#------------------------------------------------------------------------------
#$Date: 2016-03-25 10:24:34 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179749 $
#$URL: svn://www.crystallography.net/cod/cif/7/00/45/7004554.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7004554
loop_
_publ_author_name
'Jura, Marek'
'Levason, William'
'Reid, Gillian'
'Webster, Michael'
_publ_section_title
;
 Preparation and properties of sterically demanding and chiral
 distibine ligands
;
_journal_issue                   42
_journal_name_full               'Dalton Transactions'
_journal_page_first              5774
_journal_page_last               5782
_journal_paper_doi               10.1039/b808493a
_journal_year                    2008
_chemical_formula_moiety         'C28 H36 O4 Sb4'
_chemical_formula_structural     '(C14 H18 Sb2)2 O4'
_chemical_formula_sum            'C28 H36 O4 Sb4'
_chemical_formula_weight         923.57
_chemical_name_common
bis((1,8-bis(dimethylstibino)naphthalene)di(mu!3$-oxido))
_chemical_name_systematic
;
bis((1,8-bis(dimethylstibino)naphthalene)di(μ₃-oxido))
;
_space_group_IT_number           62
_symmetry_cell_setting           orthorhombic
_symmetry_Int_Tables_number      62
_symmetry_space_group_name_Hall  '-P 2ac 2n'
_symmetry_space_group_name_H-M   'P n m a'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_date             2008-06-20
_audit_creation_method           'SHELXL-97 + hand edit'
_audit_update_record
' 2008-06-20 revised (improved) disorder treatment of 1 naphthyl group.'
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   20.032(2)
_cell_length_b                   13.1268(10)
_cell_length_c                   10.7375(10)
_cell_measurement_reflns_used    3592
_cell_measurement_temperature    120(2)
_cell_measurement_theta_max      27.48
_cell_measurement_theta_min      2.91
_cell_volume                     2823.5(4)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      120(2)
_diffrn_measured_fraction_theta_full 0.995
_diffrn_measured_fraction_theta_max 0.995
_diffrn_measurement_device_type
'Bruker-Nonius 95mm CCD camera on κ-goniostat'
_diffrn_measurement_method       'φ & ω scans'
_diffrn_radiation_monochromator  '10cm confocal mirrors'
_diffrn_radiation_source         'Bruker-Nonius FR591 rotating anode'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0327
_diffrn_reflns_av_sigmaI/netI    0.0233
_diffrn_reflns_limit_h_max       26
_diffrn_reflns_limit_h_min       -22
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_k_min       -16
_diffrn_reflns_limit_l_max       13
_diffrn_reflns_limit_l_min       -13
_diffrn_reflns_number            23985
_diffrn_reflns_theta_full        27.50
_diffrn_reflns_theta_max         27.50
_diffrn_reflns_theta_min         3.59
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    3.819
_exptl_absorpt_correction_T_max  1.0000
_exptl_absorpt_correction_T_min  0.6765
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
'G.M. Sheldrick, (2007). SADABS. Version 2007/2. Bruker AXS Inc.'
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    2.173
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             1760
_exptl_crystal_size_max          0.11
_exptl_crystal_size_mid          0.06
_exptl_crystal_size_min          0.03
_refine_diff_density_max         0.875
_refine_diff_density_min         -1.391
_refine_diff_density_rms         0.161
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.376
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     233
_refine_ls_number_reflns         3358
_refine_ls_number_restraints     11
_refine_ls_restrained_S_all      1.375
_refine_ls_R_factor_all          0.0537
_refine_ls_R_factor_gt           0.0494
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0000P)²+26.4000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1035
_refine_ls_wR_factor_ref         0.1053
_reflns_number_gt                3114
_reflns_number_total             3358
_reflns_threshold_expression     I>2sigma(I)
_cod_data_source_file            b808493a.txt
_cod_data_source_block           07mj004_[C28H36O4Sb4]
_cod_database_code               7004554
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, -y, z+1/2'
'-x, y+1/2, -z'
'x+1/2, -y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, y, -z-1/2'
'x, -y-1/2, z'
'-x-1/2, y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Sb1 Sb 0.33397(3) 0.2500 0.78926(6) 0.02872(16) Uani 1 2 d S . .
