#------------------------------------------------------------------------------
#$Date: 2016-03-25 10:42:24 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179760 $
#$URL: svn://www.crystallography.net/cod/cif/7/00/56/7005671.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7005671
loop_
_publ_author_name
'Chandrasekaran, P.'
'Mague, Joel T.'
'Balakrishna, Maravanji S.'
_publ_section_title
;
 One-dimensional silver(I) coordination polymers containing
 cyclodiphosphazane, cis-{(o-MeOC(6)H(4)O)P(mu-N(t)Bu)}(2).
;
_journal_issue                   27
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              2957
_journal_page_last               2962
_journal_paper_doi               10.1039/b704303a
_journal_year                    2007
_chemical_formula_moiety         'C23 H32 Ag N3 O4 P2'
_chemical_formula_sum            'C23 H32 Ag N3 O4 P2'
_chemical_formula_weight         584.33
_chemical_name_systematic
;
?
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 105.269(1)
_cell_angle_gamma                90.00
_cell_formula_units_Z            8
_cell_length_a                   16.482(1)
_cell_length_b                   16.069(1)
_cell_length_c                   22.312(2)
_cell_measurement_reflns_used    8660
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      28.29
_cell_measurement_theta_min      2.36
_cell_volume                     5700.7(7)
_computing_cell_refinement       'Bruker SMART (Bruker-AXS, 2000)'
_computing_data_collection       'Bruker SMART (Bruker-AXS, 2000)'
_computing_data_reduction        'Bruker SAINT+ (Bruker-AXS, 2004)'
_computing_molecular_graphics    'Bruker SHELXTL (Bruker-AXS, 2000a)'
_computing_publication_material  'Bruker SHELXTL (Bruker-AXS, 2000a)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      100(2)
_diffrn_measured_fraction_theta_full 0.996
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measurement_device_type  'Bruker-AXS Smart APEX CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0365
_diffrn_reflns_av_sigmaI/netI    0.0230
_diffrn_reflns_limit_h_max       21
_diffrn_reflns_limit_h_min       -22
_diffrn_reflns_limit_k_max       21
_diffrn_reflns_limit_k_min       -21
_diffrn_reflns_limit_l_max       29
_diffrn_reflns_limit_l_min       -29
_diffrn_reflns_number            99847
_diffrn_reflns_theta_full        28.35
_diffrn_reflns_theta_max         28.35
_diffrn_reflns_theta_min         2.19
_exptl_absorpt_coefficient_mu    0.849
_exptl_absorpt_correction_T_max  0.8532
_exptl_absorpt_correction_T_min  0.7487
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'SADABS (Sheldrick, 2002)'
_exptl_crystal_colour            Colorless
_exptl_crystal_density_diffrn    1.362
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Block
_exptl_crystal_F_000             2400
_exptl_crystal_size_max          0.26
_exptl_crystal_size_mid          0.21
_exptl_crystal_size_min          0.19
_refine_diff_density_max         3.559
_refine_diff_density_min         -1.129
_refine_diff_density_rms         0.099
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.031
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     656
_refine_ls_number_reflns         14182
_refine_ls_number_restraints     58
_refine_ls_restrained_S_all      1.047
_refine_ls_R_factor_all          0.0484
_refine_ls_R_factor_gt           0.0427
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0601P)²+8.0821P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1091
_refine_ls_wR_factor_ref         0.1128
_reflns_number_gt                12593
_reflns_number_total             14182
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b704303a.txt
_cod_data_source_block           msb229
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_cell_volume        5700.8(6)
_cod_original_sg_symbol_H-M      P2(1)/n
_cod_database_code               7005671
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.371654(12) 0.254130(11) 0.167995(9) 0.02155(6) Uani 1 1 d . A .
Ag2 Ag 0.181434(17) 0.015755(15) 0.221187(13) 0.04205(8) Uani 1 1 d . . .
P1 P 0.47611(4) 0.14498(4) 0.18372(3) 0.01891(12) Uani 1 1 d . . .
