#------------------------------------------------------------------------------
#$Date: 2016-03-25 10:21:20 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179748 $
#$URL: svn://www.crystallography.net/cod/cif/7/00/44/7004439.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7004439
loop_
_publ_author_name
'Orto, Peter J.'
'Nichol, Gary S.'
'Okumura, Noriko'
'Evans, Dennis H.'
'Arratia-Pérez, Ramiro'
'Ramirez-Tagle, Rodrigo'
'Wang, Ruiyao'
'Zheng, Zhiping'
_publ_section_title
;
 Cluster carbonyls of the [Re6(μ3-Se)8]2+ core: synthesis, structural
 characterization, and computational analysis
;
_journal_issue                   32
_journal_name_full               'Dalton Transactions'
_journal_page_first              4247
_journal_page_last               4253
_journal_paper_doi               10.1039/b806973e
_journal_year                    2008
_chemical_formula_moiety         'C31 H75 O P5 Re6 Se8 2+, 2 Sb F6 -'
_chemical_formula_sum            'C31 H75 F12 O P5 Re6 Sb2 Se8'
_chemical_formula_weight         2839.14
_chemical_name_systematic
;
?
;
_space_group_IT_number           11
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yb'
_symmetry_space_group_name_H-M   'P 1 21/m 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 103.052(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   13.5933(13)
_cell_length_b                   13.7409(13)
_cell_length_c                   18.5607(17)
_cell_measurement_reflns_used    7241
_cell_measurement_temperature    220(2)
_cell_measurement_theta_max      28.25
_cell_measurement_theta_min      2.15
_cell_volume                     3377.3(6)
_computing_cell_refinement       'SAINT (Bruker, 2007)'
_computing_data_collection       'SMART (Bruker, 2007)'
_computing_data_reduction        SAINT
_computing_molecular_graphics    'DIAMOND (Brandenburg & Putz, 1999)'
_computing_publication_material  'SHELXTL and local programs'
_computing_structure_refinement  SHELXTL
_computing_structure_solution    'SHELXTL (Sheldrick, 2008)'
_diffrn_ambient_temperature      220(2)
_diffrn_measured_fraction_theta_full 0.988
_diffrn_measured_fraction_theta_max 0.988
_diffrn_measurement_device_type  'Bruker SMART 1000 CCD diffractometer'
_diffrn_measurement_method       'thin-slice ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0508
_diffrn_reflns_av_sigmaI/netI    0.0489
_diffrn_reflns_limit_h_max       16
_diffrn_reflns_limit_h_min       -15
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_k_min       -16
_diffrn_reflns_limit_l_max       22
_diffrn_reflns_limit_l_min       -21
_diffrn_reflns_number            23004
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         1.69
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    15.979
_exptl_absorpt_correction_T_max  0.5021
_exptl_absorpt_correction_T_min  0.0831
_exptl_absorpt_correction_type   numerical
_exptl_absorpt_process_details   'SADABS 2007/4; Sheldrick, 1996'
_exptl_crystal_colour            orange
_exptl_crystal_density_diffrn    2.792
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       plate
_exptl_crystal_F_000             2552
_exptl_crystal_size_max          0.31
_exptl_crystal_size_mid          0.28
_exptl_crystal_size_min          0.05
_refine_diff_density_max         2.835
_refine_diff_density_min         -4.881
_refine_diff_density_rms         0.343
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.038
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     443
_refine_ls_number_reflns         6149
_refine_ls_number_restraints     266
_refine_ls_restrained_S_all      1.021
_refine_ls_R_factor_all          0.0698
_refine_ls_R_factor_gt           0.0494
_refine_ls_shift/su_max          0.009
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0716P)²+78.9899P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1364
_refine_ls_wR_factor_ref         0.1510
_reflns_number_gt                4494
_reflns_number_total             6149
_reflns_threshold_expression     I>2σ(I)
_cod_data_source_file            b806973e.txt
_cod_data_source_block           zz165
_cod_original_cell_volume        3377.3(5)
_cod_original_sg_symbol_H-M      'P 21/m'
_cod_database_code               7004439
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z'
'-x, -y, -z'
'x, -y-1/2, z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Re1 Re 0.21530(4) 0.65356(3) 0.70295(3) 0.01628(16) Uani 1 1 d . . .
Re2 Re 0.40998(3) 0.65361(3) 0.70263(3) 0.01584(16) Uani 1 1 d . . .
Re3 Re 0.34476(5) 0.7500 0.80614(4) 0.01778(18) Uani 1 2 d S . .
Re4 Re 0.28067(5) 0.7500 0.59998(4) 0.01491(18) Uani 1 2 d S . .
Se1 Se 0.52755(13) 0.7500 0.80122(10) 0.0209(4) Uani 1 2 d S . .
Se2 Se 0.34354(10) 0.56726(9) 0.80132(7) 0.0219(3) Uani 1 1 d . . .
Se3 Se 0.15860(14) 0.7500 0.80157(11) 0.0245(4) Uani 1 2 d S . .
Se4 Se 0.28221(9) 0.56651(9) 0.60450(7) 0.0187(3) Uani 1 1 d . . .
Se5 Se 0.09690(13) 0.7500 0.60493(10) 0.0202(4) Uani 1 2 d S . .
Se6 Se 0.46720(12) 0.7500 0.60407(10) 0.0185(4) Uani 1 2 d S . .
P1 P 0.0851(3) 0.5254(3) 0.6971(2) 0.0253(8) Uani 1 1 d . . .
P2 P 0.5373(2) 0.5261(3) 0.6964(2) 0.0235(7) Uani 1 1 d . . .
P3 P 0.3896(6) 0.7500 0.9423(4) 0.0558(16) Uani 1 2 d S . .
Sb1 Sb 0.84278(15) 0.2551(15) 0.80676(12) 0.0440(11) Uani 0.313(10) 1 d PDU A
-1
F1 F 0.898(2) 0.340(2) 0.8811(16) 0.137(9) Uani 0.627(19) 1 d PDU A -1
F2 F 0.955(2) 0.243(7) 0.770(2) 0.128(14) Uani 0.313(10) 1 d PDU A -1
F3 F 0.803(3) 0.349(2) 0.7402(16) 0.116(9) Uani 0.627(19) 1 d PDU A -1
F4 F 0.725(2) 0.283(3) 0.833(3) 0.108(10) Uani 0.313(10) 1 d PDU A -1
Sb1' Sb 0.84278(15) 0.2551(15) 0.80676(12) 0.0440(11) Uani 0.187(10) 1 d PDU A
-
F1' F 0.818(4) 0.342(3) 0.873(2) 0.122(9) Uani 0.373(19) 1 d PDU A -2
F2' F 0.9791(16) 0.257(8) 0.841(4) 0.129(16) Uani 0.187(10) 1 d PDU A -2
F3' F 0.859(4) 0.342(4) 0.739(3) 0.115(11) Uani 0.373(19) 1 d PDU A -2
F4' F 0.720(3) 0.225(5) 0.752(3) 0.112(13) Uani 0.187(10) 1 d PDU A -2
Sb2 Sb 0.74992(13) 0.7442(13) 0.49900(11) 0.0338(11) Uani 0.255(7) 1 d PDU B -1
F5 F 0.6553(12) 0.6543(13) 0.5014(11) 0.060(5) Uani 0.511(13) 1 d PDU B -1
F6 F 0.8388(12) 0.6816(16) 0.5696(9) 0.066(5) Uani 0.511(13) 1 d PDU B -1
F7 F 0.793(2) 0.673(3) 0.4293(12) 0.053(8) Uani 0.255(7) 1 d PDU B -1
F8 F 0.711(3) 0.811(3) 0.5723(19) 0.049(9) Uani 0.255(7) 1 d PDU B -1
Sb2' Sb 0.74992(13) 0.7442(13) 0.49900(11) 0.0338(11) Uani 0.245(7) 1 d PDU B
-2
F5' F 0.6609(12) 0.6798(15) 0.4283(11) 0.062(5) Uani 0.489(13) 1 d PDU B -2
F6' F 0.8434(13) 0.6500(14) 0.5002(11) 0.059(5) Uani 0.489(13) 1 d PDU B -2
F7' F 0.797(3) 0.806(2) 0.4273(19) 0.078(16) Uani 0.245(7) 1 d PDU B -2
F8' F 0.697(4) 0.684(4) 0.5685(15) 0.064(8) Uani 0.245(7) 1 d PDU B -2
O O 0.2252(10) 0.7500 0.4241(7) 0.032(3) Uani 1 2 d S . .
C1 C 0.0225(12) 0.4964(13) 0.6013(9) 0.048(3) Uani 1 1 d U C .
H1A H -0.0086 0.5559 0.5774 0.057 Uiso 1 1 calc R . .
H1B H 0.0740 0.4757 0.5752 0.057 Uiso 1 1 calc R . .
C2 C -0.0578(12) 0.4181(13) 0.5923(9) 0.048(3) Uani 1 1 d U . .
H2A H -0.0262 0.3546 0.5939 0.073 Uiso 1 1 calc R C .
H2B H -0.1053 0.4264 0.5451 0.073 Uiso 1 1 calc R . .
H2C H -0.0932 0.4232 0.6320 0.073 Uiso 1 1 calc R . .
C3 C 0.1296(13) 0.4086(12) 0.7395(11) 0.0503(6) Uani 0.48(2) 1 d PU C 1
H3A H 0.0788 0.3598 0.7181 0.060 Uiso 0.48(2) 1 calc PR C 1
H3B H 0.1911 0.3920 0.7230 0.060 Uiso 0.48(2) 1 calc PR C 1
C4 C 0.150(3) 0.396(3) 0.814(2) 0.0503(10) Uani 0.48(2) 1 d PU C 1
H4A H 0.1700 0.4577 0.8384 0.075 Uiso 0.48(2) 1 calc PR C 1
H4B H 0.2054 0.3496 0.8284 0.075 Uiso 0.48(2) 1 calc PR C 1
H4C H 0.0910 0.3712 0.8287 0.075 Uiso 0.48(2) 1 calc PR C 1
C3' C 0.1296(13) 0.4086(12) 0.7395(11) 0.0503(6) Uani 0.52(2) 1 d PU C 2
H3'1 H 0.1514 0.4194 0.7929 0.060 Uiso 0.52(2) 1 calc PR C 2
H3'2 H 0.0712 0.3648 0.7318 0.060 Uiso 0.52(2) 1 calc PR C 2
C4' C 0.210(2) 0.357(2) 0.717(2) 0.0504(10) Uani 0.52(2) 1 d PU C 2
H4'1 H 0.1824 0.3225 0.6709 0.076 Uiso 0.52(2) 1 calc PR C 2
H4'2 H 0.2402 0.3110 0.7547 0.076 Uiso 0.52(2) 1 calc PR C 2
H4'3 H 0.2603 0.4032 0.7088 0.076 Uiso 0.52(2) 1 calc PR C 2
C5 C -0.0194(14) 0.5542(15) 0.7393(13) 0.069(4) Uani 1 1 d U C .
