#------------------------------------------------------------------------------
#$Date: 2016-03-25 10:51:43 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179767 $
#$URL: svn://www.crystallography.net/cod/cif/7/00/63/7006303.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7006303
loop_
_publ_author_name
'Kozlova, Marina N.'
'Ferlay, Sylvie'
'Solovieva, Svetlana E.'
'Antipin, Igor S.'
'Konovalov, Alexander I.'
'Kyritsakas, Nathalie'
'Hosseini, Mir Wais'
_publ_section_title
;
 Molecular tectonics: on the formation of 1-D silver coordination
 networks by thiacalixarenes bearing nitrile groups.
;
_journal_issue                   44
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              5126
_journal_page_last               5131
_journal_paper_doi               10.1039/b712351e
_journal_year                    2007
_chemical_formula_moiety
'4(C56 H68 Ag N4 O4 S4), 4(F6 Sb), 7(C2 H2 Cl6)'
_chemical_formula_sum            'C232 H280 Ag4 Cl24 F24 N16 O16 S16 Sb4'
_chemical_formula_weight         6286.96
_chemical_name_systematic
;
?
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 94.169(2)
_cell_angle_gamma                90.00
_cell_formula_units_Z            1
_cell_length_a                   16.4840(3)
_cell_length_b                   15.0260(4)
_cell_length_c                   28.9440(6)
_cell_measurement_reflns_used    16787
_cell_measurement_temperature    173(2)
_cell_measurement_theta_max      27.878
_cell_measurement_theta_min      0.998
_cell_volume                     7150.1(3)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      173(2)
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0364
_diffrn_reflns_av_sigmaI/netI    0.0652
_diffrn_reflns_limit_h_max       21
_diffrn_reflns_limit_h_min       -21
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_k_min       -19
_diffrn_reflns_limit_l_max       38
_diffrn_reflns_limit_l_min       -38
_diffrn_reflns_number            30216
_diffrn_reflns_theta_full        27.88
_diffrn_reflns_theta_max         27.88
_diffrn_reflns_theta_min         1.53
_exptl_absorpt_coefficient_mu    1.052
_exptl_absorpt_correction_T_max  0.9021
_exptl_absorpt_correction_T_min  0.9021
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   sadabs
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.460
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             3184
_exptl_crystal_size_max          0.14
_exptl_crystal_size_mid          0.12
_exptl_crystal_size_min          0.10
_refine_diff_density_max         1.970
_refine_diff_density_min         -1.731
_refine_diff_density_rms         0.176
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.038
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     737
_refine_ls_number_reflns         17018
_refine_ls_number_restraints     14
_refine_ls_restrained_S_all      1.039
_refine_ls_R_factor_all          0.1425
_refine_ls_R_factor_gt           0.0952
_refine_ls_shift/su_max          0.015
_refine_ls_shift/su_mean         0.001
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1800P)²+24.7861P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2798
_refine_ls_wR_factor_ref         0.2959
_reflns_number_gt                10411
_reflns_number_total             17018
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b712351e.txt
_cod_data_source_block           shelxl_3-SbF6
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 

The following automatic conversions were performed:

'_exptl_crystal_density_meas' value 'none' was changed to '?' - the
value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 3008 2015-01-20 13:52:24Z robertas 
;
_cod_original_sg_symbol_H-M      P21/c
_cod_database_code               7006303
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.87961(3) 0.17808(5) 0.34380(3) 0.0621(2) Uani 1 1 d . . .
S1 S 0.38380(11) 0.04927(11) 0.46152(6) 0.0377(4) Uani 1 1 d . . .
C1 C 0.4328(4) 0.1538(4) 0.4578(2) 0.0323(13) Uani 1 1 d . . .
C2 C 0.3886(4) 0.2307(4) 0.4429(2) 0.0332(13) Uani 1 1 d . . .
C3 C 0.4283(4) 0.3125(4) 0.4461(2) 0.0322(13) Uani 1 1 d . . .
C4 C 0.5082(4) 0.3186(4) 0.4649(2) 0.0335(13) Uani 1 1 d . . .
H4 H 0.5339 0.3752 0.4669 0.040 Uiso 1 1 calc R . .
C5 C 0.5514(4) 0.2440(4) 0.4807(2) 0.0371(14) Uani 1 1 d . . .
C6 C 0.5124(4) 0.1604(4) 0.4762(2) 0.0344(13) Uani 1 1 d . . .
H6 H 0.5412 0.1081 0.4858 0.041 Uiso 1 1 calc R . .
C7 C 0.6396(7) 0.2489(8) 0.5022(5) 0.0883(18) Uani 1 1 d . . .
C8 C 0.6708(7) 0.3410(8) 0.5053(5) 0.0883(18) Uani 1 1 d . . .
H8A H 0.7291 0.3399 0.5150 0.132 Uiso 1 1 calc R . .
H8B H 0.6418 0.3743 0.5281 0.132 Uiso 1 1 calc R . .
H8C H 0.6624 0.3697 0.4750 0.132 Uiso 1 1 calc R . .
C9 C 0.6914(6) 0.1838(8) 0.4809(5) 0.0883(18) Uani 1 1 d . . .
H9A H 0.6987 0.2015 0.4488 0.132 Uiso 1 1 calc R . .
H9B H 0.6657 0.1250 0.4811 0.132 Uiso 1 1 calc R . .
H9C H 0.7445 0.1813 0.4984 0.132 Uiso 1 1 calc R . .
C10 C 0.6370(6) 0.2135(8) 0.5535(4) 0.0883(18) Uani 1 1 d . . .
H10A H 0.6927 0.2057 0.5672 0.132 Uiso 1 1 calc R . .
H10B H 0.6084 0.1564 0.5533 0.132 Uiso 1 1 calc R . .
H10C H 0.6085 0.2567 0.5719 0.132 Uiso 1 1 calc R . .
