#------------------------------------------------------------------------------
#$Date: 2016-03-25 10:09:59 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179742 $
#$URL: svn://www.crystallography.net/cod/cif/7/00/38/7003807.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7003807
loop_
_publ_author_name
'Ge, Qingchun'
'Hor, T. S. Andy'
_publ_section_title
;
 Stepwise assembly of linearly-aligned Ru--M--Ru (M = Pd, Pt)
 heterotrimetallic complexes with σ-4-ethynylpyridine spacer
;
_journal_issue                   22
_journal_name_full               'Dalton Transactions'
_journal_page_first              2929
_journal_page_last               2936
_journal_paper_doi               10.1039/b719820e
_journal_year                    2008
_chemical_formula_sum            'C57 H48 Cl N P4 Ru'
_chemical_formula_weight         1007.36
_chemical_name_systematic
;
?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                108.1380(10)
_cell_angle_beta                 94.0600(10)
_cell_angle_gamma                94.7290(10)
_cell_formula_units_Z            2
_cell_length_a                   13.5514(6)
_cell_length_b                   13.5933(6)
_cell_length_c                   13.8171(7)
_cell_measurement_reflns_used    5836
_cell_measurement_temperature    223(2)
_cell_measurement_theta_max      27.50
_cell_measurement_theta_min      2.39
_cell_volume                     2397.98(19)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      223(2)
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0248
_diffrn_reflns_av_sigmaI/netI    0.0291
_diffrn_reflns_limit_h_max       17
_diffrn_reflns_limit_h_min       -17
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_k_min       -17
_diffrn_reflns_limit_l_max       17
_diffrn_reflns_limit_l_min       -17
_diffrn_reflns_number            31494
_diffrn_reflns_theta_full        27.50
_diffrn_reflns_theta_max         27.50
_diffrn_reflns_theta_min         1.52
_exptl_absorpt_coefficient_mu    0.556
_exptl_absorpt_correction_T_max  0.8970
_exptl_absorpt_correction_T_min  0.7841
_exptl_absorpt_correction_type   'Sadabs, (Sheldrick 2001)'
_exptl_crystal_colour            YELLOW
_exptl_crystal_density_diffrn    1.395
_exptl_crystal_density_meas      0
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       BLOCK
_exptl_crystal_F_000             1036
_exptl_crystal_size_max          0.46
_exptl_crystal_size_mid          0.24
_exptl_crystal_size_min          0.20
_refine_diff_density_max         0.496
_refine_diff_density_min         -0.262
_refine_diff_density_rms         0.066
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.035
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     577
_refine_ls_number_reflns         10991
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.035
_refine_ls_R_factor_all          0.0372
_refine_ls_R_factor_gt           0.0323
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0404P)²+0.9274P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0781
_refine_ls_wR_factor_ref         0.0806
_reflns_number_gt                9765
_reflns_number_total             10991
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b719820e.txt
_cod_data_source_block           6088
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7003807
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ru1 Ru 0.744318(10) 0.802584(10) 0.688230(10) 0.01898(5) Uani 1 1 d . . .
P1 P 0.91811(3) 0.80775(3) 0.68924(4) 0.02307(10) Uani 1 1 d . . .
P2 P 0.81598(3) 0.94833(4) 0.82517(4) 0.02442(10) Uani 1 1 d . . .
P3 P 0.57355(3) 0.78803(4) 0.69885(3) 0.02202(10) Uani 1 1 d . . .
P4 P 0.67003(3) 0.65899(3) 0.54981(3) 0.02343(10) Uani 1 1 d . . .
Cl1 Cl 0.74825(4) 0.91890(4) 0.58411(3) 0.03049(10) Uani 1 1 d . . .
N1 N 0.76785(17) 0.49547(15) 1.04859(15) 0.0478(5) Uani 1 1 d . . .
C1 C 0.74703(13) 0.71183(13) 0.77583(13) 0.0232(3) Uani 1 1 d . . .
C2 C 0.74831(15) 0.65901(15) 0.83212(15) 0.0307(4) Uani 1 1 d . . .
C3 C 0.84775(19) 0.53244(18) 1.01523(18) 0.0455(5) Uani 1 1 d . . .