H5A H -0.0624 0.4965 0.7365 0.083 Uiso 1 1 calc R . .
H5B H 0.0078 0.5684 0.7918 0.083 Uiso 1 1 calc R . .
C6 C -0.0800(14) 0.6329(15) 0.7077(13) 0.071(4) Uani 1 1 d U . .
H6A H -0.0607 0.6532 0.6628 0.106 Uiso 1 1 calc R C .
H6B H -0.0707 0.6867 0.7425 0.106 Uiso 1 1 calc R . .
H6C H -0.1503 0.6132 0.6961 0.106 Uiso 1 1 calc R . .
C7 C 0.5175(12) 0.4087(11) 0.7369(9) 0.0416(6) Uani 0.50(2) 1 d PU D 1
H7A H 0.4458 0.3920 0.7204 0.050 Uiso 0.50(2) 1 calc PR D 1
H7B H 0.5558 0.3597 0.7164 0.050 Uiso 0.50(2) 1 calc PR D 1
C8 C 0.543(2) 0.401(2) 0.8116(18) 0.0416(10) Uani 0.50(2) 1 d PU D 1
H8A H 0.6134 0.3826 0.8272 0.062 Uiso 0.50(2) 1 calc PR D 1
H8B H 0.5012 0.3520 0.8275 0.062 Uiso 0.50(2) 1 calc PR D 1
H8C H 0.5325 0.4632 0.8335 0.062 Uiso 0.50(2) 1 calc PR D 1
C7' C 0.5175(12) 0.4087(11) 0.7369(9) 0.0416(6) Uani 0.50(2) 1 d PU D 2
H7'1 H 0.5738 0.3668 0.7318 0.050 Uiso 0.50(2) 1 calc PR D 2
H7'2 H 0.5245 0.4196 0.7900 0.050 Uiso 0.50(2) 1 calc PR D 2
C8' C 0.425(2) 0.353(2) 0.7114(19) 0.0416(10) Uani 0.50(2) 1 d PU D 2
H8'1 H 0.3728 0.3782 0.7337 0.062 Uiso 0.50(2) 1 calc PR D 2
H8'2 H 0.4381 0.2850 0.7256 0.062 Uiso 0.50(2) 1 calc PR D 2
H8'3 H 0.4042 0.3573 0.6580 0.062 Uiso 0.50(2) 1 calc PR D 2
C9 C 0.5388(12) 0.4965(12) 0.5999(9) 0.045(3) Uani 1 1 d U D .
H9A H 0.4712 0.4744 0.5748 0.054 Uiso 1 1 calc R . .
H9B H 0.5530 0.5562 0.5753 0.054 Uiso 1 1 calc R . .
C10 C 0.6159(13) 0.4182(12) 0.5899(9) 0.046(3) Uani 1 1 d U . .
H10A H 0.6837 0.4439 0.6062 0.069 Uiso 1 1 calc R D .
H10B H 0.6041 0.4003 0.5381 0.069 Uiso 1 1 calc R . .
H10C H 0.6082 0.3613 0.6191 0.069 Uiso 1 1 calc R . .
C11 C 0.6670(11) 0.5553(13) 0.7403(9) 0.0431(6) Uani 0.44(2) 1 d PU D 1
H11A H 0.7094 0.5098 0.7201 0.052 Uiso 0.44(2) 1 calc PR D 1
H11B H 0.6802 0.6201 0.7226 0.052 Uiso 0.44(2) 1 calc PR D 1
C12 C 0.705(2) 0.556(3) 0.819(2) 0.0431(10) Uani 0.44(2) 1 d PU D 1
H12A H 0.7753 0.5348 0.8304 0.065 Uiso 0.44(2) 1 calc PR D 1
H12B H 0.6656 0.5121 0.8419 0.065 Uiso 0.44(2) 1 calc PR D 1
H12C H 0.7011 0.6213 0.8377 0.065 Uiso 0.44(2) 1 calc PR D 1
C11' C 0.6670(11) 0.5553(13) 0.7403(9) 0.0431(6) Uani 0.56(2) 1 d PU D 2
H11C H 0.6704 0.5687 0.7926 0.052 Uiso 0.56(2) 1 calc PR D 2
H11D H 0.7083 0.4973 0.7380 0.052 Uiso 0.56(2) 1 calc PR D 2
C12' C 0.7153(19) 0.641(2) 0.7087(17) 0.0430(10) Uani 0.56(2) 1 d PU D 2
H12D H 0.6819 0.7006 0.7171 0.064 Uiso 0.56(2) 1 calc PR D 2
H12E H 0.7083 0.6313 0.6559 0.064 Uiso 0.56(2) 1 calc PR D 2
H12F H 0.7863 0.6444 0.7328 0.064 Uiso 0.56(2) 1 calc PR D 2
C13 C 0.288(2) 0.7500 0.9893(14) 0.0558(16) Uani 1 2 d SDU . .
H13A H 0.3104 0.7708 1.0409 0.067 Uiso 0.50 1 calc PR E -1
H13B H 0.2319 0.7917 0.9643 0.067 Uiso 0.50 1 calc PR E -1
C14 C 0.257(3) 0.6414(15) 0.9838(19) 0.0563(19) Uani 0.50 1 d PDU F -1
H14A H 0.2025 0.6309 1.0084 0.085 Uiso 0.50 1 calc PR F -1
H14B H 0.3150 0.6020 1.0073 0.085 Uiso 0.50 1 calc PR F -1
H14C H 0.2359 0.6230 0.9321 0.085 Uiso 0.50 1 calc PR F -1
C15 C 0.4597(15) 0.6442(14) 0.9867(9) 0.0558(16) Uani 1 1 d DU . .
H15A H 0.4108 0.5920 0.9878 0.067 Uiso 1 1 calc R F .
H15B H 0.5037 0.6218 0.9549 0.067 Uiso 1 1 calc R . .
C16 C 0.5251(15) 0.6560(14) 1.0654(9) 0.0588(19) Uani 1 1 d DU F .
H16A H 0.5680 0.7127 1.0673 0.088 Uiso 1 1 calc R . .
H16B H 0.5666 0.5985 1.0787 0.088 Uiso 1 1 calc R . .
H16C H 0.4817 0.6642 1.1000 0.088 Uiso 1 1 calc R . .
C17 C 0.2454(12) 0.7500 0.4864(12) 0.023(4) Uani 1 2 d S . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Se Se -0.0929 2.2259 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Re Re -1.0185 7.2310 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
P1 Re1 Se5 90.49(9) . . ?
P1 Re1 Se3 94.18(9) . . ?
Se5 Re1 Se3 89.86(5) . . ?
P1 Re1 Se2 93.88(9) . . ?
Se5 Re1 Se2 175.63(4) . . ?
Se3 Re1 Se2 89.78(5) . . ?
P1 Re1 Se4 90.12(9) . . ?
Se5 Re1 Se4 90.14(5) . . ?
Se3 Re1 Se4 175.70(5) . . ?
Se2 Re1 Se4 89.89(4) . . ?
P1 Re1 Re4 132.69(9) . . ?
Se5 Re1 Re4 58.47(4) . . ?
Se3 Re1 Re4 118.08(3) . . ?
Se2 Re1 Re4 118.06(4) . . ?
Se4 Re1 Re4 58.50(3) . . ?
P1 Re1 Re3 137.59(9) . . ?
Se5 Re1 Re3 118.16(3) . . ?
Se3 Re1 Re3 58.18(4) . . ?
Se2 Re1 Re3 58.17(3) . . ?
Se4 Re1 Re3 118.22(4) . . ?
Re4 Re1 Re3 89.72(2) . . ?
P1 Re1 Re2 134.70(9) . . ?
Se5 Re1 Re2 118.34(4) . . ?
Se3 Re1 Re2 118.15(5) . . ?
Se2 Re1 Re2 58.21(3) . . ?
Se4 Re1 Re2 58.25(3) . . ?
Re4 Re1 Re2 59.88(2) . . ?
Re3 Re1 Re2 59.98(2) . . ?
P1 Re1 Re1 135.20(8) . 4_575 ?
Se5 Re1 Re1 58.23(2) . 4_575 ?
Se3 Re1 Re1 58.24(3) . 4_575 ?
Se2 Re1 Re1 118.10(3) . 4_575 ?
Se4 Re1 Re1 118.35(3) . 4_575 ?
Re4 Re1 Re1 59.862(13) . 4_575 ?
Re3 Re1 Re1 59.941(13) . 4_575 ?
Re2 Re1 Re1 89.987(15) . 4_575 ?
P2 Re2 Se2 94.00(9) . . ?
P2 Re2 Se1 94.03(9) . . ?
Se2 Re2 Se1 89.56(5) . . ?
P2 Re2 Se4 90.30(9) . . ?
Se2 Re2 Se4 90.00(4) . . ?
Se1 Re2 Se4 175.67(4) . . ?
P2 Re2 Se6 90.25(9) . . ?
Se2 Re2 Se6 175.75(4) . . ?
Se1 Re2 Se6 90.10(5) . . ?
Se4 Re2 Se6 90.02(5) . . ?
P2 Re2 Re4 132.70(9) . . ?
Se2 Re2 Re4 118.19(4) . . ?
Se1 Re2 Re4 118.09(3) . . ?
Se4 Re2 Re4 58.53(3) . . ?
Se6 Re2 Re4 58.43(4) . . ?
P2 Re2 Re3 137.58(8) . . ?
Se2 Re2 Re3 58.20(3) . . ?
Se1 Re2 Re3 58.04(4) . . ?
Se4 Re2 Re3 118.28(4) . . ?
Se6 Re2 Re3 118.24(3) . . ?
Re4 Re2 Re3 89.73(2) . . ?
P2 Re2 Re1 135.02(9) . . ?
Se2 Re2 Re1 58.32(3) . . ?
Se1 Re2 Re1 117.99(4) . . ?
