#------------------------------------------------------------------------------
#$Date: 2016-03-25 09:44:41 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179732 $
#$URL: svn://www.crystallography.net/cod/cif/7/00/28/7002829.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7002829
loop_
_publ_author_name
'Jin, Jun-Cheng'
'Wang, Yao-Yu'
'Zhang, Wei-Hong'
'Lermontov, Anatoly S.'
'Lermontova, Elmira Kh.'
'Shi, Qi-Zhen'
_publ_section_title
;
 New types of di-, tetra-, hexa- and octanuclear Ag(i) complexes
 containing 1,3-adamantanedicarboxylic acid
;
_journal_issue                   46
_journal_name_full               'Dalton Transactions'
_journal_page_first              10181
_journal_page_last               10191
_journal_paper_doi               10.1039/b909309e
_journal_year                    2009
_chemical_formula_moiety         'C72 H90 Ag12 O27, 5.18(H2 O)'
_chemical_formula_sum            'C72 H100.36 Ag12 O32.18'
_chemical_formula_weight         2775.20
_chemical_name_systematic
;
?
;
_space_group_IT_number           13
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yc'
_symmetry_space_group_name_H-M   'P 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 110.220(4)
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   18.480(4)
_cell_length_b                   13.463(3)
_cell_length_c                   18.374(4)
_cell_measurement_reflns_used    2004
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      20.899
_cell_measurement_theta_min      2.245
_cell_volume                     4289.7(16)
_computing_cell_refinement       APEX2
_computing_data_collection       'APEX2 (Bruker, 2005)'
_computing_data_reduction        APEX2
_computing_molecular_graphics    APEX2
_computing_publication_material  APEX2
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.994
_diffrn_measured_fraction_theta_max 0.994
_diffrn_measurement_device_type  'Bruker APEX SMART II'
_diffrn_measurement_method       ω
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0620
_diffrn_reflns_av_sigmaI/netI    0.0996
_diffrn_reflns_limit_h_max       23
_diffrn_reflns_limit_h_min       -18
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_k_min       -16
_diffrn_reflns_limit_l_max       22
_diffrn_reflns_limit_l_min       -21
_diffrn_reflns_number            23561
_diffrn_reflns_theta_full        26.46
_diffrn_reflns_theta_max         26.46
_diffrn_reflns_theta_min         1.92
_diffrn_standards_decay_%        0
_diffrn_standards_interval_time  0
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    2.753
_exptl_absorpt_correction_T_max  0.6671
_exptl_absorpt_correction_T_min  0.5235
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    2.149
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             2708
_exptl_crystal_size_max          0.27
_exptl_crystal_size_mid          0.22
_exptl_crystal_size_min          0.16
_refine_diff_density_max         1.136
_refine_diff_density_min         -0.819
_refine_diff_density_rms         0.139
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.853
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     559
_refine_ls_number_reflns         8817
_refine_ls_number_restraints     24
_refine_ls_restrained_S_all      0.856
_refine_ls_R_factor_all          0.1078
_refine_ls_R_factor_gt           0.0474
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0706P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1202
_refine_ls_wR_factor_ref         0.1359
_reflns_number_gt                4114
_reflns_number_total             8817
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b909309e.txt
_cod_data_source_block           xb2462
_cod_original_cell_volume        4289.6(14)
_cod_original_sg_symbol_H-M      'P 2/c'
_cod_database_code               7002829
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.24287(4) 0.52848(5) 0.63973(3) 0.0543(2) Uani 1 1 d . . .
Ag2 Ag 0.51037(4) 0.53292(6) 0.57608(4) 0.0587(2) Uani 1 1 d . . .
Ag3 Ag 0.29887(4) 0.61875(5) 0.81613(4) 0.0536(2) Uani 1 1 d . . .
Ag4 Ag -0.05159(3) 0.42651(5) 0.45956(4) 0.0594(2) Uani 1 1 d . . .
Ag5 Ag 0.40451(4) 0.54699(6) 0.70705(4) 0.0701(2) Uani 1 1 d . . .
Ag6 Ag 0.19586(4) 0.72934(6) 0.69425(5) 0.0779(3) Uani 1 1 d . . .
O1 O 0.5000 0.4021(10) 0.7500 0.147(5) Uani 1 2 d S . .
H1B H 0.4956 0.3669 0.7867 0.176 Uiso 1 1 d R . .
O2 O 0.4299(3) 0.4077(5) 0.5734(3) 0.0631(16) Uani 1 1 d . . .
O3 O 0.1320(3) 0.4547(4) 0.5309(3) 0.0481(13) Uani 1 1 d . . .
O5 O -0.1351(3) 0.2818(5) 0.4543(3) 0.0763(19) Uani 1 1 d . . .
H5C H -0.1283 0.2247 0.4670 0.092 Uiso 1 1 d R . .
H5D H -0.1760 0.3063 0.4494 0.092 Uiso 1 1 d R . .
O6 O 0.4006(3) 0.3787(4) 0.4491(3) 0.0546(15) Uani 1 1 d . . .
O8 O 0.2693(3) 0.4072(4) 0.7269(3) 0.0643(17) Uani 1 1 d . D .
O9 O 0.2722(3) 0.3628(4) 1.0623(3) 0.0583(15) Uani 1 1 d . . .
O10 O 0.3993(3) 0.3742(4) 1.1020(3) 0.0509(14) Uani 1 1 d . . .
O11 O 0.3814(3) 0.7064(4) 0.7814(3) 0.0573(15) Uani 1 1 d . . .
C1 C 0.3913(4) 0.3639(6) 0.5136(5) 0.045(2) Uani 1 1 d . . .
C2 C 0.3270(4) 0.2970(5) 0.5165(4) 0.0395(18) Uani 1 1 d . . .
C3 C 0.3472(4) 0.2459(6) 0.5946(4) 0.047(2) Uani 1 1 d . . .
H3A H 0.3592 0.2951 0.6357 0.056 Uiso 1 1 calc R . .
H3B H 0.3921 0.2039 0.6036 0.056 Uiso 1 1 calc R . .
C4 C 0.3072(5) 0.2192(6) 0.4520(5) 0.053(2) Uani 1 1 d . . .
H4A H 0.3511 0.1759 0.4594 0.064 Uiso 1 1 calc R . .
H4B H 0.2952 0.2519 0.4021 0.064 Uiso 1 1 calc R . .
C5 C 0.2567(4) 0.3645(5) 0.5041(4) 0.0379(18) Uani 1 1 d . . .
H5A H 0.2444 0.3986 0.4548 0.046 Uiso 1 1 calc R . .
H5B H 0.2691 0.4143 0.5447 0.046 Uiso 1 1 calc R . .
C6 C 0.2377(5) 0.1579(6) 0.4532(4) 0.052(2) Uani 1 1 d . . .
H6 H 0.2252 0.1078 0.4120 0.063 Uiso 1 1 calc R . .
C7 C 0.1675(4) 0.2282(6) 0.4395(5) 0.049(2) Uani 1 1 d . . .
H7A H 0.1561 0.2622 0.3903 0.059 Uiso 1 1 calc R . .
H7B H 0.1225 0.1896 0.4377 0.059 Uiso 1 1 calc R . .
C8 C 0.2585(5) 0.1061(6) 0.5319(5) 0.059(2) Uani 1 1 d . . .
H8A H 0.2154 0.0660 0.5333 0.071 Uiso 1 1 calc R . .
H8B H 0.3024 0.0627 0.5398 0.071 Uiso 1 1 calc R . .
C9 C 0.1856(4) 0.3037(6) 0.5048(4) 0.0390(18) Uani 1 1 d . E .
C10 C 0.2774(5) 0.1823(6) 0.5948(5) 0.052(2) Uani 1 1 d . . .
H10 H 0.2903 0.1486 0.6450 0.063 Uiso 1 1 calc R . .
C11 C 0.2069(4) 0.2486(6) 0.5827(4) 0.049(2) Uani 1 1 d . . .
H11A H 0.2180 0.2964 0.6246 0.059 Uiso 1 1 calc R . .
H11B H 0.1637 0.2082 0.5834 0.059 Uiso 1 1 calc R . .
C12 C 0.1178(4) 0.3715(7) 0.4986(4) 0.045(2) Uani 1 1 d . . .
C13 C 0.3266(5) 0.4020(6) 0.7858(5) 0.049(2) Uani 1 1 d . . .
C14 C 0.3302(4) 0.3197(6) 0.8437(4) 0.046(2) Uani 1 1 d . D .
C15 C 0.3305(4) 0.3692(5) 0.9191(4) 0.0401(18) Uani 1 1 d . . .
H15A H 0.2832 0.4068 0.9091 0.048 Uiso 1 1 calc R D .
H15B H 0.3735 0.4150 0.9373 0.048 Uiso 1 1 calc R . .
C16 C 0.2628(5) 0.2477(6) 0.8146(4) 0.049(2) Uani 1 1 d . . .
H16A H 0.2146 0.2839 0.8015 0.059 Uiso 1 1 calc R D .
H16B H 0.2641 0.2146 0.7681 0.059 Uiso 1 1 calc R . .
C17 C 0.4061(5) 0.2595(6) 0.8609(5) 0.052(2) Uani 1 1 d . . .
H17A H 0.4064 0.2270 0.8139 0.062 Uiso 1 1 calc R D .
H17B H 0.4500 0.3041 0.8784 0.062 Uiso 1 1 calc R . .