H3 H 0.9103 0.5220 1.0420 0.055 Uiso 1 1 calc R . .
C4 C 0.84602(17) 0.58491(17) 0.94441(17) 0.0393(5) Uani 1 1 d . . .
H4 H 0.9057 0.6080 0.9236 0.047 Uiso 1 1 calc R . .
C5 C 0.75449(15) 0.60335(14) 0.90397(14) 0.0289(4) Uani 1 1 d . . .
C6 C 0.67029(17) 0.56472(16) 0.93862(17) 0.0389(5) Uani 1 1 d . . .
H6 H 0.6064 0.5743 0.9142 0.047 Uiso 1 1 calc R . .
C7 C 0.6814(2) 0.51234(18) 1.00894(19) 0.0476(6) Uani 1 1 d . . .
H7 H 0.6232 0.4866 1.0304 0.057 Uiso 1 1 calc R . .
C10 C 0.54883(14) 0.65703(14) 0.60289(15) 0.0291(4) Uani 1 1 d . . .
H10A H 0.4927 0.6517 0.5521 0.035 Uiso 1 1 calc R . .
H10B H 0.5387 0.6019 0.6342 0.035 Uiso 1 1 calc R . .
C16 C 0.94600(15) 0.93019(16) 0.79770(17) 0.0366(5) Uani 1 1 d . . .
H16A H 0.9866 0.9212 0.8553 0.044 Uiso 1 1 calc R . .
H16B H 0.9778 0.9870 0.7773 0.044 Uiso 1 1 calc R . .
C1A C 0.98632(14) 0.82661(15) 0.58579(15) 0.0298(4) Uani 1 1 d . . .
C2A C 1.0543(2) 0.9113(2) 0.5978(2) 0.0586(7) Uani 1 1 d . . .
H2A H 1.0701 0.9614 0.6628 0.070 Uiso 1 1 calc R . .
C3A C 1.0999(2) 0.9238(3) 0.5151(2) 0.0705(9) Uani 1 1 d . . .
H3A H 1.1458 0.9827 0.5250 0.085 Uiso 1 1 calc R . .
C4A C 1.0802(2) 0.8537(2) 0.4212(2) 0.0550(7) Uani 1 1 d . . .
H4A H 1.1115 0.8637 0.3659 0.066 Uiso 1 1 calc R . .
C5A C 1.0137(2) 0.7673(2) 0.4070(2) 0.0600(7) Uani 1 1 d . . .
H5A H 0.9995 0.7174 0.3417 0.072 Uiso 1 1 calc R . .
C6A C 0.9673(2) 0.75384(18) 0.48952(19) 0.0507(6) Uani 1 1 d . . .
H6A H 0.9223 0.6942 0.4794 0.061 Uiso 1 1 calc R . .
C1B C 0.98104(13) 0.70870(15) 0.72463(14) 0.0268(4) Uani 1 1 d . . .
C2B C 1.05531(15) 0.72944(19) 0.80534(16) 0.0381(5) Uani 1 1 d . . .
H2B H 1.0763 0.7985 0.8461 0.046 Uiso 1 1 calc R . .
C3B C 1.09856(17) 0.6475(2) 0.82568(18) 0.0487(6) Uani 1 1 d . . .
H3B H 1.1477 0.6617 0.8813 0.058 Uiso 1 1 calc R . .
C4B C 1.07062(19) 0.5470(2) 0.7660(2) 0.0502(6) Uani 1 1 d . . .
H4B H 1.1016 0.4925 0.7795 0.060 Uiso 1 1 calc R . .
C5B C 0.99698(19) 0.52532(19) 0.6861(2) 0.0496(6) Uani 1 1 d . . .
H5B H 0.9774 0.4561 0.6451 0.060 Uiso 1 1 calc R . .
C6B C 0.95180(16) 0.60562(16) 0.66632(18) 0.0376(5) Uani 1 1 d . . .
H6B H 0.9005 0.5902 0.6126 0.045 Uiso 1 1 calc R . .
C1C C 0.80290(16) 1.08169(15) 0.82823(15) 0.0315(4) Uani 1 1 d . . .