O1 O 0.3105(3) 0.2233(3) 0.42440(18) 0.0426(11) Uani 1 1 d . . .
C11 C 0.2531(5) 0.2341(6) 0.4572(4) 0.059(2) Uani 1 1 d . . .
H11A H 0.2589 0.2927 0.4727 0.071 Uiso 1 1 calc R . .
H11B H 0.2577 0.1864 0.4809 0.071 Uiso 1 1 calc R . .
C12 C 0.1708(5) 0.2274(7) 0.4263(4) 0.066(2) Uani 1 1 d . . .
H12A H 0.1695 0.2724 0.4013 0.079 Uiso 1 1 calc R . .
H12B H 0.1654 0.1677 0.4120 0.079 Uiso 1 1 calc R . .
C13 C 0.1021(6) 0.2434(8) 0.4569(5) 0.085(4) Uani 1 1 d . . .
H13A H 0.1057 0.2019 0.4836 0.102 Uiso 1 1 calc R . .
H13B H 0.1036 0.3052 0.4688 0.102 Uiso 1 1 calc R . .
C14 C 0.0271(7) 0.2274(8) 0.4272(5) 0.093(4) Uani 1 1 d . . .
N1 N -0.0290(7) 0.2157(8) 0.4038(5) 0.115(4) Uani 1 1 d . . .
S2 S 0.37656(11) 0.41440(10) 0.43458(6) 0.0362(4) Uani 1 1 d . . .
C15 C 0.3247(4) 0.4056(4) 0.3790(2) 0.0318(13) Uani 1 1 d . . .
C16 C 0.2468(4) 0.4424(4) 0.3744(2) 0.0356(14) Uani 1 1 d . . .
H16 H 0.2226 0.4624 0.4013 0.043 Uiso 1 1 calc R . .
C17 C 0.2038(4) 0.4505(4) 0.3315(2) 0.0357(14) Uani 1 1 d . . .
C18 C 0.2408(4) 0.4202(4) 0.2929(2) 0.0361(14) Uani 1 1 d . . .
H18 H 0.2125 0.4244 0.2632 0.043 Uiso 1 1 calc R . .
C19 C 0.3188(4) 0.3837(4) 0.2969(2) 0.0295(12) Uani 1 1 d . . .
C20 C 0.3617(4) 0.3753(4) 0.3401(2) 0.0319(13) Uani 1 1 d . . .
C21 C 0.1176(4) 0.4918(6) 0.3271(3) 0.0531(19) Uani 1 1 d . . .
C22 C 0.1252(6) 0.5880(7) 0.3444(4) 0.080(3) Uani 1 1 d . . .
H22A H 0.1358 0.5883 0.3781 0.119 Uiso 1 1 calc R . .
H22B H 0.0745 0.6200 0.3359 0.119 Uiso 1 1 calc R . .
H22C H 0.1703 0.6174 0.3301 0.119 Uiso 1 1 calc R . .
C23 C 0.0805(6) 0.4906(9) 0.2792(4) 0.086(3) Uani 1 1 d . . .
H23A H 0.0222 0.5031 0.2793 0.129 Uiso 1 1 calc R . .
H23B H 0.0883 0.4318 0.2655 0.129 Uiso 1 1 calc R . .
H23C H 0.1063 0.5359 0.2608 0.129 Uiso 1 1 calc R . .
C24 C 0.0636(6) 0.4376(9) 0.3592(5) 0.089(4) Uani 1 1 d . . .
H24A H 0.0916 0.4325 0.3901 0.133 Uiso 1 1 calc R . .
H24B H 0.0537 0.3781 0.3462 0.133 Uiso 1 1 calc R . .
H24C H 0.0116 0.4683 0.3614 0.133 Uiso 1 1 calc R . .
O2 O 0.4354(3) 0.3345(3) 0.34440(15) 0.0362(10) Uani 1 1 d . . .
C25 C 0.5049(4) 0.3929(5) 0.3426(3) 0.0439(16) Uani 1 1 d . . .
H25A H 0.5069 0.4361 0.3685 0.053 Uiso 1 1 calc R . .
H25B H 0.5023 0.4262 0.3130 0.053 Uiso 1 1 calc R . .
C26 C 0.5773(5) 0.3332(6) 0.3466(3) 0.054(2) Uani 1 1 d . . .
H26A H 0.5745 0.2902 0.3206 0.064 Uiso 1 1 calc R . .
H26B H 0.5784 0.2993 0.3759 0.064 Uiso 1 1 calc R . .
C27 C 0.6547(5) 0.3901(7) 0.3455(3) 0.060(2) Uani 1 1 d . . .
H27A H 0.6494 0.4309 0.3185 0.072 Uiso 1 1 calc R . .
H27B H 0.6615 0.4266 0.3740 0.072 Uiso 1 1 calc R . .
C28 C 0.7267(6) 0.3324(7) 0.3421(3) 0.064(2) Uani 1 1 d . . .
N2 N 0.7805(5) 0.2870(7) 0.3392(3) 0.082(3) Uani 1 1 d . . .
S3 S 0.36452(12) 0.36431(11) 0.24397(6) 0.0421(4) Uani 1 1 d . . .
C29 C 0.4205(4) 0.2636(4) 0.2491(2) 0.0341(14) Uani 1 1 d . . .
C30 C 0.4977(4) 0.2639(4) 0.2331(2) 0.0353(14) Uani 1 1 d . . .
H30 H 0.5202 0.3187 0.2238 0.042 Uiso 1 1 calc R . .
C31 C 0.5437(4) 0.1860(4) 0.2302(2) 0.0371(14) Uani 1 1 d . . .
C32 C 0.5093(4) 0.1084(4) 0.2465(2) 0.0363(14) Uani 1 1 d . . .
H32 H 0.5400 0.0549 0.2469 0.044 Uiso 1 1 calc R . .