C18 C 0.4122(5) 0.1821(7) 0.9231(5) 0.060(2) Uani 1 1 d . D .
H18 H 0.4605 0.1452 0.9341 0.072 Uiso 1 1 calc R . .
C19 C 0.3443(6) 0.1101(7) 0.8939(6) 0.074(3) Uani 1 1 d . . .
H19A H 0.3480 0.0599 0.9328 0.089 Uiso 1 1 calc R D .
H19B H 0.3448 0.0772 0.8471 0.089 Uiso 1 1 calc R . .
C20 C 0.2676(5) 0.1712(6) 0.8765(5) 0.058(2) Uani 1 1 d . D .
H20 H 0.2234 0.1262 0.8578 0.069 Uiso 1 1 calc R . .
C21 C 0.2678(5) 0.2212(6) 0.9510(4) 0.050(2) Uani 1 1 d . . .
H21A H 0.2699 0.1711 0.9896 0.060 Uiso 1 1 calc R D .
H21B H 0.2206 0.2590 0.9409 0.060 Uiso 1 1 calc R . .
C22 C 0.3372(4) 0.2904(6) 0.9822(4) 0.0421(19) Uani 1 1 d . D .
C23 C 0.4110(4) 0.2311(6) 0.9978(5) 0.051(2) Uani 1 1 d . . .
H23A H 0.4145 0.1805 1.0364 0.061 Uiso 1 1 calc R D .
H23B H 0.4552 0.2748 1.0181 0.061 Uiso 1 1 calc R . .
C24 C 0.3359(5) 0.3457(6) 1.0545(4) 0.0428(19) Uani 1 1 d . . .
C25 C 0.1367(4) 0.5430(7) 0.7562(5) 0.051(2) Uani 1 1 d . . .
C26 C 0.0696(4) 0.4750(6) 0.7536(4) 0.0437(19) Uani 1 1 d . . .
C27 C 0.0473(4) 0.4079(6) 0.6816(4) 0.050(2) Uani 1 1 d . . .
H27A H 0.0344 0.4484 0.6351 0.061 Uiso 1 1 calc R . .
H27B H 0.0905 0.3656 0.6837 0.061 Uiso 1 1 calc R . .
C28 C 0.0000 0.5411(8) 0.7500 0.046(3) Uani 1 2 d S . .
H28A H 0.0137 0.5834 0.7955 0.055 Uiso 1 1 d R . .
C30 C 0.0904(5) 0.4115(7) 0.8253(5) 0.059(2) Uani 1 1 d . . .
H30A H 0.1045 0.4534 0.8710 0.071 Uiso 1 1 calc R . .
H30B H 0.1342 0.3698 0.8286 0.071 Uiso 1 1 calc R . .
C31 C -0.0200(5) 0.3458(6) 0.6787(5) 0.056(2) Uani 1 1 d . . .
H31 H -0.0340 0.3035 0.6325 0.067 Uiso 1 1 calc R . .
C32 C 0.0000 0.2804(9) 0.7500 0.069(4) Uani 1 2 d S . .
H32A H -0.0435 0.2382 0.7470 0.082 Uiso 1 1 d R . .
C33 C 0.3657(5) 0.7897(7) 0.7514(5) 0.052(2) Uani 1 1 d . . .
C34 C 0.4304(4) 0.8546(5) 0.7484(4) 0.0412(18) Uani 1 1 d . . .
C35 C 0.5000 0.7921(8) 0.7500 0.047(3) Uani 1 2 d S . .
H35A H 0.5152 0.7496 0.7954 0.057 Uiso 1 1 d R . .
C36 C 0.4575(5) 0.9229(6) 0.8218(5) 0.058(2) Uani 1 1 d . . .
H36A H 0.4147 0.9633 0.8235 0.070 Uiso 1 1 calc R . .
H36B H 0.4746 0.8822 0.8682 0.070 Uiso 1 1 calc R . .
C37 C 0.4082(5) 0.9215(7) 0.6778(5) 0.064(2) Uani 1 1 d . . .
H37A H 0.3646 0.9625 0.6766 0.076 Uiso 1 1 calc R . .
H37B H 0.3929 0.8814 0.6311 0.076 Uiso 1 1 calc R . .
C38 C 0.4774(6) 0.9891(7) 0.6803(6) 0.077(3) Uani 1 1 d . . .
H38 H 0.4616 1.0310 0.6339 0.092 Uiso 1 1 calc R . .
C39 C 0.5000 1.0546(9) 0.7500 0.093(6) Uani 1 2 d S . .
H39A H 0.5427 1.0968 0.7506 0.111 Uiso 1 1 d R . .
O15 O 0.0703(14) 0.0876(18) 0.960(2) 0.40(2) Uani 0.65 1 d P . .
H15D H 0.0442 0.1065 0.9838 0.479 Uiso 0.65 1 d PR . .
H15C H 0.1149 0.0770 0.9836 0.479 Uiso 0.65 1 d PR . .
O18 O 0.039(3) -0.010(4) 0.806(3) 0.33(3) Uiso 0.35 1 d P . .
H18C H 0.0459 0.0149 0.8471 0.398 Uiso 0.35 1 d PR . .
H18D H 0.0205 -0.0638 0.7936 0.398 Uiso 0.35 1 d PR . .
O16 O 0.9606(8) 0.8000(10) 0.8308(9) 0.137(5) Uani 0.59 1 d PU A 1
H16C H 0.9891 0.7666 0.8646 0.164 Uiso 0.59 1 d PR A 1
H16D H 0.9384 0.7485 0.8170 0.164 Uiso 0.59 1 d PR A 1
O17 O 0.8326(11) 0.9842(14) 0.8017(12) 0.281(9) Uani 0.82 1 d PU B 1
H17D H 0.8062 0.9707 0.7582 0.337 Uiso 0.82 1 d PR B 1
H17C H 0.8201 0.9681 0.8376 0.337 Uiso 0.82 1 d PR B 1
O17A O 0.889(3) 0.892(3) 0.820(3) 0.117(15) Uiso 0.18 1 d P C 2
H17E H 0.8780 0.8951 0.7740 0.140 Uiso 0.18 1 d PR C 2
H17F H 0.9035 0.9148 0.8628 0.140 Uiso 0.18 1 d PR C 2
O14A O 0.1965(12) 0.5330(12) 0.8185(12) 0.041(5) Uiso 0.45 1 d P . 2
O14 O 0.1897(8) 0.5661(11) 0.8150(9) 0.040(4) Uani 0.55 1 d PU . 1
O7 O 0.3902(10) 0.4529(13) 0.7989(10) 0.057(4) Uani 0.59 1 d P D 1
O7A O 0.3724(13) 0.4713(18) 0.8057(15) 0.036(6) Uiso 0.41 1 d P . 2
O4 O 0.0504(8) 0.3322(11) 0.4734(8) 0.067(4) Uani 0.63 1 d PU E 1
O4A O 0.0522(12) 0.3472(14) 0.4511(10) 0.024(5) Uiso 0.37 1 d P E 2
O13 O 0.1264(9) 0.6064(12) 0.6938(11) 0.053(4) Uani 0.52 1 d P . 1
O13A O 0.1342(11) 0.5719(12) 0.6909(12) 0.036(5) Uiso 0.48 1 d P . 2
O12 O 0.2962(9) 0.8282(12) 0.7329(11) 0.066(4) Uani 0.62 1 d P . 1
O12A O 0.303(2) 0.816(2) 0.7100(17) 0.058(9) Uiso 0.38 1 d P . 2
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O8 Ag1 O9 154.1(2) . 4_565 ?
O8 Ag1 O3 101.46(19) . . ?
O9 Ag1 O3 93.58(19) 4_565 . ?
O8 Ag1 O13A 84.7(4) . . ?
O9 Ag1 O13A 118.5(4) 4_565 . ?
O3 Ag1 O13A 81.7(5) . . ?
O8 Ag1 Ag5 79.21(15) . . ?
O9 Ag1 Ag5 76.60(13) 4_565 . ?
O3 Ag1 Ag5 146.08(12) . . ?
O13A Ag1 Ag5 131.6(5) . . ?
O8 Ag1 Ag6 115.05(15) . . ?
O9 Ag1 Ag6 77.99(15) 4_565 . ?
O3 Ag1 Ag6 110.94(12) . . ?
O13A Ag1 Ag6 48.8(4) . . ?
Ag5 Ag1 Ag6 98.81(3) . . ?
O8 Ag1 Ag3 69.12(15) . . ?
O9 Ag1 Ag3 108.89(15) 4_565 . ?
O3 Ag1 Ag3 145.43(12) . . ?
O13A Ag1 Ag3 64.7(5) . . ?
Ag5 Ag1 Ag3 66.98(2) . . ?
Ag6 Ag1 Ag3 52.17(2) . . ?
O6 Ag2 O2 160.1(2) 3_666 . ?
O6 Ag2 O10 118.36(19) 3_666 4_565 ?
O2 Ag2 O10 78.75(19) . 4_565 ?
O6 Ag2 Ag2 79.50(14) 3_666 3_666 ?
O2 Ag2 Ag2 83.11(15) . 3_666 ?
O10 Ag2 Ag2 119.25(12) 4_565 3_666 ?
O14 Ag3 O11 158.2(4) . . ?
O14 Ag3 O14A 11.9(7) . . ?
O11 Ag3 O14A 164.9(6) . . ?
O14 Ag3 O7A 106.2(7) . . ?