Sb2 Sb 0.20132(3) 0.2500 0.61873(6) 0.03587(18) Uani 1 2 d S . .
Sb3 Sb 0.33516(3) 0.12612(4) 0.51846(5) 0.04081(16) Uani 1 1 d . . .
O1 O 0.2756(2) 0.1484(4) 0.6802(4) 0.0321(10) Uani 1 1 d . . .
O2 O 0.2716(3) 0.2500 0.4726(6) 0.0303(15) Uani 1 2 d S . .
O3 O 0.3809(3) 0.2500 0.6133(6) 0.0350(16) Uani 1 2 d S . .
C1 C 0.2589(5) 0.2500 0.9329(10) 0.037(2) Uani 1 2 d S . .
C2 C 0.2862(5) 0.2500 1.0521(10) 0.042(3) Uani 1 2 d S . .
H2 H 0.3334 0.2500 1.0614 0.050 Uiso 1 2 calc SR . .
C3 C 0.2457(6) 0.2500 1.1593(11) 0.045(3) Uani 1 2 d S . .
H3 H 0.2654 0.2500 1.2397 0.053 Uiso 1 2 calc SR . .
C4 C 0.1786(6) 0.2500 1.1472(11) 0.046(3) Uani 1 2 d S . .
H4 H 0.1515 0.2500 1.2198 0.055 Uiso 1 2 calc SR . .
C5 C 0.1476(5) 0.2500 1.0284(10) 0.039(2) Uani 1 2 d S . .
C6 C 0.0777(5) 0.2500 1.0180(12) 0.042(3) Uani 1 2 d S . .
H6 H 0.0512 0.2500 1.0914 0.051 Uiso 1 2 calc SR . .
C7 C 0.0478(5) 0.2500 0.9062(12) 0.047(3) Uani 1 2 d S . .
H7 H 0.0004 0.2500 0.9012 0.057 Uiso 1 2 calc SR . .
C8 C 0.0859(5) 0.2500 0.7966(11) 0.042(3) Uani 1 2 d S . .
H8 H 0.0637 0.2500 0.7185 0.050 Uiso 1 2 calc SR . .
C9 C 0.1555(5) 0.2500 0.7991(10) 0.039(2) Uani 1 2 d S . .
C10 C 0.1890(5) 0.2500 0.9186(10) 0.033(2) Uani 1 2 d S . .
C11 C 0.3950(4) 0.1317(6) 0.8621(7) 0.0390(17) Uani 1 1 d . . .
H11A H 0.3725 0.0661 0.8511 0.058 Uiso 1 1 calc R . .
H11B H 0.4028 0.1437 0.9510 0.058 Uiso 1 1 calc R . .
H11C H 0.4378 0.1309 0.8179 0.058 Uiso 1 1 calc R . .
C12 C 0.1427(4) 0.1330(9) 0.5389(9) 0.063(3) Uani 1 1 d . . .
H12A H 0.1456 0.1369 0.4480 0.095 Uiso 1 1 calc R . .
H12B H 0.0962 0.1412 0.5649 0.095 Uiso 1 1 calc R . .
H12C H 0.1593 0.0666 0.5670 0.095 Uiso 1 1 calc R . .