Se4 Re2 Re1 58.32(3) . . ?
Se6 Re2 Re1 118.32(4) . . ?
Re4 Re2 Re1 59.90(2) . . ?
Re3 Re2 Re1 59.97(2) . . ?
P2 Re2 Re2 134.86(8) . 4_575 ?
Se2 Re2 Re2 118.15(3) . 4_575 ?
Se1 Re2 Re2 58.25(2) . 4_575 ?
Se4 Re2 Re2 118.39(3) . 4_575 ?
Se6 Re2 Re2 58.29(2) . 4_575 ?
Re4 Re2 Re2 59.869(13) . 4_575 ?
Re3 Re2 Re2 59.962(13) . 4_575 ?
Re1 Re2 Re2 90.014(14) . 4_575 ?
P3 Re3 Se1 91.14(19) . . ?
P3 Re3 Se2 91.99(3) . . ?
Se1 Re3 Se2 89.85(3) . . ?
P3 Re3 Se2 91.99(3) . 4_575 ?
Se1 Re3 Se2 89.85(3) . 4_575 ?
Se2 Re3 Se2 176.02(7) . 4_575 ?
P3 Re3 Se3 92.79(19) . . ?
Se1 Re3 Se3 176.08(7) . . ?
Se2 Re3 Se3 90.02(3) . . ?
Se2 Re3 Se3 90.02(3) 4_575 . ?
P3 Re3 Re1 135.49(13) . . ?
Se1 Re3 Re1 118.44(4) . . ?
Se2 Re3 Re1 58.38(3) . . ?
Se2 Re3 Re1 118.48(4) 4_575 . ?
Se3 Re3 Re1 58.36(4) . . ?
P3 Re3 Re1 135.49(13) . 4_575 ?
Se1 Re3 Re1 118.45(4) . 4_575 ?
Se2 Re3 Re1 118.48(4) . 4_575 ?
Se2 Re3 Re1 58.38(3) 4_575 4_575 ?
Se3 Re3 Re1 58.36(4) . 4_575 ?
Re1 Re3 Re1 60.12(3) . 4_575 ?
P3 Re3 Re2 134.38(14) . . ?
Se1 Re3 Re2 58.41(4) . . ?
Se2 Re3 Re2 58.30(3) . . ?
Se2 Re3 Re2 118.36(4) 4_575 . ?
Se3 Re3 Re2 118.39(4) . . ?
Re1 Re3 Re2 60.05(2) . . ?
Re1 Re3 Re2 90.13(3) 4_575 . ?
P3 Re3 Re2 134.38(14) . 4_575 ?
Se1 Re3 Re2 58.41(4) . 4_575 ?
Se2 Re3 Re2 118.36(4) . 4_575 ?
Se2 Re3 Re2 58.30(3) 4_575 4_575 ?
Se3 Re3 Re2 118.39(4) . 4_575 ?
Re1 Re3 Re2 90.13(3) . 4_575 ?
Re1 Re3 Re2 60.05(2) 4_575 4_575 ?
Re2 Re3 Re2 60.08(3) . 4_575 ?
C17 Re4 Se6 91.8(4) . . ?
C17 Re4 Se5 91.9(4) . . ?
Se6 Re4 Se5 176.28(7) . . ?
C17 Re4 Se4 91.86(3) . . ?
Se6 Re4 Se4 89.90(3) . . ?
Se5 Re4 Se4 89.98(3) . . ?
C17 Re4 Se4 91.86(3) . 4_575 ?
Se6 Re4 Se4 89.90(3) . 4_575 ?
Se5 Re4 Se4 89.98(3) . 4_575 ?
Se4 Re4 Se4 176.28(6) . 4_575 ?
C17 Re4 Re2 134.8(3) . . ?
Se6 Re4 Re2 58.43(4) . . ?
Se5 Re4 Re2 118.54(4) . . ?
Se4 Re4 Re2 58.34(3) . . ?
Se4 Re4 Re2 118.59(4) 4_575 . ?
C17 Re4 Re2 134.8(3) . 4_575 ?
Se6 Re4 Re2 58.43(4) . 4_575 ?
Se5 Re4 Re2 118.54(4) . 4_575 ?
Se4 Re4 Re2 118.59(4) . 4_575 ?
Se4 Re4 Re2 58.33(3) 4_575 4_575 ?
Re2 Re4 Re2 60.26(3) . 4_575 ?
C17 Re4 Re1 134.8(3) . . ?
Se6 Re4 Re1 118.64(4) . . ?
Se5 Re4 Re1 58.33(4) . . ?
Se4 Re4 Re1 58.38(3) . . ?
Se4 Re4 Re1 118.64(4) 4_575 . ?
Re2 Re4 Re1 60.22(2) . . ?
Re2 Re4 Re1 90.43(3) 4_575 . ?
C17 Re4 Re1 134.8(3) . 4_575 ?
Se6 Re4 Re1 118.64(4) . 4_575 ?
Se5 Re4 Re1 58.33(4) . 4_575 ?
Se4 Re4 Re1 118.64(4) . 4_575 ?
Se4 Re4 Re1 58.38(3) 4_575 4_575 ?
Re2 Re4 Re1 90.43(3) . 4_575 ?
Re2 Re4 Re1 60.22(2) 4_575 4_575 ?
Re1 Re4 Re1 60.28(3) . 4_575 ?
Re3 Se1 Re2 63.56(4) . . ?
Re3 Se1 Re2 63.56(4) . 4_575 ?
Re2 Se1 Re2 63.50(5) . 4_575 ?
Re3 Se2 Re2 63.51(4) . . ?
Re3 Se2 Re1 63.46(3) . . ?
Re2 Se2 Re1 63.47(3) . . ?
Re3 Se3 Re1 63.46(5) . 4_575 ?
Re3 Se3 Re1 63.46(5) . . ?
Re1 Se3 Re1 63.52(5) 4_575 . ?
Re2 Se4 Re1 63.43(3) . . ?
Re2 Se4 Re4 63.13(3) . . ?
Re1 Se4 Re4 63.13(3) . . ?
Re1 Se5 Re1 63.54(5) . 4_575 ?
Re1 Se5 Re4 63.19(4) . . ?
Re1 Se5 Re4 63.19(4) 4_575 . ?
Re4 Se6 Re2 63.15(4) . . ?
Re4 Se6 Re2 63.15(4) . 4_575 ?
Re2 Se6 Re2 63.43(5) . 4_575 ?
C5 P1 C3 102.7(9) . . ?
C5 P1 C1 103.2(9) . . ?
C3 P1 C1 105.2(9) . . ?
C5 P1 Re1 116.5(7) . . ?
C3 P1 Re1 116.2(6) . . ?
C1 P1 Re1 111.6(5) . . ?
C11 P2 C7 103.3(8) . . ?
C11 P2 C9 105.2(8) . . ?
C7 P2 C9 103.9(8) . . ?
C11 P2 Re2 116.2(6) . . ?
C7 P2 Re2 115.8(5) . . ?
C9 P2 Re2 111.2(5) . . ?
C13 P3 C15 99.3(9) . 4_575 ?
C13 P3 C15 99.3(9) . . ?
C15 P3 C15 105.3(12) 4_575 . ?
C13 P3 Re3 117.4(9) . . ?
C15 P3 Re3 116.4(6) 4_575 . ?
C15 P3 Re3 116.4(6) . . ?
F3 Sb1 F4 83.3(18) . . ?
F3 Sb1 F2 87(3) . . ?
F4 Sb1 F2 171(3) . . ?
F3 Sb1 F1 94(2) . . ?
F4 Sb1 F1 84.3(17) . . ?
F2 Sb1 F1 96.3(19) . . ?
F6 Sb2 F5 91.1(9) . . ?
F6 Sb2 F8 87.4(17) . . ?
F5 Sb2 F8 89.7(11) . . ?
F6 Sb2 F7 89.5(10) . . ?
F5 Sb2 F7 89.8(11) . . ?
F8 Sb2 F7 176.9(19) . . ?
C2 C1 P1 115.3(12) . . ?
C2 C1 H1A 108.4 . . ?
P1 C1 H1A 108.4 . . ?
C2 C1 H1B 108.4 . . ?
P1 C1 H1B 108.4 . . ?
H1A C1 H1B 107.5 . . ?
C1 C2 H2A 109.5 . . ?
C1 C2 H2B 109.5 . . ?
H2A C2 H2B 109.5 . . ?
C1 C2 H2C 109.5 . . ?
H2A C2 H2C 109.5 . . ?
H2B C2 H2C 109.5 . . ?
C4 C3 P1 121.5(19) . . ?
C4 C3 H3A 106.9 . . ?
P1 C3 H3A 106.9 . . ?
C4 C3 H3B 106.9 . . ?
P1 C3 H3B 106.9 . . ?
H3A C3 H3B 106.7 . . ?
H4'1 C4' H4'2 109.5 . . ?
H4'1 C4' H4'3 109.5 . . ?
H4'2 C4' H4'3 109.5 . . ?
C6 C5 P1 115.5(16) . . ?
C6 C5 H5A 108.4 . . ?
P1 C5 H5A 108.4 . . ?
C6 C5 H5B 108.4 . . ?
P1 C5 H5B 108.4 . . ?
H5A C5 H5B 107.5 . . ?
C5 C6 H6A 109.5 . . ?
C5 C6 H6B 109.5 . . ?
H6A C6 H6B 109.5 . . ?
C5 C6 H6C 109.5 . . ?
H6A C6 H6C 109.5 . . ?
H6B C6 H6C 109.5 . . ?
C8 C7 P2 117.6(17) . . ?
C8 C7 H7A 107.9 . . ?
P2 C7 H7A 107.9 . . ?
C8 C7 H7B 107.9 . . ?
P2 C7 H7B 107.9 . . ?
H7A C7 H7B 107.2 . . ?
H8'1 C8' H8'2 109.5 . . ?
H8'1 C8' H8'3 109.5 . . ?
H8'2 C8' H8'3 109.5 . . ?
C10 C9 P2 115.4(11) . . ?
C10 C9 H9A 108.4 . . ?
P2 C9 H9A 108.4 . . ?
C10 C9 H9B 108.4 . . ?
P2 C9 H9B 108.4 . . ?
H9A C9 H9B 107.5 . . ?
C9 C10 H10A 109.5 . . ?
C9 C10 H10B 109.5 . . ?
H10A C10 H10B 109.5 . . ?
C9 C10 H10C 109.5 . . ?
H10A C10 H10C 109.5 . . ?