O11 Ag3 O7A 87.3(6) . . ?
O14A Ag3 O7A 94.5(7) . . ?
O14 Ag3 O6 113.6(4) . 4_566 ?
O11 Ag3 O6 85.04(19) . 4_566 ?
O14A Ag3 O6 110.0(6) . 4_566 ?
O7A Ag3 O6 80.7(6) . 4_566 ?
O14 Ag3 Ag6 77.9(4) . . ?
O11 Ag3 Ag6 80.26(15) . . ?
O14A Ag3 Ag6 86.8(5) . . ?
O7A Ag3 Ag6 127.4(6) . . ?
O6 Ag3 Ag6 147.03(13) 4_566 . ?
O14 Ag3 Ag1 83.8(4) . . ?
O11 Ag3 Ag1 85.71(15) . . ?
O14A Ag3 Ag1 81.2(5) . . ?
O7A Ag3 Ag1 67.4(6) . . ?
O6 Ag3 Ag1 147.18(12) 4_566 . ?
Ag6 Ag3 Ag1 60.87(3) . . ?
O4 Ag4 O3 165.1(4) . 3_566 ?
O4 Ag4 O4A 12.0(6) . . ?
O3 Ag4 O4A 162.5(5) 3_566 . ?
O4 Ag4 O5 92.7(4) . . ?
O3 Ag4 O5 98.3(2) 3_566 . ?
O4A Ag4 O5 99.2(5) . . ?
O4 Ag4 Ag4 87.0(4) . 3_566 ?
O3 Ag4 Ag4 78.53(14) 3_566 3_566 ?
O4A Ag4 Ag4 86.1(5) . 3_566 ?
O5 Ag4 Ag4 152.03(14) . 3_566 ?
O10 Ag5 O7 169.2(5) 4_565 . ?
O10 Ag5 O7A 163.6(6) 4_565 . ?
O7 Ag5 O7A 11.3(8) . . ?
O10 Ag5 O1 117.31(15) 4_565 . ?
O7 Ag5 O1 65.0(4) . . ?
O7A Ag5 O1 76.2(5) . . ?
O10 Ag5 Ag1 86.48(14) 4_565 . ?
O7 Ag5 Ag1 84.0(4) . . ?
O7A Ag5 Ag1 77.7(6) . . ?
O1 Ag5 Ag1 125.4(2) . . ?
O10 Ag5 Ag5 97.76(14) 4_565 2_656 ?
O7 Ag5 Ag5 91.4(4) . 2_656 ?
O7A Ag5 Ag5 98.3(6) . 2_656 ?
O1 Ag5 Ag5 49.5(2) . 2_656 ?
Ag1 Ag5 Ag5 174.55(2) . 2_656 ?
O13 Ag6 O12 158.5(7) . . ?
O13 Ag6 O12A 158.5(10) . . ?
O12 Ag6 O12A 13.1(8) . . ?
O13 Ag6 O13A 10.0(7) . . ?
O12 Ag6 O13A 152.4(6) . . ?
O12A Ag6 O13A 149.2(9) . . ?
O13 Ag6 O5 84.7(5) . 3_566 ?
O12 Ag6 O5 112.9(5) . 3_566 ?
O12A Ag6 O5 102.1(7) . 3_566 ?
O13A Ag6 O5 83.8(5) . 3_566 ?
O13 Ag6 Ag3 80.2(5) . . ?
O12 Ag6 Ag3 78.4(5) . . ?
O12A Ag6 Ag3 81.2(9) . . ?
O13A Ag6 Ag3 74.8(5) . . ?
O5 Ag6 Ag3 137.84(15) 3_566 . ?
O13 Ag6 Ag1 63.2(5) . . ?
O12 Ag6 Ag1 109.4(4) . . ?
O12A Ag6 Ag1 99.3(7) . . ?
O13A Ag6 Ag1 53.5(4) . . ?
O5 Ag6 Ag1 71.07(14) 3_566 . ?
Ag3 Ag6 Ag1 66.96(3) . . ?
Ag5 O1 Ag5 81.0(4) 2_656 . ?
Ag5 O1 H1B 115.1 2_656 . ?
Ag5 O1 H1B 115.1 . . ?
C1 O2 Ag2 123.8(5) . . ?
C12 O3 Ag4 130.0(5) . 3_566 ?
C12 O3 Ag1 135.1(5) . . ?
Ag4 O3 Ag1 92.1(2) 3_566 . ?
Ag4 O5 Ag6 97.2(2) . 3_566 ?
Ag4 O5 H5C 135.4 . . ?
Ag6 O5 H5C 102.7 3_566 . ?
Ag4 O5 H5D 103.4 . . ?
Ag6 O5 H5D 81.7 3_566 . ?
H5C O5 H5D 118.6 . . ?
C1 O6 Ag2 129.1(5) . 3_666 ?
C1 O6 Ag3 127.7(5) . 4_565 ?
Ag2 O6 Ag3 98.62(19) 3_666 4_565 ?
C13 O8 Ag1 125.9(6) . . ?
C24 O9 Ag1 129.5(5) . 4_566 ?
C24 O10 Ag5 120.7(5) . 4_566 ?
C24 O10 Ag2 129.0(5) . 4_566 ?
Ag5 O10 Ag2 97.6(2) 4_566 4_566 ?
C33 O11 Ag3 122.5(5) . . ?
O2 C1 O6 122.2(7) . . ?
O2 C1 C2 118.4(7) . . ?
O6 C1 C2 119.3(7) . . ?
C1 C2 C3 111.4(6) . . ?
C1 C2 C4 111.2(6) . . ?
C3 C2 C4 109.8(6) . . ?
C1 C2 C5 106.1(6) . . ?
C3 C2 C5 109.2(6) . . ?
C4 C2 C5 109.1(6) . . ?
C2 C3 C10 108.6(6) . . ?
C2 C3 H3A 110.0 . . ?
C10 C3 H3A 110.0 . . ?
C2 C3 H3B 110.0 . . ?
C10 C3 H3B 110.0 . . ?
H3A C3 H3B 108.4 . . ?
C2 C4 C6 109.5(6) . . ?
C2 C4 H4A 109.8 . . ?
C6 C4 H4A 109.8 . . ?
C2 C4 H4B 109.8 . . ?
C6 C4 H4B 109.8 . . ?
H4A C4 H4B 108.2 . . ?
C2 C5 C9 111.2(6) . . ?
C2 C5 H5A 109.4 . . ?
C9 C5 H5A 109.4 . . ?
C2 C5 H5B 109.4 . . ?
C9 C5 H5B 109.4 . . ?
H5A C5 H5B 108.0 . . ?
C8 C6 C4 108.8(7) . . ?
C8 C6 C7 110.6(6) . . ?
C4 C6 C7 109.0(6) . . ?
C8 C6 H6 109.5 . . ?
C4 C6 H6 109.5 . . ?
C7 C6 H6 109.5 . . ?
C9 C7 C6 109.7(6) . . ?
C9 C7 H7A 109.7 . . ?
C6 C7 H7A 109.7 . . ?
C9 C7 H7B 109.7 . . ?
C6 C7 H7B 109.7 . . ?
H7A C7 H7B 108.2 . . ?
C10 C8 C6 109.5(7) . . ?
C10 C8 H8A 109.8 . . ?
C6 C8 H8A 109.8 . . ?
C10 C8 H8B 109.8 . . ?
C6 C8 H8B 109.8 . . ?
H8A C8 H8B 108.2 . . ?
C7 C9 C12 113.0(6) . . ?
C7 C9 C11 109.1(6) . . ?
C12 C9 C11 107.4(6) . . ?
C7 C9 C5 107.6(6) . . ?
C12 C9 C5 111.1(6) . . ?
C11 C9 C5 108.5(6) . . ?
C8 C10 C11 109.1(7) . . ?
C8 C10 C3 110.5(6) . . ?
C11 C10 C3 110.2(7) . . ?
C8 C10 H10 109.0 . . ?
C11 C10 H10 109.0 . . ?
C3 C10 H10 109.0 . . ?
C10 C11 C9 110.4(6) . . ?
C10 C11 H11A 109.6 . . ?
C9 C11 H11A 109.6 . . ?
C10 C11 H11B 109.6 . . ?
C9 C11 H11B 109.6 . . ?
H11A C11 H11B 108.1 . . ?
O3 C12 O4A 123.4(11) . . ?
O3 C12 O4 123.9(10) . . ?
O4A C12 O4 21.1(10) . . ?
O3 C12 C9 118.0(7) . . ?
O4A C12 C9 117.7(11) . . ?
O4 C12 C9 116.8(10) . . ?
O7A C13 O8 121.0(14) . . ?
O7A C13 O7 20.7(13) . . ?
O8 C13 O7 125.3(10) . . ?
O7A C13 C14 119.1(14) . . ?
O8 C13 C14 118.3(8) . . ?
O7 C13 C14 115.7(10) . . ?
C16 C14 C13 112.6(7) . . ?
C16 C14 C15 109.9(6) . . ?
C13 C14 C15 107.4(6) . . ?
C16 C14 C17 108.1(6) . . ?
C13 C14 C17 109.9(6) . . ?
C15 C14 C17 108.8(6) . . ?
C14 C15 C22 110.7(6) . . ?
C14 C15 H15A 109.5 . . ?
C22 C15 H15A 109.5 . . ?
C14 C15 H15B 109.5 . . ?
C22 C15 H15B 109.5 . . ?