C33 C 0.4318(4) 0.1065(4) 0.2620(2) 0.0344(13) Uani 1 1 d . . .
C34 C 0.3852(4) 0.1846(4) 0.2631(2) 0.0378(15) Uani 1 1 d . . .
C35 C 0.6284(5) 0.1817(5) 0.2123(3) 0.0454(17) Uani 1 1 d . . .
C36 C 0.6898(5) 0.1379(6) 0.2484(3) 0.060(2) Uani 1 1 d . . .
H36A H 0.7453 0.1527 0.2412 0.090 Uiso 1 1 calc R . .
H36B H 0.6826 0.0732 0.2476 0.090 Uiso 1 1 calc R . .
H36C H 0.6802 0.1601 0.2794 0.090 Uiso 1 1 calc R . .
C37 C 0.6599(6) 0.2736(6) 0.2007(4) 0.065(3) Uani 1 1 d . . .
H37A H 0.6226 0.3013 0.1770 0.098 Uiso 1 1 calc R . .
H37B H 0.7140 0.2681 0.1889 0.098 Uiso 1 1 calc R . .
H37C H 0.6635 0.3106 0.2286 0.098 Uiso 1 1 calc R . .
C38 C 0.6221(5) 0.1253(6) 0.1677(3) 0.054(2) Uani 1 1 d . . .
H38A H 0.5897 0.1573 0.1433 0.082 Uiso 1 1 calc R . .
H38B H 0.5959 0.0684 0.1737 0.082 Uiso 1 1 calc R . .
H38C H 0.6767 0.1143 0.1576 0.082 Uiso 1 1 calc R . .
O3 O 0.3093(3) 0.1828(3) 0.27907(18) 0.0495(13) Uani 1 1 d . . .
C39 C 0.2478(7) 0.1718(11) 0.2446(5) 0.113(3) Uani 1 1 d . . .
H39A H 0.2490 0.1123 0.2300 0.135 Uiso 1 1 calc R . .
H39B H 0.2481 0.2188 0.2206 0.135 Uiso 1 1 calc R . .
C40 C 0.1750(6) 0.1824(11) 0.2765(5) 0.113(3) Uani 1 1 d D . .
H40A H 0.1685 0.1274 0.2946 0.135 Uiso 1 1 calc R . .
H40B H 0.1858 0.2324 0.2984 0.135 Uiso 1 1 calc R . .
C41 C 0.0995(6) 0.2002(11) 0.2463(5) 0.113(3) Uani 1 1 d D . .
H41A H 0.1041 0.2580 0.2303 0.135 Uiso 1 1 calc R . .
H41B H 0.0916 0.1530 0.2225 0.135 Uiso 1 1 calc R . .
C42 C 0.0321(8) 0.2018(11) 0.2744(5) 0.113(3) Uani 1 1 d . . .
N3 N -0.0286(5) 0.1926(6) 0.2906(4) 0.082(3) Uani 1 1 d . . .
S4 S 0.39209(11) -0.00089(11) 0.27248(6) 0.0401(4) Uani 1 1 d . . .
C43 C 0.3405(4) 0.0053(4) 0.3232(2) 0.0335(13) Uani 1 1 d . . .
C44 C 0.2611(4) -0.0272(4) 0.3217(3) 0.0388(15) Uani 1 1 d . . .
H44 H 0.2353 -0.0448 0.2927 0.047 Uiso 1 1 calc R . .
C45 C 0.2184(4) -0.0346(4) 0.3612(2) 0.0384(15) Uani 1 1 d . . .
C46 C 0.2579(4) -0.0062(4) 0.4030(2) 0.0368(14) Uani 1 1 d . . .
H46 H 0.2297 -0.0092 0.4305 0.044 Uiso 1 1 calc R . .
C47 C 0.3370(4) 0.0261(4) 0.4055(2) 0.0334(13) Uani 1 1 d . . .
C48 C 0.3798(4) 0.0308(4) 0.3659(2) 0.0316(13) Uani 1 1 d . . .
C49 C 0.1324(4) -0.0740(5) 0.3598(3) 0.0463(17) Uani 1 1 d . . .
C50 C 0.0733(5) -0.0055(6) 0.3759(4) 0.061(2) Uani 1 1 d . . .
H50A H 0.0637 0.0402 0.3520 0.091 Uiso 1 1 calc R . .
H50B H 0.0962 0.0222 0.4046 0.091 Uiso 1 1 calc R . .
H50C H 0.0217 -0.0346 0.3816 0.091 Uiso 1 1 calc R . .
C51 C 0.1353(6) -0.1583(7) 0.3909(5) 0.089(4) Uani 1 1 d . . .
H51A H 0.1418 -0.1405 0.4235 0.133 Uiso 1 1 calc R . .
H51B H 0.1815 -0.1956 0.3836 0.133 Uiso 1 1 calc R . .
H51C H 0.0847 -0.1919 0.3852 0.133 Uiso 1 1 calc R . .
C52 C 0.0999(5) -0.1036(8) 0.3107(4) 0.073(3) Uani 1 1 d . . .
H52A H 0.0435 -0.1236 0.3115 0.110 Uiso 1 1 calc R . .
H52B H 0.1334 -0.1525 0.3003 0.110 Uiso 1 1 calc R . .
H52C H 0.1024 -0.0533 0.2893 0.110 Uiso 1 1 calc R . .
O4 O 0.4589(3) 0.0614(3) 0.36750(16) 0.0356(10) Uani 1 1 d . . .
C53 C 0.5196(4) -0.0052(5) 0.3763(3) 0.0410(15) Uani 1 1 d . . .
H53A H 0.5093 -0.0566 0.3553 0.049 Uiso 1 1 calc R . .
H53B H 0.5200 -0.0263 0.4088 0.049 Uiso 1 1 calc R . .
