#------------------------------------------------------------------------------
#$Date: 2016-03-25 09:58:19 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179736 $
#$URL: svn://www.crystallography.net/cod/cif/7/00/32/7003224.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7003224
loop_
_publ_author_name
'Huang, Yong-Qing'
'Shen, Zhong-Liang'
'Okamura, Taka-aki'
'Wang, Yan'
'Wang, Xiao-Feng'
'Sun, Wei-Yin'
'Yu, Jin-Quan'
'Ueyama, Norikazu'
_publ_section_title
;
 Silver(i) complexes with oxazoline-containing tripodal ligands:
 structure variation via counter anions and reaction conditions
;
_journal_issue                   2
_journal_name_full               'Dalton Transactions'
_journal_page_first              204
_journal_page_last               213
_journal_paper_doi               10.1039/b714502k
_journal_year                    2008
_chemical_formula_moiety         'C16 H18 Ag2 N5 O10'
_chemical_formula_sum            'C16 H18 Ag2 N5 O10'
_chemical_formula_weight         656.09
_chemical_name_common            (Ag2(L)(NO3)2)-MeOH
_chemical_name_systematic
;
[Ag2(L)(NO3)2]-MeOH
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                116.370(4)
_cell_angle_beta                 96.813(3)
_cell_angle_gamma                98.940(4)
_cell_formula_units_Z            2
_cell_length_a                   8.3073(10)
_cell_length_b                   11.3195(19)
_cell_length_c                   12.486(2)
_cell_measurement_reflns_used    485
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      18.59
_cell_measurement_theta_min      2.54
_cell_volume                     1015.5(3)
_computing_cell_refinement       'SAINT (Bruker, 2001)'
_computing_data_collection       'SMART (Bruker, 2001)'
_computing_data_reduction        'SAINT (Bruker, 2001)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.984
_diffrn_measured_fraction_theta_max 0.984
_diffrn_measurement_device_type  'Bruker Smart Apex CCD'
_diffrn_measurement_method       'omega and phi scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0492
_diffrn_reflns_av_sigmaI/netI    0.1314
_diffrn_reflns_limit_h_max       9
_diffrn_reflns_limit_h_min       -9
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       -8
_diffrn_reflns_limit_l_max       14
_diffrn_reflns_limit_l_min       -14
_diffrn_reflns_number            5099
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         1.86
_exptl_absorpt_coefficient_mu    1.997
_exptl_absorpt_correction_T_max  0.9612
_exptl_absorpt_correction_T_min  0.8566
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'sadabs(Bruker, 2001)'
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    2.146
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       plate
_exptl_crystal_F_000             646
_exptl_crystal_size_max          0.08
_exptl_crystal_size_mid          0.04
_exptl_crystal_size_min          0.02
_refine_diff_density_max         0.660
_refine_diff_density_min         -0.598
_refine_diff_density_rms         0.133
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.993
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     298
_refine_ls_number_reflns         3514
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      0.993
_refine_ls_R_factor_all          0.1505
_refine_ls_R_factor_gt           0.0744
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0680P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1473
_refine_ls_wR_factor_ref         0.1803
_reflns_number_gt                1836
_reflns_number_total             3514
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b714502k.txt
_cod_data_source_block           5
_cod_original_cell_volume        1015.6(3)
_cod_database_code               7003224
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.92934(12) 0.05060(12) 0.33803(8) 0.0584(4) Uani 1 1 d . . .
Ag2 Ag 1.08048(15) 0.32588(13) 0.84914(10) 0.0748(5) Uani 1 1 d . . .
N1 N 0.8045(11) -0.1317(10) -0.3734(7) 0.040(2) Uani 1 1 d . . .
N2 N 1.1083(11) 0.3346(10) 0.0280(8) 0.043(3) Uani 1 1 d . . .
N3 N 0.6908(11) -0.0617(10) 0.2079(8) 0.043(3) Uani 1 1 d . . .
N4 N 0.8512(15) 0.1621(11) 0.6094(10) 0.051(3) Uani 1 1 d . . .
N5 N 1.2864(16) 0.5110(13) 0.7896(10) 0.059(3) Uani 1 1 d . . .
O1 O 0.5527(9) -0.2083(8) -0.3505(6) 0.049(2) Uani 1 1 d . . .
O2 O 1.0988(9) 0.3140(8) 0.1967(6) 0.042(2) Uani 1 1 d . . .