H15A C15 H15B 108.1 . . ?
C20 C16 C14 109.9(7) . . ?
C20 C16 H16A 109.7 . . ?
C14 C16 H16A 109.7 . . ?
C20 C16 H16B 109.7 . . ?
C14 C16 H16B 109.7 . . ?
H16A C16 H16B 108.2 . . ?
C18 C17 C14 109.7(6) . . ?
C18 C17 H17A 109.7 . . ?
C14 C17 H17A 109.7 . . ?
C18 C17 H17B 109.7 . . ?
C14 C17 H17B 109.7 . . ?
H17A C17 H17B 108.2 . . ?
C17 C18 C19 109.4(7) . . ?
C17 C18 C23 111.0(7) . . ?
C19 C18 C23 108.9(7) . . ?
C17 C18 H18 109.2 . . ?
C19 C18 H18 109.2 . . ?
C23 C18 H18 109.2 . . ?
C18 C19 C20 108.2(7) . . ?
C18 C19 H19A 110.1 . . ?
C20 C19 H19A 110.1 . . ?
C18 C19 H19B 110.1 . . ?
C20 C19 H19B 110.1 . . ?
H19A C19 H19B 108.4 . . ?
C16 C20 C21 110.9(7) . . ?
C16 C20 C19 108.8(7) . . ?
C21 C20 C19 109.1(7) . . ?
C16 C20 H20 109.4 . . ?
C21 C20 H20 109.4 . . ?
C19 C20 H20 109.4 . . ?
C20 C21 C22 110.3(6) . . ?
C20 C21 H21A 109.6 . . ?
C22 C21 H21A 109.6 . . ?
C20 C21 H21B 109.6 . . ?
C22 C21 H21B 109.6 . . ?
H21A C21 H21B 108.1 . . ?
C23 C22 C21 109.5(7) . . ?
C23 C22 C24 112.0(6) . . ?
C21 C22 C24 111.0(6) . . ?
C23 C22 C15 109.7(6) . . ?
C21 C22 C15 107.4(6) . . ?
C24 C22 C15 107.2(6) . . ?
C22 C23 C18 110.3(6) . . ?
C22 C23 H23A 109.6 . . ?
C18 C23 H23A 109.6 . . ?
C22 C23 H23B 109.6 . . ?
C18 C23 H23B 109.6 . . ?
H23A C23 H23B 108.1 . . ?
O9 C24 O10 123.5(7) . . ?
O9 C24 C22 119.0(7) . . ?
O10 C24 C22 117.5(7) . . ?
O14 C25 O13A 121.6(13) . . ?
O14 C25 O14A 20.9(11) . . ?
O13A C25 O14A 128.3(14) . . ?
O14 C25 O13 114.4(12) . . ?
O13A C25 O13 20.7(11) . . ?
O14A C25 O13 128.7(13) . . ?
O14 C25 C26 125.0(10) . . ?
O13A C25 C26 113.4(11) . . ?
O14A C25 C26 113.6(11) . . ?
O13 C25 C26 117.6(9) . . ?
C30 C26 C25 110.7(7) . . ?
C30 C26 C27 109.3(7) . . ?
C25 C26 C27 110.7(6) . . ?
C30 C26 C28 108.8(5) . . ?
C25 C26 C28 108.1(6) . . ?
C27 C26 C28 109.2(6) . . ?
C31 C27 C26 109.5(6) . . ?
C31 C27 H27A 109.8 . . ?
C26 C27 H27A 109.8 . . ?
C31 C27 H27B 109.8 . . ?
C26 C27 H27B 109.8 . . ?
H27A C27 H27B 108.2 . . ?
C26 C28 C26 109.8(9) . 2_556 ?
C26 C28 H28A 109.5 . . ?
C26 C28 H28A 109.9 2_556 . ?
C26 C30 C31 109.0(7) . 2_556 ?
C26 C30 H30A 109.9 . . ?
C31 C30 H30A 109.9 2_556 . ?
C26 C30 H30B 109.9 . . ?
C31 C30 H30B 109.9 2_556 . ?
H30A C30 H30B 108.3 . . ?
C27 C31 C32 110.2(7) . . ?
C27 C31 C30 111.0(7) . 2_556 ?
C32 C31 C30 108.8(6) . 2_556 ?
C27 C31 H31 108.9 . . ?
C32 C31 H31 108.9 . . ?
C30 C31 H31 108.9 2_556 . ?
C31 C32 C31 108.9(10) 2_556 . ?
C31 C32 H32A 109.8 2_556 . ?
C31 C32 H32A 110.0 . . ?
O12A C33 O11 125.3(17) . . ?
O12A C33 O12 22.7(15) . . ?
O11 C33 O12 121.9(10) . . ?
O12A C33 C34 114.3(17) . . ?
O11 C33 C34 118.4(8) . . ?
O12 C33 C34 118.8(10) . . ?
C33 C34 C37 113.2(7) . . ?
C33 C34 C35 110.9(6) . . ?
C37 C34 C35 108.7(6) . . ?
C33 C34 C36 109.5(6) . . ?
C37 C34 C36 107.4(6) . . ?
C35 C34 C36 106.9(6) . . ?
C34 C35 C34 113.3(9) 2_656 . ?
C34 C35 H35A 108.5 2_656 . ?
C34 C35 H35A 109.4 . . ?
C38 C36 C34 110.2(7) 2_656 . ?
C38 C36 H36A 109.6 2_656 . ?
C34 C36 H36A 109.6 . . ?
C38 C36 H36B 109.6 2_656 . ?
C34 C36 H36B 109.6 . . ?
H36A C36 H36B 108.1 . . ?
C34 C37 C38 110.2(7) . . ?
C34 C37 H37A 109.6 . . ?
C38 C37 H37A 109.6 . . ?
C34 C37 H37B 109.6 . . ?
C38 C37 H37B 109.6 . . ?
H37A C37 H37B 108.1 . . ?
C39 C38 C36 112.5(8) . 2_656 ?
C39 C38 C37 110.8(7) . . ?
C36 C38 C37 108.0(7) 2_656 . ?
C39 C38 H38 108.5 . . ?
C36 C38 H38 108.5 2_656 . ?
C37 C38 H38 108.5 . . ?
C38 C39 C38 107.4(10) . 2_656 ?
C38 C39 H39A 110.0 . . ?
C38 C39 H39A 110.6 2_656 . ?
H15D O15 H15C 117.4 . . ?
H18C O18 H18D 123.9 . . ?
H16C O16 H16D 83.4 . . ?
H17D O17 H17C 120.8 . . ?
H17E O17A H17F 153.5 . . ?
C25 O14A Ag3 113.5(12) . . ?
C25 O14 Ag3 124.0(10) . . ?
C13 O7 Ag5 120.0(11) . . ?
C13 O7A Ag5 115.9(16) . . ?
C13 O7A Ag3 107.2(13) . . ?
Ag5 O7A Ag3 90.2(9) . . ?
C12 O4 Ag4 119.1(10) . . ?
C12 O4A Ag4 117.8(12) . . ?
C25 O13 Ag6 125.0(11) . . ?
C25 O13A Ag6 113.0(11) . . ?
C25 O13A Ag1 120.6(11) . . ?
Ag6 O13A Ag1 77.6(6) . . ?
C33 O12 Ag6 119.1(10) . . ?
C33 O12A Ag6 123(2) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 O8 2.220(6) . ?
Ag1 O9 2.235(5) 4_565 ?
Ag1 O3 2.520(5) . ?
Ag1 O13A 2.560(18) . ?
Ag1 Ag5 2.8215(11) . ?
Ag1 Ag6 3.1101(12) . ?
Ag1 Ag3 3.2763(11) . ?
Ag2 O6 2.206(5) 3_666 ?
Ag2 O2 2.237(6) . ?
Ag2 O10 2.585(5) 4_565 ?
Ag2 Ag2 2.8299(14) 3_666 ?
Ag3 O14 2.132(14) . ?
Ag3 O11 2.190(5) . ?
Ag3 O14A 2.23(2) . ?
Ag3 O7A 2.45(2) . ?
Ag3 O6 2.516(5) 4_566 ?
Ag3 Ag6 2.8123(11) . ?
Ag4 O4 2.213(15) . ?
Ag4 O3 2.231(5) 3_566 ?
Ag4 O4A 2.25(2) . ?
Ag4 O5 2.467(6) . ?
Ag4 Ag4 2.7930(14) 3_566 ?
Ag5 O10 2.176(5) 4_565 ?
Ag5 O7 2.197(17) . ?
Ag5 O7A 2.33(2) . ?
Ag5 O1 2.565(10) . ?
Ag5 Ag5 3.3312(15) 2_656 ?
Ag6 O13 2.093(16) . ?
Ag6 O12 2.192(16) . ?
Ag6 O12A 2.23(3) . ?
Ag6 O13A 2.397(18) . ?
Ag6 O5 2.572(6) 3_566 ?
O1 Ag5 2.565(10) 2_656 ?
O1 H1B 0.8500 . ?
O2 C1 1.233(8) . ?
O3 C12 1.252(9) . ?
O3 Ag4 2.231(5) 3_566 ?
O5 Ag6 2.572(6) 3_566 ?
O5 H5C 0.8001 . ?
O5 H5D 0.7997 . ?
O6 C1 1.271(9) . ?
O6 Ag2 2.206(5) 3_666 ?
O6 Ag3 2.516(5) 4_565 ?