P2 P 0.46077(4) -0.00361(4) 0.21880(3) 0.02215(13) Uani 1 1 d . . .
P3 P 0.33057(4) 0.36560(4) 0.09300(3) 0.01902(12) Uani 1 1 d . . .
P4 P 0.29660(7) 0.51109(6) 0.12706(6) 0.0198(2) Uani 0.823(3) 1 d PD A 5
O7 O 0.27762(15) 0.58277(14) 0.07170(12) 0.0248(5) Uani 0.823(3) 1 d PD A 5
O8 O 0.16711(18) 0.64797(15) -0.02222(11) 0.0272(6) Uani 0.823(3) 1 d PD A 5
C38 C 0.24610(18) 0.66027(17) 0.08112(13) 0.0204(6) Uani 0.823(3) 1 d PD A 5
C39 C 0.2720(2) 0.7030(2) 0.13675(16) 0.0254(8) Uani 0.823(3) 1 d PD A 5
H39 H 0.3116 0.6787 0.1711 0.030 Uiso 0.823(3) 1 calc PR A 5
C40 C 0.2397(2) 0.7821(2) 0.14225(19) 0.0345(8) Uani 0.823(3) 1 d PD A 5
H40 H 0.2566 0.8115 0.1805 0.041 Uiso 0.823(3) 1 calc PR A 5
C41 C 0.1832(2) 0.8174(2) 0.09187(16) 0.0344(8) Uani 0.823(3) 1 d PD A 5
H41 H 0.1616 0.8714 0.0956 0.041 Uiso 0.823(3) 1 calc PR A 5
C42 C 0.1574(4) 0.7751(3) 0.0358(2) 0.0293(6) Uani 0.823(3) 1 d PD A 5
H42 H 0.1187 0.8003 0.0013 0.035 Uiso 0.823(3) 1 calc PR A 5
C43 C 0.18840(19) 0.69595(18) 0.03039(14) 0.0214(6) Uani 0.823(3) 1 d PD A 5
C44 C 0.1094(3) 0.6830(3) -0.07463(17) 0.0357(9) Uani 0.823(3) 1 d PD A 5
H44A H 0.0573 0.6976 -0.0638 0.054 Uiso 0.823(3) 1 calc PR A 5
H44B H 0.0971 0.6425 -0.1087 0.054 Uiso 0.823(3) 1 calc PR A 5
H44C H 0.1339 0.7332 -0.0877 0.054 Uiso 0.823(3) 1 calc PR A 5
P4A P 0.2798(3) 0.5091(3) 0.1059(3) 0.0198(2) Uani 0.177(3) 1 d PD A 6
O7A O 0.2701(8) 0.5682(7) 0.0437(5) 0.0248(5) Uani 0.177(3) 1 d PD A 6
O8A O 0.2709(10) 0.6974(10) 0.1179(6) 0.0272(6) Uani 0.177(3) 1 d PD A 6
C38A C 0.2128(8) 0.6310(7) 0.0245(5) 0.0204(6) Uani 0.177(3) 1 d PD A 6
C39A C 0.1596(10) 0.6294(12) -0.0354(6) 0.0254(8) Uani 0.177(3) 1 d PD A 6
H39A H 0.1584 0.5817 -0.0608 0.030 Uiso 0.177(3) 1 calc PR A 6
C41A C 0.1097(11) 0.7667(9) -0.0205(7) 0.0344(8) Uani 0.177(3) 1 d PD A 6
H41A H 0.0740 0.8129 -0.0351 0.041 Uiso 0.177(3) 1 calc PR A 6
C40A C 0.1081(13) 0.6974(10) -0.0583(9) 0.0345(8) Uani 0.177(3) 1 d PD A 6
H40A H 0.0722 0.6964 -0.0994 0.041 Uiso 0.177(3) 1 calc PR A 6
C42A C 0.164(2) 0.7675(15) 0.0391(10) 0.0293(6) Uani 0.177(3) 1 d PD A 6
H42A H 0.1662 0.8154 0.0644 0.035 Uiso 0.177(3) 1 calc PR A 6
C43A C 0.2158(9) 0.6999(8) 0.0624(6) 0.0214(6) Uani 0.177(3) 1 d PD A 6
C44A C 0.2603(14) 0.7620(13) 0.1592(9) 0.0357(9) Uani 0.177(3) 1 d PD A 6
H44D H 0.3021 0.7553 0.1992 0.054 Uiso 0.177(3) 1 calc PR A 6
H44E H 0.2037 0.7586 0.1654 0.054 Uiso 0.177(3) 1 calc PR A 6
H44F H 0.2679 0.8162 0.1414 0.054 Uiso 0.177(3) 1 calc PR A 6
O1 O 0.55887(11) 0.18142(11) 0.16642(8) 0.0235(4) Uani 1 1 d . . .
O2 O 0.59740(15) 0.23662(14) 0.06893(11) 0.0387(5) Uani 1 1 d . . .
O3 O 0.54475(12) -0.06280(11) 0.22208(9) 0.0290(4) Uani 1 1 d . . .
O4 O 0.69625(13) -0.12477(12) 0.26389(10) 0.0302(4) Uani 1 1 d . . .
O5 O 0.33210(12) 0.33506(12) 0.02455(8) 0.0262(4) Uani 1 1 d . A .
O6 O 0.34933(19) 0.24614(17) -0.06585(11) 0.0526(7) Uani 1 1 d . . .
N1 N 0.50438(13) 0.08836(13) 0.24993(10) 0.0212(4) Uani 1 1 d . . .
N2 N 0.45253(14) 0.05049(13) 0.15137(10) 0.0225(4) Uani 1 1 d . B .
N3 N 0.24362(14) 0.42282(14) 0.09003(11) 0.0257(5) Uani 1 1 d D A .
N4 N 0.37743(13) 0.45906(13) 0.11047(10) 0.0230(4) Uani 1 1 d D A .
N5 N 0.25863(17) 0.18302(17) 0.18501(14) 0.0402(6) Uani 1 1 d . . .
N6 N 0.3929(2) 0.34000(17) 0.25546(12) 0.0449(7) Uani 1 1 d . . .
C1 C 0.51411(17) 0.11655(17) 0.31501(12) 0.0258(5) Uani 1 1 d . . .
C2 C 0.5725(2) 0.1919(2) 0.32622(14) 0.0392(7) Uani 1 1 d . . .
H2A H 0.6262 0.1767 0.3181 0.059 Uiso 1 1 calc R . .
H2B H 0.5824 0.2102 0.3694 0.059 Uiso 1 1 calc R . .
H2C H 0.5465 0.2372 0.2983 0.059 Uiso 1 1 calc R . .
C3 C 0.42923(18) 0.13879(18) 0.32605(13) 0.0302(6) Uani 1 1 d . . .
H3A H 0.4046 0.1857 0.2994 0.045 Uiso 1 1 calc R . .
H3B H 0.4371 0.1542 0.3697 0.045 Uiso 1 1 calc R . .
H3C H 0.3915 0.0907 0.3162 0.045 Uiso 1 1 calc R . .
C4 C 0.55373(19) 0.0442(2) 0.35672(13) 0.0352(7) Uani 1 1 d . . .
H4A H 0.5147 -0.0030 0.3495 0.053 Uiso 1 1 calc R . .
H4B H 0.5658 0.0614 0.4003 0.053 Uiso 1 1 calc R . .
H4C H 0.6061 0.0277 0.3471 0.053 Uiso 1 1 calc R . .
C5 C 0.40583(18) 0.02572(17) 0.08762(12) 0.0286(5) Uani 1 1 d D . .