C2C C 0.87879(19) 1.16124(16) 0.87508(18) 0.0445(5) Uani 1 1 d . . .
H2C H 0.9370 1.1468 0.9070 0.053 Uiso 1 1 calc R . .
C3C C 0.8687(2) 1.26204(18) 0.8748(2) 0.0569(7) Uani 1 1 d . . .
H3C H 0.9203 1.3156 0.9062 0.068 Uiso 1 1 calc R . .
C4C C 0.7837(2) 1.28397(18) 0.8289(2) 0.0561(7) Uani 1 1 d . . .
H4C H 0.7774 1.3522 0.8286 0.067 Uiso 1 1 calc R . .
C5C C 0.7082(2) 1.20617(18) 0.78356(18) 0.0477(6) Uani 1 1 d . . .
H5C H 0.6498 1.2214 0.7528 0.057 Uiso 1 1 calc R . .
C6C C 0.71728(17) 1.10472(16) 0.78269(16) 0.0373(5) Uani 1 1 d . . .
H6C H 0.6652 1.0517 0.7512 0.045 Uiso 1 1 calc R . .
C1D C 0.81259(15) 0.95654(15) 0.95901(14) 0.0319(4) Uani 1 1 d . . .
C2D C 0.76307(17) 1.03154(18) 1.02527(16) 0.0423(5) Uani 1 1 d . . .
H2D H 0.7378 1.0844 1.0036 0.051 Uiso 1 1 calc R . .
C3D C 0.7511(2) 1.0282(2) 1.12325(19) 0.0584(7) Uani 1 1 d . . .
H3D H 0.7181 1.0792 1.1678 0.070 Uiso 1 1 calc R . .
C4D C 0.7872(2) 0.9510(3) 1.15542(19) 0.0624(8) Uani 1 1 d . . .
H4D H 0.7779 0.9486 1.2215 0.075 Uiso 1 1 calc R . .
C5D C 0.8368(2) 0.8772(2) 1.0914(2) 0.0564(7) Uani 1 1 d . . .
H5D H 0.8622 0.8250 1.1140 0.068 Uiso 1 1 calc R . .
C6D C 0.84960(17) 0.87940(18) 0.99373(17) 0.0420(5) Uani 1 1 d . . .
H6D H 0.8835 0.8285 0.9503 0.050 Uiso 1 1 calc R . .
C1E C 0.49419(13) 0.87287(14) 0.65891(14) 0.0258(4) Uani 1 1 d . . .
C2E C 0.47577(16) 0.96358(16) 0.73233(16) 0.0365(5) Uani 1 1 d . . .
H2E H 0.4984 0.9758 0.8014 0.044 Uiso 1 1 calc R . .
C3E C 0.42434(18) 1.03627(18) 0.70498(17) 0.0430(5) Uani 1 1 d . . .
H3E H 0.4135 1.0982 0.7552 0.052 Uiso 1 1 calc R . .
C4E C 0.38903(18) 1.01828(19) 0.60476(18) 0.0454(6) Uani 1 1 d . . .
H4E H 0.3535 1.0673 0.5862 0.054 Uiso 1 1 calc R . .
C5E C 0.4061(2) 0.9281(2) 0.53181(18) 0.0515(6) Uani 1 1 d . . .
H5E H 0.3811 0.9150 0.4632 0.062 Uiso 1 1 calc R . .
C6E C 0.45983(18) 0.85619(18) 0.55809(16) 0.0411(5) Uani 1 1 d . . .
H6E H 0.4729 0.7958 0.5071 0.049 Uiso 1 1 calc R . .
C1F C 0.51758(13) 0.77369(14) 0.81057(14) 0.0268(4) Uani 1 1 d . . .
C2F C 0.56125(18) 0.82661(19) 0.90772(17) 0.0435(5) Uani 1 1 d . . .
H2F H 0.6212 0.8699 0.9169 0.052 Uiso 1 1 calc R . .
C3F C 0.5175(2) 0.8167(2) 0.99235(19) 0.0592(7) Uani 1 1 d . . .
H3F H 0.5471 0.8545 1.0586 0.071 Uiso 1 1 calc R . .