H10B C10 H10C 109.5 . . ?
C12 C11 P2 123.4(18) . . ?
C12 C11 H11A 106.5 . . ?
P2 C11 H11A 106.5 . . ?
C12 C11 H11B 106.5 . . ?
P2 C11 H11B 106.5 . . ?
H11A C11 H11B 106.5 . . ?
H12D C12' H12E 109.5 . . ?
H12D C12' H12F 109.5 . . ?
H12E C12' H12F 109.5 . . ?
C14 C13 C14 150(4) . 4_575 ?
C14 C13 P3 101.0(18) . . ?
C14 C13 P3 101.0(18) 4_575 . ?
C14 C13 H13A 111.6 . . ?
C14 C13 H13A 78.6 4_575 . ?
P3 C13 H13A 111.6 . . ?
C14 C13 H13B 111.6 . . ?
C14 C13 H13B 40.3 4_575 . ?
P3 C13 H13B 111.6 . . ?
H13A C13 H13B 109.4 . . ?
C13 C14 H14A 109.5 . . ?
C13 C14 H14B 109.5 . . ?
H14A C14 H14B 109.5 . . ?
C13 C14 H14C 109.5 . . ?
H14A C14 H14C 109.5 . . ?
H14B C14 H14C 109.5 . . ?
C16 C15 P3 118.3(13) . . ?
C16 C15 H15A 107.7 . . ?
P3 C15 H15A 107.7 . . ?
C16 C15 H15B 107.7 . . ?
P3 C15 H15B 107.7 . . ?
H15A C15 H15B 107.1 . . ?
C15 C16 H16A 109.5 . . ?
C15 C16 H16B 109.5 . . ?
H16A C16 H16B 109.5 . . ?
C15 C16 H16C 109.5 . . ?
H16A C16 H16C 109.5 . . ?
H16B C16 H16C 109.5 . . ?
O C17 Re4 179.4(15) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Re1 P1 2.481(3) . ?
Re1 Se5 2.5167(15) . ?
Re1 Se3 2.5175(17) . ?
Re1 Se2 2.5181(13) . ?
Re1 Se4 2.5193(13) . ?
Re1 Re4 2.6391(8) . ?
Re1 Re3 2.6455(8) . ?
Re1 Re2 2.6476(7) . ?
Re1 Re1 2.6502(10) 4_575 ?
Re2 P2 2.483(3) . ?
Re2 Se2 2.5152(13) . ?
Re2 Se1 2.5171(15) . ?
Re2 Se4 2.5174(13) . ?
Re2 Se6 2.5196(16) . ?
Re2 Re4 2.6384(8) . ?
Re2 Re3 2.6459(8) . ?
Re2 Re2 2.6489(10) 4_575 ?
Re3 P3 2.462(7) . ?
Re3 Se1 2.5070(19) . ?
Re3 Se2 2.5125(13) . ?
Re3 Se2 2.5125(13) 4_575 ?
Re3 Se3 2.513(2) . ?
Re3 Re1 2.6455(8) 4_575 ?
Re3 Re2 2.6459(8) 4_575 ?
Re4 C17 2.05(2) . ?
Re4 Se6 2.5196(17) . ?
Re4 Se5 2.5204(18) . ?
Re4 Se4 2.5226(12) . ?
Re4 Se4 2.5226(12) 4_575 ?
Re4 Re2 2.6385(8) 4_575 ?
Re4 Re1 2.6391(8) 4_575 ?
Se1 Re2 2.5171(15) 4_575 ?
Se3 Re1 2.5175(17) 4_575 ?
Se5 Re1 2.5167(15) 4_575 ?
Se6 Re2 2.5197(15) 4_575 ?
P1 C5 1.81(2) . ?
P1 C3 1.830(17) . ?
P1 C1 1.833(15) . ?
P2 C11 1.812(15) . ?
P2 C7 1.825(15) . ?
P2 C9 1.841(15) . ?
P3 C13 1.80(3) . ?
P3 C15 1.829(19) 4_575 ?
P3 C15 1.829(18) . ?
Sb1 F3 1.788(18) . ?
Sb1 F4 1.815(18) . ?
Sb1 F2 1.822(17) . ?
Sb1 F1 1.831(17) . ?
Sb2 F6 1.790(14) . ?
Sb2 F5 1.791(15) . ?
Sb2 F8 1.814(17) . ?
Sb2 F7 1.817(17) . ?
O C17 1.13(2) . ?
C1 C2 1.514(19) . ?
C1 H1A 0.9800 . ?
C1 H1B 0.9800 . ?
C2 H2A 0.9700 . ?
C2 H2B 0.9700 . ?
C2 H2C 0.9700 . ?
C3 C4 1.36(4) . ?
C3 H3A 0.9800 . ?
C3 H3B 0.9800 . ?
C4 H4A 0.9700 . ?
C4 H4B 0.9700 . ?
C4 H4C 0.9700 . ?
C4' H4'1 0.9700 . ?
C4' H4'2 0.9700 . ?
C4' H4'3 0.9700 . ?
C5 C6 1.40(3) . ?
C5 H5A 0.9800 . ?
C5 H5B 0.9800 . ?
C6 H6A 0.9700 . ?
C6 H6B 0.9700 . ?
C6 H6C 0.9700 . ?
C7 C8 1.35(3) . ?
C7 H7A 0.9800 . ?
C7 H7B 0.9800 . ?
C8 H8A 0.9700 . ?
C8 H8B 0.9700 . ?
C8 H8C 0.9700 . ?
C8' H8'1 0.9700 . ?
C8' H8'2 0.9700 . ?
C8' H8'3 0.9700 . ?
C9 C10 1.542(19) . ?
C9 H9A 0.9800 . ?
C9 H9B 0.9800 . ?
C10 H10A 0.9700 . ?
C10 H10B 0.9700 . ?
C10 H10C 0.9700 . ?
C11 C12 1.44(4) . ?
C11 H11A 0.9800 . ?
C11 H11B 0.9800 . ?
C12 H12A 0.9700 . ?
C12 H12B 0.9700 . ?
C12 H12C 0.9700 . ?
C12' H12D 0.9700 . ?
C12' H12E 0.9700 . ?
C12' H12F 0.9700 . ?
C13 C14 1.545(18) . ?
C13 C14 1.545(18) 4_575 ?
C13 H13A 0.9800 . ?
C13 H13B 0.9800 . ?
C14 H14A 0.9700 . ?
C14 H14B 0.9700 . ?
C14 H14C 0.9700 . ?
C15 C16 1.539(15) . ?
C15 H15A 0.9800 . ?
C15 H15B 0.9800 . ?
C16 H16A 0.9700 . ?
C16 H16B 0.9700 . ?
C16 H16C 0.9700 . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
P1 Re1 Re2 P2 -0.01(18) . . . . ?
Se5 Re1 Re2 P2 -123.20(12) . . . . ?
Se3 Re1 Re2 P2 130.22(12) . . . . ?
Se2 Re1 Re2 P2 59.90(12) . . . . ?
Se4 Re1 Re2 P2 -52.50(12) . . . . ?
Re4 Re1 Re2 P2 -121.92(12) . . . . ?
Re3 Re1 Re2 P2 128.89(12) . . . . ?
Re1 Re1 Re2 P2 -176.45(12) 4_575 . . . ?
P1 Re1 Re2 Se2 -59.91(13) . . . . ?
Se5 Re1 Re2 Se2 176.90(5) . . . . ?
Se3 Re1 Re2 Se2 70.32(5) . . . . ?
Se4 Re1 Re2 Se2 -112.39(5) . . . . ?
Re4 Re1 Re2 Se2 178.18(4) . . . . ?
Re3 Re1 Re2 Se2 68.99(4) . . . . ?
Re1 Re1 Re2 Se2 123.66(4) 4_575 . . . ?
P1 Re1 Re2 Se1 -130.13(12) . . . . ?
Se5 Re1 Re2 Se1 106.68(5) . . . . ?
Se3 Re1 Re2 Se1 0.10(5) . . . . ?
Se2 Re1 Re2 Se1 -70.22(5) . . . . ?
Se4 Re1 Re2 Se1 177.39(5) . . . . ?
Re4 Re1 Re2 Se1 107.96(4) . . . . ?
Re3 Re1 Re2 Se1 -1.23(3) . . . . ?
Re1 Re1 Re2 Se1 53.43(3) 4_575 . . . ?
P1 Re1 Re2 Se4 52.48(12) . . . . ?
Se5 Re1 Re2 Se4 -70.70(5) . . . . ?
Se3 Re1 Re2 Se4 -177.29(5) . . . . ?
Se2 Re1 Re2 Se4 112.39(5) . . . . ?
Re4 Re1 Re2 Se4 -69.43(4) . . . . ?
Re3 Re1 Re2 Se4 -178.62(4) . . . . ?
Re1 Re1 Re2 Se4 -123.95(3) 4_575 . . . ?
P1 Re1 Re2 Se6 123.09(12) . . . . ?
Se5 Re1 Re2 Se6 -0.10(5) . . . . ?
Se3 Re1 Re2 Se6 -106.68(5) . . . . ?
Se2 Re1 Re2 Se6 -177.00(5) . . . . ?
Se4 Re1 Re2 Se6 70.60(5) . . . . ?
Re4 Re1 Re2 Se6 1.18(3) . . . . ?
Re3 Re1 Re2 Se6 -108.01(4) . . . . ?
Re1 Re1 Re2 Se6 -53.35(3) 4_575 . . . ?
P1 Re1 Re2 Re4 121.91(12) . . . . ?
Se5 Re1 Re2 Re4 -1.28(3) . . . . ?
Se3 Re1 Re2 Re4 -107.86(4) . . . . ?
Se2 Re1 Re2 Re4 -178.18(4) . . . . ?
Se4 Re1 Re2 Re4 69.43(4) . . . . ?
Re3 Re1 Re2 Re4 -109.19(2) . . . . ?
Re1 Re1 Re2 Re4 -54.524(14) 4_575 . . . ?
P1 Re1 Re2 Re3 -128.90(12) . . . . ?
Se5 Re1 Re2 Re3 107.92(4) . . . . ?
Se3 Re1 Re2 Re3 1.33(3) . . . . ?
Se2 Re1 Re2 Re3 -68.99(4) . . . . ?
Se4 Re1 Re2 Re3 178.62(4) . . . . ?
Re4 Re1 Re2 Re3 109.19(2) . . . . ?