C13A C 0.3929(8) 0.1330(10) 0.3623(17) 0.025(4) Uani 0.50 1 d PD . -1
C14A C 0.4112(9) 0.0390(14) 0.3148(17) 0.048(4) Uani 0.50 1 d PD . -1
H14A H 0.3943 -0.0220 0.3505 0.058 Uiso 0.50 1 calc PR . -1
C15A C 0.4548(9) 0.0351(17) 0.2138(17) 0.055(5) Uani 0.50 1 d PD . -1
H15A H 0.4673 -0.0298 0.1823 0.067 Uiso 0.50 1 calc PR . -1
C16A C 0.4810(15) 0.1212(17) 0.157(2) 0.049(7) Uani 0.50 1 d PD . -1
H16A H 0.5100 0.1165 0.0871 0.059 Uiso 0.50 1 calc PR . -1
C17A C 0.4625(7) 0.2152(12) 0.2073(14) 0.043(5) Uani 0.50 1 d PD . -1
C18A C 0.4900(9) 0.3011(16) 0.1505(17) 0.050(5) Uani 0.50 1 d PD . -1
H18A H 0.5206 0.2938 0.0836 0.060 Uiso 0.50 1 calc PR . -1
C19A C 0.4722(16) 0.398(2) 0.193(2) 0.049(7) Uani 0.50 1 d PD . -1
H19A H 0.4898 0.4565 0.1527 0.059 Uiso 0.50 1 calc PR . -1
C20A C 0.4284(9) 0.4087(14) 0.2937(16) 0.044(4) Uani 0.50 1 d PD . -1
H20A H 0.4163 0.4750 0.3212 0.053 Uiso 0.50 1 calc PR . -1
C21A C 0.4026(9) 0.3239(10) 0.3539(19) 0.030(4) Uani 0.50 1 d PD . -1
C22A C 0.4178(6) 0.2260(8) 0.3115(12) 0.025(4) Uani 0.50 1 d PD . -1
C23 C 0.3982(5) 0.0163(7) 0.6039(10) 0.067(3) Uani 1 1 d . . .
H23A H 0.4406 0.0483 0.6270 0.101 Uiso 1 1 calc R . .
H23B H 0.4066 -0.0395 0.5453 0.101 Uiso 1 1 calc R . .
H23C H 0.3763 -0.0107 0.6786 0.101 Uiso 1 1 calc R . .
C24 C 0.2695(6) 0.0191(7) 0.4349(11) 0.074(3) Uani 1 1 d . . .
H24A H 0.2407 -0.0109 0.4990 0.110 Uiso 1 1 calc R . .
H24B H 0.2957 -0.0348 0.3947 0.110 Uiso 1 1 calc R . .
H24C H 0.2419 0.0535 0.3724 0.110 Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O3 Sb1 C11 94.2(2) . . ?
O3 Sb1 C11 94.2(2) . 7_565 ?
C11 Sb1 C11 93.9(4) . 7_565 ?
O3 Sb1 O1 75.61(19) . . ?
C11 Sb1 O1 93.5(3) . . ?
C11 Sb1 O1 167.9(2) 7_565 . ?
O3 Sb1 O1 75.61(19) . 7_565 ?
C11 Sb1 O1 167.9(2) . 7_565 ?
C11 Sb1 O1 93.5(3) 7_565 7_565 ?
O1 Sb1 O1 77.8(3) . 7_565 ?
O3 Sb1 C1 162.2(3) . . ?
C11 Sb1 C1 97.9(3) . . ?
C11 Sb1 C1 97.9(3) 7_565 . ?
O1 Sb1 C1 90.6(2) . . ?
O1 Sb1 C1 90.6(2) 7_565 . ?
O3 Sb1 Sb2 81.87(18) . . ?
C11 Sb1 Sb2 133.0(2) . . ?
C11 Sb1 Sb2 133.0(2) 7_565 . ?
O1 Sb1 Sb2 40.05(13) . . ?
O1 Sb1 Sb2 40.05(13) 7_565 . ?
C1 Sb1 Sb2 80.3(3) . . ?
O1 Sb2 O1 78.7(3) . 7_565 ?
O1 Sb2 O2 76.17(18) . . ?
O1 Sb2 O2 76.17(18) 7_565 . ?
O1 Sb2 C12 93.4(3) . . ?
O1 Sb2 C12 168.5(3) 7_565 . ?
O2 Sb2 C12 94.0(3) . . ?
O1 Sb2 C12 168.5(3) . 7_565 ?
O1 Sb2 C12 93.4(3) 7_565 7_565 ?
O2 Sb2 C12 94.0(3) . 7_565 ?