O8 C13 1.227(9) . ?
O9 C24 1.254(8) . ?
O9 Ag1 2.235(5) 4_566 ?
O10 C24 1.255(8) . ?
O10 Ag5 2.176(5) 4_566 ?
O10 Ag2 2.585(5) 4_566 ?
O11 C33 1.240(9) . ?
C1 C2 1.508(10) . ?
C2 C3 1.516(10) . ?
C2 C4 1.529(10) . ?
C2 C5 1.536(9) . ?
C3 C10 1.550(10) . ?
C3 H3A 0.9700 . ?
C3 H3B 0.9700 . ?
C4 C6 1.534(10) . ?
C4 H4A 0.9700 . ?
C4 H4B 0.9700 . ?
C5 C9 1.553(9) . ?
C5 H5A 0.9700 . ?
C5 H5B 0.9700 . ?
C6 C8 1.530(10) . ?
C6 C7 1.555(11) . ?
C6 H6 0.9800 . ?
C7 C9 1.519(10) . ?
C7 H7A 0.9700 . ?
C7 H7B 0.9700 . ?
C8 C10 1.493(11) . ?
C8 H8A 0.9700 . ?
C8 H8B 0.9700 . ?
C9 C12 1.521(10) . ?
C9 C11 1.537(10) . ?
C10 C11 1.531(10) . ?
C10 H10 0.9800 . ?
C11 H11A 0.9700 . ?
C11 H11B 0.9700 . ?
C12 O4A 1.27(2) . ?
C12 O4 1.284(15) . ?
C13 O7A 1.23(3) . ?
C13 O7 1.309(19) . ?
C13 C14 1.522(11) . ?
C14 C16 1.522(11) . ?
C14 C15 1.536(9) . ?
C14 C17 1.553(10) . ?
C15 C22 1.544(9) . ?
C15 H15A 0.9700 . ?
C15 H15B 0.9700 . ?
C16 C20 1.515(10) . ?
C16 H16A 0.9700 . ?
C16 H16B 0.9700 . ?
C17 C18 1.521(11) . ?
C17 H17A 0.9700 . ?
C17 H17B 0.9700 . ?
C18 C19 1.529(12) . ?
C18 C23 1.529(11) . ?
C18 H18 0.9800 . ?
C19 C20 1.573(11) . ?
C19 H19A 0.9700 . ?
C19 H19B 0.9700 . ?
C20 C21 1.524(10) . ?
C20 H20 0.9800 . ?
C21 C22 1.526(10) . ?
C21 H21A 0.9700 . ?
C21 H21B 0.9700 . ?
C22 C23 1.520(10) . ?
C22 C24 1.531(10) . ?
C23 H23A 0.9700 . ?
C23 H23B 0.9700 . ?
C25 O14 1.220(16) . ?
C25 O13A 1.25(2) . ?
C25 O14A 1.29(2) . ?
C25 O13 1.389(18) . ?
C25 C26 1.529(10) . ?
C26 C30 1.504(11) . ?
C26 C27 1.537(10) . ?
C26 C28 1.547(9) . ?
C27 C31 1.484(10) . ?
C27 H27A 0.9700 . ?
C27 H27B 0.9700 . ?
C28 C26 1.547(9) 2_556 ?
C28 H28A 0.9701 . ?
C30 C31 1.554(11) 2_556 ?
C30 H30A 0.9700 . ?
C30 H30B 0.9700 . ?
C31 C32 1.514(10) . ?
C31 C30 1.554(11) 2_556 ?
C31 H31 0.9800 . ?
C32 C31 1.514(10) 2_556 ?
C32 H32A 0.9701 . ?
C33 O12A 1.20(3) . ?
C33 O12 1.314(18) . ?
C33 C34 1.497(11) . ?
C34 C37 1.515(11) . ?
C34 C35 1.528(9) . ?
C34 C36 1.564(10) . ?
C35 C34 1.528(9) 2_656 ?
C35 H35A 0.9699 . ?
C36 C38 1.509(11) 2_656 ?
C36 H36A 0.9700 . ?
C36 H36B 0.9700 . ?
C37 C38 1.557(12) . ?
C37 H37A 0.9700 . ?
C37 H37B 0.9700 . ?
C38 C39 1.490(12) . ?
C38 C36 1.509(11) 2_656 ?
C38 H38 0.9800 . ?
C39 C38 1.490(12) 2_656 ?
C39 H39A 0.9701 . ?
O15 H15D 0.8002 . ?
O15 H15C 0.8001 . ?
O18 H18C 0.7999 . ?
O18 H18D 0.8000 . ?
O16 H16C 0.8001 . ?
O16 H16D 0.8002 . ?
O17 H17D 0.8000 . ?
O17 H17C 0.8003 . ?
O17A H17E 0.8002 . ?
O17A H17F 0.7999 . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
O8 Ag1 Ag3 O14 -70.9(4) . . . . ?
O9 Ag1 Ag3 O14 136.6(4) 4_565 . . . ?
O3 Ag1 Ag3 O14 8.8(5) . . . . ?
O13A Ag1 Ag3 O14 23.2(6) . . . . ?
Ag5 Ag1 Ag3 O14 -157.7(4) . . . . ?
Ag6 Ag1 Ag3 O14 79.5(4) . . . . ?
O8 Ag1 Ag3 O11 128.3(2) . . . . ?
O9 Ag1 Ag3 O11 -24.2(2) 4_565 . . . ?
O3 Ag1 Ag3 O11 -152.0(3) . . . . ?
O13A Ag1 Ag3 O11 -137.6(4) . . . . ?
Ag5 Ag1 Ag3 O11 41.49(15) . . . . ?
Ag6 Ag1 Ag3 O11 -81.23(15) . . . . ?
O8 Ag1 Ag3 O14A -59.2(5) . . . . ?
O9 Ag1 Ag3 O14A 148.3(5) 4_565 . . . ?
O3 Ag1 Ag3 O14A 20.5(5) . . . . ?
O13A Ag1 Ag3 O14A 34.9(6) . . . . ?
Ag5 Ag1 Ag3 O14A -146.0(5) . . . . ?
Ag6 Ag1 Ag3 O14A 91.2(5) . . . . ?
O8 Ag1 Ag3 O7A 39.5(7) . . . . ?
O9 Ag1 Ag3 O7A -113.1(7) 4_565 . . . ?
O3 Ag1 Ag3 O7A 119.1(7) . . . . ?
O13A Ag1 Ag3 O7A 133.6(8) . . . . ?
Ag5 Ag1 Ag3 O7A -47.4(6) . . . . ?
Ag6 Ag1 Ag3 O7A -170.1(6) . . . . ?
O8 Ag1 Ag3 O6 54.3(3) . . . 4_566 ?
O9 Ag1 Ag3 O6 -98.2(3) 4_565 . . 4_566 ?
O3 Ag1 Ag3 O6 134.0(3) . . . 4_566 ?
O13A Ag1 Ag3 O6 148.5(5) . . . 4_566 ?
Ag5 Ag1 Ag3 O6 -32.5(2) . . . 4_566 ?
Ag6 Ag1 Ag3 O6 -155.2(2) . . . 4_566 ?
O8 Ag1 Ag3 Ag6 -150.46(17) . . . . ?
O9 Ag1 Ag3 Ag6 57.03(14) 4_565 . . . ?
O3 Ag1 Ag3 Ag6 -70.8(2) . . . . ?
O13A Ag1 Ag3 Ag6 -56.3(4) . . . . ?
Ag5 Ag1 Ag3 Ag6 122.73(3) . . . . ?
O8 Ag1 Ag5 O10 159.5(2) . . . 4_565 ?
O9 Ag1 Ag5 O10 -11.2(2) 4_565 . . 4_565 ?
O3 Ag1 Ag5 O10 65.0(3) . . . 4_565 ?
O13A Ag1 Ag5 O10 -127.6(5) . . . 4_565 ?
Ag6 Ag1 Ag5 O10 -86.47(15) . . . 4_565 ?
Ag3 Ag1 Ag5 O10 -128.73(15) . . . 4_565 ?
O8 Ag1 Ag5 O7 -15.3(5) . . . . ?
O9 Ag1 Ag5 O7 174.0(5) 4_565 . . . ?
O3 Ag1 Ag5 O7 -109.8(5) . . . . ?
O13A Ag1 Ag5 O7 57.6(7) . . . . ?
Ag6 Ag1 Ag5 O7 98.7(5) . . . . ?
Ag3 Ag1 Ag5 O7 56.5(5) . . . . ?
O8 Ag1 Ag5 O7A -24.7(6) . . . . ?
O9 Ag1 Ag5 O7A 164.6(6) 4_565 . . . ?
O3 Ag1 Ag5 O7A -119.2(6) . . . . ?
O13A Ag1 Ag5 O7A 48.2(8) . . . . ?
Ag6 Ag1 Ag5 O7A 89.3(6) . . . . ?
Ag3 Ag1 Ag5 O7A 47.0(6) . . . . ?
O8 Ag1 Ag5 O1 38.19(16) . . . . ?
O9 Ag1 Ag5 O1 -132.50(16) 4_565 . . . ?
O3 Ag1 Ag5 O1 -56.3(2) . . . . ?
O13A Ag1 Ag5 O1 111.1(5) . . . . ?
Ag6 Ag1 Ag5 O1 152.19(3) . . . . ?
Ag3 Ag1 Ag5 O1 109.93(4) . . . . ?
