#------------------------------------------------------------------------------
#$Date: 2016-02-16 03:10:39 +0200 (Tue, 16 Feb 2016) $
#$Revision: 176453 $
#$URL: svn://www.crystallography.net/cod/cif/7/00/38/7003846.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7003846
loop_
_publ_author_name
'Dawe, Louise N.'
'Thompson, Laurence K.'
_publ_section_title
;
 Complete and ‘incomplete’ [2 × 2] grids by
 self-assembly with a sterically hindered ditopic imidazole hydrazone
 ligand---structural and magnetic studies
;
_journal_issue                   27
_journal_name_full               'Dalton Transactions'
_journal_page_first              3610
_journal_page_last               3618
_journal_paper_doi               10.1039/b800529j
_journal_year                    2008
_chemical_formula_sum            'C22 H34.5 B2 Co2 F8 N12 O8.75'
_chemical_formula_weight         898.56
_chemical_name_systematic
;
?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_Int_Tables_number      2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                107.465(3)
_cell_angle_beta                 107.784(3)
_cell_angle_gamma                95.447(4)
_cell_formula_units_Z            2
_cell_length_a                   9.882(2)
_cell_length_b                   14.623(3)
_cell_length_c                   14.928(4)
_cell_measurement_reflns_used    6994
_cell_measurement_temperature    153(2)
_cell_measurement_theta_max      30.6329
_cell_measurement_theta_min      2.4002
_cell_volume                     1917.6(8)
_computing_cell_refinement       'CrystalClear (Rigaku/MSC Inc., 2005)'
_computing_data_collection       'CrystalClear (Rigaku/MSC Inc., 2005)'
_computing_data_reduction        'CrystalClear (Rigaku/MSC Inc., 2005)'
_computing_molecular_graphics    'CrystalStructure3.7.0(Rigaku/MSC Inc.,2005)'
_computing_publication_material  'CrystalStructure3.7.0(Rigaku/MSC Inc.,2005)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SIR92 (Altomare et al., 1994)'
_diffrn_ambient_temperature      153(2)
_diffrn_detector_area_resol_mean 14.63
_diffrn_measured_fraction_theta_full 0.989
_diffrn_measured_fraction_theta_max 0.989
_diffrn_measurement_device_type  'Rigaku Saturn'
_diffrn_measurement_method       ω
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71070
_diffrn_reflns_av_R_equivalents  0.0453
_diffrn_reflns_av_sigmaI/netI    0.0553
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_k_min       -17
_diffrn_reflns_limit_l_max       18
_diffrn_reflns_limit_l_min       -17
_diffrn_reflns_number            18471
_diffrn_reflns_theta_full        26.50
_diffrn_reflns_theta_max         26.50
_diffrn_reflns_theta_min         2.62
_exptl_absorpt_coefficient_mu    0.964
_exptl_absorpt_correction_T_max  0.9356
_exptl_absorpt_correction_T_min  0.8491
_exptl_absorpt_correction_type   numerical
_exptl_crystal_colour            Brown
_exptl_crystal_density_diffrn    1.556
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Prism
_exptl_crystal_F_000             913
_exptl_crystal_size_max          0.28
_exptl_crystal_size_mid          0.12
_exptl_crystal_size_min          0.10
_refine_diff_density_max         1.330
_refine_diff_density_min         -1.127
_refine_diff_density_rms         0.134
_refine_ls_extinction_coef       0.0021(15)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.077
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     552
_refine_ls_number_reflns         7865
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.077
_refine_ls_R_factor_all          0.1092
_refine_ls_R_factor_gt           0.0988
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1591P)²+4.5988P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2752
_refine_ls_wR_factor_ref         0.2902
_reflns_number_gt                6636
_reflns_number_total             7865
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b800529j.txt
_cod_data_source_block           shelxl_1
_cod_depositor_comments
;
The following automatic conversions were performed:
'_exptl_absorpt_correction_type' value 'Numerical' changed to 'numerical'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_formula_sum        'C22 H34.50 B2 Co2 F8 N12 O8.75 '
_cod_database_code               7003846
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Co1 Co 0.70618(7) 0.21433(5) 0.87768(5) 0.0353(2) Uani 1 1 d . . .
Co2 Co 0.32833(9) 0.27361(7) 0.61266(7) 0.0526(3) Uani 1 1 d . . .
F1 F 0.9323(12) 0.0114(6) 0.7506(8) 0.145(4) Uani 0.75 1 d P . .