O3 O 0.4925(9) -0.1815(8) 0.0380(6) 0.0388(19) Uani 1 1 d . . .
O4 O 0.7607(13) 0.0981(11) 0.5087(8) 0.082(3) Uani 1 1 d . . .
O5 O 0.7960(12) 0.2253(10) 0.7008(8) 0.073(3) Uani 1 1 d . . .
O6 O 1.0026(12) 0.1657(11) 0.6253(9) 0.079(3) Uani 1 1 d . . .
O7 O 1.3501(13) 0.4388(13) 0.8186(12) 0.107(4) Uani 1 1 d . . .
O8 O 1.1455(15) 0.5137(13) 0.8018(13) 0.115(5) Uani 1 1 d . . .
O9 O 1.3647(13) 0.5765(11) 0.7485(10) 0.090(4) Uani 1 1 d . . .
O10 O 0.891(2) 0.3445(14) 0.4457(14) 0.126(6) Uani 1 1 d . . .
C1 C 0.7476(13) -0.0511(11) -0.1666(9) 0.033(3) Uani 1 1 d . . .
C2 C 0.8687(13) 0.0687(11) -0.1101(9) 0.034(3) Uani 1 1 d . . .
H2B H 0.9215 0.1007 -0.1569 0.041 Uiso 1 1 calc R . .
C3 C 0.9116(13) 0.1410(11) 0.0162(9) 0.032(3) Uani 1 1 d . . .
C4 C 0.8313(13) 0.0913(11) 0.0846(9) 0.030(3) Uani 1 1 d . . .
H4A H 0.8582 0.1405 0.1695 0.036 Uiso 1 1 calc R . .
C5 C 0.7132(13) -0.0290(11) 0.0290(9) 0.034(3) Uani 1 1 d . . .
C6 C 0.6684(12) -0.0996(11) -0.0989(9) 0.030(3) Uani 1 1 d . . .
H6A H 0.5851 -0.1792 -0.1378 0.037 Uiso 1 1 calc R . .
C7 C 0.7046(14) -0.1334(12) -0.3028(9) 0.037(3) Uani 1 1 d . . .
C8 C 0.5457(16) -0.2783(15) -0.4829(10) 0.064(4) Uani 1 1 d . . .
H8A H 0.5318 -0.3751 -0.5126 0.077 Uiso 1 1 calc R . .
H8B H 0.4534 -0.2632 -0.5268 0.077 Uiso 1 1 calc R . .
C9 C 0.7040(15) -0.2203(15) -0.4997(10) 0.062(4) Uani 1 1 d . . .
H9A H 0.6876 -0.1679 -0.5423 0.075 Uiso 1 1 calc R . .
H9B H 0.7583 -0.2910 -0.5461 0.075 Uiso 1 1 calc R . .
C10 C 0.6342(13) -0.0876(11) 0.0974(9) 0.029(3) Uani 1 1 d . . .
C11 C 0.4503(14) -0.2381(11) 0.1177(9) 0.040(3) Uani 1 1 d . . .
H11A H 0.4691 -0.3288 0.0877 0.048 Uiso 1 1 calc R . .
H11B H 0.3346 -0.2417 0.1242 0.048 Uiso 1 1 calc R . .
C12 C 0.5667(13) -0.1411(12) 0.2404(10) 0.042(3) Uani 1 1 d . . .
H12A H 0.5078 -0.0833 0.2972 0.051 Uiso 1 1 calc R . .
H12B H 0.6188 -0.1900 0.2762 0.051 Uiso 1 1 calc R . .
C13 C 1.0428(15) 0.2689(13) 0.0784(11) 0.046(3) Uani 1 1 d . . .
C14 C 1.2234(16) 0.4415(13) 0.2434(11) 0.059(4) Uani 1 1 d . . .
H14A H 1.3291 0.4374 0.2822 0.070 Uiso 1 1 calc R . .
H14B H 1.1859 0.5173 0.3014 0.070 Uiso 1 1 calc R . .
C15 C 1.2371(16) 0.4526(14) 0.1256(11) 0.066(4) Uani 1 1 d . . .
H15A H 1.2147 0.5373 0.1332 0.079 Uiso 1 1 calc R . .
H15B H 1.3474 0.4475 0.1084 0.079 Uiso 1 1 calc R . .
C16 C 0.876(4) 0.460(5) 0.457(3) 0.220(17) Uani 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N1 Ag1 N3 149.7(3) 2_755 . ?
