eu5 . O108 . 2.378(8) yes
Eu5 . O112 . 2.343(9) yes
Eu5 . O125 . 2.344(9) yes
Eu5 . O129 . 2.397(8) yes
O1 . H11 . 1.012 no
O11 . H111 . 1.005 no
O12 . H121 . 1.011 no
O13 . H131 . 1.012 no
O14 . H141 . 1.010 no
O21 . C22 . 1.251(16) yes
C22 . C23 . 1.444(18) yes
C22 . C26 . 1.470(18) yes
C23 . C24 . 1.369(18) yes
C23 . H231 . 1.011 no
C24 . O25 . 1.361(16) yes
C24 . C32 . 1.465(18) yes
C26 . C27 . 1.381(18) yes
C26 . C31 . 1.387(19) yes
C27 . C28 . 1.38(2) yes
C27 . H271 . 1.017 no
C28 . C29 . 1.39(2) yes
C28 . H281 . 1.017 no
C29 . C30 . 1.38(2) yes
C29 . H291 . 1.010 no
C30 . C31 . 1.404(19) yes
C30 . H301 . 1.030 no
C31 . H311 . 1.027 no
C32 . C33 . 1.351(18) yes
C32 . C37 . 1.421(19) yes
C33 . C34 . 1.395(18) yes
C33 . H331 . 1.019 no
C34 . C35 . 1.39(2) yes
C34 . H341 . 1.030 no
C35 . C36 . 1.37(2) yes
C35 . H351 . 1.004 no
C36 . C37 . 1.390(18) yes
C36 . H361 . 1.017 no
C37 . H371 . 1.023 no
O38 . C39 . 1.258(16) yes
C39 . C40 . 1.387(19) yes
C39 . C43 . 1.53(2) yes
C40 . C41 . 1.390(19) yes
C40 . H401 . 1.021 no
C41 . O42 . 1.304(16) yes
C41 . C49 . 1.490(18) yes
C43 . C44 . 1.35(2) yes
C43 . C48 . 1.39(2) yes
C44 . C45 . 1.36(2) yes
C44 . H441 . 1.027 no
C45 . C46 . 1.37(3) yes
C45 . H451 . 1.027 no
C46 . C47 . 1.35(3) yes
C46 . H461 . 1.007 no
C47 . C48 . 1.43(2) yes
C47 . H471 . 1.023 no
C48 . H481 . 1.007 no
C49 . C50 . 1.41(2) yes
C49 . C54 . 1.38(2) yes
C50 . C51 . 1.38(2) yes
C50 . H501 . 1.011 no
C51 . C52 . 1.33(3) yes
C51 . H511 . 1.019 no
C52 . C53 . 1.35(3) yes
C52 . H521 . 1.004 no
C53 . C54 . 1.38(2) yes
C53 . H531 . 1.009 no
C54 . H541 . 1.025 no
O55 . C56 . 1.298(16) yes
C56 . C57 . 1.403(19) yes
C56 . C66 . 1.492(18) yes
C57 . C58 . 1.404(18) yes
C57 . H571 . 1.020 no
C58 . O59 . 1.274(15) yes
C58 . C60 . 1.496(19) yes
C60 . C61 . 1.376(19) yes
C60 . C65 . 1.402(18) yes
C61 . C62 . 1.38(2) yes
C61 . H611 . 1.024 no
C62 . C63 . 1.38(2) yes
C62 . H621 . 1.018 no
C63 . C64 . 1.38(2) yes
C63 . H631 . 1.041 no
C64 . C65 . 1.378(19) yes
C64 . H641 . 1.024 no
C65 . H651 . 1.024 no
C66 . C67 . 1.37(2) yes
C66 . C72 . 1.39(2) yes
C67 . C68 . 1.39(2) yes
C67 . H671 . 1.023 no
C68 . C69 . 1.38(2) yes
C68 . H681 . 1.025 no
C69 . C70 . 1.39(3) yes
C69 . H691 . 1.021 no
C70 . C72 . 1.37(2) yes
C70 . H701 . 1.037 no
C72 . H721 . 1.030 no
O73 . C74 . 1.302(14) yes
C74 . C75 . 1.385(19) yes
C74 . C78 . 1.50(2) yes
C75 . C76 . 1.465(19) yes
C75 . H751 . 1.012 no
C76 . O77 . 1.242(14) yes
C76 . C85 . 1.491(17) yes
C78 . C79 . 1.39(2) yes
C78 . C84 . 1.370(19) yes
C79 . C80 . 1.41(2) yes
C79 . H791 . 1.019 no
C80 . C82 . 1.36(2) yes
C80 . H801 . 1.008 no