F2 F 1.1354(7) 0.0445(6) 0.7285(9) 0.149(4) Uani 0.75 1 d P . .
F3 F 0.9797(10) 0.1316(6) 0.7019(6) 0.102(2) Uani 0.75 1 d P . .
F4 F 0.9426(14) -0.0181(8) 0.6000(7) 0.157(4) Uani 0.75 1 d P . .
F5 F 0.6662(6) 0.7039(6) 0.7644(6) 0.093(2) Uani 0.75 1 d P . .
F6 F 0.8954(7) 0.6889(5) 0.8326(5) 0.0839(19) Uani 0.75 1 d P . .
F7 F 0.8456(9) 0.8102(6) 0.7783(8) 0.126(4) Uani 0.75 1 d P . .
F8 F 0.7935(13) 0.6651(9) 0.6682(7) 0.149(4) Uani 0.75 1 d P . .
F9 F 0.7346(10) 0.3593(8) 0.5939(11) 0.104(4) Uani 0.50 1 d P . .
F10 F 0.8928(17) 0.2959(11) 0.528(2) 0.198(11) Uani 0.50 1 d P . .
F11 F 0.8303(14) 0.4362(11) 0.5127(8) 0.108(4) Uani 0.50 1 d P . .
F12 F 0.9685(11) 0.4170(15) 0.6476(9) 0.141(7) Uani 0.50 1 d P . .
O1 O 0.3508(5) 0.3252(4) 0.8660(4) 0.0712(15) Uani 1 1 d . . .
O2 O 0.8298(5) -0.0361(4) 0.9925(4) 0.0593(12) Uani 1 1 d . . .
O3 O 0.4833(6) 0.3965(4) 0.6361(5) 0.0727(14) Uani 1 1 d . . .
O4 O 0.2445(6) 0.3692(4) 0.7075(4) 0.0704(14) Uani 1 1 d . . .
O5 O 0.1589(7) 0.1602(5) 0.5820(5) 0.099(2) Uani 1 1 d . . .
O6 O 0.1844(8) 0.3093(7) 0.4960(5) 0.112(3) Uani 1 1 d . . .
O7 O 0.5921(10) 0.4283(6) 0.3504(8) 0.109(4) Uani 0.75 1 d P . .
O8 O 0.807(3) 0.4468(18) 0.3561(13) 0.140(9) Uani 0.40 1 d P . .
O9 O 0.9043(11) 0.3535(9) 0.3307(7) 0.087(3) Uani 0.60 1 d P . .
O10 O 0.8467(6) 0.1469(5) 0.2109(6) 0.097(2) Uani 1 1 d . . .
N1 N 0.6929(4) 0.2859(3) 1.0050(3) 0.0370(9) Uani 1 1 d . . .
N2 N 0.6858(5) 0.3676(3) 1.1507(4) 0.0439(11) Uani 1 1 d . . .
H2 H 0.7124 0.3947 1.2162 0.053 Uiso 1 1 calc R . .
N3 N 0.5382(5) 0.2589(3) 0.8248(3) 0.0370(9) Uani 1 1 d . . .
N4 N 0.4815(5) 0.2324(4) 0.7199(4) 0.0420(10) Uani 1 1 d . . .
N5 N 0.6795(5) 0.1580(3) 0.7418(4) 0.0416(10) Uani 1 1 d . . .
H6 H 0.7330 0.1283 0.7208 0.038 Uiso 1 1 d . . .
N6 N 0.4210(6) 0.1815(4) 0.5222(4) 0.0509(12) Uani 1 1 d . . .
N7 N 0.5897(5) 0.0975(3) 0.8708(3) 0.0349(9) Uani 1 1 d . . .
N8 N 0.4103(5) -0.0191(4) 0.8389(4) 0.0439(11) Uani 1 1 d . . .
H12 H 0.3208 -0.0527 0.8169 0.053 Uiso 1 1 calc R . .
N9 N 0.9045(5) 0.0962(4) 0.9624(4) 0.0452(11) Uani 1 1 d . . .
N10 N 0.8868(5) 0.1747(3) 0.9291(4) 0.0390(10) Uani 1 1 d . . .
N11 N 1.1339(5) 0.2068(4) 0.9474(4) 0.0511(12) Uani 1 1 d . . .
H16 H 1.1523 0.1557 0.9650 0.061 Uiso 1 1 calc R . .
