#------------------------------------------------------------------------------
#$Date: 2017-07-11 15:10:40 +0300 (Tue, 11 Jul 2017) $
#$Revision: 198633 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/00/59/7005973.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7005973
loop_
_publ_author_name
'Chong, Siew Huay'
'Henderson, William'
'Hor, T. S. Andy'
_publ_section_title
;
 Stable diplatinum complexes with functional thiolato bridges from
 dialkylation of [Pt2(mu-S)2(P-P)2] [P-P=2 x PPh3, Ph2P(CH2)3PPh2].
;
_journal_issue                   36
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              4008
_journal_page_last               4016
_journal_paper_doi               10.1039/b707526j
_journal_year                    2007
_chemical_formula_sum            'C77 H69 F6 O2 P5 Pt2 S2'
_chemical_formula_weight         1749.47
_chemical_name_systematic
;
?
;
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.508(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   17.5679(16)
_cell_length_b                   19.0008(16)
_cell_length_c                   21.5327(19)
_cell_measurement_reflns_used    5961
_cell_measurement_temperature    223(2)
_cell_measurement_theta_max      26.84
_cell_measurement_theta_min      2.32
_cell_volume                     7187.4(11)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      223(2)
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0574
_diffrn_reflns_av_sigmaI/netI    0.0669
_diffrn_reflns_limit_h_max       20
_diffrn_reflns_limit_h_min       -22
_diffrn_reflns_limit_k_max       24
_diffrn_reflns_limit_k_min       -15
_diffrn_reflns_limit_l_max       27
_diffrn_reflns_limit_l_min       -27
_diffrn_reflns_number            24358
_diffrn_reflns_theta_full        27.50
_diffrn_reflns_theta_max         27.50
_diffrn_reflns_theta_min         1.58
_exptl_absorpt_coefficient_mu    4.119
_exptl_absorpt_correction_T_max  0.6835
_exptl_absorpt_correction_T_min  0.3036
_exptl_absorpt_correction_type   'Sadabs, (Sheldrick 2001)'
_exptl_crystal_colour            Yellow
_exptl_crystal_density_diffrn    1.617
_exptl_crystal_density_meas      0
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Block
_exptl_crystal_F_000             3456
_exptl_crystal_size_max          0.38
_exptl_crystal_size_mid          0.20
_exptl_crystal_size_min          0.10
_refine_diff_density_max         2.377
_refine_diff_density_min         -0.593
_refine_diff_density_rms         0.137
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.985
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     457
_refine_ls_number_reflns         8243
_refine_ls_number_restraints     49
_refine_ls_restrained_S_all      0.988
_refine_ls_R_factor_all          0.0702
_refine_ls_R_factor_gt           0.0435
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0609P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1117
_refine_ls_wR_factor_ref         0.1243
_reflns_number_gt                5509
_reflns_number_total             8243
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b707526j.txt
_cod_data_source_block           6372
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 

The following automatic conversions were performed:

'_refine_ls_hydrogen_treatment' value 'contr' was replaced with the
value 'constr' as specified in the replacement file
'src/cod-tools/trunk/data/replacement-values/replacement_values.lst'.

Automatic conversion script
Id: cif_fix_values 5376 2017-05-30 11:51:03Z andrius 
;
_cod_original_sg_symbol_H-M      C2/c
_cod_database_code               7005973
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Pt1 Pt 0.494544(10) 0.252894(9) 0.330354(9) 0.04068(9) Uani 1 1 d . . .
S1 S 0.58687(8) 0.27176(9) 0.25410(7) 0.0524(3) Uani 1 1 d . . .
P1 P 0.59322(8) 0.24003(7) 0.40036(8) 0.0470(3) Uani 1 1 d . . .
P2 P 0.39391(8) 0.23908(7) 0.39533(7) 0.0419(3) Uani 1 1 d . . .