C4F C 0.4311(2) 0.7515(2) 0.9797(2) 0.0569(7) Uani 1 1 d . . .
H4F H 0.4016 0.7446 1.0372 0.068 Uiso 1 1 calc R . .
C5F C 0.38857(19) 0.6974(2) 0.8840(2) 0.0575(7) Uani 1 1 d . . .
H5F H 0.3301 0.6519 0.8755 0.069 Uiso 1 1 calc R . .
C6F C 0.43013(16) 0.7083(2) 0.79882(19) 0.0452(6) Uani 1 1 d . . .
H6F H 0.3992 0.6714 0.7329 0.054 Uiso 1 1 calc R . .
C1G C 0.64164(17) 0.66753(15) 0.42163(14) 0.0343(4) Uani 1 1 d . . .
C2G C 0.5517(2) 0.6216(2) 0.36398(18) 0.0537(6) Uani 1 1 d . . .
H2G H 0.5042 0.5870 0.3919 0.064 Uiso 1 1 calc R . .
C3G C 0.5313(3) 0.6263(3) 0.2663(2) 0.0807(11) Uani 1 1 d . . .
H3G H 0.4696 0.5966 0.2289 0.097 Uiso 1 1 calc R . .
C4G C 0.6000(4) 0.6737(3) 0.2242(2) 0.0906(14) Uani 1 1 d . . .
H4G H 0.5859 0.6762 0.1575 0.109 Uiso 1 1 calc R . .
C5G C 0.6894(3) 0.7178(2) 0.2779(2) 0.0766(11) Uani 1 1 d . . .
H5G H 0.7369 0.7493 0.2473 0.092 Uiso 1 1 calc R . .
C6G C 0.7116(2) 0.71674(17) 0.37888(18) 0.0512(6) Uani 1 1 d . . .
H6G H 0.7727 0.7489 0.4164 0.061 Uiso 1 1 calc R . .
C1H C 0.70521(13) 0.52653(14) 0.52109(14) 0.0264(4) Uani 1 1 d . . .
C2H C 0.74493(15) 0.47765(16) 0.43104(16) 0.0349(4) Uani 1 1 d . . .
H2H H 0.7503 0.5113 0.3813 0.042 Uiso 1 1 calc R . .
C3H C 0.77688(17) 0.37971(17) 0.41310(18) 0.0441(5) Uani 1 1 d . . .
H3H H 0.8043 0.3479 0.3519 0.053 Uiso 1 1 calc R . .
C4H C 0.76848(19) 0.32920(17) 0.48458(19) 0.0470(6) Uani 1 1 d . . .
H4H H 0.7890 0.2623 0.4719 0.056 Uiso 1 1 calc R . .
C5H C 0.73003(19) 0.37663(17) 0.57472(19) 0.0449(5) Uani 1 1 d . . .
H5H H 0.7247 0.3421 0.6238 0.054 Uiso 1 1 calc R . .
C6H C 0.69907(16) 0.47473(15) 0.59394(16) 0.0346(4) Uani 1 1 d . . .
H6H H 0.6737 0.5068 0.6563 0.042 Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ru Ru -1.2594 0.8363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C1 Ru1 P3 84.63(5) . . ?
C1 Ru1 P1 89.59(5) . . ?
P3 Ru1 P1 174.200(16) . . ?
C1 Ru1 P2 91.64(5) . . ?
P3 Ru1 P2 107.461(17) . . ?
P1 Ru1 P2 72.134(17) . . ?
C1 Ru1 P4 89.37(5) . . ?
P3 Ru1 P4 71.774(17) . . ?
P1 Ru1 P4 108.741(17) . . ?
P2 Ru1 P4 178.676(17) . . ?
C1 Ru1 Cl1 177.38(5) . . ?
P3 Ru1 Cl1 97.495(16) . . ?
P1 Ru1 Cl1 88.268(16) . . ?
P2 Ru1 Cl1 86.268(17) . . ?
P4 Ru1 Cl1 92.750(17) . . ?
C1B P1 C1A 103.11(8) . . ?
C1B P1 C16 107.08(10) . . ?
C1A P1 C16 106.14(10) . . ?