H17 H 1.2036 0.2458 0.9434 0.061 Uiso 1 1 calc R . .
N12 N 0.8354(5) 0.3246(3) 0.8816(3) 0.0358(9) Uani 1 1 d . . .
C1 C 0.7600(6) 0.3114(4) 1.1019(4) 0.0417(12) Uani 1 1 d . . .
H1 H 0.8472 0.2932 1.1330 0.050 Uiso 1 1 calc R . .
C2 C 0.5631(6) 0.3758(4) 1.0825(5) 0.0458(13) Uani 1 1 d . . .
C3 C 0.4566(8) 0.4323(6) 1.1120(6) 0.0634(18) Uani 1 1 d . . .
H3 H 0.3819 0.3890 1.1193 0.076 Uiso 1 1 calc R . .
H4 H 0.4111 0.4594 1.0603 0.076 Uiso 1 1 calc R . .
H5 H 0.5069 0.4859 1.1760 0.076 Uiso 1 1 calc R . .
C4 C 0.5685(6) 0.3236(4) 0.9915(4) 0.0407(12) Uani 1 1 d . . .
C5 C 0.4737(6) 0.3026(5) 0.8866(4) 0.0456(13) Uani 1 1 d . . .
C6 C 0.5698(6) 0.1809(4) 0.6820(4) 0.0397(11) Uani 1 1 d . . .
C7 C 0.5389(7) 0.1531(4) 0.5727(4) 0.0463(13) Uani 1 1 d . . .
C8 C 0.6254(9) 0.1037(6) 0.5264(5) 0.0636(18) Uani 1 1 d . . .
H7 H 0.7078 0.0855 0.5640 0.076 Uiso 1 1 calc R . .
C9 C 0.5895(10) 0.0814(6) 0.4247(6) 0.073(2) Uani 1 1 d . . .
H8 H 0.6485 0.0486 0.3914 0.088 Uiso 1 1 calc R . .
C10 C 0.4682(11) 0.1067(6) 0.3712(6) 0.075(2) Uani 1 1 d . . .
H9 H 0.4405 0.0900 0.3006 0.090 Uiso 1 1 calc R . .
C11 C 0.3869(9) 0.1572(6) 0.4227(5) 0.0622(18) Uani 1 1 d . . .
H10 H 0.3035 0.1752 0.3859 0.075 Uiso 1 1 calc R . .
C12 C 0.4485(6) 0.0677(4) 0.8299(4) 0.0404(11) Uani 1 1 d . . .
H11 H 0.3832 0.1020 0.7987 0.048 Uiso 1 1 calc R . .
C13 C 0.5298(6) -0.0468(4) 0.8869(5) 0.0427(12) Uani 1 1 d . . .
C14 C 0.5219(7) -0.1410(4) 0.9051(5) 0.0531(15) Uani 1 1 d . . .
H13 H 0.4399 -0.1897 0.8511 0.064 Uiso 1 1 calc R . .
H14 H 0.5083 -0.1316 0.9694 0.064 Uiso 1 1 calc R . .
H15 H 0.6122 -0.1642 0.9070 0.064 Uiso 1 1 calc R . .
C15 C 0.6449(6) 0.0267(4) 0.9072(4) 0.0397(11) Uani 1 1 d . . .
C16 C 0.7965(6) 0.0285(4) 0.9563(5) 0.0434(12) Uani 1 1 d . . .
C17 C 1.0010(6) 0.2249(4) 0.9268(4) 0.0426(12) Uani 1 1 d . . .
C18 C 0.9747(6) 0.3148(4) 0.9027(4) 0.0413(12) Uani 1 1 d . . .
C19 C 1.0789(6) 0.3832(5) 0.9017(5) 0.0484(13) Uani 1 1 d . . .
H18 H 1.1768 0.3755 0.9175 0.058 Uiso 1 1 calc R . .
C20 C 1.0401(7) 0.4633(5) 0.8777(5) 0.0529(15) Uani 1 1 d . . .
H19 H 1.1105 0.5114 0.8765 0.063 Uiso 1 1 calc R . .
C21 C 0.8960(6) 0.4720(4) 0.8551(5) 0.0480(14) Uani 1 1 d . . .
H20 H 0.8667 0.5266 0.8384 0.058 Uiso 1 1 calc R . .
C22 C 0.7964(6) 0.4018(4) 0.8571(4) 0.0433(12) Uani 1 1 d . . .