C1 C 0.6077(6) 0.3655(5) 0.2494(5) 0.060(3) Uani 0.50 1 d PDU A -1
H1A H 0.6455 0.3777 0.2814 0.072 Uiso 0.50 1 calc PR A -1
H1B H 0.6297 0.3759 0.2088 0.072 Uiso 0.50 1 calc PR A -1
C2 C 0.5362(6) 0.4108(5) 0.2584(7) 0.079(4) Uani 0.50 1 d PDU A -1
H2A H 0.5259 0.4159 0.3028 0.095 Uiso 0.50 1 calc PR A -1
H2B H 0.4923 0.3877 0.2388 0.095 Uiso 0.50 1 calc PR A -1
C3 C 0.5483(8) 0.4837(6) 0.2292(8) 0.109(6) Uani 0.50 1 d PDU A -1
C4 C 0.5253(17) 0.6112(8) 0.2629(17) 0.186(13) Uani 0.50 1 d PDU A -1
H4A H 0.5624 0.6252 0.2315 0.224 Uiso 0.50 1 calc PR A -1
H4B H 0.5404 0.6331 0.3023 0.224 Uiso 0.50 1 calc PR A -1
C5 C 0.446(2) 0.6387(17) 0.244(3) 0.36(3) Uani 0.50 1 d PDU A -1
H5A H 0.4488 0.6894 0.2382 0.537 Uiso 0.50 1 calc PR A -1
H5B H 0.4100 0.6276 0.2759 0.537 Uiso 0.50 1 calc PR A -1
H5C H 0.4307 0.6167 0.2051 0.537 Uiso 0.50 1 calc PR A -1
O1 O 0.5276(10) 0.5347(6) 0.2700(7) 0.157(7) Uani 0.50 1 d PDU A -1
O2 O 0.5700(9) 0.4977(7) 0.1794(7) 0.157(6) Uani 0.50 1 d PDU A -1
C1A C 0.6595(3) 0.3126(3) 0.3883(3) 0.0604(15) Uani 1 1 d . A .
C2A C 0.7331(3) 0.3037(3) 0.3710(3) 0.0642(16) Uani 1 1 d . . .
H2A' H 0.7533 0.2579 0.3688 0.077 Uiso 1 1 calc R A .
C3A C 0.7790(4) 0.3604(4) 0.3564(3) 0.082(2) Uani 1 1 d . A .
H3A H 0.8290 0.3526 0.3427 0.099 Uiso 1 1 calc R . .
C4A C 0.7529(5) 0.4269(4) 0.3617(5) 0.111(3) Uani 1 1 d . . .
H4A' H 0.7848 0.4654 0.3531 0.134 Uiso 1 1 calc R A .
C5A C 0.6800(6) 0.4375(4) 0.3797(7) 0.175(6) Uani 1 1 d . A .
H5A' H 0.6610 0.4836 0.3828 0.211 Uiso 1 1 calc R . .
C6A C 0.6328(5) 0.3805(4) 0.3935(5) 0.142(5) Uani 1 1 d . . .
H6A H 0.5826 0.3885 0.4064 0.171 Uiso 1 1 calc R A .
C1B C 0.5771(3) 0.2378(3) 0.4840(3) 0.0590(16) Uani 1 1 d . A .
C2B C 0.5469(3) 0.1779(3) 0.5101(3) 0.0628(15) Uani 1 1 d . . .
H2B' H 0.5365 0.1387 0.4847 0.075 Uiso 1 1 calc R A .
C3B C 0.5312(4) 0.1745(4) 0.5739(3) 0.081(2) Uani 1 1 d . A .
H3B H 0.5107 0.1330 0.5908 0.097 Uiso 1 1 calc R . .
C4B C 0.5451(5) 0.2301(5) 0.6111(4) 0.090(2) Uani 1 1 d . . .
H4B' H 0.5333 0.2280 0.6535 0.109 Uiso 1 1 calc R A .
C5B C 0.5768(5) 0.2901(6) 0.5864(4) 0.106(3) Uani 1 1 d . A .
H5B' H 0.5876 0.3286 0.6123 0.128 Uiso 1 1 calc R . .
C6B C 0.5930(4) 0.2941(4) 0.5229(3) 0.085(2) Uani 1 1 d . . .
H6B H 0.6149 0.3353 0.5066 0.102 Uiso 1 1 calc R A .
C1C C 0.6496(3) 0.1609(3) 0.3877(3) 0.0505(13) Uani 1 1 d . A .
C2C C 0.7085(3) 0.1431(3) 0.4298(3) 0.0558(14) Uani 1 1 d . . .