N1 Ag1 O4 123.6(3) 2_755 . ?
N3 Ag1 O4 86.5(3) . . ?
N2 Ag2 O8 128.0(4) 1_556 . ?
N2 Ag2 O6 142.9(4) 1_556 . ?
O8 Ag2 O6 89.0(4) . . ?
N2 Ag2 O7 112.4(4) 1_556 . ?
O8 Ag2 O7 48.1(4) . . ?
O6 Ag2 O7 89.6(4) . . ?
N2 Ag2 O5 120.5(3) 1_556 . ?
O8 Ag2 O5 93.0(4) . . ?
O6 Ag2 O5 49.4(3) . . ?
O7 Ag2 O5 126.9(4) . . ?
C7 N1 C9 105.1(9) . . ?
C7 N1 Ag1 132.5(7) . 2_755 ?
C9 N1 Ag1 121.9(7) . 2_755 ?
C13 N2 C15 106.7(9) . . ?
C13 N2 Ag2 138.7(8) . 1_554 ?
C15 N2 Ag2 114.5(7) . 1_554 ?
C10 N3 C12 107.4(9) . . ?
C10 N3 Ag1 134.0(8) . . ?
C12 N3 Ag1 118.1(6) . . ?
O4 N4 O5 121.2(12) . . ?
O4 N4 O6 121.6(12) . . ?
O5 N4 O6 117.2(12) . . ?
O7 N5 O8 116.9(14) . . ?
O7 N5 O9 119.7(14) . . ?
O8 N5 O9 123.4(15) . . ?
C7 O1 C8 104.5(9) . . ?
C13 O2 C14 108.1(9) . . ?
C10 O3 C11 106.5(8) . . ?
N4 O4 Ag1 111.3(8) . . ?
N4 O5 Ag2 95.0(8) . . ?
N4 O6 Ag2 98.2(8) . . ?
N5 O7 Ag2 94.4(9) . . ?
N5 O8 Ag2 99.8(10) . . ?
C6 C1 C2 120.7(10) . . ?
C6 C1 C7 118.5(10) . . ?
C2 C1 C7 120.7(10) . . ?
C1 C2 C3 120.0(10) . . ?
C1 C2 H2B 120.0 . . ?
C3 C2 H2B 120.0 . . ?
C2 C3 C4 119.1(10) . . ?
C2 C3 C13 120.7(10) . . ?
C4 C3 C13 120.2(10) . . ?
C5 C4 C3 121.1(10) . . ?
C5 C4 H4A 119.4 . . ?
C3 C4 H4A 119.4 . . ?
C4 C5 C6 119.1(10) . . ?
C4 C5 C10 122.6(10) . . ?
C6 C5 C10 118.3(10) . . ?
C1 C6 C5 119.9(10) . . ?
C1 C6 H6A 120.1 . . ?
C5 C6 H6A 120.1 . . ?
N1 C7 O1 119.5(9) . . ?
N1 C7 C1 124.4(10) . . ?
O1 C7 C1 116.0(9) . . ?
C9 C8 O1 105.8(9) . . ?
C9 C8 H8A 110.6 . . ?
O1 C8 H8A 110.6 . . ?
C9 C8 H8B 110.6 . . ?
O1 C8 H8B 110.6 . . ?
H8A C8 H8B 108.7 . . ?
C8 C9 N1 104.5(9) . . ?
C8 C9 H9A 110.8 . . ?
N1 C9 H9A 110.8 . . ?
C8 C9 H9B 110.8 . . ?
N1 C9 H9B 110.8 . . ?
H9A C9 H9B 108.9 . . ?
N3 C10 O3 117.0(9) . . ?
N3 C10 C5 126.5(10) . . ?
O3 C10 C5 116.5(9) . . ?
O3 C11 C12 104.1(8) . . ?
O3 C11 H11A 110.9 . . ?
C12 C11 H11A 110.9 . . ?
O3 C11 H11B 110.9 . . ?
C12 C11 H11B 110.9 . . ?
H11A C11 H11B 109.0 . . ?
N3 C12 C11 102.8(8) . . ?
N3 C12 H12A 111.2 . . ?
C11 C12 H12A 111.2 . . ?
N3 C12 H12B 111.2 . . ?
C11 C12 H12B 111.2 . . ?
H12A C12 H12B 109.1 . . ?
N2 C13 O2 118.3(11) . . ?
N2 C13 C3 126.2(11) . . ?