H21 H 0.6977 0.4078 0.8409 0.052 Uiso 1 1 calc R . .
B1 B 0.9971(10) 0.0376(8) 0.6945(8) 0.052(2) Uani 0.75 1 d P . .
B2 B 0.8027(11) 0.7142(9) 0.7617(8) 0.058(3) Uani 0.75 1 d P . .
B3 B 0.8520(17) 0.3781(16) 0.5727(13) 0.067(5) Uani 0.50 1 d P . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N5 Co1 N3 81.84(19) . . ?
N5 Co1 N7 90.0(2) . . ?
N3 Co1 N7 90.54(19) . . ?
N5 Co1 N1 165.76(19) . . ?
N3 Co1 N1 83.96(19) . . ?
N7 Co1 N1 91.02(18) . . ?
N5 Co1 N12 87.6(2) . . ?
N3 Co1 N12 93.65(19) . . ?
N7 Co1 N12 174.86(17) . . ?
N1 Co1 N12 92.38(18) . . ?
N5 Co1 N10 96.7(2) . . ?
N3 Co1 N10 175.85(18) . . ?
N7 Co1 N10 93.34(18) . . ?
N1 Co1 N10 97.45(19) . . ?
N12 Co1 N10 82.40(18) . . ?
O5 Co2 N6 92.2(3) . . ?
O5 Co2 O4 89.8(3) . . ?
N6 Co2 O4 177.5(2) . . ?
O5 Co2 O3 173.7(3) . . ?
N6 Co2 O3 90.6(2) . . ?
O4 Co2 O3 87.5(2) . . ?
O5 Co2 N4 95.0(3) . . ?
N6 Co2 N4 78.8(2) . . ?
O4 Co2 N4 99.6(2) . . ?
O3 Co2 N4 91.1(2) . . ?
O5 Co2 O6 86.3(3) . . ?
N6 Co2 O6 96.1(3) . . ?
O4 Co2 O6 85.4(3) . . ?
O3 Co2 O6 87.8(3) . . ?
N4 Co2 O6 174.8(2) . . ?
C1 N1 C4 106.9(5) . . ?
C1 N1 Co1 142.4(4) . . ?
C4 N1 Co1 110.7(4) . . ?
C1 N2 C2 109.5(5) . . ?
C5 N3 N4 125.0(4) . . ?
C5 N3 Co1 118.1(4) . . ?
N4 N3 Co1 116.4(3) . . ?
C6 N4 N3 107.9(4) . . ?
C6 N4 Co2 113.1(4) . . ?
N3 N4 Co2 137.5(4) . . ?
C6 N5 Co1 113.5(4) . . ?
C11 N6 C7 117.3(6) . . ?
C11 N6 Co2 127.2(5) . . ?
C7 N6 Co2 115.0(4) . . ?
C12 N7 C15 107.4(4) . . ?
C12 N7 Co1 128.1(4) . . ?
C15 N7 Co1 124.5(3) . . ?
C12 N8 C13 109.8(5) . . ?
C16 N9 N10 125.6(4) . . ?
C17 N10 N9 117.8(4) . . ?
C17 N10 Co1 115.4(4) . . ?
N9 N10 Co1 126.7(3) . . ?
C22 N12 C18 119.5(5) . . ?
C22 N12 Co1 126.3(4) . . ?
C18 N12 Co1 113.9(4) . . ?
N1 C1 N2 109.4(5) . . ?
C4 C2 N2 104.5(5) . . ?
C4 C2 C3 132.5(6) . . ?
N2 C2 C3 122.9(6) . . ?
C2 C4 N1 109.7(5) . . ?
C2 C4 C5 133.9(5) . . ?
N1 C4 C5 116.4(5) . . ?
O1 C5 N3 128.8(6) . . ?
O1 C5 C4 121.4(5) . . ?
N3 C5 C4 109.8(5) . . ?
N5 C6 N4 120.1(5) . . ?
N5 C6 C7 122.5(5) . . ?
N4 C6 C7 117.3(5) . . ?
N6 C7 C8 122.8(6) . . ?
N6 C7 C6 114.8(5) . . ?
C8 C7 C6 122.4(6) . . ?
C9 C8 C7 118.6(7) . . ?
C10 C9 C8 119.8(8) . . ?
C9 C10 C11 118.5(7) . . ?
N6 C11 C10 122.9(7) . . ?
N7 C12 N8 109.4(5) . . ?