C54 C 0.5991(4) 0.0381(5) 0.3678(3) 0.0423(16) Uani 1 1 d . . .
H54A H 0.6069 0.0910 0.3880 0.051 Uiso 1 1 calc R . .
H54B H 0.5974 0.0586 0.3352 0.051 Uiso 1 1 calc R . .
C55 C 0.6725(4) -0.0262(5) 0.3773(3) 0.0475(17) Uani 1 1 d . . .
H55A H 0.6767 -0.0444 0.4102 0.057 Uiso 1 1 calc R . .
H55B H 0.6646 -0.0803 0.3580 0.057 Uiso 1 1 calc R . .
C56 C 0.7458(4) 0.0188(6) 0.3663(3) 0.0524(19) Uani 1 1 d . . .
N4 N 0.8018(5) 0.0576(6) 0.3563(3) 0.074(2) Uani 1 1 d . . .
Sb1 Sb 0.87031(3) 0.74928(4) 0.893615(19) 0.0575(2) Uani 1 1 d D . .
F1 F 0.8011(7) 0.6918(8) 0.8512(4) 0.0986(13) Uani 0.678(7) 1 d PD A 1
F2 F 0.9188(7) 0.6502(7) 0.9171(4) 0.0986(13) Uani 0.678(7) 1 d PD A 1
F3 F 0.9461(6) 0.7598(8) 0.8492(4) 0.0986(13) Uani 0.678(7) 1 d PD A 1
F4 F 0.9411(6) 0.8181(8) 0.9325(4) 0.0986(13) Uani 0.678(7) 1 d PD A 1
F5 F 0.8233(7) 0.8571(7) 0.8702(4) 0.0986(13) Uani 0.678(7) 1 d PD A 1
F6 F 0.7964(7) 0.7523(8) 0.9393(4) 0.0986(13) Uani 0.678(7) 1 d PD A 1
F1A F 0.9209(13) 0.6826(15) 0.8512(7) 0.0986(13) Uani 0.322(7) 1 d PD A 2
F2A F 0.8627(15) 0.8502(13) 0.8601(8) 0.0986(13) Uani 0.322(7) 1 d PD A 2
F3A F 0.8162(14) 0.8010(17) 0.9409(7) 0.0986(13) Uani 0.322(7) 1 d PD A 2
F4A F 0.8741(15) 0.6394(13) 0.9275(8) 0.0986(13) Uani 0.322(7) 1 d PD A 2
F5A F 0.9620(12) 0.7611(18) 0.9333(8) 0.0986(13) Uani 0.322(7) 1 d PD A 2
F6A F 0.7729(11) 0.7062(18) 0.8653(8) 0.0986(13) Uani 0.322(7) 1 d PD A 2
C57 C 0.3731(5) 0.1543(6) 0.0868(3) 0.0490(18) Uani 1 1 d . . .
H57 H 0.3146 0.1521 0.0750 0.059 Uiso 1 1 calc R . .
Cl1 Cl 0.4258(2) 0.06844(17) 0.06048(8) 0.0822(8) Uani 1 1 d . . .
Cl2 Cl 0.37949(17) 0.1357(2) 0.14687(7) 0.0742(7) Uani 1 1 d . . .
Cl3 Cl 0.41251(17) 0.25610(15) 0.07299(10) 0.0688(5) Uani 1 1 d . . .
C58 C 0.8769(13) 0.0171(13) 0.9692(7) 0.0688(5) Uani 0.50 1 d P . .
H58 H 0.9149 -0.0324 0.9626 0.083 Uiso 0.50 1 calc PR . .
Cl4 Cl 0.7930(3) -0.0278(3) 0.99354(18) 0.0688(5) Uani 0.50 1 d P . .
Cl5 Cl 0.9283(3) 0.0918(3) 1.00869(18) 0.0688(5) Uani 0.50 1 d P . .
Cl6 Cl 0.8514(3) 0.0731(3) 0.91830(14) 0.0601(11) Uani 0.50 1 d P . .
C59 C 0.9139(10) 0.0232(18) 0.4730(7) 0.096(8) Uani 0.50 1 d PD . .
H59 H 0.9201 0.0192 0.4390 0.115 Uiso 0.50 1 calc PR . .
Cl7 Cl 1.0000 0.0000 0.5000 0.187(4) Uani 1 2 d S . .
Cl8 Cl 0.9159(8) 0.1403(7) 0.4897(5) 0.179(5) Uani 0.50 1 d P . .
Cl9 Cl 0.8240(3) -0.0233(4) 0.48422(17) 0.0770(14) Uani 0.50 1 d PD . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N3 Ag1 N4 127.2(3) 1_655 . ?
N3 Ag1 N1 93.3(5) 1_655 1_655 ?
N4 Ag1 N1 115.3(4) . 1_655 ?
N3 Ag1 N2 113.6(4) 1_655 . ?
N4 Ag1 N2 99.7(3) . . ?
N1 Ag1 N2 107.0(3) 1_655 . ?
C1 S1 C47 106.7(3) . . ?
C6 C1 C2 120.8(6) . . ?
C6 C1 S1 117.6(5) . . ?
C2 C1 S1 121.0(5) . . ?
O1 C2 C3 121.6(6) . . ?
O1 C2 C1 120.2(6) . . ?
C3 C2 C1 118.1(6) . . ?
C4 C3 C2 120.7(6) . . ?
C4 C3 S2 116.4(5) . . ?
C2 C3 S2 122.2(5) . . ?
C5 C4 C3 121.6(6) . . ?
C5 C4 H4 119.2 . . ?
C3 C4 H4 119.2 . . ?
C4 C5 C6 118.0(6) . . ?
C4 C5 C7 122.7(7) . . ?
C6 C5 C7 119.3(7) . . ?
C1 C6 C5 120.7(6) . . ?
C1 C6 H6 119.6 . . ?