Re1 Re1 Re2 Re3 54.666(14) 4_575 . . . ?
P1 Re1 Re2 Re2 176.43(12) . . . 4_575 ?
Se5 Re1 Re2 Re2 53.25(3) . . . 4_575 ?
Se3 Re1 Re2 Re2 -53.34(3) . . . 4_575 ?
Se2 Re1 Re2 Re2 -123.66(4) . . . 4_575 ?
Se4 Re1 Re2 Re2 123.95(3) . . . 4_575 ?
Re4 Re1 Re2 Re2 54.524(14) . . . 4_575 ?
Re3 Re1 Re2 Re2 -54.667(14) . . . 4_575 ?
Re1 Re1 Re2 Re2 0.0 4_575 . . 4_575 ?
P1 Re1 Re3 P3 0.5(2) . . . . ?
Se5 Re1 Re3 P3 127.4(2) . . . . ?
Se3 Re1 Re3 P3 57.0(2) . . . . ?
Se2 Re1 Re3 P3 -55.4(2) . . . . ?
Se4 Re1 Re3 P3 -125.8(2) . . . . ?
Re4 Re1 Re3 P3 -179.20(19) . . . . ?
Re2 Re1 Re3 P3 -124.43(19) . . . . ?
Re1 Re1 Re3 P3 126.06(19) 4_575 . . . ?
P1 Re1 Re3 Se1 126.14(13) . . . . ?
Se5 Re1 Re3 Se1 -106.97(6) . . . . ?
Se3 Re1 Re3 Se1 -177.38(5) . . . . ?
Se2 Re1 Re3 Se1 70.30(5) . . . . ?
Se4 Re1 Re3 Se1 -0.09(5) . . . . ?
Re4 Re1 Re3 Se1 -53.53(4) . . . . ?
Re2 Re1 Re3 Se1 1.24(3) . . . . ?
Re1 Re1 Re3 Se1 -108.27(4) 4_575 . . . ?
P1 Re1 Re3 Se2 55.84(13) . . . . ?
Se5 Re1 Re3 Se2 -177.27(6) . . . . ?
Se3 Re1 Re3 Se2 112.32(5) . . . . ?
Se4 Re1 Re3 Se2 -70.39(5) . . . . ?
Re4 Re1 Re3 Se2 -123.83(4) . . . . ?
Re2 Re1 Re3 Se2 -69.06(4) . . . . ?
Re1 Re1 Re3 Se2 -178.57(4) 4_575 . . . ?
P1 Re1 Re3 Se2 -126.98(13) . . . 4_575 ?
Se5 Re1 Re3 Se2 -0.08(7) . . . 4_575 ?
Se3 Re1 Re3 Se2 -70.49(5) . . . 4_575 ?
Se2 Re1 Re3 Se2 177.18(8) . . . 4_575 ?
Se4 Re1 Re3 Se2 106.79(5) . . . 4_575 ?
Re4 Re1 Re3 Se2 53.35(5) . . . 4_575 ?
Re2 Re1 Re3 Se2 108.13(5) . . . 4_575 ?
Re1 Re1 Re3 Se2 -1.39(4) 4_575 . . 4_575 ?
P1 Re1 Re3 Se3 -56.49(13) . . . . ?
Se5 Re1 Re3 Se3 70.41(6) . . . . ?
Se2 Re1 Re3 Se3 -112.32(5) . . . . ?
Se4 Re1 Re3 Se3 177.29(5) . . . . ?
Re4 Re1 Re3 Se3 123.85(4) . . . . ?
Re2 Re1 Re3 Se3 178.62(4) . . . . ?
Re1 Re1 Re3 Se3 69.11(3) 4_575 . . . ?
P1 Re1 Re3 Re1 -125.59(13) . . . 4_575 ?
Se5 Re1 Re3 Re1 1.30(5) . . . 4_575 ?
Se3 Re1 Re3 Re1 -69.11(3) . . . 4_575 ?
Se2 Re1 Re3 Re1 178.57(4) . . . 4_575 ?
Se4 Re1 Re3 Re1 108.18(4) . . . 4_575 ?
Re4 Re1 Re3 Re1 54.74(2) . . . 4_575 ?
Re2 Re1 Re3 Re1 109.514(19) . . . 4_575 ?
P1 Re1 Re3 Re2 124.89(13) . . . . ?
Se5 Re1 Re3 Re2 -108.21(5) . . . . ?
Se3 Re1 Re3 Re2 -178.62(4) . . . . ?
Se2 Re1 Re3 Re2 69.06(4) . . . . ?
Se4 Re1 Re3 Re2 -1.33(4) . . . . ?
Re4 Re1 Re3 Re2 -54.774(19) . . . . ?
Re1 Re1 Re3 Re2 -109.514(19) 4_575 . . . ?
P1 Re1 Re3 Re2 179.65(13) . . . 4_575 ?
Se5 Re1 Re3 Re2 -53.45(5) . . . 4_575 ?
Se3 Re1 Re3 Re2 -123.86(3) . . . 4_575 ?
Se2 Re1 Re3 Re2 123.82(4) . . . 4_575 ?
Se4 Re1 Re3 Re2 53.43(4) . . . 4_575 ?
Re4 Re1 Re3 Re2 -0.02(2) . . . 4_575 ?
Re2 Re1 Re3 Re2 54.76(2) . . . 4_575 ?
Re1 Re1 Re3 Re2 -54.755(14) 4_575 . . 4_575 ?
P2 Re2 Re3 P3 0.6(2) . . . . ?
Se2 Re2 Re3 P3 56.80(19) . . . . ?
Se1 Re2 Re3 P3 -55.30(19) . . . . ?
Se4 Re2 Re3 P3 127.32(19) . . . . ?
Se6 Re2 Re3 P3 -125.86(19) . . . . ?
Re4 Re2 Re3 P3 -179.22(19) . . . . ?
Re1 Re2 Re3 P3 125.99(19) . . . . ?
Re2 Re2 Re3 P3 -124.46(19) 4_575 . . . ?
P2 Re2 Re3 Se1 55.94(13) . . . . ?
Se2 Re2 Re3 Se1 112.10(5) . . . . ?
Se4 Re2 Re3 Se1 -177.38(5) . . . . ?
Se6 Re2 Re3 Se1 -70.57(5) . . . . ?
Re4 Re2 Re3 Se1 -123.92(3) . . . . ?
Re1 Re2 Re3 Se1 -178.72(3) . . . . ?
Re2 Re2 Re3 Se1 -69.17(3) 4_575 . . . ?
P2 Re2 Re3 Se2 -56.16(13) . . . . ?
Se1 Re2 Re3 Se2 -112.10(5) . . . . ?
Se4 Re2 Re3 Se2 70.52(5) . . . . ?
Se6 Re2 Re3 Se2 177.33(6) . . . . ?
Re4 Re2 Re3 Se2 123.98(4) . . . . ?
Re1 Re2 Re3 Se2 69.18(4) . . . . ?
Re2 Re2 Re3 Se2 178.73(4) 4_575 . . . ?
P2 Re2 Re3 Se2 126.33(13) . . . 4_575 ?
Se2 Re2 Re3 Se2 -177.51(7) . . . 4_575 ?
Se1 Re2 Re3 Se2 70.39(5) . . . 4_575 ?
Se4 Re2 Re3 Se2 -106.99(5) . . . 4_575 ?
Se6 Re2 Re3 Se2 -0.17(7) . . . 4_575 ?
Re4 Re2 Re3 Se2 -53.53(5) . . . 4_575 ?
Re1 Re2 Re3 Se2 -108.32(5) . . . 4_575 ?
Re2 Re2 Re3 Se2 1.23(4) 4_575 . . 4_575 ?
P2 Re2 Re3 Se3 -126.68(13) . . . . ?
Se2 Re2 Re3 Se3 -70.52(5) . . . . ?
Se1 Re2 Re3 Se3 177.38(4) . . . . ?
Se4 Re2 Re3 Se3 0.00(5) . . . . ?
Se6 Re2 Re3 Se3 106.81(5) . . . . ?
Re4 Re2 Re3 Se3 53.46(4) . . . . ?
Re1 Re2 Re3 Se3 -1.34(3) . . . . ?
Re2 Re2 Re3 Se3 108.21(4) 4_575 . . . ?
P2 Re2 Re3 Re1 -125.35(13) . . . . ?
Se2 Re2 Re3 Re1 -69.18(4) . . . . ?
Se1 Re2 Re3 Re1 178.72(3) . . . . ?
Se4 Re2 Re3 Re1 1.34(4) . . . . ?
Se6 Re2 Re3 Re1 108.15(5) . . . . ?
Re4 Re2 Re3 Re1 54.795(19) . . . . ?
Re2 Re2 Re3 Re1 109.548(19) 4_575 . . . ?
P2 Re2 Re3 Re1 179.84(12) . . . 4_575 ?
Se2 Re2 Re3 Re1 -123.99(4) . . . 4_575 ?
Se1 Re2 Re3 Re1 123.91(3) . . . 4_575 ?
Se4 Re2 Re3 Re1 -53.48(4) . . . 4_575 ?
Se6 Re2 Re3 Re1 53.34(5) . . . 4_575 ?
Re4 Re2 Re3 Re1 -0.02(2) . . . 4_575 ?
Re1 Re2 Re3 Re1 -54.81(2) . . . 4_575 ?
Re2 Re2 Re3 Re1 54.737(14) 4_575 . . 4_575 ?
P2 Re2 Re3 Re2 125.11(12) . . . 4_575 ?
Se2 Re2 Re3 Re2 -178.73(4) . . . 4_575 ?
Se1 Re2 Re3 Re2 69.17(3) . . . 4_575 ?
Se4 Re2 Re3 Re2 -108.21(4) . . . 4_575 ?
Se6 Re2 Re3 Re2 -1.40(5) . . . 4_575 ?
Re4 Re2 Re3 Re2 -54.75(2) . . . 4_575 ?
Re1 Re2 Re3 Re2 -109.548(19) . . . 4_575 ?
P2 Re2 Re4 C17 0.1(5) . . . . ?
Se2 Re2 Re4 C17 -126.9(4) . . . . ?
Se1 Re2 Re4 C17 127.0(4) . . . . ?
Se4 Re2 Re4 C17 -56.1(4) . . . . ?
Se6 Re2 Re4 C17 56.1(4) . . . . ?
Re3 Re2 Re4 C17 180.0(4) . . . . ?
Re1 Re2 Re4 C17 -125.2(4) . . . . ?