C6 C 0.3113(5) 0.0320(8) 0.0801(5) 0.061(3) Uani 0.535(7) 1 d PD B 3
H6A H 0.2965 0.0898 0.0864 0.091 Uiso 0.535(7) 1 calc PR B 3
H6B H 0.2957 -0.0037 0.1109 0.091 Uiso 0.535(7) 1 calc PR B 3
H6C H 0.2811 0.0139 0.0382 0.091 Uiso 0.535(7) 1 calc PR B 3
C7 C 0.4266(6) -0.0659(5) 0.0774(4) 0.0500(15) Uani 0.535(7) 1 d PD B 3
H7A H 0.3852 -0.1022 0.0887 0.075 Uiso 0.535(7) 1 calc PR B 3
H7B H 0.4829 -0.0792 0.1035 0.075 Uiso 0.535(7) 1 calc PR B 3
H7C H 0.4250 -0.0745 0.0336 0.075 Uiso 0.535(7) 1 calc PR B 3
C8 C 0.4313(13) 0.0811(8) 0.0405(7) 0.078(5) Uani 0.535(7) 1 d PD B 3
H8A H 0.4176 0.1391 0.0473 0.117 Uiso 0.535(7) 1 calc PR B 3
H8B H 0.4008 0.0640 -0.0015 0.117 Uiso 0.535(7) 1 calc PR B 3
H8C H 0.4919 0.0759 0.0454 0.117 Uiso 0.535(7) 1 calc PR B 3
C6A C 0.3241(6) -0.0153(8) 0.0873(5) 0.061(3) Uani 0.465(7) 1 d PD B 4
H6AA H 0.2840 0.0269 0.0934 0.091 Uiso 0.465(7) 1 calc PR B 4
H6AB H 0.3333 -0.0563 0.1210 0.091 Uiso 0.465(7) 1 calc PR B 4
H6AC H 0.3014 -0.0433 0.0474 0.091 Uiso 0.465(7) 1 calc PR B 4
C7A C 0.4621(6) -0.0379(6) 0.0671(4) 0.0500(15) Uani 0.465(7) 1 d PD B 4
H7AA H 0.5072 -0.0089 0.0545 0.075 Uiso 0.465(7) 1 calc PR B 4
H7AB H 0.4284 -0.0702 0.0320 0.075 Uiso 0.465(7) 1 calc PR B 4
H7AC H 0.4866 -0.0755 0.1017 0.075 Uiso 0.465(7) 1 calc PR B 4
C8A C 0.3967(16) 0.1027(9) 0.0468(8) 0.078(5) Uani 0.465(7) 1 d PD B 4
H8AA H 0.3819 0.1505 0.0690 0.117 Uiso 0.465(7) 1 calc PR B 4
H8AB H 0.3523 0.0934 0.0084 0.117 Uiso 0.465(7) 1 calc PR B 4
H8AC H 0.4500 0.1138 0.0366 0.117 Uiso 0.465(7) 1 calc PR B 4
C9 C 0.62293(16) 0.13916(16) 0.14903(12) 0.0224(5) Uani 1 1 d . . .
C10 C 0.66503(17) 0.07258(18) 0.18112(13) 0.0274(5) Uani 1 1 d . . .
H10 H 0.6500 0.0514 0.2165 0.033 Uiso 1 1 calc R . .
C11 C 0.73038(18) 0.0363(2) 0.16120(14) 0.0337(6) Uani 1 1 d . . .
H11 H 0.7595 -0.0104 0.1827 0.040 Uiso 1 1 calc R . .
C12 C 0.75279(19) 0.0680(2) 0.11052(15) 0.0353(7) Uani 1 1 d . . .
H12 H 0.7978 0.0434 0.0976 0.042 Uiso 1 1 calc R . .
C13 C 0.71022(19) 0.13543(19) 0.07829(14) 0.0328(6) Uani 1 1 d . . .
H13 H 0.7261 0.1569 0.0434 0.039 Uiso 1 1 calc R . .
C14 C 0.64448(17) 0.17165(17) 0.09688(12) 0.0268(5) Uani 1 1 d . . .
C15 C 0.6174(4) 0.2720(3) 0.0161(2) 0.0701(14) Uani 1 1 d . . .
H15A H 0.6734 0.2974 0.0287 0.105 Uiso 1 1 calc R . .
H15B H 0.5757 0.3146 -0.0022 0.105 Uiso 1 1 calc R . .
H15C H 0.6170 0.2284 -0.0147 0.105 Uiso 1 1 calc R . .
C16 C 0.55004(17) -0.14391(15) 0.24391(12) 0.0243(5) Uani 1 1 d . . .
C17 C 0.48128(19) -0.19293(18) 0.24344(14) 0.0322(6) Uani 1 1 d . . .
H17 H 0.4262 -0.1712 0.2275 0.039 Uiso 1 1 calc R . .
C18 C 0.4918(2) -0.27406(18) 0.26603(15) 0.0370(7) Uani 1 1 d . . .
H18 H 0.4442 -0.3068 0.2670 0.044 Uiso 1 1 calc R . .
C19 C 0.5717(2) -0.30657(17) 0.28696(14) 0.0345(6) Uani 1 1 d . . .
H19 H 0.5791 -0.3622 0.3019 0.041 Uiso 1 1 calc R . .
C20 C 0.64146(19) -0.25843(16) 0.28632(13) 0.0299(6) Uani 1 1 d . . .
H20 H 0.6962 -0.2816 0.3002 0.036 Uiso 1 1 calc R . .
C21 C 0.63181(17) -0.17665(16) 0.26559(12) 0.0243(5) Uani 1 1 d . . .
C22 C 0.77948(19) -0.1588(2) 0.28410(17) 0.0403(7) Uani 1 1 d . . .
H22A H 0.7907 -0.1758 0.3277 0.060 Uiso 1 1 calc R . .
H22B H 0.8205 -0.1166 0.2799 0.060 Uiso 1 1 calc R . .
H22C H 0.7841 -0.2072 0.2585 0.060 Uiso 1 1 calc R . .
C23 C 0.15709(16) 0.39497(18) 0.08697(13) 0.0279(5) Uani 1 1 d . . .
C24 C 0.09781(19) 0.4640(2) 0.05448(14) 0.0354(7) Uani 1 1 d . A .
H24A H 0.1090 0.5148 0.0796 0.053 Uiso 1 1 calc R . .
H24B H 0.0394 0.4466 0.0495 0.053 Uiso 1 1 calc R . .
H24C H 0.1070 0.4747 0.0135 0.053 Uiso 1 1 calc R . .
C25 C 0.14631(18) 0.3791(2) 0.15181(13) 0.0315(6) Uani 1 1 d . A .