C5 C6 H6 119.6 . . ?
C9 C7 C8 116.1(11) . . ?
C9 C7 C5 111.0(9) . . ?
C8 C7 C5 112.6(8) . . ?
C9 C7 C10 103.2(10) . . ?
C8 C7 C10 106.9(11) . . ?
C5 C7 C10 106.0(9) . . ?
C7 C8 H8A 109.5 . . ?
C7 C8 H8B 109.5 . . ?
H8A C8 H8B 109.5 . . ?
C7 C8 H8C 109.5 . . ?
H8A C8 H8C 109.5 . . ?
H8B C8 H8C 109.5 . . ?
C7 C9 H9A 109.5 . . ?
C7 C9 H9B 109.5 . . ?
H9A C9 H9B 109.5 . . ?
C7 C9 H9C 109.5 . . ?
H9A C9 H9C 109.5 . . ?
H9B C9 H9C 109.5 . . ?
C7 C10 H10A 109.5 . . ?
C7 C10 H10B 109.5 . . ?
H10A C10 H10B 109.5 . . ?
C7 C10 H10C 109.5 . . ?
H10A C10 H10C 109.5 . . ?
H10B C10 H10C 109.5 . . ?
C2 O1 C11 112.9(6) . . ?
O1 C11 C12 101.8(7) . . ?
O1 C11 H11A 111.4 . . ?
C12 C11 H11A 111.4 . . ?
O1 C11 H11B 111.4 . . ?
C12 C11 H11B 111.4 . . ?
H11A C11 H11B 109.3 . . ?
C13 C12 C11 108.1(8) . . ?
C13 C12 H12A 110.1 . . ?
C11 C12 H12A 110.1 . . ?
C13 C12 H12B 110.1 . . ?
C11 C12 H12B 110.1 . . ?
H12A C12 H12B 108.4 . . ?
C14 C13 C12 105.4(10) . . ?
C14 C13 H13A 110.7 . . ?
C12 C13 H13A 110.7 . . ?
C14 C13 H13B 110.7 . . ?
C12 C13 H13B 110.7 . . ?
H13A C13 H13B 108.8 . . ?
N1 C14 C13 178.6(19) . . ?
C14 N1 Ag1 165.5(13) . 1_455 ?
C15 S2 C3 107.5(3) . . ?
C16 C15 C20 120.2(6) . . ?
C16 C15 S2 116.0(5) . . ?
C20 C15 S2 123.2(5) . . ?
C17 C16 C15 121.9(6) . . ?
C17 C16 H16 119.0 . . ?
C15 C16 H16 119.0 . . ?
C16 C17 C18 117.7(6) . . ?
C16 C17 C21 121.1(6) . . ?
C18 C17 C21 121.2(6) . . ?
C19 C18 C17 121.2(6) . . ?
C19 C18 H18 119.4 . . ?
C17 C18 H18 119.4 . . ?
C18 C19 C20 120.9(6) . . ?
C18 C19 S3 116.0(5) . . ?
C20 C19 S3 122.5(5) . . ?
O2 C20 C15 120.8(6) . . ?
O2 C20 C19 120.9(5) . . ?
C15 C20 C19 118.1(6) . . ?
C23 C21 C22 109.7(8) . . ?
C23 C21 C17 112.9(7) . . ?
C22 C21 C17 107.4(6) . . ?
C23 C21 C24 109.7(9) . . ?
C22 C21 C24 109.6(9) . . ?
C17 C21 C24 107.5(7) . . ?
C21 C22 H22A 109.5 . . ?
C21 C22 H22B 109.5 . . ?
H22A C22 H22B 109.5 . . ?
C21 C22 H22C 109.5 . . ?
H22A C22 H22C 109.5 . . ?
H22B C22 H22C 109.5 . . ?
C21 C23 H23A 109.5 . . ?
C21 C23 H23B 109.5 . . ?
H23A C23 H23B 109.5 . . ?
C21 C23 H23C 109.5 . . ?
H23A C23 H23C 109.5 . . ?
H23B C23 H23C 109.5 . . ?
C21 C24 H24A 109.5 . . ?
C21 C24 H24B 109.5 . . ?
H24A C24 H24B 109.5 . . ?
C21 C24 H24C 109.5 . . ?
H24A C24 H24C 109.5 . . ?
H24B C24 H24C 109.5 . . ?
C20 O2 C25 115.3(5) . . ?
O2 C25 C26 105.3(6) . . ?
O2 C25 H25A 110.7 . . ?
C26 C25 H25A 110.7 . . ?
O2 C25 H25B 110.7 . . ?
C26 C25 H25B 110.7 . . ?
H25A C25 H25B 108.8 . . ?
C25 C26 C27 108.9(7) . . ?
C25 C26 H26A 109.9 . . ?
C27 C26 H26A 109.9 . . ?
C25 C26 H26B 109.9 . . ?
C27 C26 H26B 109.9 . . ?
H26A C26 H26B 108.3 . . ?
C28 C27 C26 110.3(8) . . ?
C28 C27 H27A 109.6 . . ?
C26 C27 H27A 109.6 . . ?
C28 C27 H27B 109.6 . . ?
C26 C27 H27B 109.6 . . ?
H27A C27 H27B 108.1 . . ?
N2 C28 C27 178.5(11) . . ?
C28 N2 Ag1 169.2(10) . . ?
C29 S3 C19 108.6(3) . . ?
C30 C29 C34 120.9(6) . . ?
C30 C29 S3 117.1(5) . . ?
C34 C29 S3 121.6(5) . . ?
C29 C30 C31 122.1(6) . . ?
C29 C30 H30 118.9 . . ?
C31 C30 H30 118.9 . . ?
C32 C31 C30 116.3(6) . . ?
C32 C31 C35 119.0(6) . . ?
C30 C31 C35 124.6(6) . . ?