O8 Ag1 Ag5 Ag5 18.2(4) . . . 2_656 ?
O9 Ag1 Ag5 Ag5 -152.5(4) 4_565 . . 2_656 ?
O3 Ag1 Ag5 Ag5 -76.3(5) . . . 2_656 ?
O13A Ag1 Ag5 Ag5 91.1(6) . . . 2_656 ?
Ag6 Ag1 Ag5 Ag5 132.2(4) . . . 2_656 ?
Ag3 Ag1 Ag5 Ag5 89.9(4) . . . 2_656 ?
O14 Ag3 Ag6 O13 -24.7(7) . . . . ?
O11 Ag3 Ag6 O13 155.5(5) . . . . ?
O14A Ag3 Ag6 O13 -16.8(7) . . . . ?
O7A Ag3 Ag6 O13 76.5(9) . . . . ?
O6 Ag3 Ag6 O13 -139.7(6) 4_566 . . . ?
Ag1 Ag3 Ag6 O13 65.0(5) . . . . ?
O14 Ag3 Ag6 O12 153.2(6) . . . . ?
O11 Ag3 Ag6 O12 -26.7(5) . . . . ?
O14A Ag3 Ag6 O12 161.1(7) . . . . ?
O7A Ag3 Ag6 O12 -105.6(9) . . . . ?
O6 Ag3 Ag6 O12 38.2(5) 4_566 . . . ?
Ag1 Ag3 Ag6 O12 -117.2(4) . . . . ?
O14 Ag3 Ag6 O12A 166.2(7) . . . . ?
O11 Ag3 Ag6 O12A -13.6(6) . . . . ?
O14A Ag3 Ag6 O12A 174.1(8) . . . . ?
O7A Ag3 Ag6 O12A -92.6(10) . . . . ?
O6 Ag3 Ag6 O12A 51.2(7) 4_566 . . . ?
Ag1 Ag3 Ag6 O12A -104.1(6) . . . . ?
O14 Ag3 Ag6 O13A -33.3(6) . . . . ?
O11 Ag3 Ag6 O13A 146.9(5) . . . . ?
O14A Ag3 Ag6 O13A -25.3(7) . . . . ?
O7A Ag3 Ag6 O13A 67.9(9) . . . . ?
O6 Ag3 Ag6 O13A -148.3(5) 4_566 . . . ?
Ag1 Ag3 Ag6 O13A 56.4(4) . . . . ?
O14 Ag3 Ag6 O5 -95.4(4) . . . 3_566 ?
O11 Ag3 Ag6 O5 84.8(2) . . . 3_566 ?
O14A Ag3 Ag6 O5 -87.5(5) . . . 3_566 ?
O7A Ag3 Ag6 O5 5.8(8) . . . 3_566 ?
O6 Ag3 Ag6 O5 149.6(3) 4_566 . . 3_566 ?
Ag1 Ag3 Ag6 O5 -5.73(19) . . . 3_566 ?
O14 Ag3 Ag6 Ag1 -89.7(4) . . . . ?
O11 Ag3 Ag6 Ag1 90.51(15) . . . . ?
O14A Ag3 Ag6 Ag1 -81.7(5) . . . . ?
O7A Ag3 Ag6 Ag1 11.5(7) . . . . ?
O6 Ag3 Ag6 Ag1 155.3(2) 4_566 . . . ?
O8 Ag1 Ag6 O13 -59.9(6) . . . . ?
O9 Ag1 Ag6 O13 143.8(6) 4_565 . . . ?
O3 Ag1 Ag6 O13 54.6(6) . . . . ?
O13A Ag1 Ag6 O13 -2.8(11) . . . . ?
Ag5 Ag1 Ag6 O13 -142.0(5) . . . . ?
Ag3 Ag1 Ag6 O13 -90.4(5) . . . . ?
O8 Ag1 Ag6 O12 98.1(6) . . . . ?
O9 Ag1 Ag6 O12 -58.2(5) 4_565 . . . ?
O3 Ag1 Ag6 O12 -147.4(5) . . . . ?
O13A Ag1 Ag6 O12 155.2(8) . . . . ?
Ag5 Ag1 Ag6 O12 16.0(5) . . . . ?
Ag3 Ag1 Ag6 O12 67.6(5) . . . . ?
O8 Ag1 Ag6 O12A 106.8(8) . . . . ?
O9 Ag1 Ag6 O12A -49.5(8) 4_565 . . . ?
O3 Ag1 Ag6 O12A -138.8(8) . . . . ?
O13A Ag1 Ag6 O12A 163.9(10) . . . . ?
Ag5 Ag1 Ag6 O12A 24.6(8) . . . . ?
Ag3 Ag1 Ag6 O12A 76.2(8) . . . . ?
O8 Ag1 Ag6 O13A -57.1(6) . . . . ?
O9 Ag1 Ag6 O13A 146.6(6) 4_565 . . . ?
O3 Ag1 Ag6 O13A 57.3(6) . . . . ?
Ag5 Ag1 Ag6 O13A -139.2(6) . . . . ?
Ag3 Ag1 Ag6 O13A -87.7(6) . . . . ?
O8 Ag1 Ag6 O5 -153.5(2) . . . 3_566 ?
O9 Ag1 Ag6 O5 50.19(19) 4_565 . . 3_566 ?
O3 Ag1 Ag6 O5 -39.07(19) . . . 3_566 ?
O13A Ag1 Ag6 O5 -96.4(6) . . . 3_566 ?
Ag5 Ag1 Ag6 O5 124.35(13) . . . 3_566 ?
Ag3 Ag1 Ag6 O5 175.94(13) . . . 3_566 ?
O8 Ag1 Ag6 Ag3 30.56(17) . . . . ?
O9 Ag1 Ag6 Ag3 -125.75(14) 4_565 . . . ?
O3 Ag1 Ag6 Ag3 145.00(13) . . . . ?
O13A Ag1 Ag6 Ag3 87.7(6) . . . . ?
Ag5 Ag1 Ag6 Ag3 -51.58(3) . . . . ?
O10 Ag5 O1 Ag5 76.06(19) 4_565 . . 2_656 ?
O7 Ag5 O1 Ag5 -115.7(5) . . . 2_656 ?
O7A Ag5 O1 Ag5 -114.0(7) . . . 2_656 ?
Ag1 Ag5 O1 Ag5 -177.55(5) . . . 2_656 ?
O6 Ag2 O2 C1 -42.9(10) 3_666 . . . ?
O10 Ag2 O2 C1 108.0(6) 4_565 . . . ?
Ag2 Ag2 O2 C1 -13.8(6) 3_666 . . . ?
O8 Ag1 O3 C12 -43.9(7) . . . . ?
O9 Ag1 O3 C12 114.9(7) 4_565 . . . ?
O13A Ag1 O3 C12 -126.8(8) . . . . ?
Ag5 Ag1 O3 C12 43.8(8) . . . . ?
Ag6 Ag1 O3 C12 -166.6(7) . . . . ?
Ag3 Ag1 O3 C12 -113.6(7) . . . . ?
O8 Ag1 O3 Ag4 117.3(2) . . . 3_566 ?
O9 Ag1 O3 Ag4 -83.8(2) 4_565 . . 3_566 ?
O13A Ag1 O3 Ag4 34.5(4) . . . 3_566 ?
Ag5 Ag1 O3 Ag4 -155.00(9) . . . 3_566 ?
Ag6 Ag1 O3 Ag4 -5.35(19) . . . 3_566 ?
Ag3 Ag1 O3 Ag4 47.6(3) . . . 3_566 ?
O4 Ag4 O5 Ag6 -97.2(4) . . . 3_566 ?
O3 Ag4 O5 Ag6 92.9(2) 3_566 . . 3_566 ?
O4A Ag4 O5 Ag6 -87.0(5) . . . 3_566 ?
Ag4 Ag4 O5 Ag6 174.00(14) 3_566 . . 3_566 ?
O9 Ag1 O8 C13 44.3(9) 4_565 . . . ?
O3 Ag1 O8 C13 168.5(7) . . . . ?
O13A Ag1 O8 C13 -111.0(8) . . . . ?
Ag5 Ag1 O8 C13 23.1(6) . . . . ?
Ag6 Ag1 O8 C13 -71.6(7) . . . . ?
Ag3 Ag1 O8 C13 -46.2(6) . . . . ?
O14 Ag3 O11 C33 27.7(14) . . . . ?
O14A Ag3 O11 C33 59(2) . . . . ?
O7A Ag3 O11 C33 156.9(9) . . . . ?
O6 Ag3 O11 C33 -122.2(6) 4_566 . . . ?
Ag6 Ag3 O11 C33 28.2(6) . . . . ?
Ag1 Ag3 O11 C33 89.3(6) . . . . ?
Ag2 O2 C1 O6 8.4(11) . . . . ?
Ag2 O2 C1 C2 -166.7(5) . . . . ?
Ag2 O6 C1 O2 7.0(11) 3_666 . . . ?
Ag3 O6 C1 O2 -143.8(6) 4_565 . . . ?
Ag2 O6 C1 C2 -177.9(5) 3_666 . . . ?
Ag3 O6 C1 C2 31.3(10) 4_565 . . . ?
O2 C1 C2 C3 -34.3(9) . . . . ?
O6 C1 C2 C3 150.4(7) . . . . ?
O2 C1 C2 C4 -157.2(7) . . . . ?
O6 C1 C2 C4 27.6(10) . . . . ?