H25A H 0.1856 0.3356 0.1723 0.047 Uiso 1 1 calc R . .
H25B H 0.0885 0.3611 0.1486 0.047 Uiso 1 1 calc R . .
H25C H 0.1579 0.4305 0.1763 0.047 Uiso 1 1 calc R . .
C26 C 0.14062(19) 0.3156(2) 0.04838(16) 0.0383(7) Uani 1 1 d . A .
H26A H 0.1491 0.3264 0.0072 0.057 Uiso 1 1 calc R . .
H26B H 0.0826 0.2974 0.0438 0.057 Uiso 1 1 calc R . .
H26C H 0.1795 0.2721 0.0692 0.057 Uiso 1 1 calc R . .
C27 C 0.46740(17) 0.48259(16) 0.12477(13) 0.0285(6) Uani 1 1 d D . .
C28 C 0.4755(3) 0.5650(4) 0.0929(4) 0.071(2) Uani 0.711(4) 1 d PD A 1
H28A H 0.4500 0.5597 0.0481 0.106 Uiso 0.711(4) 1 calc PR A 1
H28B H 0.5351 0.5793 0.1002 0.106 Uiso 0.711(4) 1 calc PR A 1
H28C H 0.4467 0.6089 0.1098 0.106 Uiso 0.711(4) 1 calc PR A 1
C29 C 0.5146(3) 0.4162(3) 0.0991(2) 0.0414(10) Uani 0.711(4) 1 d PD A 1
H29A H 0.4902 0.4108 0.0542 0.062 Uiso 0.711(4) 1 calc PR A 1
H29B H 0.5102 0.3629 0.1193 0.062 Uiso 0.711(4) 1 calc PR A 1
H29C H 0.5739 0.4320 0.1072 0.062 Uiso 0.711(4) 1 calc PR A 1
C30 C 0.5076(3) 0.4891(4) 0.1958(2) 0.0466(11) Uani 0.711(4) 1 d PD A 1
H30A H 0.4775 0.4525 0.2178 0.070 Uiso 0.711(4) 1 calc PR A 1
H30B H 0.5039 0.5467 0.2093 0.070 Uiso 0.711(4) 1 calc PR A 1
H30C H 0.5667 0.4723 0.2052 0.070 Uiso 0.711(4) 1 calc PR A 1
C28A C 0.4772(9) 0.5120(9) 0.0612(7) 0.071(2) Uani 0.289(4) 1 d PD A 2
H28D H 0.4336 0.4862 0.0279 0.106 Uiso 0.289(4) 1 calc PR A 2
H28E H 0.5328 0.4959 0.0571 0.106 Uiso 0.289(4) 1 calc PR A 2
H28F H 0.4715 0.5727 0.0584 0.106 Uiso 0.289(4) 1 calc PR A 2
C29A C 0.5198(6) 0.4076(7) 0.1465(6) 0.0414(10) Uani 0.289(4) 1 d PD A 2
H29D H 0.5175 0.3706 0.1112 0.062 Uiso 0.289(4) 1 calc PR A 2
H29E H 0.4983 0.3782 0.1776 0.062 Uiso 0.289(4) 1 calc PR A 2
H29F H 0.5781 0.4245 0.1650 0.062 Uiso 0.289(4) 1 calc PR A 2
C30A C 0.4733(7) 0.5557(8) 0.1662(6) 0.0466(11) Uani 0.289(4) 1 d PD A 2
H30D H 0.4474 0.6040 0.1418 0.070 Uiso 0.289(4) 1 calc PR A 2
H30E H 0.5325 0.5676 0.1862 0.070 Uiso 0.289(4) 1 calc PR A 2
H30F H 0.4438 0.5437 0.1981 0.070 Uiso 0.289(4) 1 calc PR A 2
C31 C 0.31465(16) 0.3750(2) -0.03295(12) 0.0297(6) Uani 1 1 d . . .
C32 C 0.28994(18) 0.4570(2) -0.04298(14) 0.0349(6) Uani 1 1 d . A .
H32 H 0.2832 0.4901 -0.0093 0.042 Uiso 1 1 calc R . .
C33 C 0.27480(19) 0.4917(2) -0.10252(15) 0.0384(7) Uani 1 1 d . . .
H33 H 0.2579 0.5481 -0.1096 0.046 Uiso 1 1 calc R A .
C34 C 0.2846(2) 0.4436(2) -0.14954(16) 0.0433(8) Uani 1 1 d . A .
H34 H 0.2743 0.4671 -0.1899 0.052 Uiso 1 1 calc R . .
C35 C 0.3090(2) 0.3619(3) -0.14120(15) 0.0469(9) Uani 1 1 d . . .
H35 H 0.3153 0.3298 -0.1754 0.056 Uiso 1 1 calc R A .
C36 C 0.32471(19) 0.3255(2) -0.08146(14) 0.0381(7) Uani 1 1 d . A .
C37 C 0.3587(4) 0.1944(3) -0.1158(2) 0.0869(19) Uani 1 1 d . . .
H37A H 0.3066 0.1955 -0.1494 0.130 Uiso 1 1 calc R . .
H37B H 0.3707 0.1372 -0.1009 0.130 Uiso 1 1 calc R . .
H37C H 0.4053 0.2152 -0.1314 0.130 Uiso 1 1 calc R . .
C45 C 0.2289(2) 0.1257(2) 0.19939(16) 0.0384(7) Uani 1 1 d . A .
C46 C 0.3672(2) 0.40128(19) 0.26649(14) 0.0370(7) Uani 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N5 Ag1 N6 96.05(11) . . ?
N5 Ag1 P1 101.09(7) . . ?
N6 Ag1 P1 111.23(8) . . ?
N5 Ag1 P3 112.95(7) . . ?
N6 Ag1 P3 95.35(7) . . ?
P1 Ag1 P3 134.06(2) . . ?
C45 Ag2 C46 173.87(13) . 2_545 ?
O1 P1 N2 109.73(10) . . ?
O1 P1 N1 110.27(10) . . ?
N2 P1 N1 82.46(10) . . ?
O1 P1 Ag1 108.36(7) . . ?