Re2 Re2 Re4 C17 125.2(4) 4_575 . . . ?
P2 Re2 Re4 Se6 -55.94(12) . . . . ?
Se2 Re2 Re4 Se6 177.03(5) . . . . ?
Se1 Re2 Re4 Se6 70.99(6) . . . . ?
Se4 Re2 Re4 Se6 -112.12(5) . . . . ?
Re3 Re2 Re4 Se6 123.93(3) . . . . ?
Re1 Re2 Re4 Se6 178.78(3) . . . . ?
Re2 Re2 Re4 Se6 69.10(3) 4_575 . . . ?
P2 Re2 Re4 Se5 126.56(12) . . . . ?
Se2 Re2 Re4 Se5 -0.48(5) . . . . ?
Se1 Re2 Re4 Se5 -106.51(6) . . . . ?
Se4 Re2 Re4 Se5 70.37(5) . . . . ?
Se6 Re2 Re4 Se5 -177.51(4) . . . . ?
Re3 Re2 Re4 Se5 -53.57(4) . . . . ?
Re1 Re2 Re4 Se5 1.28(3) . . . . ?
Re2 Re2 Re4 Se5 -108.40(4) 4_575 . . . ?
P2 Re2 Re4 Se4 56.19(12) . . . . ?
Se2 Re2 Re4 Se4 -70.85(5) . . . . ?
Se1 Re2 Re4 Se4 -176.88(6) . . . . ?
Se6 Re2 Re4 Se4 112.12(5) . . . . ?
Re3 Re2 Re4 Se4 -123.94(4) . . . . ?
Re1 Re2 Re4 Se4 -69.09(4) . . . . ?
Re2 Re2 Re4 Se4 -178.77(4) 4_575 . . . ?
P2 Re2 Re4 Se4 -126.23(12) . . . 4_575 ?
Se2 Re2 Re4 Se4 106.73(5) . . . 4_575 ?
Se1 Re2 Re4 Se4 0.70(7) . . . 4_575 ?
Se4 Re2 Re4 Se4 177.58(7) . . . 4_575 ?
Se6 Re2 Re4 Se4 -70.29(5) . . . 4_575 ?
Re3 Re2 Re4 Se4 53.64(5) . . . 4_575 ?
Re1 Re2 Re4 Se4 108.49(5) . . . 4_575 ?
Re2 Re2 Re4 Se4 -1.19(4) 4_575 . . 4_575 ?
P2 Re2 Re4 Re2 -125.04(11) . . . 4_575 ?
Se2 Re2 Re4 Re2 107.92(4) . . . 4_575 ?
Se1 Re2 Re4 Re2 1.89(5) . . . 4_575 ?
Se4 Re2 Re4 Re2 178.77(4) . . . 4_575 ?
Se6 Re2 Re4 Re2 -69.10(3) . . . 4_575 ?
Re3 Re2 Re4 Re2 54.83(2) . . . 4_575 ?
Re1 Re2 Re4 Re2 109.680(19) . . . 4_575 ?
P2 Re2 Re4 Re1 125.28(12) . . . . ?
Se2 Re2 Re4 Re1 -1.76(4) . . . . ?
Se1 Re2 Re4 Re1 -107.79(5) . . . . ?
Se4 Re2 Re4 Re1 69.09(4) . . . . ?
Se6 Re2 Re4 Re1 -178.78(3) . . . . ?
Re3 Re2 Re4 Re1 -54.850(19) . . . . ?
Re2 Re2 Re4 Re1 -109.680(19) 4_575 . . . ?
P2 Re2 Re4 Re1 -179.85(11) . . . 4_575 ?
Se2 Re2 Re4 Re1 53.11(4) . . . 4_575 ?
Se1 Re2 Re4 Re1 -52.92(5) . . . 4_575 ?
Se4 Re2 Re4 Re1 123.96(4) . . . 4_575 ?
Se6 Re2 Re4 Re1 -123.92(3) . . . 4_575 ?
Re3 Re2 Re4 Re1 0.02(2) . . . 4_575 ?
Re1 Re2 Re4 Re1 54.87(2) . . . 4_575 ?
Re2 Re2 Re4 Re1 -54.814(14) 4_575 . . 4_575 ?
P1 Re1 Re4 C17 0.3(5) . . . . ?
Se5 Re1 Re4 C17 -56.2(4) . . . . ?
Se3 Re1 Re4 C17 -126.9(4) . . . . ?
Se2 Re1 Re4 C17 126.9(4) . . . . ?
Se4 Re1 Re4 C17 56.1(4) . . . . ?
Re3 Re1 Re4 C17 180.0(4) . . . . ?
Re2 Re1 Re4 C17 125.1(4) . . . . ?
Re1 Re1 Re4 C17 -125.2(4) 4_575 . . . ?
P1 Re1 Re4 Se6 -126.01(12) . . . . ?
Se5 Re1 Re4 Se6 177.50(4) . . . . ?
Se3 Re1 Re4 Se6 106.80(6) . . . . ?
Se2 Re1 Re4 Se6 0.57(5) . . . . ?
Se4 Re1 Re4 Se6 -70.21(4) . . . . ?
Re3 Re1 Re4 Se6 53.68(4) . . . . ?
Re2 Re1 Re4 Se6 -1.18(3) . . . . ?
Re1 Re1 Re4 Se6 108.49(3) 4_575 . . . ?
P1 Re1 Re4 Se5 56.48(12) . . . . ?
Se3 Re1 Re4 Se5 -70.70(6) . . . . ?
Se2 Re1 Re4 Se5 -176.93(5) . . . . ?
Se4 Re1 Re4 Se5 112.29(5) . . . . ?
Re3 Re1 Re4 Se5 -123.82(4) . . . . ?
Re2 Re1 Re4 Se5 -178.68(3) . . . . ?
Re1 Re1 Re4 Se5 -69.02(3) 4_575 . . . ?
P1 Re1 Re4 Se4 -55.81(12) . . . . ?
Se5 Re1 Re4 Se4 -112.29(5) . . . . ?
Se3 Re1 Re4 Se4 177.01(6) . . . . ?
Se2 Re1 Re4 Se4 70.78(5) . . . . ?
Re3 Re1 Re4 Se4 123.89(4) . . . . ?
Re2 Re1 Re4 Se4 69.03(4) . . . . ?
Re1 Re1 Re4 Se4 178.69(4) 4_575 . . . ?
P1 Re1 Re4 Se4 126.77(12) . . . 4_575 ?
Se5 Re1 Re4 Se4 70.28(5) . . . 4_575 ?
Se3 Re1 Re4 Se4 -0.42(7) . . . 4_575 ?
Se2 Re1 Re4 Se4 -106.65(5) . . . 4_575 ?
Se4 Re1 Re4 Se4 -177.43(7) . . . 4_575 ?
Re3 Re1 Re4 Se4 -53.54(4) . . . 4_575 ?
Re2 Re1 Re4 Se4 -108.40(4) . . . 4_575 ?
Re1 Re1 Re4 Se4 1.27(4) 4_575 . . 4_575 ?
P1 Re1 Re4 Re2 -124.83(12) . . . . ?
Se5 Re1 Re4 Re2 178.68(3) . . . . ?
Se3 Re1 Re4 Re2 107.98(5) . . . . ?
Se2 Re1 Re4 Re2 1.75(4) . . . . ?
Se4 Re1 Re4 Re2 -69.03(4) . . . . ?
Re3 Re1 Re4 Re2 54.862(19) . . . . ?
Re1 Re1 Re4 Re2 109.668(18) 4_575 . . . ?
P1 Re1 Re4 Re2 -179.68(12) . . . 4_575 ?
Se5 Re1 Re4 Re2 123.84(3) . . . 4_575 ?
Se3 Re1 Re4 Re2 53.13(5) . . . 4_575 ?
Se2 Re1 Re4 Re2 -53.09(4) . . . 4_575 ?
Se4 Re1 Re4 Re2 -123.87(4) . . . 4_575 ?
Re3 Re1 Re4 Re2 0.02(2) . . . 4_575 ?
Re2 Re1 Re4 Re2 -54.85(2) . . . 4_575 ?
Re1 Re1 Re4 Re2 54.820(14) 4_575 . . 4_575 ?
P1 Re1 Re4 Re1 125.50(12) . . . 4_575 ?
Se5 Re1 Re4 Re1 69.02(3) . . . 4_575 ?
Se3 Re1 Re4 Re1 -1.69(5) . . . 4_575 ?
Se2 Re1 Re4 Re1 -107.91(4) . . . 4_575 ?
Se4 Re1 Re4 Re1 -178.69(4) . . . 4_575 ?
Re3 Re1 Re4 Re1 -54.81(2) . . . 4_575 ?
Re2 Re1 Re4 Re1 -109.668(18) . . . 4_575 ?
P3 Re3 Se1 Re2 144.01(2) . . . . ?
Se2 Re3 Se1 Re2 52.03(4) . . . . ?
Se2 Re3 Se1 Re2 -124.01(4) 4_575 . . . ?
Se3 Re3 Se1 Re2 -35.99(2) . . . . ?
Re1 Re3 Se1 Re2 -1.26(3) . . . . ?
Re1 Re3 Se1 Re2 -70.72(3) 4_575 . . . ?
Re2 Re3 Se1 Re2 -71.98(4) 4_575 . . . ?
P3 Re3 Se1 Re2 -144.01(2) . . . 4_575 ?
Se2 Re3 Se1 Re2 124.01(4) . . . 4_575 ?
Se2 Re3 Se1 Re2 -52.02(4) 4_575 . . 4_575 ?
Se3 Re3 Se1 Re2 35.99(2) . . . 4_575 ?
Re1 Re3 Se1 Re2 70.72(3) . . . 4_575 ?
Re1 Re3 Se1 Re2 1.27(3) 4_575 . . 4_575 ?
Re2 Re3 Se1 Re2 71.98(4) . . . 4_575 ?
P2 Re2 Se1 Re3 -145.93(9) . . . . ?
Se2 Re2 Se1 Re3 -51.95(4) . . . . ?
Se4 Re2 Se1 Re3 32.2(7) . . . . ?
Se6 Re2 Se1 Re3 123.82(4) . . . . ?
Re4 Re2 Se1 Re3 70.15(4) . . . . ?
Re1 Re2 Se1 Re3 1.26(3) . . . . ?
Re2 Re2 Se1 Re3 72.08(3) 4_575 . . . ?