C1B P1 Ru1 119.23(6) . . ?
C1A P1 Ru1 123.79(6) . . ?
C16 P1 Ru1 95.45(6) . . ?
C1D P2 C1C 102.60(9) . . ?
C1D P2 C16 105.58(10) . . ?
C1C P2 C16 104.33(10) . . ?
C1D P2 Ru1 123.19(6) . . ?
C1C P2 Ru1 122.57(7) . . ?
C16 P2 Ru1 95.35(6) . . ?
C1E P3 C1F 102.29(8) . . ?
C1E P3 C10 107.89(9) . . ?
C1F P3 C10 104.13(9) . . ?
C1E P3 Ru1 121.60(6) . . ?
C1F P3 Ru1 123.43(6) . . ?
C10 P3 Ru1 94.99(6) . . ?
C1G P4 C1H 101.75(9) . . ?
C1G P4 C10 105.16(10) . . ?
C1H P4 C10 106.00(9) . . ?
C1G P4 Ru1 122.43(7) . . ?
C1H P4 Ru1 124.48(6) . . ?
C10 P4 Ru1 93.89(6) . . ?
C7 N1 C3 115.25(18) . . ?
C2 C1 Ru1 177.90(17) . . ?
C1 C2 C5 175.6(2) . . ?
N1 C3 C4 125.0(2) . . ?
C3 C4 C5 119.2(2) . . ?
C6 C5 C4 116.01(18) . . ?
C6 C5 C2 122.33(19) . . ?
C4 C5 C2 121.66(19) . . ?
C7 C6 C5 119.5(2) . . ?
N1 C7 C6 125.0(2) . . ?
P3 C10 P4 96.03(9) . . ?
P2 C16 P1 96.93(9) . . ?
C2A C1A C6A 117.7(2) . . ?
C2A C1A P1 123.47(18) . . ?
C6A C1A P1 118.85(16) . . ?
C1A C2A C3A 120.7(3) . . ?
C4A C3A C2A 121.5(3) . . ?
C3A C4A C5A 119.2(2) . . ?
C4A C5A C6A 119.9(3) . . ?
C1A C6A C5A 121.0(2) . . ?
C6B C1B C2B 118.47(18) . . ?
C6B C1B P1 116.95(14) . . ?
C2B C1B P1 124.58(16) . . ?
C1B C2B C3B 119.8(2) . . ?
C4B C3B C2B 120.9(2) . . ?
C3B C4B C5B 119.9(2) . . ?
C4B C5B C6B 119.9(2) . . ?
C5B C6B C1B 121.0(2) . . ?
C6C C1C C2C 119.13(19) . . ?
C6C C1C P2 120.20(16) . . ?
C2C C1C P2 120.66(17) . . ?
C3C C2C C1C 120.0(2) . . ?
C4C C3C C2C 120.4(2) . . ?
C5C C4C C3C 119.9(2) . . ?
C4C C5C C6C 120.5(2) . . ?
C1C C6C C5C 120.1(2) . . ?
C2D C1D C6D 118.5(2) . . ?
C2D C1D P2 121.28(17) . . ?
C6D C1D P2 119.75(17) . . ?
C3D C2D C1D 120.1(2) . . ?
C4D C3D C2D 120.4(3) . . ?
C3D C4D C5D 120.1(2) . . ?
C4D C5D C6D 120.3(3) . . ?
C5D C6D C1D 120.6(2) . . ?
C6E C1E C2E 118.73(17) . . ?
C6E C1E P3 123.07(15) . . ?
C2E C1E P3 117.89(14) . . ?
C3E C2E C1E 120.63(19) . . ?
C4E C3E C2E 120.3(2) . . ?
C3E C4E C5E 119.4(2) . . ?
C4E C5E C6E 120.7(2) . . ?
C1E C6E C5E 120.2(2) . . ?
C2F C1F C6F 118.75(19) . . ?
C2F C1F P3 120.76(15) . . ?
C6F C1F P3 120.48(16) . . ?
C1F C2F C3F 120.5(2) . . ?
C4F C3F C2F 120.2(2) . . ?
C5F C4F C3F 119.7(2) . . ?