N2 P1 Ag1 121.15(8) . . ?
N1 P1 Ag1 122.58(8) . . ?
O1 P1 P2 124.73(7) . . ?
N2 P1 P2 41.84(7) . . ?
N1 P1 P2 41.79(8) . . ?
Ag1 P1 P2 126.90(3) . . ?
O3 P2 N1 102.72(11) . . ?
O3 P2 N2 101.61(10) . . ?
N1 P2 N2 81.11(10) . . ?
O3 P2 P1 113.60(7) . . ?
N1 P2 P1 41.29(7) . . ?
N2 P2 P1 40.95(7) . . ?
O5 P3 N4 111.71(11) . . ?
O5 P3 N3 110.70(11) . . ?
N4 P3 N3 81.76(11) . . ?
O5 P3 Ag1 110.99(7) . . ?
N4 P3 Ag1 118.10(8) . . ?
N3 P3 Ag1 120.62(8) . . ?
O5 P3 P4A 118.71(15) . . ?
N4 P3 P4A 45.39(14) . . ?
N3 P3 P4A 36.37(15) . . ?
Ag1 P3 P4A 130.15(13) . . ?
O5 P3 P4 128.15(8) . . ?
N4 P3 P4 40.76(7) . . ?
N3 P3 P4 42.82(9) . . ?
Ag1 P3 P4 120.82(4) . . ?
P4A P3 P4 10.81(11) . . ?
O7 P4 N4 100.67(12) . . ?
O7 P4 N3 103.77(12) . . ?
N4 P4 N3 79.67(11) . . ?
O7 P4 P3 115.20(9) . . ?
N4 P4 P3 40.54(8) . . ?
N3 P4 P3 40.89(7) . . ?
C38 O7 P4 121.1(2) . . ?
C43 O8 C44 116.7(3) . . ?
C39 C38 O7 122.9(3) . . ?
C39 C38 C43 120.4(3) . . ?
O7 C38 C43 116.6(3) . . ?
C38 C39 C40 119.7(3) . . ?
C38 C39 H39 120.1 . . ?
C40 C39 H39 120.1 . . ?
C41 C40 C39 119.6(4) . . ?
C41 C40 H40 120.2 . . ?
C39 C40 H40 120.2 . . ?
C40 C41 C42 121.0(3) . . ?
C40 C41 H41 119.5 . . ?
C42 C41 H41 119.5 . . ?
C41 C42 C43 119.7(3) . . ?
C41 C42 H42 120.2 . . ?
C43 C42 H42 120.2 . . ?
O8 C43 C42 125.0(3) . . ?
O8 C43 C38 115.4(3) . . ?
C42 C43 C38 119.6(3) . . ?
N3 P4A O7A 112.6(5) . . ?
N3 P4A N4 83.9(3) . . ?
O7A P4A N4 101.2(5) . . ?
N3 P4A P3 41.42(15) . . ?
O7A P4A P3 113.3(5) . . ?
N4 P4A P3 42.49(13) . . ?
C38A O7A P4A 126.3(10) . . ?
C43A O8A C44A 114.2(14) . . ?
O7A C38A C43A 119.1(11) . . ?
O7A C38A C39A 119.6(12) . . ?
C43A C38A C39A 120.9(12) . . ?
C38A C39A C40A 120.4(17) . . ?
C38A C39A H39A 119.8 . . ?
C40A C39A H39A 119.8 . . ?
C40A C41A C42A 119.3(18) . . ?
C40A C41A H41A 120.4 . . ?
C42A C41A H41A 120.4 . . ?
C41A C40A C39A 119.4(19) . . ?
C41A C40A H40A 120.3 . . ?
C39A C40A H40A 120.3 . . ?
C43A C42A C41A 121.8(18) . . ?
C43A C42A H42A 119.1 . . ?
C41A C42A H42A 119.1 . . ?
O8A C43A C38A 116.7(13) . . ?
O8A C43A C42A 124.9(13) . . ?
C38A C43A C42A 118.3(14) . . ?
O8A C44A H44D 109.5 . . ?
O8A C44A H44E 109.5 . . ?
H44D C44A H44E 109.5 . . ?
O8A C44A H44F 109.5 . . ?
H44D C44A H44F 109.5 . . ?
H44E C44A H44F 109.5 . . ?
C9 O1 P1 129.54(16) . . ?
C14 O2 C15 117.4(3) . . ?
C16 O3 P2 121.81(17) . . ?
C21 O4 C22 116.6(2) . . ?
C31 O5 P3 132.93(19) . . ?
C36 O6 C37 115.6(3) . . ?
C1 N1 P1 128.46(17) . . ?
C1 N1 P2 125.81(17) . . ?
P1 N1 P2 96.92(11) . . ?
C5 N2 P1 131.07(17) . . ?
C5 N2 P2 127.44(18) . . ?
P1 N2 P2 97.21(11) . . ?
C23 N3 P4A 127.1(3) . . ?
C23 N3 P3 129.41(18) . . ?
P4A N3 P3 102.2(2) . . ?
C23 N3 P4 128.37(18) . . ?
P4A N3 P4 14.7(2) . . ?
P3 N3 P4 96.29(12) . . ?
C27 N4 P3 130.42(17) . . ?
C27 N4 P4 128.84(19) . . ?
P3 N4 P4 98.70(12) . . ?
C27 N4 P4A 137.4(2) . . ?
P3 N4 P4A 92.1(2) . . ?
P4 N4 P4A 15.71(16) . . ?
C45 N5 Ag1 152.1(3) . . ?
C46 N6 Ag1 135.8(3) . . ?
N1 C1 C4 106.4(2) . . ?
N1 C1 C3 111.2(2) . . ?
C4 C1 C3 110.1(2) . . ?
N1 C1 C2 107.6(2) . . ?
C4 C1 C2 110.8(2) . . ?
C3 C1 C2 110.7(2) . . ?
C1 C2 H2A 109.5 . . ?
C1 C2 H2B 109.5 . . ?
H2A C2 H2B 109.5 . . ?
C1 C2 H2C 109.5 . . ?
H2A C2 H2C 109.5 . . ?