P2 Re2 Se1 Re2 141.99(9) . . . 4_575 ?
Se2 Re2 Se1 Re2 -124.02(4) . . . 4_575 ?
Se4 Re2 Se1 Re2 -39.9(7) . . . 4_575 ?
Se6 Re2 Se1 Re2 51.74(4) . . . 4_575 ?
Re4 Re2 Se1 Re2 -1.92(6) . . . 4_575 ?
Re3 Re2 Se1 Re2 -72.08(3) . . . 4_575 ?
Re1 Re2 Se1 Re2 -70.82(4) . . . 4_575 ?
P3 Re3 Se2 Re2 -143.24(19) . . . . ?
Se1 Re3 Se2 Re2 -52.11(5) . . . . ?
Se2 Re3 Se2 Re2 33.5(10) 4_575 . . . ?
Se3 Re3 Se2 Re2 123.97(5) . . . . ?
Re1 Re3 Se2 Re2 72.01(3) . . . . ?
Re1 Re3 Se2 Re2 70.60(4) 4_575 . . . ?
Re2 Re3 Se2 Re2 1.25(4) 4_575 . . . ?
P3 Re3 Se2 Re1 144.74(19) . . . . ?
Se1 Re3 Se2 Re1 -124.12(5) . . . . ?
Se2 Re3 Se2 Re1 -38.5(10) 4_575 . . . ?
Se3 Re3 Se2 Re1 51.96(5) . . . . ?
Re1 Re3 Se2 Re1 -1.41(4) 4_575 . . . ?
Re2 Re3 Se2 Re1 -72.01(3) . . . . ?
Re2 Re3 Se2 Re1 -70.76(4) 4_575 . . . ?
P2 Re2 Se2 Re3 145.83(9) . . . . ?
Se1 Re2 Se2 Re3 51.82(4) . . . . ?
Se4 Re2 Se2 Re3 -123.88(4) . . . . ?
Se6 Re2 Se2 Re3 -33.6(7) . . . . ?
Re4 Re2 Se2 Re3 -70.20(4) . . . . ?
Re1 Re2 Se2 Re3 -71.98(3) . . . . ?
Re2 Re2 Se2 Re3 -1.25(4) 4_575 . . . ?
P2 Re2 Se2 Re1 -142.19(8) . . . . ?
Se1 Re2 Se2 Re1 123.80(4) . . . . ?
Se4 Re2 Se2 Re1 -51.89(4) . . . . ?
Se6 Re2 Se2 Re1 38.4(7) . . . . ?
Re4 Re2 Se2 Re1 1.79(4) . . . . ?
Re3 Re2 Se2 Re1 71.98(3) . . . . ?
Re2 Re2 Se2 Re1 70.74(3) 4_575 . . . ?
P1 Re1 Se2 Re3 -145.99(9) . . . . ?
Se5 Re1 Se2 Re3 33.5(7) . . . . ?
Se3 Re1 Se2 Re3 -51.82(4) . . . . ?
Se4 Re1 Se2 Re3 123.90(4) . . . . ?
Re4 Re1 Se2 Re3 70.28(4) . . . . ?
Re2 Re1 Se2 Re3 72.06(3) . . . . ?
Re1 Re1 Se2 Re3 1.40(4) 4_575 . . . ?
P1 Re1 Se2 Re2 141.95(9) . . . . ?
Se5 Re1 Se2 Re2 -38.6(7) . . . . ?
Se3 Re1 Se2 Re2 -123.88(4) . . . . ?
Se4 Re1 Se2 Re2 51.84(4) . . . . ?
Re4 Re1 Se2 Re2 -1.78(4) . . . . ?
Re3 Re1 Se2 Re2 -72.06(3) . . . . ?
Re1 Re1 Se2 Re2 -70.66(3) 4_575 . . . ?
P3 Re3 Se3 Re1 143.96(2) . . . 4_575 ?
Se1 Re3 Se3 Re1 -36.04(2) . . . 4_575 ?
Se2 Re3 Se3 Re1 -124.05(4) . . . 4_575 ?
Se2 Re3 Se3 Re1 51.97(4) 4_575 . . 4_575 ?
Re1 Re3 Se3 Re1 -72.08(4) . . . 4_575 ?
Re2 Re3 Se3 Re1 -70.72(3) . . . 4_575 ?
Re2 Re3 Se3 Re1 -1.36(3) 4_575 . . 4_575 ?
P3 Re3 Se3 Re1 -143.96(2) . . . . ?
Se1 Re3 Se3 Re1 36.04(2) . . . . ?
Se2 Re3 Se3 Re1 -51.97(4) . . . . ?
Se2 Re3 Se3 Re1 124.05(4) 4_575 . . . ?
Re1 Re3 Se3 Re1 72.08(4) 4_575 . . . ?
Re2 Re3 Se3 Re1 1.36(3) . . . . ?
Re2 Re3 Se3 Re1 70.72(3) 4_575 . . . ?
P1 Re1 Se3 Re3 145.68(9) . . . . ?
Se5 Re1 Se3 Re3 -123.84(4) . . . . ?
Se2 Re1 Se3 Re3 51.81(4) . . . . ?
Se4 Re1 Se3 Re3 -33.8(7) . . . . ?
Re4 Re1 Se3 Re3 -70.28(4) . . . . ?
Re2 Re1 Se3 Re3 -1.36(4) . . . . ?
Re1 Re1 Se3 Re3 -71.99(3) 4_575 . . . ?
P1 Re1 Se3 Re1 -142.33(9) . . . 4_575 ?
Se5 Re1 Se3 Re1 -51.85(4) . . . 4_575 ?
Se2 Re1 Se3 Re1 123.80(4) . . . 4_575 ?
Se4 Re1 Se3 Re1 38.2(7) . . . 4_575 ?
Re4 Re1 Se3 Re1 1.72(6) . . . 4_575 ?
Re3 Re1 Se3 Re1 71.99(3) . . . 4_575 ?
Re2 Re1 Se3 Re1 70.64(4) . . . 4_575 ?
P2 Re2 Se4 Re1 145.89(9) . . . . ?
Se2 Re2 Se4 Re1 51.89(4) . . . . ?
Se1 Re2 Se4 Re1 -32.3(7) . . . . ?
Se6 Re2 Se4 Re1 -123.86(4) . . . . ?
Re4 Re2 Se4 Re1 -71.75(3) . . . . ?
Re3 Re2 Se4 Re1 -1.36(4) . . . . ?
Re2 Re2 Se4 Re1 -70.54(3) 4_575 . . . ?
P2 Re2 Se4 Re4 -142.36(9) . . . . ?
Se2 Re2 Se4 Re4 123.63(4) . . . . ?
Se1 Re2 Se4 Re4 39.5(7) . . . . ?
Se6 Re2 Se4 Re4 -52.12(4) . . . . ?
Re3 Re2 Se4 Re4 70.39(4) . . . . ?
Re1 Re2 Se4 Re4 71.75(3) . . . . ?
Re2 Re2 Se4 Re4 1.21(4) 4_575 . . . ?
P1 Re1 Se4 Re2 -145.68(9) . . . . ?
Se5 Re1 Se4 Re2 123.83(4) . . . . ?
Se3 Re1 Se4 Re2 33.8(7) . . . . ?
Se2 Re1 Se4 Re2 -51.80(4) . . . . ?
Re4 Re1 Se4 Re2 71.76(3) . . . . ?
Re3 Re1 Se4 Re2 1.36(4) . . . . ?
Re1 Re1 Se4 Re2 70.48(3) 4_575 . . . ?
P1 Re1 Se4 Re4 142.55(9) . . . . ?
Se5 Re1 Se4 Re4 52.06(4) . . . . ?
Se3 Re1 Se4 Re4 -37.9(7) . . . . ?
Se2 Re1 Se4 Re4 -123.57(4) . . . . ?
Re3 Re1 Se4 Re4 -70.40(4) . . . . ?
Re2 Re1 Se4 Re4 -71.76(3) . . . . ?
Re1 Re1 Se4 Re4 -1.28(4) 4_575 . . . ?
C17 Re4 Se4 Re2 143.9(4) . . . . ?
Se6 Re4 Se4 Re2 52.12(5) . . . . ?
Se5 Re4 Se4 Re2 -124.17(5) . . . . ?
Se4 Re4 Se4 Re2 -34.8(10) 4_575 . . . ?
Re2 Re4 Se4 Re2 -1.21(4) 4_575 . . . ?
Re1 Re4 Se4 Re2 -72.21(3) . . . . ?
Re1 Re4 Se4 Re2 -70.92(4) 4_575 . . . ?
C17 Re4 Se4 Re1 -143.9(4) . . . . ?
Se6 Re4 Se4 Re1 124.33(5) . . . . ?
Se5 Re4 Se4 Re1 -51.96(5) . . . . ?
Se4 Re4 Se4 Re1 37.4(10) 4_575 . . . ?
Re2 Re4 Se4 Re1 72.21(3) . . . . ?
Re2 Re4 Se4 Re1 71.00(4) 4_575 . . . ?
Re1 Re4 Se4 Re1 1.29(4) 4_575 . . . ?
P1 Re1 Se5 Re1 146.03(9) . . . 4_575 ?
Se3 Re1 Se5 Re1 51.85(4) . . . 4_575 ?
Se2 Re1 Se5 Re1 -33.4(7) . . . 4_575 ?
Se4 Re1 Se5 Re1 -123.85(4) . . . 4_575 ?
Re4 Re1 Se5 Re1 -71.77(2) . . . 4_575 ?
Re3 Re1 Se5 Re1 -1.33(5) . . . 4_575 ?
Re2 Re1 Se5 Re1 -70.47(4) . . . 4_575 ?
P1 Re1 Se5 Re4 -142.20(9) . . . . ?
Se3 Re1 Se5 Re4 123.62(4) . . . . ?
Se2 Re1 Se5 Re4 38.3(7) . . . . ?
Se4 Re1 Se5 Re4 -52.08(3) . . . . ?
Re3 Re1 Se5 Re4 70.44(4) . . . . ?
Re2 Re1 Se5 Re4 1.29(3) . . . . ?
Re1 Re1 Se5 Re4 71.77(2) 4_575 . . . ?
C17 Re4 Se5 Re1 143.85(2) . . . . ?
Se6 Re4 Se5 Re1 -36.15(2) . . . . ?
Se4 Re4 Se5 Re1 51.99(4) . . . . ?
Se4 Re4 Se5 Re1 -124.29(4) 4_575 . . . ?