H2C H 0.7168 0.1705 0.4656 0.067 Uiso 1 1 calc R A .
C3C C 0.7540(3) 0.0855(3) 0.4181(3) 0.071(2) Uani 1 1 d . A .
H3C H 0.7941 0.0745 0.4457 0.085 Uiso 1 1 calc R . .
C4C C 0.7417(4) 0.0441(3) 0.3672(4) 0.0738(19) Uani 1 1 d . . .
H4C H 0.7732 0.0051 0.3597 0.089 Uiso 1 1 calc R A .
C5C C 0.6827(4) 0.0599(3) 0.3265(3) 0.0728(19) Uani 1 1 d . A .
H5C' H 0.6735 0.0307 0.2920 0.087 Uiso 1 1 calc R . .
C6C C 0.6368(3) 0.1182(3) 0.3361(3) 0.0599(15) Uani 1 1 d . . .
H6C H 0.5974 0.1289 0.3078 0.072 Uiso 1 1 calc R A .
C1D C 0.3816(3) 0.1512(3) 0.4269(2) 0.0465(12) Uani 1 1 d . A .
C2D C 0.4292(3) 0.0980(3) 0.4066(3) 0.0601(15) Uani 1 1 d . . .
H2D H 0.4672 0.1079 0.3774 0.072 Uiso 1 1 calc R A .
C3D C 0.4210(4) 0.0305(3) 0.4290(4) 0.084(2) Uani 1 1 d . A .
H3D H 0.4519 -0.0058 0.4136 0.101 Uiso 1 1 calc R . .
C4D C 0.3679(4) 0.0159(3) 0.4737(4) 0.086(2) Uani 1 1 d . . .
H4D H 0.3651 -0.0293 0.4911 0.104 Uiso 1 1 calc R A .
C5D C 0.3188(4) 0.0682(3) 0.4928(3) 0.080(2) Uani 1 1 d . A .
H5D H 0.2807 0.0580 0.5218 0.096 Uiso 1 1 calc R . .
C6D C 0.3258(3) 0.1349(3) 0.4695(3) 0.0629(15) Uani 1 1 d . . .
H6D H 0.2922 0.1702 0.4827 0.076 Uiso 1 1 calc R A .
C1E C 0.3005(3) 0.2543(3) 0.3597(3) 0.0513(14) Uani 1 1 d . A .
C2E C 0.2750(3) 0.2043(4) 0.3174(3) 0.0728(18) Uani 1 1 d . . .
H2E H 0.3035 0.1632 0.3108 0.087 Uiso 1 1 calc R A .
C3E C 0.2078(5) 0.2150(5) 0.2848(4) 0.099(3) Uani 1 1 d . A .
H3E H 0.1910 0.1816 0.2555 0.118 Uiso 1 1 calc R . .
C4E C 0.1654(5) 0.2752(6) 0.2954(5) 0.111(3) Uani 1 1 d . . .
H4E H 0.1194 0.2823 0.2736 0.133 Uiso 1 1 calc R A .
C5E C 0.1898(4) 0.3246(4) 0.3377(4) 0.091(2) Uani 1 1 d . A .
H5E H 0.1613 0.3656 0.3448 0.109 Uiso 1 1 calc R . .
C6E C 0.2572(3) 0.3129(3) 0.3694(3) 0.0673(17) Uani 1 1 d . . .
H6E H 0.2739 0.3463 0.3987 0.081 Uiso 1 1 calc R A .
C1F C 0.3983(3) 0.3038(3) 0.4576(2) 0.0497(13) Uani 1 1 d . A .
C2F C 0.3859(3) 0.2916(4) 0.5193(3) 0.0685(17) Uani 1 1 d . . .
H2F H 0.3728 0.2460 0.5324 0.082 Uiso 1 1 calc R A .
C3F C 0.3921(4) 0.3448(5) 0.5629(4) 0.099(3) Uani 1 1 d . A .
H3F H 0.3840 0.3351 0.6052 0.119 Uiso 1 1 calc R . .
C4F C 0.4099(5) 0.4110(5) 0.5443(5) 0.118(4) Uani 1 1 d . . .
H4F H 0.4137 0.4474 0.5738 0.142 Uiso 1 1 calc R A .