H2B C2 H2C 109.5 . . ?
C1 C3 H3A 109.5 . . ?
C1 C3 H3B 109.5 . . ?
H3A C3 H3B 109.5 . . ?
C1 C3 H3C 109.5 . . ?
H3A C3 H3C 109.5 . . ?
H3B C3 H3C 109.5 . . ?
C1 C4 H4A 109.5 . . ?
C1 C4 H4B 109.5 . . ?
H4A C4 H4B 109.5 . . ?
C1 C4 H4C 109.5 . . ?
H4A C4 H4C 109.5 . . ?
H4B C4 H4C 109.5 . . ?
N2 C5 C6A 111.2(5) . . ?
N2 C5 C8 109.8(8) . . ?
C6A C5 C8 131.8(10) . . ?
N2 C5 C8A 107.5(9) . . ?
C6A C5 C8A 114.1(11) . . ?
C8 C5 C8A 27.1(11) . . ?
N2 C5 C6 110.2(4) . . ?
C6A C5 C6 30.4(5) . . ?
C8 C5 C6 110.2(9) . . ?
C8A C5 C6 86.8(10) . . ?
N2 C5 C7A 105.3(4) . . ?
C6A C5 C7A 108.7(6) . . ?
C8 C5 C7A 83.4(7) . . ?
C8A C5 C7A 109.7(8) . . ?
C6 C5 C7A 133.9(6) . . ?
N2 C5 C7 108.6(3) . . ?
C6A C5 C7 79.3(5) . . ?
C8 C5 C7 110.1(6) . . ?
C8A C5 C7 132.8(7) . . ?
C6 C5 C7 107.9(5) . . ?
C7A C5 C7 30.8(4) . . ?
C5 C6 H6A 109.5 . . ?
C5 C6 H6B 109.5 . . ?
H6A C6 H6B 109.5 . . ?
C5 C6 H6C 109.5 . . ?
H6A C6 H6C 109.5 . . ?
H6B C6 H6C 109.5 . . ?
C5 C7 H7A 109.5 . . ?
C5 C7 H7B 109.5 . . ?
H7A C7 H7B 109.5 . . ?
C5 C7 H7C 109.5 . . ?
H7A C7 H7C 109.5 . . ?
H7B C7 H7C 109.5 . . ?
C5 C8 H8A 109.5 . . ?
C5 C8 H8B 109.5 . . ?
H8A C8 H8B 109.5 . . ?
C5 C8 H8C 109.5 . . ?
H8A C8 H8C 109.5 . . ?
H8B C8 H8C 109.5 . . ?
C5 C6A H6AA 109.5 . . ?
C5 C6A H6AB 109.5 . . ?
H6AA C6A H6AB 109.5 . . ?
C5 C6A H6AC 109.5 . . ?
H6AA C6A H6AC 109.5 . . ?
H6AB C6A H6AC 109.5 . . ?
C5 C7A H7AA 109.5 . . ?
C5 C7A H7AB 109.5 . . ?
H7AA C7A H7AB 109.5 . . ?
C5 C7A H7AC 109.5 . . ?
H7AA C7A H7AC 109.5 . . ?
H7AB C7A H7AC 109.5 . . ?
C5 C8A H8AA 109.5 . . ?
C5 C8A H8AB 109.5 . . ?
H8AA C8A H8AB 109.5 . . ?
C5 C8A H8AC 109.5 . . ?
H8AA C8A H8AC 109.5 . . ?
H8AB C8A H8AC 109.5 . . ?
C10 C9 O1 123.5(2) . . ?
C10 C9 C14 121.3(2) . . ?
O1 C9 C14 115.2(2) . . ?
C9 C10 C11 119.1(3) . . ?
C9 C10 H10 120.4 . . ?
C11 C10 H10 120.4 . . ?
C12 C11 C10 120.2(3) . . ?
C12 C11 H11 119.9 . . ?
C10 C11 H11 119.9 . . ?
C11 C12 C13 120.5(3) . . ?
C11 C12 H12 119.8 . . ?
C13 C12 H12 119.8 . . ?
C12 C13 C14 120.1(3) . . ?
C12 C13 H13 119.9 . . ?
C14 C13 H13 119.9 . . ?
O2 C14 C13 125.8(3) . . ?
O2 C14 C9 115.5(2) . . ?
C13 C14 C9 118.7(3) . . ?
O2 C15 H15A 109.5 . . ?
O2 C15 H15B 109.5 . . ?
H15A C15 H15B 109.5 . . ?
O2 C15 H15C 109.5 . . ?
H15A C15 H15C 109.5 . . ?
H15B C15 H15C 109.5 . . ?
C17 C16 O3 124.0(2) . . ?
C17 C16 C21 120.0(2) . . ?
O3 C16 C21 116.0(2) . . ?
C16 C17 C18 120.6(3) . . ?
C16 C17 H17 119.7 . . ?
C18 C17 H17 119.7 . . ?
C19 C18 C17 119.6(3) . . ?
C19 C18 H18 120.2 . . ?
C17 C18 H18 120.2 . . ?
C18 C19 C20 120.3(3) . . ?
C18 C19 H19 119.8 . . ?
C20 C19 H19 119.8 . . ?
C21 C20 C19 120.6(3) . . ?
C21 C20 H20 119.7 . . ?
C19 C20 H20 119.7 . . ?
O4 C21 C20 124.6(2) . . ?
O4 C21 C16 116.5(2) . . ?
C20 C21 C16 118.9(3) . . ?
O4 C22 H22A 109.5 . . ?
O4 C22 H22B 109.5 . . ?
H22A C22 H22B 109.5 . . ?
O4 C22 H22C 109.5 . . ?
H22A C22 H22C 109.5 . . ?
H22B C22 H22C 109.5 . . ?
N3 C23 C26 107.8(2) . . ?
N3 C23 C25 111.0(2) . . ?
C26 C23 C25 110.4(3) . . ?
N3 C23 C24 106.9(2) . . ?
C26 C23 C24 110.0(3) . . ?
C25 C23 C24 110.6(2) . . ?
C23 C24 H24A 109.5 . . ?
C23 C24 H24B 109.5 . . ?