C82 . C83 . 1.36(2) yes
C82 . H821 . 1.033 no
C83 . C84 . 1.43(2) yes
C83 . H831 . 1.000 no
C84 . H841 . 1.013 no
C85 . C86 . 1.366(19) yes
C85 . C90 . 1.39(2) yes
C86 . C87 . 1.38(2) yes
C86 . H861 . 1.013 no
C87 . C88 . 1.36(2) yes
C87 . H871 . 1.015 no
C88 . C89 . 1.36(2) yes
C88 . H881 . 1.017 no
C89 . C90 . 1.39(2) yes
C89 . H891 . 1.032 no
C90 . H901 . 1.008 no
O91 . C92 . 1.240(16) yes
C92 . C93 . 1.45(2) yes
C92 . C102 . 1.49(2) yes
C93 . C94 . 1.39(2) yes
C93 . H931 . 1.023 no
C94 . O95 . 1.281(16) yes
C94 . C96 . 1.512(18) yes
C96 . C97 . 1.39(2) yes
C96 . C101 . 1.41(2) yes
C97 . C98 . 1.37(2) yes
C97 . H971 . 1.029 no
C98 . C99 . 1.39(3) yes
C98 . H981 . 1.038 no
C99 . C100 . 1.36(3) yes
C99 . H991 . 1.023 no
C100 . C101 . 1.37(2) yes
C100 . H1001 . 1.030 no
C101 . H1011 . 1.023 no
C102 . C103 . 1.39(2) yes
C102 . C107 . 1.40(2) yes
C103 . C104 . 1.41(2) yes
C103 . H1031 . 1.024 no
C104 . C105 . 1.35(2) yes
C104 . H1041 . 1.026 no
C105 . C106 . 1.37(2) yes
C105 . H1051 . 1.031 no
C106 . C107 . 1.40(2) yes
C106 . H1061 . 1.036 no
C107 . H1071 . 1.013 no
O108 . C109 . 1.273(14) yes
C109 . C110 . 1.40(2) yes
C109 . C113 . 1.508(19) yes
C110 . C111 . 1.40(2) yes
C110 . H1101 . 1.006 no
C111 . O112 . 1.279(15) yes
C111 . C119 . 1.488(19) yes
C113 . C114 . 1.37(2) yes
C113 . C118 . 1.393(18) yes
C114 . C115 . 1.43(2) yes
C114 . H1141 . 1.013 no
C115 . C116 . 1.38(2) yes
C115 . H1151 . 1.024 no
C116 . C117 . 1.37(2) yes
C116 . H1161 . 1.023 no
C117 . C118 . 1.37(2) yes
C117 . H1171 . 1.017 no
C118 . H1181 . 1.015 no
C119 . C120 . 1.365(19) yes
C119 . C124 . 1.37(2) yes
C120 . C121 . 1.36(2) yes
C120 . H1201 . 1.022 no
C121 . C122 . 1.37(2) yes
C121 . H1211 . 1.023 no
C122 . C123 . 1.37(3) yes
C122 . H1221 . 1.021 no
C123 . C124 . 1.41(2) yes
C123 . H1231 . 1.032 no
C124 . H1241 . 1.018 no
O125 . C126 . 1.283(14) yes
C126 . C127 . 1.421(19) yes
C126 . C130 . 1.469(19) yes
C127 . C128 . 1.417(18) yes
C127 . H1271 . 1.018 no
C128 . O129 . 1.265(15) yes
C128 . C136 . 1.505(18) yes
C130 . C131 . 1.371(18) yes
C130 . C135 . 1.395(19) yes
C131 . C132 . 1.363(19) yes
C131 . H1311 . 1.020 no
C132 . C133 . 1.39(2) yes
C132 . H1321 . 1.013 no
C133 . C134 . 1.41(2) yes
C133 . H1331 . 1.019 no
C134 . C135 . 1.38(2) yes
C134 . H1341 . 1.027 no
C135 . H1351 . 1.021 no
C136 . C137 . 1.34(2) yes
C136 . C141 . 1.38(2) yes
C137 . C138 . 1.42(2) yes
C137 . H1371 . 1.027 no
C138 . C139 . 1.36(2) yes
C138 . H1381 . 1.026 no
C139 . C140 . 1.33(2) yes
C139 . H1391 . 1.006 no
C140 . C141 . 1.37(2) yes
C140 . H1401 . 1.004 no
C141 . H1411 . 1.030 no
O142 . C143 . 1.251(15) yes