O2 C1 C2 C5 84.4(8) . . . . ?
O6 C1 C2 C5 -90.9(8) . . . . ?
C1 C2 C3 C10 177.5(6) . . . . ?
C4 C2 C3 C10 -58.9(8) . . . . ?
C5 C2 C3 C10 60.7(8) . . . . ?
C1 C2 C4 C6 -175.8(6) . . . . ?
C3 C2 C4 C6 60.5(8) . . . . ?
C5 C2 C4 C6 -59.2(8) . . . . ?
C1 C2 C5 C9 179.3(6) . . . . ?
C3 C2 C5 C9 -60.5(8) . . . . ?
C4 C2 C5 C9 59.5(7) . . . . ?
C2 C4 C6 C8 -60.2(8) . . . . ?
C2 C4 C6 C7 60.6(8) . . . . ?
C8 C6 C7 C9 57.4(8) . . . . ?
C4 C6 C7 C9 -62.2(8) . . . . ?
C4 C6 C8 C10 60.5(8) . . . . ?
C7 C6 C8 C10 -59.3(9) . . . . ?
C6 C7 C9 C12 -176.4(6) . . . . ?
C6 C7 C9 C11 -56.9(8) . . . . ?
C6 C7 C9 C5 60.5(8) . . . . ?
C2 C5 C9 C7 -60.1(7) . . . . ?
C2 C5 C9 C12 175.7(6) . . . . ?
C2 C5 C9 C11 57.8(8) . . . . ?
C6 C8 C10 C11 60.8(8) . . . . ?
C6 C8 C10 C3 -60.5(9) . . . . ?
C2 C3 C10 C8 59.7(8) . . . . ?
C2 C3 C10 C11 -61.0(8) . . . . ?
C8 C10 C11 C9 -61.8(8) . . . . ?
C3 C10 C11 C9 59.8(8) . . . . ?
C7 C9 C11 C10 59.8(8) . . . . ?
C12 C9 C11 C10 -177.3(7) . . . . ?
C5 C9 C11 C10 -57.1(8) . . . . ?
Ag4 O3 C12 O4A 14.4(14) 3_566 . . . ?
Ag1 O3 C12 O4A 169.6(10) . . . . ?
Ag4 O3 C12 O4 -11.0(14) 3_566 . . . ?
Ag1 O3 C12 O4 144.2(9) . . . . ?
Ag4 O3 C12 C9 -177.3(4) 3_566 . . . ?
Ag1 O3 C12 C9 -22.1(10) . . . . ?
C7 C9 C12 O3 -156.0(7) . . . . ?
C11 C9 C12 O3 83.6(8) . . . . ?
C5 C9 C12 O3 -35.0(9) . . . . ?
C7 C9 C12 O4A 13.0(13) . . . . ?
C11 C9 C12 O4A -107.5(11) . . . . ?
C5 C9 C12 O4A 134.0(11) . . . . ?
C7 C9 C12 O4 36.8(12) . . . . ?
C11 C9 C12 O4 -83.7(11) . . . . ?
C5 C9 C12 O4 157.8(9) . . . . ?
Ag1 O8 C13 O7A 7.1(15) . . . . ?
Ag1 O8 C13 O7 -17.2(16) . . . . ?
Ag1 O8 C13 C14 172.7(5) . . . . ?
O7A C13 C14 C16 171.6(12) . . . . ?
O8 C13 C14 C16 5.7(10) . . . . ?
O7 C13 C14 C16 -165.3(11) . . . . ?
O7A C13 C14 C15 50.4(14) . . . . ?
O8 C13 C14 C15 -115.5(8) . . . . ?
O7 C13 C14 C15 73.5(12) . . . . ?
O7A C13 C14 C17 -67.8(13) . . . . ?
O8 C13 C14 C17 126.3(8) . . . . ?
O7 C13 C14 C17 -44.7(13) . . . . ?
C16 C14 C15 C22 59.3(8) . . . . ?
C13 C14 C15 C22 -177.9(6) . . . . ?
C17 C14 C15 C22 -58.9(8) . . . . ?
C13 C14 C16 C20 -176.9(6) . . . . ?
C15 C14 C16 C20 -57.1(8) . . . . ?
C17 C14 C16 C20 61.5(8) . . . . ?
C16 C14 C17 C18 -60.8(8) . . . . ?
C13 C14 C17 C18 175.9(7) . . . . ?
C15 C14 C17 C18 58.6(9) . . . . ?
C14 C17 C18 C19 61.3(8) . . . . ?
C14 C17 C18 C23 -58.8(9) . . . . ?
C17 C18 C19 C20 -60.4(8) . . . . ?
C23 C18 C19 C20 61.0(9) . . . . ?
C14 C16 C20 C21 57.9(9) . . . . ?
C14 C16 C20 C19 -62.0(8) . . . . ?
C18 C19 C20 C16 60.7(9) . . . . ?
C18 C19 C20 C21 -60.3(9) . . . . ?
C16 C20 C21 C22 -60.4(9) . . . . ?
C19 C20 C21 C22 59.4(8) . . . . ?
C20 C21 C22 C23 -59.1(8) . . . . ?
C20 C21 C22 C24 176.8(6) . . . . ?
C20 C21 C22 C15 59.9(8) . . . . ?
C14 C15 C22 C23 59.0(8) . . . . ?
C14 C15 C22 C21 -59.9(8) . . . . ?
C14 C15 C22 C24 -179.2(6) . . . . ?
C21 C22 C23 C18 59.8(8) . . . . ?
C24 C22 C23 C18 -176.6(7) . . . . ?
C15 C22 C23 C18 -57.7(9) . . . . ?
C17 C18 C23 C22 58.7(9) . . . . ?
C19 C18 C23 C22 -61.7(9) . . . . ?
Ag1 O9 C24 O10 15.4(12) 4_566 . . . ?
Ag1 O9 C24 C22 -162.3(5) 4_566 . . . ?
Ag5 O10 C24 O9 2.4(10) 4_566 . . . ?
Ag2 O10 C24 O9 -130.5(7) 4_566 . . . ?
Ag5 O10 C24 C22 -179.8(5) 4_566 . . . ?
Ag2 O10 C24 C22 47.3(9) 4_566 . . . ?
C23 C22 C24 O9 -151.0(7) . . . . ?
C21 C22 C24 O9 -28.4(10) . . . . ?
C15 C22 C24 O9 88.6(8) . . . . ?
C23 C22 C24 O10 31.1(10) . . . . ?
C21 C22 C24 O10 153.8(7) . . . . ?
C15 C22 C24 O10 -89.3(8) . . . . ?
O14 C25 C26 C30 -20.6(14) . . . . ?
O13A C25 C26 C30 157.3(10) . . . . ?
O14A C25 C26 C30 -0.4(13) . . . . ?
O13 C25 C26 C30 179.9(11) . . . . ?
O14 C25 C26 C27 -142.0(12) . . . . ?
O13A C25 C26 C27 35.9(12) . . . . ?
O14A C25 C26 C27 -121.8(11) . . . . ?
O13 C25 C26 C27 58.5(13) . . . . ?
O14 C25 C26 C28 98.4(12) . . . . ?
O13A C25 C26 C28 -83.6(10) . . . . ?
O14A C25 C26 C28 118.6(11) . . . . ?
O13 C25 C26 C28 -61.1(12) . . . . ?
C30 C26 C27 C31 60.2(9) . . . . ?
C25 C26 C27 C31 -177.6(7) . . . . ?
C28 C26 C27 C31 -58.7(9) . . . . ?
C30 C26 C28 C26 -60.3(5) . . . 2_556 ?
C25 C26 C28 C26 179.4(7) . . . 2_556 ?
C27 C26 C28 C26 58.9(5) . . . 2_556 ?
C25 C26 C30 C31 178.5(6) . . . 2_556 ?
C27 C26 C30 C31 -59.4(8) . . . 2_556 ?
C28 C26 C30 C31 59.9(8) . . . 2_556 ?
C26 C27 C31 C32 -60.8(9) . . . . ?
C26 C27 C31 C30 59.8(9) . . . 2_556 ?
C27 C31 C32 C31 61.7(5) . . . 2_556 ?
C30 C31 C32 C31 -60.2(5) 2_556 . . 2_556 ?
Ag3 O11 C33 O12A -32.2(18) . . . . ?
Ag3 O11 C33 O12 -5.2(15) . . . . ?
Ag3 O11 C33 C34 164.4(5) . . . . ?
O12A C33 C34 C37 -17.3(16) . . . . ?
O11 C33 C34 C37 147.9(8) . . . . ?
O12 C33 C34 C37 -42.2(14) . . . . ?
O12A C33 C34 C35 -139.8(14) . . . . ?
O11 C33 C34 C35 25.4(10) . . . . ?
O12 C33 C34 C35 -164.7(11) . . . . ?
O12A C33 C34 C36 102.6(15) . . . . ?
O11 C33 C34 C36 -92.3(9) . . . . ?
O12 C33 C34 C36 77.7(14) . . . . ?
C33 C34 C35 C34 -176.9(7) . . . 2_656 ?
C37 C34 C35 C34 58.1(5) . . . 2_656 ?
C36 C34 C35 C34 -57.6(5) . . . 2_656 ?
C33 C34 C36 C38 -179.8(8) . . . 2_656 ?
C37 C34 C36 C38 -56.5(9) . . . 2_656 ?
C35 C34 C36 C38 60.0(9) . . . 2_656 ?