C5F C 0.4223(4) 0.4251(4) 0.4833(5) 0.097(3) Uani 1 1 d . A .
H5F H 0.4342 0.4712 0.4709 0.116 Uiso 1 1 calc R . .
C6F C 0.4173(4) 0.3716(3) 0.4391(3) 0.0715(18) Uani 1 1 d . . .
H6F H 0.4269 0.3814 0.3971 0.086 Uiso 1 1 calc R A .
P3 P 0.5000 0.05617(13) 0.7500 0.0621(6) Uani 1 2 d S . .
F1 F 0.5000 -0.0262(3) 0.7500 0.104(2) Uani 1 2 d S . .
F2 F 0.5825(2) 0.0573(3) 0.7214(2) 0.1138(15) Uani 1 1 d . . .
F3 F 0.4625(2) 0.0562(2) 0.68286(19) 0.0981(13) Uani 1 1 d . . .
F4 F 0.5000 0.1400(4) 0.7500 0.143(3) Uani 1 2 d S . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
P2 Pt1 P1 99.76(5) . . ?
P2 Pt1 S1 91.30(5) . 2_655 ?
P1 Pt1 S1 168.85(5) . 2_655 ?
P2 Pt1 S1 172.79(5) . . ?
P1 Pt1 S1 87.32(5) . . ?
S1 Pt1 S1 81.59(6) 2_655 . ?
C1 S1 Pt1 103.3(4) . 2_655 ?
C1 S1 Pt1 109.2(3) . . ?
Pt1 S1 Pt1 95.70(5) 2_655 . ?
C1C P1 C1A 104.7(3) . . ?
C1C P1 C1B 102.5(3) . . ?
C1A P1 C1B 105.2(3) . . ?
C1C P1 Pt1 113.39(19) . . ?
C1A P1 Pt1 107.7(2) . . ?
C1B P1 Pt1 121.8(2) . . ?
C1D P2 C1F 110.4(2) . . ?
C1D P2 C1E 101.1(2) . . ?
C1F P2 C1E 103.5(2) . . ?
C1D P2 Pt1 115.57(18) . . ?
C1F P2 Pt1 110.27(19) . . ?
C1E P2 Pt1 115.00(19) . . ?
C2 C1 S1 112.1(7) . . ?
C1 C2 C3 109.8(9) . . ?
O2 C3 O1 121.3(13) . . ?
O2 C3 C2 128.7(15) . . ?
O1 C3 C2 109.9(12) . . ?
O1 C4 C5 113.0(13) . . ?
C3 O1 C4 130(2) . . ?
C2A C1A C6A 117.7(6) . . ?
C2A C1A P1 123.6(4) . . ?
C6A C1A P1 118.5(5) . . ?
C1A C2A C3A 121.5(6) . . ?
C4A C3A C2A 120.7(7) . . ?
C3A C4A C5A 119.0(7) . . ?
C4A C5A C6A 120.6(8) . . ?
C1A C6A C5A 120.4(7) . . ?
C2B C1B C6B 117.9(7) . . ?
C2B C1B P1 119.0(5) . . ?
C6B C1B P1 123.1(6) . . ?
C1B C2B C3B 121.1(6) . . ?
C4B C3B C2B 120.6(7) . . ?
C3B C4B C5B 119.4(8) . . ?
C4B C5B C6B 120.6(8) . . ?
C1B C6B C5B 120.4(8) . . ?
C6C C1C C2C 119.1(5) . . ?
C6C C1C P1 121.1(4) . . ?
C2C C1C P1 119.9(4) . . ?
C3C C2C C1C 119.7(5) . . ?
C4C C3C C2C 121.0(6) . . ?
C3C C4C C5C 119.7(6) . . ?
C4C C5C C6C 120.8(6) . . ?
C5C C6C C1C 119.6(6) . . ?
C6D C1D C2D 118.6(5) . . ?
C6D C1D P2 122.8(4) . . ?
C2D C1D P2 118.5(4) . . ?
C3D C2D C1D 120.1(6) . . ?
C4D C3D C2D 120.5(6) . . ?
C3D C4D C5D 119.5(6) . . ?
C6D C5D C4D 119.8(6) . . ?
C5D C6D C1D 121.2(6) . . ?
C6E C1E C2E 118.8(6) . . ?