O2 C13 C3 115.4(11) . . ?
O2 C14 C15 102.2(9) . . ?
O2 C14 H14A 111.3 . . ?
C15 C14 H14A 111.3 . . ?
O2 C14 H14B 111.3 . . ?
C15 C14 H14B 111.3 . . ?
H14A C14 H14B 109.2 . . ?
N2 C15 C14 104.4(9) . . ?
N2 C15 H15A 110.9 . . ?
C14 C15 H15A 110.9 . . ?
N2 C15 H15B 110.9 . . ?
C14 C15 H15B 110.9 . . ?
H15A C15 H15B 108.9 . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 N1 2.169(9) 2_755 ?
Ag1 N3 2.191(9) . ?
Ag1 O4 2.592(10) . ?
Ag2 N2 2.174(9) 1_556 ?
Ag2 O8 2.449(12) . ?
Ag2 O6 2.494(10) . ?
Ag2 O7 2.558(12) . ?
Ag2 O5 2.562(9) . ?
N1 C7 1.285(13) . ?
N1 C9 1.488(12) . ?
N1 Ag1 2.169(9) 2_755 ?
N2 C13 1.272(14) . ?
N2 C15 1.489(14) . ?
N2 Ag2 2.174(9) 1_554 ?
N3 C10 1.286(12) . ?
N3 C12 1.473(13) . ?
N4 O4 1.212(12) . ?
N4 O5 1.235(12) . ?
N4 O6 1.241(12) . ?
N5 O7 1.196(14) . ?
N5 O8 1.201(14) . ?
N5 O9 1.227(14) . ?
O1 C7 1.306(12) . ?
O1 C8 1.472(12) . ?
O2 C13 1.324(13) . ?
O2 C14 1.462(13) . ?
O3 C10 1.330(12) . ?
O3 C11 1.451(12) . ?
O10 C16 1.27(4) . ?
C1 C6 1.372(13) . ?
C1 C2 1.381(14) . ?
C1 C7 1.494(14) . ?
C2 C3 1.383(14) . ?
C2 H2B 0.9300 . ?
C3 C4 1.392(14) . ?
C3 C13 1.482(16) . ?
C4 C5 1.372(14) . ?
C4 H4A 0.9300 . ?
C5 C6 1.399(13) . ?
C5 C10 1.450(14) . ?
C6 H6A 0.9300 . ?
C8 C9 1.457(16) . ?
C8 H8A 0.9700 . ?
C8 H8B 0.9700 . ?
C9 H9A 0.9700 . ?
C9 H9B 0.9700 . ?
C11 C12 1.520(14) . ?
C11 H11A 0.9700 . ?
C11 H11B 0.9700 . ?
C12 H12A 0.9700 . ?
C12 H12B 0.9700 . ?
C14 C15 1.547(16) . ?
C14 H14A 0.9700 . ?
C14 H14B 0.9700 . ?
C15 H15A 0.9700 . ?
C15 H15B 0.9700 . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
N1 Ag1 N3 C10 -23.1(15) 2_755 . . . ?
O4 Ag1 N3 C10 151.6(11) . . . . ?
N1 Ag1 N3 C12 148.4(8) 2_755 . . . ?
O4 Ag1 N3 C12 -36.9(8) . . . . ?
O5 N4 O4 Ag1 160.6(9) . . . . ?
O6 N4 O4 Ag1 -20.2(15) . . . . ?
N1 Ag1 O4 N4 -5.2(10) 2_755 . . . ?
N3 Ag1 O4 N4 178.0(9) . . . . ?
O4 N4 O5 Ag2 -177.0(10) . . . . ?
O6 N4 O5 Ag2 3.8(12) . . . . ?
N2 Ag2 O5 N4 -137.8(7) 1_556 . . . ?
O8 Ag2 O5 N4 83.9(8) . . . . ?
O6 Ag2 O5 N4 -2.2(7) . . . . ?
O7 Ag2 O5 N4 46.8(9) . . . . ?
O4 N4 O6 Ag2 176.9(10) . . . . ?
O5 N4 O6 Ag2 -3.9(12) . . . . ?
N2 Ag2 O6 N4 90.8(9) 1_556 . . . ?
O8 Ag2 O6 N4 -92.6(8) . . . . ?
O7 Ag2 O6 N4 -140.7(8) . . . . ?
O5 Ag2 O6 N4 2.2(7) . . . . ?