C12 Sb2 C12 93.2(6) . 7_565 ?
O1 Sb2 C9 91.1(2) . . ?
O1 Sb2 C9 91.1(2) 7_565 . ?
O2 Sb2 C9 163.4(3) . . ?
C12 Sb2 C9 97.4(3) . . ?
C12 Sb2 C9 97.4(3) 7_565 . ?
O1 Sb2 Sb1 40.52(13) . . ?
O1 Sb2 Sb1 40.52(13) 7_565 . ?
O2 Sb2 Sb1 82.66(17) . . ?
C12 Sb2 Sb1 133.4(3) . . ?
C12 Sb2 Sb1 133.4(3) 7_565 . ?
C9 Sb2 Sb1 80.8(3) . . ?
O1 Sb2 Sb3 80.84(13) . 7_565 ?
O1 Sb2 Sb3 38.66(13) 7_565 7_565 ?
O2 Sb2 Sb3 38.57(10) . 7_565 ?
C12 Sb2 Sb3 132.3(3) . 7_565 ?
C12 Sb2 Sb3 87.8(3) 7_565 7_565 ?
C9 Sb2 Sb3 129.8(2) . 7_565 ?
Sb1 Sb2 Sb3 61.207(17) . 7_565 ?
O1 Sb2 Sb3 38.66(13) . . ?
O1 Sb2 Sb3 80.84(13) 7_565 . ?
O2 Sb2 Sb3 38.57(10) . . ?
C12 Sb2 Sb3 87.8(3) . . ?
C12 Sb2 Sb3 132.3(3) 7_565 . ?
C9 Sb2 Sb3 129.8(2) . . ?
Sb1 Sb2 Sb3 61.207(17) . . ?
Sb3 Sb2 Sb3 58.74(2) 7_565 . ?
C13A Sb3 O2 96.6(5) . . ?
C13A Sb3 C24 91.9(5) . . ?
O2 Sb3 C24 92.2(3) . . ?
C13A Sb3 C23 92.8(6) . . ?
O2 Sb3 C23 167.5(3) . . ?
C24 Sb3 C23 95.8(4) . . ?
C13A Sb3 O3 96.6(4) . . ?
O2 Sb3 O3 77.49(19) . . ?
C24 Sb3 O3 167.3(3) . . ?
C23 Sb3 O3 93.2(3) . . ?
C13A Sb3 O1 169.6(4) . . ?
O2 Sb3 O1 75.4(2) . . ?
C24 Sb3 O1 95.1(4) . . ?
C23 Sb3 O1 94.2(3) . . ?
O3 Sb3 O1 75.3(2) . . ?
C13A Sb3 C21A 14.2(4) . 7_565 ?
O2 Sb3 C21A 87.5(4) . 7_565 ?
C24 Sb3 C21A 103.1(5) . 7_565 ?
C23 Sb3 C21A 100.1(5) . 7_565 ?
O3 Sb3 C21A 84.1(4) . 7_565 ?
O1 Sb3 C21A 155.5(4) . 7_565 ?
C13A Sb3 Sb3 87.4(4) . 7_565 ?
O2 Sb3 Sb3 40.00(13) . 7_565 ?
C24 Sb3 Sb3 131.4(3) . 7_565 ?
C23 Sb3 Sb3 132.8(3) . 7_565 ?
O3 Sb3 Sb3 40.10(14) . 7_565 ?
O1 Sb3 Sb3 82.11(13) . 7_565 ?
C21A Sb3 Sb3 73.6(3) 7_565 7_565 ?
C13A Sb3 Sb2 134.8(5) . . ?
O2 Sb3 Sb2 38.26(18) . . ?
C24 Sb3 Sb2 87.8(3) . . ?
C23 Sb3 Sb2 132.3(3) . . ?
O3 Sb3 Sb2 79.50(16) . . ?
O1 Sb3 Sb2 38.19(13) . . ?
C21A Sb3 Sb2 125.4(4) 7_565 . ?