C33 C32 C31 122.4(6) . . ?
C33 C32 H32 118.8 . . ?
C31 C32 H32 118.8 . . ?
C32 C33 C34 120.6(6) . . ?
C32 C33 S4 115.8(5) . . ?
C34 C33 S4 123.1(5) . . ?
O3 C34 C29 121.9(6) . . ?
O3 C34 C33 120.5(6) . . ?
C29 C34 C33 117.6(6) . . ?
C37 C35 C31 111.9(6) . . ?
C37 C35 C38 108.5(7) . . ?
C31 C35 C38 107.4(6) . . ?
C37 C35 C36 108.6(7) . . ?
C31 C35 C36 111.0(7) . . ?
C38 C35 C36 109.5(7) . . ?
C35 C36 H36A 109.5 . . ?
C35 C36 H36B 109.5 . . ?
H36A C36 H36B 109.5 . . ?
C35 C36 H36C 109.5 . . ?
H36A C36 H36C 109.5 . . ?
H36B C36 H36C 109.5 . . ?
C35 C37 H37A 109.5 . . ?
C35 C37 H37B 109.5 . . ?
H37A C37 H37B 109.5 . . ?
C35 C37 H37C 109.5 . . ?
H37A C37 H37C 109.5 . . ?
H37B C37 H37C 109.5 . . ?
C35 C38 H38A 109.5 . . ?
C35 C38 H38B 109.5 . . ?
H38A C38 H38B 109.5 . . ?
C35 C38 H38C 109.5 . . ?
H38A C38 H38C 109.5 . . ?
H38B C38 H38C 109.5 . . ?
C34 O3 C39 113.7(6) . . ?
O3 C39 C40 96.7(11) . . ?
O3 C39 H39A 112.4 . . ?
C40 C39 H39A 112.4 . . ?
O3 C39 H39B 112.4 . . ?
C40 C39 H39B 112.4 . . ?
H39A C39 H39B 110.0 . . ?
C41 C40 C39 108.4(11) . . ?
C41 C40 H40A 110.0 . . ?
C39 C40 H40A 110.0 . . ?
C41 C40 H40B 110.0 . . ?
C39 C40 H40B 110.0 . . ?
H40A C40 H40B 108.4 . . ?
C42 C41 C40 108.7(11) . . ?
C42 C41 H41A 109.9 . . ?
C40 C41 H41A 109.9 . . ?
C42 C41 H41B 109.9 . . ?
C40 C41 H41B 110.0 . . ?
H41A C41 H41B 108.3 . . ?
N3 C42 C41 167(2) . . ?
C42 N3 Ag1 161.0(12) . 1_455 ?
C43 S4 C33 107.6(3) . . ?
C44 C43 C48 119.6(6) . . ?
C44 C43 S4 117.8(5) . . ?
C48 C43 S4 122.1(5) . . ?
C45 C44 C43 122.2(6) . . ?
C45 C44 H44 118.9 . . ?
C43 C44 H44 118.9 . . ?
C44 C45 C46 117.1(6) . . ?
C44 C45 C49 122.1(6) . . ?
C46 C45 C49 120.7(6) . . ?
C47 C46 C45 121.9(6) . . ?
C47 C46 H46 119.1 . . ?
C45 C46 H46 119.1 . . ?
C46 C47 C48 120.4(6) . . ?
C46 C47 S1 117.4(5) . . ?
C48 C47 S1 121.9(5) . . ?
O4 C48 C47 121.6(6) . . ?
O4 C48 C43 119.6(6) . . ?
C47 C48 C43 118.8(6) . . ?
C50 C49 C45 110.1(6) . . ?
C50 C49 C52 106.9(7) . . ?
C45 C49 C52 113.0(7) . . ?
C50 C49 C51 111.7(8) . . ?
C45 C49 C51 108.0(6) . . ?
C52 C49 C51 107.0(8) . . ?
C49 C50 H50A 109.5 . . ?
C49 C50 H50B 109.5 . . ?
H50A C50 H50B 109.5 . . ?
C49 C50 H50C 109.5 . . ?
H50A C50 H50C 109.5 . . ?
H50B C50 H50C 109.5 . . ?
C49 C51 H51A 109.5 . . ?
C49 C51 H51B 109.5 . . ?
H51A C51 H51B 109.5 . . ?
C49 C51 H51C 109.5 . . ?
H51A C51 H51C 109.5 . . ?
H51B C51 H51C 109.5 . . ?
C49 C52 H52A 109.5 . . ?
C49 C52 H52B 109.5 . . ?
H52A C52 H52B 109.5 . . ?
C49 C52 H52C 109.5 . . ?
H52A C52 H52C 109.5 . . ?
H52B C52 H52C 109.5 . . ?
C48 O4 C53 114.8(5) . . ?
O4 C53 C54 106.0(5) . . ?
O4 C53 H53A 110.5 . . ?
C54 C53 H53A 110.5 . . ?
O4 C53 H53B 110.5 . . ?
C54 C53 H53B 110.5 . . ?
H53A C53 H53B 108.7 . . ?
C53 C54 C55 112.2(6) . . ?
C53 C54 H54A 109.2 . . ?
C55 C54 H54A 109.2 . . ?
C53 C54 H54B 109.2 . . ?
C55 C54 H54B 109.2 . . ?
H54A C54 H54B 107.9 . . ?
C56 C55 C54 108.8(6) . . ?
C56 C55 H55A 109.9 . . ?
C54 C55 H55A 109.9 . . ?
C56 C55 H55B 109.9 . . ?
C54 C55 H55B 109.9 . . ?
H55A C55 H55B 108.3 . . ?
N4 C56 C55 176.5(9) . . ?
C56 N4 Ag1 157.4(8) . . ?
F2A Sb1 F2 155.8(9) . . ?
F2A Sb1 F1 91.2(9) . . ?