Re2 Re4 Se5 Re1 -1.30(3) . . . . ?
Re2 Re4 Se5 Re1 -71.00(3) 4_575 . . . ?
Re1 Re4 Se5 Re1 -72.30(4) 4_575 . . . ?
C17 Re4 Se5 Re1 -143.85(2) . . . 4_575 ?
Se6 Re4 Se5 Re1 36.15(2) . . . 4_575 ?
Se4 Re4 Se5 Re1 124.29(4) . . . 4_575 ?
Se4 Re4 Se5 Re1 -51.99(4) 4_575 . . 4_575 ?
Re2 Re4 Se5 Re1 71.00(3) . . . 4_575 ?
Re2 Re4 Se5 Re1 1.30(3) 4_575 . . 4_575 ?
Re1 Re4 Se5 Re1 72.30(4) . . . 4_575 ?
C17 Re4 Se6 Re2 -143.90(2) . . . . ?
Se5 Re4 Se6 Re2 36.10(2) . . . . ?
Se4 Re4 Se6 Re2 -52.04(4) . . . . ?
Se4 Re4 Se6 Re2 124.24(4) 4_575 . . . ?
Re2 Re4 Se6 Re2 72.20(4) 4_575 . . . ?
Re1 Re4 Se6 Re2 1.20(3) . . . . ?
Re1 Re4 Se6 Re2 71.00(3) 4_575 . . . ?
C17 Re4 Se6 Re2 143.90(2) . . . 4_575 ?
Se5 Re4 Se6 Re2 -36.10(2) . . . 4_575 ?
Se4 Re4 Se6 Re2 -124.24(4) . . . 4_575 ?
Se4 Re4 Se6 Re2 52.04(4) 4_575 . . 4_575 ?
Re2 Re4 Se6 Re2 -72.20(4) . . . 4_575 ?
Re1 Re4 Se6 Re2 -71.00(3) . . . 4_575 ?
Re1 Re4 Se6 Re2 -1.20(3) 4_575 . . 4_575 ?
P2 Re2 Se6 Re4 142.49(8) . . . . ?
Se2 Re2 Se6 Re4 -38.1(7) . . . . ?
Se1 Re2 Se6 Re4 -123.48(4) . . . . ?
Se4 Re2 Se6 Re4 52.20(3) . . . . ?
Re3 Re2 Se6 Re4 -70.34(4) . . . . ?
Re1 Re2 Se6 Re4 -1.20(3) . . . . ?
Re2 Re2 Se6 Re4 -71.77(2) 4_575 . . . ?
P2 Re2 Se6 Re2 -145.74(8) . . . 4_575 ?
Se2 Re2 Se6 Re2 33.7(7) . . . 4_575 ?
Se1 Re2 Se6 Re2 -51.71(4) . . . 4_575 ?
Se4 Re2 Se6 Re2 123.96(4) . . . 4_575 ?
Re4 Re2 Se6 Re2 71.77(2) . . . 4_575 ?
Re3 Re2 Se6 Re2 1.43(5) . . . 4_575 ?
Re1 Re2 Se6 Re2 70.57(4) . . . 4_575 ?
Se5 Re1 P1 C5 -74.3(8) . . . . ?
Se3 Re1 P1 C5 15.6(8) . . . . ?
Se2 Re1 P1 C5 105.6(8) . . . . ?
Se4 Re1 P1 C5 -164.5(8) . . . . ?
Re4 Re1 P1 C5 -119.6(8) . . . . ?
Re3 Re1 P1 C5 60.8(8) . . . . ?
Re2 Re1 P1 C5 153.1(8) . . . . ?
Re1 Re1 P1 C5 -31.9(8) 4_575 . . . ?
Se5 Re1 P1 C3 164.4(7) . . . . ?
Se3 Re1 P1 C3 -105.7(7) . . . . ?
Se2 Re1 P1 C3 -15.7(7) . . . . ?
Se4 Re1 P1 C3 74.2(7) . . . . ?
Re4 Re1 P1 C3 119.1(7) . . . . ?
Re3 Re1 P1 C3 -60.5(7) . . . . ?
Re2 Re1 P1 C3 31.8(7) . . . . ?
Re1 Re1 P1 C3 -153.3(7) 4_575 . . . ?
Se5 Re1 P1 C1 43.9(7) . . . . ?
Se3 Re1 P1 C1 133.8(7) . . . . ?
Se2 Re1 P1 C1 -136.2(7) . . . . ?
Se4 Re1 P1 C1 -46.3(7) . . . . ?
Re4 Re1 P1 C1 -1.4(7) . . . . ?
Re3 Re1 P1 C1 179.0(7) . . . . ?
Re2 Re1 P1 C1 -88.7(7) . . . . ?
Re1 Re1 P1 C1 86.2(7) 4_575 . . . ?
Se2 Re2 P2 C11 -104.2(7) . . . . ?
Se1 Re2 P2 C11 -14.3(7) . . . . ?
Se4 Re2 P2 C11 165.8(7) . . . . ?
Se6 Re2 P2 C11 75.8(7) . . . . ?
Re4 Re2 P2 C11 120.7(7) . . . . ?
Re3 Re2 P2 C11 -59.1(7) . . . . ?
Re1 Re2 P2 C11 -151.7(6) . . . . ?
Re2 Re2 P2 C11 33.3(7) 4_575 . . . ?
Se2 Re2 P2 C7 17.2(6) . . . . ?
Se1 Re2 P2 C7 107.1(6) . . . . ?
Se4 Re2 P2 C7 -72.8(6) . . . . ?
Se6 Re2 P2 C7 -162.8(6) . . . . ?
Re4 Re2 P2 C7 -117.9(6) . . . . ?
Re3 Re2 P2 C7 62.3(6) . . . . ?
Re1 Re2 P2 C7 -30.3(6) . . . . ?
Re2 Re2 P2 C7 154.7(6) 4_575 . . . ?
Se2 Re2 P2 C9 135.5(7) . . . . ?
Se1 Re2 P2 C9 -134.7(7) . . . . ?
Se4 Re2 P2 C9 45.5(7) . . . . ?
Se6 Re2 P2 C9 -44.5(7) . . . . ?
Re4 Re2 P2 C9 0.4(7) . . . . ?
Re3 Re2 P2 C9 -179.4(6) . . . . ?
Re1 Re2 P2 C9 87.9(7) . . . . ?
Re2 Re2 P2 C9 -87.0(7) 4_575 . . . ?
Se1 Re3 P3 C13 180.000(8) . . . . ?
Se2 Re3 P3 C13 -90.11(3) . . . . ?
Se2 Re3 P3 C13 90.11(3) 4_575 . . . ?
Se3 Re3 P3 C13 0.000(8) . . . . ?
Re1 Re3 P3 C13 -45.60(14) . . . . ?
Re1 Re3 P3 C13 45.60(14) 4_575 . . . ?
Re2 Re3 P3 C13 -135.54(13) . . . . ?
Re2 Re3 P3 C13 135.54(13) 4_575 . . . ?
Se1 Re3 P3 C15 62.6(8) . . . 4_575 ?
Se2 Re3 P3 C15 152.5(8) . . . 4_575 ?
Se2 Re3 P3 C15 -27.3(8) 4_575 . . 4_575 ?
Se3 Re3 P3 C15 -117.4(8) . . . 4_575 ?
Re1 Re3 P3 C15 -163.0(7) . . . 4_575 ?
Re1 Re3 P3 C15 -71.8(8) 4_575 . . 4_575 ?
Re2 Re3 P3 C15 107.1(7) . . . 4_575 ?
Re2 Re3 P3 C15 18.1(8) 4_575 . . 4_575 ?
Se1 Re3 P3 C15 -62.6(8) . . . . ?
Se2 Re3 P3 C15 27.3(8) . . . . ?
Se2 Re3 P3 C15 -152.5(8) 4_575 . . . ?
Se3 Re3 P3 C15 117.4(8) . . . . ?
Re1 Re3 P3 C15 71.8(8) . . . . ?
Re1 Re3 P3 C15 163.0(7) 4_575 . . . ?
Re2 Re3 P3 C15 -18.1(8) . . . . ?
Re2 Re3 P3 C15 -107.1(7) 4_575 . . . ?
C5 P1 C1 C2 -54.6(16) . . . . ?
C3 P1 C1 C2 52.8(16) . . . . ?
Re1 P1 C1 C2 179.5(12) . . . . ?
C5 P1 C3 C4 -51(2) . . . . ?
C1 P1 C3 C4 -159(2) . . . . ?
Re1 P1 C3 C4 77(2) . . . . ?
C3 P1 C5 C6 -169.5(17) . . . . ?
C1 P1 C5 C6 -60.3(19) . . . . ?
Re1 P1 C5 C6 62.3(19) . . . . ?
C11 P2 C7 C8 51(2) . . . . ?
C9 P2 C7 C8 160.3(19) . . . . ?
Re2 P2 C7 C8 -77(2) . . . . ?
C11 P2 C9 C10 53.1(15) . . . . ?
C7 P2 C9 C10 -55.1(15) . . . . ?
Re2 P2 C9 C10 179.7(11) . . . . ?
C7 P2 C11 C12 -53(2) . . . . ?
C9 P2 C11 C12 -162(2) . . . . ?
Re2 P2 C11 C12 75(2) . . . . ?
C15 P3 C13 C14 -154.0(19) 4_575 . . . ?
C15 P3 C13 C14 -47(2) . . . . ?
Re3 P3 C13 C14 79.7(19) . . . . ?
C15 P3 C13 C14 47(2) 4_575 . . 4_575 ?
C15 P3 C13 C14 154.0(19) . . . 4_575 ?
Re3 P3 C13 C14 -79.7(19) . . . 4_575 ?
C13 P3 C15 C16 -77.0(17) . . . . ?
C15 P3 C15 C16 25(2) 4_575 . . . ?
Re3 P3 C15 C16 156.0(13) . . . . ?
Se6 Re4 C17 O 180.0(4) . . . . ?
Se5 Re4 C17 O 0.0(4) . . . . ?
Se4 Re4 C17 O 90.0(4) . . . . ?
Se4 Re4 C17 O -90.0(4) 4_575 . . . ?
Re2 Re4 C17 O 135.0(6) . . . . ?
Re2 Re4 C17 O -135.0(5) 4_575 . . . ?
Re1 Re4 C17 O 45.0(6) . . . . ?
Re1 Re4 C17 O -45.0(5) 4_575 . . . ?