Sb3 Sb3 Sb2 60.628(12) 7_565 . ?
Sb2 O1 Sb1 99.4(2) . . ?
Sb2 O1 Sb3 103.1(2) . . ?
Sb1 O1 Sb3 103.16(19) . . ?
Sb2 O2 Sb3 103.2(2) . 7_565 ?
Sb2 O2 Sb3 103.2(2) . . ?
Sb3 O2 Sb3 100.0(3) 7_565 . ?
Sb1 O3 Sb3 103.7(2) . . ?
Sb1 O3 Sb3 103.7(2) . 7_565 ?
Sb3 O3 Sb3 99.8(3) . 7_565 ?
C2 C1 C10 119.5(10) . . ?
C2 C1 Sb1 112.5(7) . . ?
C10 C1 Sb1 128.0(8) . . ?
C1 C2 C3 121.6(10) . . ?
C1 C2 H2 119.2 . . ?
C3 C2 H2 119.2 . . ?
C4 C3 C2 119.7(11) . . ?
C4 C3 H3 120.1 . . ?
C2 C3 H3 120.1 . . ?
C3 C4 C5 121.4(10) . . ?
C3 C4 H4 119.3 . . ?
C5 C4 H4 119.3 . . ?
C6 C5 C4 120.4(10) . . ?
C6 C5 C10 120.5(10) . . ?
C4 C5 C10 119.0(9) . . ?
C7 C6 C5 121.1(10) . . ?
C7 C6 H6 119.5 . . ?
C5 C6 H6 119.5 . . ?
C6 C7 C8 120.4(10) . . ?
C6 C7 H7 119.8 . . ?
C8 C7 H7 119.8 . . ?
C9 C8 C7 121.9(11) . . ?
C9 C8 H8 119.1 . . ?
C7 C8 H8 119.1 . . ?
C8 C9 C10 118.7(10) . . ?
C8 C9 Sb2 114.2(8) . . ?
C10 C9 Sb2 127.1(7) . . ?
C1 C10 C5 118.8(9) . . ?
C1 C10 C9 123.9(9) . . ?
C5 C10 C9 117.4(9) . . ?
Sb1 C11 H11A 109.5 . . ?
Sb1 C11 H11B 109.5 . . ?
H11A C11 H11B 109.5 . . ?
Sb1 C11 H11C 109.5 . . ?
H11A C11 H11C 109.5 . . ?
H11B C11 H11C 109.5 . . ?
Sb2 C12 H12A 109.5 . . ?
Sb2 C12 H12B 109.5 . . ?
H12A C12 H12B 109.5 . . ?
Sb2 C12 H12C 109.5 . . ?
H12A C12 H12C 109.5 . . ?
H12B C12 H12C 109.5 . . ?
C14A C13A C22A 121.9(16) . . ?
C14A C13A Sb3 114.4(12) . . ?
C22A C13A Sb3 123.4(11) . . ?
C13A C14A C15A 119.0(18) . . ?
C13A C14A H14A 120.5 . . ?
C15A C14A H14A 120.5 . . ?
C16A C15A C14A 123.3(19) . . ?
C16A C15A H15A 118.3 . . ?
C14A C15A H15A 118.3 . . ?
C15A C16A C17A 117(2) . . ?
C15A C16A H16A 121.7 . . ?
C17A C16A H16A 121.7 . . ?
C18A C17A C16A 116.1(18) . . ?
C18A C17A C22A 120.3(13) . . ?
C16A C17A C22A 123.6(17) . . ?
C19A C18A C17A 119.6(17) . . ?
C19A C18A H18A 120.2 . . ?
C17A C18A H18A 120.2 . . ?
C18A C19A C20A 120(2) . . ?
C18A C19A H19A 119.9 . . ?
C20A C19A H19A 119.9 . . ?
C21A C20A C19A 120.8(19) . . ?
C21A C20A H20A 119.6 . . ?
C19A C20A H20A 119.6 . . ?
C20A C21A C22A 120.3(16) . . ?
C20A C21A Sb3 110.2(11) . 7_565 ?