F2 Sb1 F1 95.8(5) . . ?
F2A Sb1 F1A 96.7(11) . . ?
F2 Sb1 F1A 65.7(8) . . ?
F1 Sb1 F1A 65.4(8) . . ?
F2A Sb1 F5A 106.0(11) . . ?
F2 Sb1 F5A 61.5(9) . . ?
F1 Sb1 F5A 155.3(9) . . ?
F1A Sb1 F5A 94.4(11) . . ?
F2A Sb1 F3A 91.5(11) . . ?
F2 Sb1 F3A 107.0(8) . . ?
F1 Sb1 F3A 112.4(9) . . ?
F1A Sb1 F3A 171.5(11) . . ?
F5A Sb1 F3A 85.3(11) . . ?
F2A Sb1 F6 109.8(9) . . ?
F2 Sb1 F6 92.7(5) . . ?
F1 Sb1 F6 94.5(5) . . ?
F1A Sb1 F6 147.3(9) . . ?
F5A Sb1 F6 96.1(9) . . ?
F3A Sb1 F6 24.9(8) . . ?
F2A Sb1 F6A 91.8(11) . . ?
F2 Sb1 F6A 102.9(9) . . ?
F1 Sb1 F6A 21.0(8) . . ?
F1A Sb1 F6A 86.3(11) . . ?
F5A Sb1 F6A 161.9(12) . . ?
F3A Sb1 F6A 91.4(11) . . ?
F6 Sb1 F6A 74.5(9) . . ?
F2A Sb1 F3 65.2(9) . . ?
F2 Sb1 F3 91.7(5) . . ?
F1 Sb1 F3 89.7(5) . . ?
F1A Sb1 F3 39.1(8) . . ?
F5A Sb1 F3 82.0(9) . . ?
F3A Sb1 F3 148.7(9) . . ?
F6 Sb1 F3 173.6(5) . . ?
F6A Sb1 F3 109.0(9) . . ?
F2A Sb1 F4 82.8(9) . . ?
F2 Sb1 F4 89.4(5) . . ?
F1 Sb1 F4 173.9(5) . . ?
F1A Sb1 F4 114.3(8) . . ?
F5A Sb1 F4 28.8(7) . . ?
F3A Sb1 F4 68.7(9) . . ?
F6 Sb1 F4 88.3(5) . . ?
F6A Sb1 F4 159.2(9) . . ?
F3 Sb1 F4 87.0(5) . . ?
F2A Sb1 F5 22.9(7) . . ?
F2 Sb1 F5 177.3(5) . . ?
F1 Sb1 F5 86.8(5) . . ?
F1A Sb1 F5 114.9(8) . . ?
F5A Sb1 F5 115.9(9) . . ?
F3A Sb1 F5 72.6(8) . . ?
F6 Sb1 F5 87.8(5) . . ?
F6A Sb1 F5 79.8(9) . . ?
F3 Sb1 F5 87.6(5) . . ?
F4 Sb1 F5 88.0(5) . . ?
F2A Sb1 F4A 177.2(10) . . ?
F2 Sb1 F4A 25.6(7) . . ?
F1 Sb1 F4A 86.1(8) . . ?
F1A Sb1 F4A 82.6(11) . . ?
F5A Sb1 F4A 76.7(11) . . ?
F3A Sb1 F4A 89.1(11) . . ?
F6 Sb1 F4A 69.9(8) . . ?
F6A Sb1 F4A 85.4(11) . . ?
F3 Sb1 F4A 115.3(8) . . ?
F4 Sb1 F4A 99.9(8) . . ?
F5 Sb1 F4A 156.0(8) . . ?
Cl3 C57 Cl2 112.0(5) . . ?
Cl3 C57 Cl1 110.1(4) . . ?
Cl2 C57 Cl1 108.4(4) . . ?
Cl3 C57 H57 108.7 . . ?
Cl2 C57 H57 108.7 . . ?
Cl1 C57 H57 108.7 . . ?
Cl6 C58 Cl4 112.7(12) . . ?
Cl6 C58 Cl5 108.6(10) . . ?
Cl4 C58 Cl5 110.1(11) . . ?
Cl6 C58 H58 108.5 . . ?
Cl4 C58 H58 108.5 . . ?
Cl5 C58 H58 108.5 . . ?
Cl7 C59 Cl9 125.0(14) . . ?
Cl7 C59 Cl8 94.8(11) . . ?
Cl9 C59 Cl8 110.3(14) . . ?
Cl7 C59 H59 108.5 . . ?
Cl9 C59 H59 108.5 . . ?
Cl8 C59 H59 108.5 . . ?
C59 Cl7 C59 179.998(4) 3_756 . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 N3 2.247(8) 1_655 ?
Ag1 N4 2.262(8) . ?
Ag1 N1 2.286(10) 1_655 ?
Ag1 N2 2.309(8) . ?
S1 C1 1.773(6) . ?
S1 C47 1.778(7) . ?
C1 C6 1.383(9) . ?
C1 C2 1.416(9) . ?
C2 O1 1.363(8) . ?
C2 C3 1.393(9) . ?
C3 C4 1.392(9) . ?
C3 S2 1.772(6) . ?
C4 C5 1.387(9) . ?
C4 H4 0.9500 . ?
C5 C6 1.413(9) . ?
C5 C7 1.542(12) . ?
C6 H6 0.9500 . ?
C7 C9 1.466(17) . ?
C7 C8 1.476(15) . ?
C7 C10 1.580(18) . ?
C8 H8A 0.9800 . ?
C8 H8B 0.9800 . ?
C8 H8C 0.9800 . ?
C9 H9A 0.9800 . ?
C9 H9B 0.9800 . ?
C9 H9C 0.9800 . ?
C10 H10A 0.9800 . ?
C10 H10B 0.9800 . ?
C10 H10C 0.9800 . ?