C33 C34 C37 C38 178.0(7) . . . . ?
C35 C34 C37 C38 -58.3(9) . . . . ?
C36 C34 C37 C38 57.0(9) . . . . ?
C34 C37 C38 C39 -61.5(9) . . . . ?
C34 C37 C38 C36 62.0(10) . . . 2_656 ?
C36 C38 C39 C38 -60.7(6) 2_656 . . 2_656 ?
C37 C38 C39 C38 60.2(5) . . . 2_656 ?
O14 C25 O14A Ag3 -59(4) . . . . ?
O13A C25 O14A Ag3 19(2) . . . . ?
O13 C25 O14A Ag3 -7(2) . . . . ?
C26 C25 O14A Ag3 173.2(7) . . . . ?
O14 Ag3 O14A C25 58(4) . . . . ?
O11 Ag3 O14A C25 -13(3) . . . . ?
O7A Ag3 O14A C25 -109.9(13) . . . . ?
O6 Ag3 O14A C25 168.4(10) 4_566 . . . ?
Ag6 Ag3 O14A C25 17.4(11) . . . . ?
Ag1 Ag3 O14A C25 -43.6(11) . . . . ?
O13A C25 O14 Ag3 -19.0(19) . . . . ?
O14A C25 O14 Ag3 96(5) . . . . ?
O13 C25 O14 Ag3 -41.1(17) . . . . ?
C26 C25 O14 Ag3 158.8(7) . . . . ?
O11 Ag3 O14 C25 46(2) . . . . ?
O14A Ag3 O14 C25 -92(4) . . . . ?
O7A Ag3 O14 C25 -80.2(15) . . . . ?
O6 Ag3 O14 C25 -167.0(11) 4_566 . . . ?
Ag6 Ag3 O14 C25 45.6(12) . . . . ?
Ag1 Ag3 O14 C25 -15.9(12) . . . . ?
O7A C13 O7 Ag5 -91(5) . . . . ?
O8 C13 O7 Ag5 -5.9(19) . . . . ?
C14 C13 O7 Ag5 164.5(7) . . . . ?
O10 Ag5 O7 C13 -11(4) 4_565 . . . ?
O7A Ag5 O7 C13 72(5) . . . . ?
O1 Ag5 O7 C13 -116.3(14) . . . . ?
Ag1 Ag5 O7 C13 17.4(12) . . . . ?
Ag5 Ag5 O7 C13 -159.6(13) 2_656 . . . ?
O8 C13 O7A Ag5 -43.2(16) . . . . ?
O7 C13 O7A Ag5 65(5) . . . . ?
C14 C13 O7A Ag5 151.3(9) . . . . ?
O8 C13 O7A Ag3 55.7(16) . . . . ?
O7 C13 O7A Ag3 164(6) . . . . ?
C14 C13 O7A Ag3 -109.9(12) . . . . ?
O10 Ag5 O7A C13 60(3) 4_565 . . . ?
O7 Ag5 O7A C13 -78(5) . . . . ?
O1 Ag5 O7A C13 -86.6(14) . . . . ?
Ag1 Ag5 O7A C13 45.1(13) . . . . ?
Ag5 Ag5 O7A C13 -131.2(13) 2_656 . . . ?
O10 Ag5 O7A Ag3 -49(3) 4_565 . . . ?
O7 Ag5 O7A Ag3 172(6) . . . . ?
O1 Ag5 O7A Ag3 164.1(8) . . . . ?
Ag1 Ag5 O7A Ag3 -64.2(6) . . . . ?
Ag5 Ag5 O7A Ag3 119.5(6) 2_656 . . . ?
O14 Ag3 O7A C13 13.9(17) . . . . ?
O11 Ag3 O7A C13 -148.6(15) . . . . ?
O14A Ag3 O7A C13 16.4(16) . . . . ?
O6 Ag3 O7A C13 126.0(15) 4_566 . . . ?
Ag6 Ag3 O7A C13 -73.0(16) . . . . ?
Ag1 Ag3 O7A C13 -62.1(14) . . . . ?
O14 Ag3 O7A Ag5 131.2(7) . . . . ?
O11 Ag3 O7A Ag5 -31.3(6) . . . . ?
O14A Ag3 O7A Ag5 133.7(8) . . . . ?
O6 Ag3 O7A Ag5 -116.8(7) 4_566 . . . ?
Ag6 Ag3 O7A Ag5 44.2(10) . . . . ?
Ag1 Ag3 O7A Ag5 55.1(6) . . . . ?
O3 C12 O4 Ag4 15.2(15) . . . . ?
O4A C12 O4 Ag4 -81(4) . . . . ?
C9 C12 O4 Ag4 -178.4(6) . . . . ?
O3 Ag4 O4 C12 -25(2) 3_566 . . . ?
O4A Ag4 O4 C12 74(4) . . . . ?
O5 Ag4 O4 C12 -162.6(10) . . . . ?
Ag4 Ag4 O4 C12 -10.6(10) 3_566 . . . ?
O3 C12 O4A Ag4 -24.7(17) . . . . ?
O4 C12 O4A Ag4 74(4) . . . . ?
C9 C12 O4A Ag4 166.9(7) . . . . ?
O4 Ag4 O4A C12 -75(4) . . . . ?
O3 Ag4 O4A C12 48(2) 3_566 . . . ?
O5 Ag4 O4A C12 -132.8(12) . . . . ?
Ag4 Ag4 O4A C12 19.6(12) 3_566 . . . ?
O14 C25 O13 Ag6 2.3(19) . . . . ?
O13A C25 O13 Ag6 -113(4) . . . . ?
O14A C25 O13 Ag6 -16(2) . . . . ?
C26 C25 O13 Ag6 163.9(8) . . . . ?
O12 Ag6 O13 C25 17(3) . . . . ?
O12A Ag6 O13 C25 53(3) . . . . ?
O13A Ag6 O13 C25 78(5) . . . . ?
O5 Ag6 O13 C25 162.8(14) 3_566 . . . ?
Ag3 Ag6 O13 C25 22.3(12) . . . . ?
Ag1 Ag6 O13 C25 91.3(13) . . . . ?
O14 C25 O13A Ag6 -29.6(17) . . . . ?
O14A C25 O13A Ag6 -53.9(18) . . . . ?
O13 C25 O13A Ag6 46(3) . . . . ?
C26 C25 O13A Ag6 152.3(7) . . . . ?
O14 C25 O13A Ag1 59.3(17) . . . . ?
O14A C25 O13A Ag1 35(2) . . . . ?
O13 C25 O13A Ag1 135(5) . . . . ?
C26 C25 O13A Ag1 -118.7(11) . . . . ?
O13 Ag6 O13A C25 -76(5) . . . . ?
O12 Ag6 O13A C25 59.7(18) . . . . ?
O12A Ag6 O13A C25 85.9(18) . . . . ?
O5 Ag6 O13A C25 -170.7(12) 3_566 . . . ?
Ag3 Ag6 O13A C25 45.9(11) . . . . ?
Ag1 Ag6 O13A C25 118.3(13) . . . . ?
O13 Ag6 O13A Ag1 166(6) . . . . ?
O12 Ag6 O13A Ag1 -58.6(15) . . . . ?
O12A Ag6 O13A Ag1 -32.3(17) . . . . ?
O5 Ag6 O13A Ag1 71.0(4) 3_566 . . . ?
Ag3 Ag6 O13A Ag1 -72.4(3) . . . . ?
O8 Ag1 O13A C25 20.6(12) . . . . ?
O9 Ag1 O13A C25 -147.4(11) 4_565 . . . ?
O3 Ag1 O13A C25 123.0(13) . . . . ?
Ag5 Ag1 O13A C25 -49.9(15) . . . . ?
Ag6 Ag1 O13A C25 -109.6(15) . . . . ?
Ag3 Ag1 O13A C25 -48.8(12) . . . . ?
O8 Ag1 O13A Ag6 130.2(5) . . . . ?
O9 Ag1 O13A Ag6 -37.8(6) 4_565 . . . ?
O3 Ag1 O13A Ag6 -127.4(4) . . . . ?
Ag5 Ag1 O13A Ag6 59.7(6) . . . . ?
Ag3 Ag1 O13A Ag6 60.8(3) . . . . ?
O12A C33 O12 Ag6 73(5) . . . . ?
O11 C33 O12 Ag6 -33.3(19) . . . . ?
C34 C33 O12 Ag6 157.1(7) . . . . ?
O13 Ag6 O12 C33 47(3) . . . . ?
O12A Ag6 O12 C33 -60(5) . . . . ?
O13A Ag6 O12 C33 27(2) . . . . ?
O5 Ag6 O12 C33 -96.5(14) 3_566 . . . ?
Ag3 Ag6 O12 C33 40.8(13) . . . . ?
Ag1 Ag6 O12 C33 -19.4(15) . . . . ?
O11 C33 O12A Ag6 11(3) . . . . ?
O12 C33 O12A Ag6 -78(5) . . . . ?
C34 C33 O12A Ag6 175.2(10) . . . . ?
O13 Ag6 O12A C33 -22(4) . . . . ?
O12 Ag6 O12A C33 85(6) . . . . ?
O13A Ag6 O12A C33 -30(3) . . . . ?
O5 Ag6 O12A C33 -128.8(18) 3_566 . . . ?
Ag3 Ag6 O12A C33 8.4(18) . . . . ?
Ag1 Ag6 O12A C33 -56.3(19) . . . . ?