H24A C24 H24B 109.5 . . ?
C23 C24 H24C 109.5 . . ?
H24A C24 H24C 109.5 . . ?
H24B C24 H24C 109.5 . . ?
C23 C25 H25A 109.5 . . ?
C23 C25 H25B 109.5 . . ?
H25A C25 H25B 109.5 . . ?
C23 C25 H25C 109.5 . . ?
H25A C25 H25C 109.5 . . ?
H25B C25 H25C 109.5 . . ?
C23 C26 H26A 109.5 . . ?
C23 C26 H26B 109.5 . . ?
H26A C26 H26B 109.5 . . ?
C23 C26 H26C 109.5 . . ?
H26A C26 H26C 109.5 . . ?
H26B C26 H26C 109.5 . . ?
N4 C27 C30A 103.5(5) . . ?
N4 C27 C29A 109.0(5) . . ?
C30A C27 C29A 120.1(7) . . ?
N4 C27 C29 108.8(3) . . ?
C30A C27 C29 146.7(5) . . ?
C29A C27 C29 40.8(5) . . ?
N4 C27 C28 109.1(3) . . ?
C30A C27 C28 66.7(7) . . ?
C29A C27 C28 137.8(5) . . ?
C29 C27 C28 108.5(4) . . ?
N4 C27 C28A 102.8(6) . . ?
C30A C27 C28A 109.0(9) . . ?
C29A C27 C28A 110.8(8) . . ?
C29 C27 C28A 71.4(6) . . ?
C28 C27 C28A 42.5(6) . . ?
N4 C27 C30 111.8(3) . . ?
C30A C27 C30 50.9(6) . . ?
C29A C27 C30 70.6(5) . . ?
C29 C27 C30 108.0(3) . . ?
C28 C27 C30 110.6(4) . . ?
C28A C27 C30 142.9(6) . . ?
C27 C28 H28A 109.5 . . ?
C27 C28 H28B 109.5 . . ?
H28A C28 H28B 109.5 . . ?
C27 C28 H28C 109.5 . . ?
H28A C28 H28C 109.5 . . ?
H28B C28 H28C 109.5 . . ?
C27 C29 H29A 109.5 . . ?
C27 C29 H29B 109.5 . . ?
H29A C29 H29B 109.5 . . ?
C27 C29 H29C 109.5 . . ?
H29A C29 H29C 109.5 . . ?
H29B C29 H29C 109.5 . . ?
C27 C30 H30A 109.5 . . ?
C27 C30 H30B 109.5 . . ?
H30A C30 H30B 109.5 . . ?
C27 C30 H30C 109.5 . . ?
H30A C30 H30C 109.5 . . ?
H30B C30 H30C 109.5 . . ?
C27 C28A H28D 109.5 . . ?
C27 C28A H28E 109.5 . . ?
H28D C28A H28E 109.5 . . ?
C27 C28A H28F 109.5 . . ?
H28D C28A H28F 109.5 . . ?
H28E C28A H28F 109.5 . . ?
C27 C29A H29D 109.5 . . ?
C27 C29A H29E 109.5 . . ?
H29D C29A H29E 109.5 . . ?
C27 C29A H29F 109.5 . . ?
H29D C29A H29F 109.5 . . ?
H29E C29A H29F 109.5 . . ?
C27 C30A H30D 109.5 . . ?
C27 C30A H30E 109.5 . . ?
H30D C30A H30E 109.5 . . ?
C27 C30A H30F 109.5 . . ?
H30D C30A H30F 109.5 . . ?
H30E C30A H30F 109.5 . . ?
C32 C31 C36 120.7(3) . . ?
C32 C31 O5 124.7(3) . . ?
C36 C31 O5 114.6(3) . . ?
C31 C32 C33 120.3(3) . . ?
C31 C32 H32 119.8 . . ?
C33 C32 H32 119.8 . . ?
C34 C33 C32 118.8(3) . . ?
C34 C33 H33 120.6 . . ?
C32 C33 H33 120.6 . . ?
C33 C34 C35 122.3(3) . . ?
C33 C34 H34 118.8 . . ?
C35 C34 H34 118.8 . . ?
C34 C35 C36 119.8(3) . . ?
C34 C35 H35 120.1 . . ?
C36 C35 H35 120.1 . . ?
O6 C36 C31 115.3(3) . . ?
O6 C36 C35 126.8(3) . . ?
C31 C36 C35 117.9(3) . . ?
O6 C37 H37A 109.5 . . ?
O6 C37 H37B 109.5 . . ?
H37A C37 H37B 109.5 . . ?
O6 C37 H37C 109.5 . . ?
H37A C37 H37C 109.5 . . ?
H37B C37 H37C 109.5 . . ?
N5 C45 Ag2 174.7(3) . . ?
N6 C46 Ag2 175.1(3) . 2 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 N5 2.301(3) . ?
Ag1 N6 2.340(3) . ?
Ag1 P1 2.4178(6) . ?
Ag1 P3 2.4228(6) . ?
Ag2 C45 2.042(3) . ?
Ag2 C46 2.054(3) 2_545 ?
P1 O1 1.6217(18) . ?
P1 N2 1.682(2) . ?
P1 N1 1.692(2) . ?
P1 P2 2.5460(9) . ?
P2 O3 1.6652(19) . ?
P2 N1 1.709(2) . ?
P2 N2 1.712(2) . ?
P3 O5 1.6107(19) . ?
P3 N4 1.687(2) . ?
P3 N3 1.689(2) . ?
P3 P4A 2.496(5) . ?
P3 P4 2.5652(11) . ?
P4 O7 1.657(2) . ?
P4 N4 1.694(2) . ?
P4 N3 1.754(3) . ?
O7 C38 1.386(3) . ?
O8 C43 1.371(4) . ?
O8 C44 1.415(4) . ?
C38 C39 1.384(4) . ?
C38 C43 1.396(4) . ?
C39 C40 1.396(4) . ?
C39 H39 0.9500 . ?
C40 C41 1.379(4) . ?
C40 H40 0.9500 . ?
C41 C42 1.388(5) . ?