O1 C11 1.397(10) . ?
C11 C12 1.574(12) . ?
C11 H11A 0.9900 . ?
C11 H11B 0.9900 . ?
C12 C13 1.506(15) . ?
C12 H12A 0.9900 . ?
C12 H12B 0.9900 . ?
C13 C14 1.474(14) . ?
C13 H13A 0.9900 . ?
C13 H13B 0.9900 . ?
C14 N1 1.119(13) . ?
N1 Ag1 2.286(10) 1_455 ?
S2 C15 1.770(6) . ?
C15 C16 1.395(9) . ?
C15 C20 1.397(9) . ?
C16 C17 1.388(10) . ?
C16 H16 0.9500 . ?
C17 C18 1.390(10) . ?
C17 C21 1.547(9) . ?
C18 C19 1.395(9) . ?
C18 H18 0.9500 . ?
C19 C20 1.397(9) . ?
C19 S3 1.779(6) . ?
C20 O2 1.359(7) . ?
C21 C23 1.475(13) . ?
C21 C22 1.531(14) . ?
C21 C24 1.562(13) . ?
C22 H22A 0.9800 . ?
C22 H22B 0.9800 . ?
C22 H22C 0.9800 . ?
C23 H23A 0.9800 . ?
C23 H23B 0.9800 . ?
C23 H23C 0.9800 . ?
C24 H24A 0.9800 . ?
C24 H24B 0.9800 . ?
C24 H24C 0.9800 . ?
O2 C25 1.447(9) . ?
C25 C26 1.492(10) . ?
C25 H25A 0.9900 . ?
C25 H25B 0.9900 . ?
C26 C27 1.538(13) . ?
C26 H26A 0.9900 . ?
C26 H26B 0.9900 . ?
C27 C28 1.480(12) . ?
C27 H27A 0.9900 . ?
C27 H27B 0.9900 . ?
C28 N2 1.126(11) . ?
S3 C29 1.773(6) . ?
C29 C30 1.385(10) . ?
C29 C34 1.395(9) . ?
C30 C31 1.401(9) . ?
C30 H30 0.9500 . ?
C31 C32 1.393(9) . ?
C31 C35 1.526(10) . ?
C32 C33 1.384(9) . ?
C32 H32 0.9500 . ?
C33 C34 1.406(9) . ?
C33 S4 1.775(7) . ?
C34 O3 1.364(8) . ?
C35 C37 1.521(11) . ?
C35 C38 1.542(11) . ?
C35 C36 1.548(12) . ?
C36 H36A 0.9800 . ?
C36 H36B 0.9800 . ?
C36 H36C 0.9800 . ?
C37 H37A 0.9800 . ?
C37 H37B 0.9800 . ?
C37 H37C 0.9800 . ?
C38 H38A 0.9800 . ?
C38 H38B 0.9800 . ?
C38 H38C 0.9800 . ?
O3 C39 1.379(17) . ?
C39 C40 1.574(15) . ?
C39 H39A 0.9900 . ?
C39 H39B 0.9900 . ?
C40 C41 1.491(9) . ?
C40 H40A 0.9900 . ?
C40 H40B 0.9900 . ?
C41 C42 1.425(15) . ?
C41 H41A 0.9900 . ?
C41 H41B 0.9900 . ?
C42 N3 1.143(13) . ?
N3 Ag1 2.247(8) 1_455 ?
S4 C43 1.750(7) . ?
C43 C44 1.396(9) . ?
C43 C48 1.408(9) . ?
C44 C45 1.391(10) . ?
C44 H44 0.9500 . ?
C45 C46 1.399(10) . ?
C45 C49 1.534(9) . ?
C46 C47 1.389(9) . ?
C46 H46 0.9500 . ?
C47 C48 1.391(9) . ?
C48 O4 1.380(7) . ?
C49 C50 1.513(11) . ?
C49 C52 1.546(12) . ?
C49 C51 1.552(12) . ?
C50 H50A 0.9800 . ?
C50 H50B 0.9800 . ?
C50 H50C 0.9800 . ?
C51 H51A 0.9800 . ?
C51 H51B 0.9800 . ?
C51 H51C 0.9800 . ?
C52 H52A 0.9800 . ?
C52 H52B 0.9800 . ?
C52 H52C 0.9800 . ?
O4 C53 1.426(8) . ?
C53 C54 1.499(9) . ?
C53 H53A 0.9900 . ?
C53 H53B 0.9900 . ?
C54 C55 1.558(10) . ?
C54 H54A 0.9900 . ?
C54 H54B 0.9900 . ?
C55 C56 1.440(11) . ?
C55 H55A 0.9900 . ?
C55 H55B 0.9900 . ?
C56 N4 1.147(11) . ?
Sb1 F2A 1.799(16) . ?
Sb1 F2 1.800(10) . ?
Sb1 F1 1.830(10) . ?
Sb1 F1A 1.831(16) . ?
Sb1 F5A 1.839(16) . ?
Sb1 F3A 1.857(16) . ?
Sb1 F6 1.863(10) . ?
Sb1 F6A 1.864(16) . ?
Sb1 F3 1.863(10) . ?
Sb1 F4 1.873(10) . ?
Sb1 F5 1.900(10) . ?
Sb1 F4A 1.919(16) . ?
C57 Cl3 1.721(9) . ?
C57 Cl2 1.756(8) . ?
C57 Cl1 1.760(8) . ?
C57 H57 1.0000 . ?
C58 Cl6 1.72(2) . ?
C58 Cl4 1.73(2) . ?
C58 Cl5 1.77(2) . ?
C58 H58 1.0000 . ?
C59 Cl7 1.61(2) . ?
C59 Cl9 1.691(9) . ?
C59 Cl8 1.82(3) . ?
C59 H59 1.0000 . ?
Cl7 C59 1.61(2) 3_756 ?