C143 . C144 . 1.446(18) yes
C143 . C147 . 1.50(2) yes
C144 . C145 . 1.377(18) yes
C144 . H1441 . 1.017 no
C145 . O146 . 1.329(15) yes
C145 . C153 . 1.465(17) yes
C147 . C148 . 1.36(2) yes
C147 . C152 . 1.38(2) yes
C148 . C149 . 1.34(2) yes
C148 . H1481 . 1.044 no
C149 . C150 . 1.39(3) yes
C149 . H1491 . 1.040 no
C150 . C151 . 1.35(3) yes
C150 . H1501 . 1.019 no
C151 . C152 . 1.45(3) yes
C151 . H1511 . 1.027 no
C152 . H1521 . 1.019 no
C153 . C154 . 1.38(2) yes
C153 . C158 . 1.40(2) yes
C154 . C155 . 1.381(19) yes
C154 . H1541 . 1.022 no
C155 . C156 . 1.38(2) yes
C155 . H1551 . 1.035 no
C156 . C157 . 1.37(3) yes
C156 . H1561 . 1.019 no
C157 . C158 . 1.44(2) yes
C157 . H1571 . 1.022 no
C158 . H1581 . 1.021 no
O159 . C160 . 1.244(14) yes
C160 . C161 . 1.474(18) yes
C160 . C164 . 1.478(17) yes
C161 . C162 . 1.332(16) yes
C161 . H1611 . 1.003 no
C162 . O163 . 1.330(14) yes
C162 . C170 . 1.480(17) yes
C164 . C165 . 1.405(19) yes
C164 . C169 . 1.397(19) yes
C165 . C166 . 1.374(19) yes
C165 . H1651 . 1.021 no
C166 . C167 . 1.40(2) yes
C166 . H1661 . 1.012 no
C167 . C168 . 1.40(2) yes
C167 . H1671 . 1.011 no
C168 . C169 . 1.366(19) yes
C168 . H1681 . 1.031 no
C169 . H1691 . 1.019 no
C170 . C171 . 1.409(18) yes
C170 . C175 . 1.396(18) yes
C171 . C172 . 1.365(19) yes
C171 . H1711 . 1.020 no
C172 . C173 . 1.37(2) yes
C172 . H1721 . 1.014 no
C173 . C174 . 1.381(18) yes
C173 . H1731 . 1.012 no
C174 . C175 . 1.381(17) yes
C174 . H1741 . 1.016 no
C175 . H1751 . 1.009 no
O176 . C177 . 1.290(15) yes
C177 . C178 . 1.385(18) yes
C177 . C182 . 1.509(18) yes
C178 . C179 . 1.381(19) yes
C178 . H1781 . 1.019 no
C179 . O180 . 1.291(16) yes
C179 . C188 . 1.536(18) yes
C182 . C183 . 1.34(2) yes
C182 . C187 . 1.41(2) yes
C183 . C184 . 1.36(2) yes
C183 . H1821 . 1.011 no
C184 . C185 . 1.35(3) yes
C184 . H1822 . 0.997 no
C185 . C186 . 1.32(3) yes
C185 . H1823 . 1.007 no
C186 . C187 . 1.41(3) yes
C186 . H1824 . 0.998 no
C187 . H1825 . 0.999 no
C188 . C189 . 1.39(2) yes
C188 . C193 . 1.41(2) yes
C189 . C190 . 1.39(2) yes
C189 . H1891 . 1.029 no
C190 . C191 . 1.36(3) yes
C190 . H1901 . 1.041 no
C191 . C192 . 1.36(3) yes
C191 . H1911 . 1.016 no
C192 . C193 . 1.39(2) yes
C192 . H1921 . 1.032 no
C193 . H1931 . 1.034 no
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_site_symmetry_D
_geom_hbond_atom_site_label_H
_geom_hbond_site_symmetry_H
_geom_hbond_atom_site_label_A
_geom_hbond_site_symmetry_A
_geom_hbond_angle_DHA
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_publ_flag
C191 . H1911 . O125 3_655 151 1.02 2.49 3.42(2) yes
O14 . H141 . C127 . 132 1.01 2.59 3.35(2) yes