N8 C13 C15 105.5(5) . . ?
N8 C13 C14 122.0(5) . . ?
C15 C13 C14 132.4(5) . . ?
C13 C15 N7 107.9(5) . . ?
C13 C15 C16 125.8(5) . . ?
N7 C15 C16 126.2(5) . . ?
O2 C16 N9 118.1(5) . . ?
O2 C16 C15 119.3(5) . . ?
N9 C16 C15 122.6(5) . . ?
N10 C17 N11 127.5(5) . . ?
N10 C17 C18 113.6(5) . . ?
N11 C17 C18 118.9(5) . . ?
N12 C18 C19 121.5(5) . . ?
N12 C18 C17 113.4(5) . . ?
C19 C18 C17 125.1(5) . . ?
C18 C19 C20 119.4(5) . . ?
C19 C20 C21 118.6(6) . . ?
C22 C21 C20 119.7(5) . . ?
N12 C22 C21 121.3(5) . . ?
F2 B1 F4 110.4(11) . . ?
F2 B1 F1 112.6(12) . . ?
F4 B1 F1 113.6(10) . . ?
F2 B1 F3 104.7(9) . . ?
F4 B1 F3 108.5(10) . . ?
F1 B1 F3 106.5(9) . . ?
F8 B2 F6 114.4(9) . . ?
F8 B2 F7 106.9(10) . . ?
F6 B2 F7 109.3(10) . . ?
F8 B2 F5 107.6(10) . . ?
F6 B2 F5 112.4(9) . . ?
F7 B2 F5 105.8(9) . . ?
F12 B3 F9 115.6(15) . . ?
F12 B3 F10 98.0(15) . . ?
F9 B3 F10 112.5(18) . . ?
F12 B3 F11 109.5(18) . . ?
F9 B3 F11 110.1(12) . . ?
F10 B3 F11 110.6(18) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Co1 N5 1.868(5) . ?
Co1 N3 1.876(4) . ?
Co1 N7 1.925(4) . ?
Co1 N1 1.926(5) . ?
Co1 N12 1.934(4) . ?
Co1 N10 1.934(4) . ?
Co2 O5 2.077(6) . ?
Co2 N6 2.091(6) . ?
Co2 O4 2.096(5) . ?
Co2 O3 2.114(5) . ?
Co2 N4 2.119(5) . ?
Co2 O6 2.122(5) . ?
F1 B1 1.316(12) . ?
F2 B1 1.286(11) . ?
F3 B1 1.377(12) . ?
F4 B1 1.306(13) . ?
F5 B2 1.357(11) . ?
F6 B2 1.344(11) . ?
F7 B2 1.351(14) . ?
F8 B2 1.334(14) . ?
F9 B3 1.318(19) . ?
F10 B3 1.35(2) . ?
F11 B3 1.39(2) . ?
F12 B3 1.27(2) . ?
O1 C5 1.260(7) . ?
O2 C16 1.245(7) . ?
O8 O9 1.76(3) . ?
N1 C1 1.309(7) . ?
N1 C4 1.379(7) . ?
N2 C1 1.350(8) . ?
N2 C2 1.367(7) . ?
N3 C5 1.322(7) . ?
N3 N4 1.405(6) . ?
N4 C6 1.349(7) . ?
N5 C6 1.320(7) . ?
N6 C11 1.342(8) . ?
N6 C7 1.356(8) . ?
N7 C12 1.309(7) . ?
N7 C15 1.389(6) . ?
N8 C12 1.348(7) . ?
N8 C13 1.349(7) . ?
N9 C16 1.347(7) . ?
N9 N10 1.387(6) . ?
N10 C17 1.302(7) . ?
N11 C17 1.325(7) . ?
N12 C22 1.342(7) . ?
N12 C18 1.347(7) . ?
C2 C4 1.363(8) . ?
C2 C3 1.488(9) . ?
C4 C5 1.478(8) . ?
C6 C7 1.482(8) . ?
C7 C8 1.382(9) . ?
C8 C9 1.375(10) . ?
C9 C10 1.373(12) . ?
C10 C11 1.390(11) . ?
C13 C15 1.379(8) . ?
C13 C14 1.482(8) . ?
C15 C16 1.446(7) . ?
C17 C18 1.489(8) . ?
C18 C19 1.372(8) . ?
C19 C20 1.378(9) . ?
C20 C21 1.387(9) . ?
C21 C22 1.367(8) . ?