C6E C1E P2 124.3(5) . . ?
C2E C1E P2 116.8(4) . . ?
C3E C2E C1E 120.1(7) . . ?
C2E C3E C4E 119.7(9) . . ?
C5E C4E C3E 120.5(7) . . ?
C4E C5E C6E 118.7(7) . . ?
C1E C6E C5E 122.2(7) . . ?
C2F C1F C6F 118.4(5) . . ?
C2F C1F P2 126.5(5) . . ?
C6F C1F P2 115.1(4) . . ?
C1F C2F C3F 121.6(7) . . ?
C4F C3F C2F 119.6(8) . . ?
C3F C4F C5F 120.4(7) . . ?
C4F C5F C6F 120.4(8) . . ?
C1F C6F C5F 119.6(7) . . ?
F1 P3 F2 90.8(2) . 2_656 ?
F1 P3 F2 90.8(2) . . ?
F2 P3 F2 178.4(4) 2_656 . ?
F1 P3 F3 90.04(18) . 2_656 ?
F2 P3 F3 91.1(2) 2_656 2_656 ?
F2 P3 F3 88.9(2) . 2_656 ?
F1 P3 F3 90.05(18) . . ?
F2 P3 F3 88.9(2) 2_656 . ?
F2 P3 F3 91.1(2) . . ?
F3 P3 F3 179.9(4) 2_656 . ?
F1 P3 F4 180.000(2) . . ?
F2 P3 F4 89.2(2) 2_656 . ?
F2 P3 F4 89.2(2) . . ?
F3 P3 F4 89.96(18) 2_656 . ?
F3 P3 F4 89.95(18) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pt1 P2 2.2795(14) . ?
Pt1 P1 2.3002(15) . ?
Pt1 S1 2.3312(14) 2_655 ?
Pt1 S1 2.3458(14) . ?
S1 C1 1.821(11) . ?
S1 Pt1 2.3312(15) 2_655 ?
P1 C1C 1.822(5) . ?
P1 C1A 1.826(6) . ?
P1 C1B 1.826(7) . ?
P2 C1D 1.816(5) . ?
P2 C1F 1.820(5) . ?
P2 C1E 1.828(6) . ?
C1 C2 1.536(5) . ?
C2 C3 1.538(5) . ?
C3 O2 1.173(18) . ?
C3 O1 1.359(9) . ?
C4 O1 1.461(10) . ?
C4 C5 1.534(5) . ?
C1A C2A 1.359(8) . ?
C1A C6A 1.377(9) . ?
C2A C3A 1.384(8) . ?
C3A C4A 1.350(10) . ?
C4A C5A 1.356(12) . ?
C5A C6A 1.398(11) . ?
C1B C2B 1.377(8) . ?
C1B C6B 1.387(9) . ?
C2B C3B 1.406(9) . ?
C3B C4B 1.347(10) . ?
C4B C5B 1.378(13) . ?
C5B C6B 1.400(11) . ?
C1C C6C 1.393(8) . ?
C1C C2C 1.411(7) . ?
C2C C3C 1.380(8) . ?
C3C C4C 1.365(9) . ?
C4C C5C 1.384(9) . ?
C5C C6C 1.386(8) . ?
C1D C6D 1.383(7) . ?
C1D C2D 1.387(7) . ?
C2D C3D 1.377(8) . ?
C3D C4D 1.373(10) . ?
C4D C5D 1.381(9) . ?
C5D C6D 1.368(8) . ?
C1E C6E 1.365(7) . ?
C1E C2E 1.388(8) . ?
C2E C3E 1.384(9) . ?
C3E C4E 1.385(14) . ?
C4E C5E 1.373(12) . ?
C5E C6E 1.380(9) . ?
C1F C2F 1.368(8) . ?
C1F C6F 1.391(8) . ?
C2F C3F 1.383(9) . ?
C3F C4F 1.358(12) . ?
C4F C5F 1.359(12) . ?
C5F C6F 1.396(9) . ?
P3 F1 1.565(6) . ?
P3 F2 1.580(4) 2_656 ?
P3 F2 1.580(4) . ?
P3 F3 1.584(4) 2_656 ?
P3 F3 1.584(4) . ?
P3 F4 1.592(7) . ?