C41 H41 0.9500 . ?
C42 C43 1.388(4) . ?
C42 H42 0.9500 . ?
C44 H44A 0.9800 . ?
C44 H44B 0.9800 . ?
C44 H44C 0.9800 . ?
P4A N3 1.514(6) . ?
P4A O7A 1.654(11) . ?
P4A N4 1.778(6) . ?
O7A C38A 1.371(13) . ?
O8A C43A 1.328(15) . ?
O8A C44A 1.429(17) . ?
C38A C43A 1.386(7) . ?
C38A C39A 1.392(7) . ?
C39A C40A 1.396(7) . ?
C39A H39A 0.9500 . ?
C41A C40A 1.394(7) . ?
C41A C42A 1.395(7) . ?
C41A H41A 0.9500 . ?
C40A H40A 0.9500 . ?
C42A C43A 1.393(7) . ?
C42A H42A 0.9500 . ?
C44A H44D 0.9800 . ?
C44A H44E 0.9800 . ?
C44A H44F 0.9800 . ?
O1 C9 1.394(3) . ?
O2 C14 1.351(4) . ?
O2 C15 1.425(4) . ?
O3 C16 1.386(3) . ?
O4 C21 1.358(3) . ?
O4 C22 1.435(3) . ?
O5 C31 1.395(3) . ?
O6 C36 1.356(4) . ?
O6 C37 1.432(4) . ?
N1 C1 1.489(3) . ?
N2 C5 1.482(3) . ?
N3 C23 1.479(3) . ?
N4 C27 1.481(3) . ?
N5 C45 1.129(4) . ?
N6 C46 1.125(4) . ?
C1 C4 1.524(4) . ?
C1 C3 1.525(4) . ?
C1 C2 1.526(4) . ?
C2 H2A 0.9800 . ?
C2 H2B 0.9800 . ?
C2 H2C 0.9800 . ?
C3 H3A 0.9800 . ?
C3 H3B 0.9800 . ?
C3 H3C 0.9800 . ?
C4 H4A 0.9800 . ?
C4 H4B 0.9800 . ?
C4 H4C 0.9800 . ?
C5 C6A 1.499(10) . ?
C5 C8 1.518(10) . ?
C5 C8A 1.520(12) . ?
C5 C6 1.525(8) . ?
C5 C7A 1.529(8) . ?
C5 C7 1.541(7) . ?
C6 H6A 0.9800 . ?
C6 H6B 0.9800 . ?
C6 H6C 0.9800 . ?
C7 H7A 0.9800 . ?
C7 H7B 0.9800 . ?
C7 H7C 0.9800 . ?
C8 H8A 0.9800 . ?
C8 H8B 0.9800 . ?
C8 H8C 0.9800 . ?
C6A H6AA 0.9800 . ?
C6A H6AB 0.9800 . ?
C6A H6AC 0.9800 . ?
C7A H7AA 0.9800 . ?
C7A H7AB 0.9800 . ?
C7A H7AC 0.9800 . ?
C8A H8AA 0.9800 . ?
C8A H8AB 0.9800 . ?
C8A H8AC 0.9800 . ?
C9 C10 1.370(4) . ?
C9 C14 1.404(4) . ?
C10 C11 1.396(4) . ?
C10 H10 0.9500 . ?
C11 C12 1.376(4) . ?
C11 H11 0.9500 . ?
C12 C13 1.385(5) . ?
C12 H12 0.9500 . ?
C13 C14 1.386(4) . ?
C13 H13 0.9500 . ?
C15 H15A 0.9800 . ?
C15 H15B 0.9800 . ?
C15 H15C 0.9800 . ?
C16 C17 1.378(4) . ?
C16 C21 1.408(4) . ?
C17 C18 1.392(4) . ?
C17 H17 0.9500 . ?
C18 C19 1.379(4) . ?
C18 H18 0.9500 . ?
C19 C20 1.389(4) . ?
C19 H19 0.9500 . ?
C20 C21 1.388(4) . ?
C20 H20 0.9500 . ?
C22 H22A 0.9800 . ?
C22 H22B 0.9800 . ?
C22 H22C 0.9800 . ?
C23 C26 1.522(4) . ?
C23 C25 1.525(4) . ?
C23 C24 1.529(4) . ?
C24 H24A 0.9800 . ?
C24 H24B 0.9800 . ?
C24 H24C 0.9800 . ?
C25 H25A 0.9800 . ?
C25 H25B 0.9800 . ?
C25 H25C 0.9800 . ?
C26 H26A 0.9800 . ?
C26 H26B 0.9800 . ?
C26 H26C 0.9800 . ?
C27 C30A 1.482(10) . ?
C27 C29A 1.487(10) . ?
C27 C29 1.519(5) . ?
C27 C28 1.526(5) . ?
C27 C28A 1.543(12) . ?
C27 C30 1.552(5) . ?
C28 H28A 0.9800 . ?
C28 H28B 0.9800 . ?
C28 H28C 0.9800 . ?
C29 H29A 0.9800 . ?
C29 H29B 0.9800 . ?
C29 H29C 0.9800 . ?
C30 H30A 0.9800 . ?
C30 H30B 0.9800 . ?
C30 H30C 0.9800 . ?
C28A H28D 0.9800 . ?
C28A H28E 0.9800 . ?
C28A H28F 0.9800 . ?
C29A H29D 0.9800 . ?
C29A H29E 0.9800 . ?
C29A H29F 0.9800 . ?
C30A H30D 0.9800 . ?
C30A H30E 0.9800 . ?
C30A H30F 0.9800 . ?
C31 C32 1.381(5) . ?
C31 C36 1.388(4) . ?
C32 C33 1.401(4) . ?
C32 H32 0.9500 . ?
C33 C34 1.347(5) . ?
C33 H33 0.9500 . ?
C34 C35 1.371(6) . ?
C34 H34 0.9500 . ?
C35 C36 1.415(5) . ?
C35 H35 0.9500 . ?
C37 H37A 0.9800 . ?
C37 H37B 0.9800 . ?
C37 H37C 0.9800 . ?
C46 Ag2 2.054(3) 2 ?