C4F C5F C6F 120.8(2) . . ?
C5F C6F C1F 120.1(2) . . ?
C6G C1G C2G 119.0(2) . . ?
C6G C1G P4 119.99(18) . . ?
C2G C1G P4 121.00(18) . . ?
C3G C2G C1G 120.9(3) . . ?
C4G C3G C2G 120.1(3) . . ?
C3G C4G C5G 120.5(3) . . ?
C4G C5G C6G 120.8(3) . . ?
C1G C6G C5G 118.7(3) . . ?
C2H C1H C6H 118.09(18) . . ?
C2H C1H P4 121.65(14) . . ?
C6H C1H P4 120.10(15) . . ?
C1H C2H C3H 121.0(2) . . ?
C4H C3H C2H 120.1(2) . . ?
C3H C4H C5H 119.8(2) . . ?
C4H C5H C6H 120.6(2) . . ?
C5H C6H C1H 120.4(2) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ru1 C1 1.9797(17) . ?
Ru1 P3 2.3252(5) . ?
Ru1 P1 2.3493(5) . ?
Ru1 P2 2.3530(5) . ?
Ru1 P4 2.3581(5) . ?
Ru1 Cl1 2.4466(4) . ?
P1 C1B 1.8219(18) . ?
P1 C1A 1.8274(19) . ?
P1 C16 1.850(2) . ?
P2 C1D 1.822(2) . ?
P2 C1C 1.8238(19) . ?
P2 C16 1.849(2) . ?
P3 C1E 1.8187(18) . ?
P3 C1F 1.8233(18) . ?
P3 C10 1.8466(19) . ?
P4 C1G 1.8267(19) . ?
P4 C1H 1.8304(19) . ?
P4 C10 1.8470(19) . ?
N1 C7 1.326(3) . ?
N1 C3 1.327(3) . ?
C1 C2 1.212(3) . ?
C2 C5 1.425(3) . ?
C3 C4 1.379(3) . ?
C4 C5 1.398(3) . ?
C5 C6 1.393(3) . ?
C6 C7 1.379(3) . ?
C1A C2A 1.374(3) . ?
C1A C6A 1.380(3) . ?
C2A C3A 1.385(3) . ?
C3A C4A 1.342(4) . ?
C4A C5A 1.374(4) . ?
C5A C6A 1.393(3) . ?
C1B C6B 1.389(3) . ?
C1B C2B 1.391(3) . ?
C2B C3B 1.394(3) . ?
C3B C4B 1.363(4) . ?
C4B C5B 1.377(4) . ?
C5B C6B 1.383(3) . ?
C1C C6C 1.385(3) . ?
C1C C2C 1.390(3) . ?
C2C C3C 1.389(3) . ?
C3C C4C 1.374(4) . ?
C4C C5C 1.370(4) . ?
C5C C6C 1.391(3) . ?
C1D C2D 1.395(3) . ?
C1D C6D 1.395(3) . ?
C2D C3D 1.389(3) . ?
C3D C4D 1.372(4) . ?
C4D C5D 1.373(4) . ?
C5D C6D 1.381(3) . ?
C1E C6E 1.379(3) . ?
C1E C2E 1.385(3) . ?
C2E C3E 1.383(3) . ?
C3E C4E 1.372(3) . ?
C4E C5E 1.372(3) . ?
C5E C6E 1.385(3) . ?
C1F C2F 1.373(3) . ?
C1F C6F 1.389(3) . ?
C2F C3F 1.386(3) . ?
C3F C4F 1.375(4) . ?
C4F C5F 1.356(4) . ?
C5F C6F 1.383(3) . ?
C1G C6G 1.384(3) . ?
C1G C2G 1.391(3) . ?
C2G C3G 1.381(4) . ?
C3G C4G 1.352(5) . ?
C4G C5G 1.361(5) . ?
C5G C6G 1.411(4) . ?
C1H C2H 1.385(3) . ?
C1H C6H 1.400(3) . ?
C2H C3H 1.388(3) . ?
C3H C4H 1.373(3) . ?
C4H C5H 1.373(3) . ?
C5H C6H 1.383(3) . ?