C22A C21A Sb3 129.5(12) . 7_565 ?
C21A C22A C13A 125.8(12) . . ?
C21A C22A C17A 118.7(14) . . ?
C13A C22A C17A 115.5(12) . . ?
Sb3 C23 H23A 109.5 . . ?
Sb3 C23 H23B 109.5 . . ?
H23A C23 H23B 109.5 . . ?
Sb3 C23 H23C 109.5 . . ?
H23A C23 H23C 109.5 . . ?
H23B C23 H23C 109.5 . . ?
Sb3 C24 H24A 109.5 . . ?
Sb3 C24 H24B 109.5 . . ?
H24A C24 H24B 109.5 . . ?
Sb3 C24 H24C 109.5 . . ?
H24A C24 H24C 109.5 . . ?
H24B C24 H24C 109.5 . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Sb1 O3 2.111(7) . ?
Sb1 C11 2.125(7) . ?
Sb1 C11 2.125(7) 7_565 ?
Sb1 O1 2.125(5) . ?
Sb1 O1 2.125(5) 7_565 ?
Sb1 C1 2.155(10) . ?
Sb1 Sb2 3.2270(9) . ?
Sb2 O1 2.105(5) . ?
Sb2 O1 2.105(5) 7_565 ?
Sb2 O2 2.108(7) . ?
Sb2 C12 2.114(9) . ?
Sb2 C12 2.114(9) 7_565 ?
Sb2 C9 2.143(11) . ?
Sb2 Sb3 3.3154(8) 7_565 ?
Sb2 Sb3 3.3154(8) . ?
Sb3 C13A 2.039(17) . ?
Sb3 O2 2.123(4) . ?
Sb3 C24 2.123(9) . ?
Sb3 C23 2.125(9) . ?
Sb3 O3 2.126(4) . ?
Sb3 O1 2.127(5) . ?
Sb3 C21A 2.319(19) 7_565 ?
Sb3 Sb3 3.2522(11) 7_565 ?
O2 Sb3 2.123(4) 7_565 ?
O3 Sb3 2.126(4) 7_565 ?
C1 C2 1.392(14) . ?
C1 C10 1.409(13) . ?
C2 C3 1.409(15) . ?
C2 H2 0.9500 . ?
C3 C4 1.350(16) . ?
C3 H3 0.9500 . ?
C4 C5 1.419(16) . ?
C4 H4 0.9500 . ?
C5 C6 1.405(15) . ?
C5 C10 1.441(14) . ?
C6 C7 1.343(17) . ?
C6 H6 0.9500 . ?
C7 C8 1.402(16) . ?
C7 H7 0.9500 . ?
C8 C9 1.396(13) . ?
C8 H8 0.9500 . ?
C9 C10 1.447(14) . ?
C11 H11A 0.9800 . ?
C11 H11B 0.9800 . ?
C11 H11C 0.9800 . ?
C12 H12A 0.9800 . ?
C12 H12B 0.9800 . ?
C12 H12C 0.9800 . ?
C13A C14A 1.385(15) . ?
C13A C22A 1.427(14) . ?
C14A C15A 1.393(16) . ?
C14A H14A 0.9500 . ?
C15A C16A 1.388(17) . ?
C15A H15A 0.9500 . ?
C16A C17A 1.397(18) . ?
C16A H16A 0.9500 . ?
C17A C18A 1.396(16) . ?
C17A C22A 1.439(15) . ?
C18A C19A 1.393(18) . ?
C18A H18A 0.9500 . ?
C19A C20A 1.403(17) . ?
C19A H19A 0.9500 . ?
C20A C21A 1.388(16) . ?
C20A H20A 0.9500 . ?
C21A C22A 1.398(16) . ?
C21A Sb3 2.319(19) 7_565 ?
C23 H23A 0.9800 . ?
C23 H23B 0.9800 . ?
C23 H23C 0.9800 . ?
C24 H24A 0.9800 . ?
C24 H24B 0.9800 . ?
C24 H24C 0.9800 . ?