O8 N5 O7 Ag2 9.0(15) . . . . ?
O9 N5 O7 Ag2 -170.3(11) . . . . ?
N2 Ag2 O7 N5 -127.0(9) 1_556 . . . ?
O8 Ag2 O7 N5 -5.3(9) . . . . ?
O6 Ag2 O7 N5 83.7(9) . . . . ?
O5 Ag2 O7 N5 48.8(11) . . . . ?
O7 N5 O8 Ag2 -9.5(15) . . . . ?
O9 N5 O8 Ag2 169.8(11) . . . . ?
N2 Ag2 O8 N5 92.4(10) 1_556 . . . ?
O6 Ag2 O8 N5 -85.0(10) . . . . ?
O7 Ag2 O8 N5 5.3(9) . . . . ?
O5 Ag2 O8 N5 -134.3(10) . . . . ?
C6 C1 C2 C3 0.1(16) . . . . ?
C7 C1 C2 C3 -177.5(10) . . . . ?
C1 C2 C3 C4 0.1(16) . . . . ?
C1 C2 C3 C13 179.3(10) . . . . ?
C2 C3 C4 C5 1.2(16) . . . . ?
C13 C3 C4 C5 -178.0(10) . . . . ?
C3 C4 C5 C6 -2.7(16) . . . . ?
C3 C4 C5 C10 176.3(10) . . . . ?
C2 C1 C6 C5 -1.6(16) . . . . ?
C7 C1 C6 C5 176.1(10) . . . . ?
C4 C5 C6 C1 2.8(16) . . . . ?
C10 C5 C6 C1 -176.2(10) . . . . ?
C9 N1 C7 O1 2.3(15) . . . . ?
Ag1 N1 C7 O1 -169.3(8) 2_755 . . . ?
C9 N1 C7 C1 -175.8(11) . . . . ?
Ag1 N1 C7 C1 12.7(19) 2_755 . . . ?
C8 O1 C7 N1 2.4(15) . . . . ?
C8 O1 C7 C1 -179.3(10) . . . . ?
C6 C1 C7 N1 -152.0(12) . . . . ?
C2 C1 C7 N1 25.6(17) . . . . ?
C6 C1 C7 O1 29.8(15) . . . . ?
C2 C1 C7 O1 -152.5(11) . . . . ?
C7 O1 C8 C9 -6.1(14) . . . . ?
O1 C8 C9 N1 7.2(15) . . . . ?
C7 N1 C9 C8 -5.9(15) . . . . ?
Ag1 N1 C9 C8 166.7(9) 2_755 . . . ?
C12 N3 C10 O3 -4.7(13) . . . . ?
Ag1 N3 C10 O3 167.5(7) . . . . ?
C12 N3 C10 C5 178.3(11) . . . . ?
Ag1 N3 C10 C5 -9.6(18) . . . . ?
C11 O3 C10 N3 -5.3(13) . . . . ?
C11 O3 C10 C5 172.1(9) . . . . ?
C4 C5 C10 N3 -21.0(18) . . . . ?
C6 C5 C10 N3 158.0(11) . . . . ?
C4 C5 C10 O3 161.9(10) . . . . ?
C6 C5 C10 O3 -19.1(15) . . . . ?
C10 O3 C11 C12 12.4(11) . . . . ?
C10 N3 C12 C11 11.9(12) . . . . ?
Ag1 N3 C12 C11 -161.7(7) . . . . ?
O3 C11 C12 N3 -14.4(11) . . . . ?
C15 N2 C13 O2 -0.6(15) . . . . ?
Ag2 N2 C13 O2 -178.5(8) 1_554 . . . ?
C15 N2 C13 C3 -178.1(11) . . . . ?
Ag2 N2 C13 C3 4(2) 1_554 . . . ?
C14 O2 C13 N2 3.7(15) . . . . ?
C14 O2 C13 C3 -178.6(10) . . . . ?
C2 C3 C13 N2 11.4(18) . . . . ?
C4 C3 C13 N2 -169.4(12) . . . . ?
C2 C3 C13 O2 -166.1(10) . . . . ?
C4 C3 C13 O2 13.1(16) . . . . ?
C13 O2 C14 C15 -4.7(13) . . . . ?
C13 N2 C15 C14 -2.5(14) . . . . ?
Ag2 N2 C15 C14 176.0(8) 1_554 . . . ?
O2 C14 C15 N2 4.2(13) . . . . ?
