#------------------------------------------------------------------------------
#$Date: 2016-03-25 11:00:33 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179772 $
#$URL: svn://www.crystallography.net/cod/cif/7/00/68/7006898.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7006898
loop_
_publ_author_name
'Moberg, Viktor'
'Homanen, Pertti'
'Selva, Simona'
'Persson, Roger'
'Haukka, Matti'
'Pakkanen, Tapani A.'
'Monari, Magda'
'Nordlander, Ebbe'
_publ_section_title
;
 Synthesis, characterization and reactivity of tetranuclear ruthenium
 hydrido clusters containing chiral phosphine ligands.
;
_journal_issue                   1
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              279
_journal_page_last               288
_journal_paper_doi               10.1039/b515273a
_journal_year                    2006
_chemical_formula_sum            'C28 H32 O11 P2 Ru4'
_chemical_formula_weight         1010.76
_chemical_name_systematic
;
?
;
_space_group_IT_number           4
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  'P 2yb'
_symmetry_space_group_name_H-M   'P 1 21 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 113.35(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   9.7272(19)
_cell_length_b                   16.058(3)
_cell_length_c                   12.132(2)
_cell_measurement_temperature    120(2)
_cell_volume                     1739.8(7)
_computing_cell_refinement       'Denzo/Scalepack (Otwinowski & Minor, 1997)'
_computing_data_collection       'Collect (Nonius, 1999)'
_computing_data_reduction        'Denzo/Scalepack (Otwinowski & Minor, 1997)'
_computing_molecular_graphics    'SHELXTL v.5.1 (Bruker Axs, 1998)'
_computing_publication_material  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SIR97 (Altomare et al. 1997)'
_diffrn_ambient_temperature      120(2)
_diffrn_measured_fraction_theta_full 0.996
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measurement_device_type  'Nonius Kappa CCD diffractometer'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0000
_diffrn_reflns_av_sigmaI/netI    0.0396
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       20
_diffrn_reflns_limit_k_min       -20
_diffrn_reflns_limit_l_max       15
_diffrn_reflns_limit_l_min       -15
_diffrn_reflns_number            7035
_diffrn_reflns_theta_full        26.35
_diffrn_reflns_theta_max         26.35
_diffrn_reflns_theta_min         2.61
_exptl_absorpt_coefficient_mu    1.848
_exptl_absorpt_correction_T_max  0.7088
_exptl_absorpt_correction_T_min  0.6551
_exptl_absorpt_correction_type   empirical
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    1.929
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             988
_exptl_crystal_size_max          0.25
_exptl_crystal_size_mid          0.25
_exptl_crystal_size_min          0.20
_refine_diff_density_max         0.489
_refine_diff_density_min         -0.671
_refine_diff_density_rms         0.138
_refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881'
_refine_ls_abs_structure_Flack   -0.012(16)
_refine_ls_extinction_coef       0.0024(2)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.090
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     411
_refine_ls_number_reflns         7035
_refine_ls_number_restraints     1
_refine_ls_restrained_S_all      1.090
_refine_ls_R_factor_all          0.0187
_refine_ls_R_factor_gt           0.0181
_refine_ls_shift/su_max          0.006
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0000P)²+0.0961P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0433
_refine_ls_wR_factor_ref         0.0436
_reflns_number_gt                6923
_reflns_number_total             7035
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b515273a.txt
_cod_data_source_block           H4Ru4(CO)10(O-DUPHOS)_(4)
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_cell_volume        1739.9(6)
_cod_original_sg_symbol_H-M      P2(1)
_cod_database_code               7006898
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ru1 Ru 0.417659(19) 0.641269(12) 0.126373(16) 0.01295(5) Uani 1 1 d . . .
Ru2 Ru 0.55156(2) 0.644408(13) 0.386180(17) 0.01627(6) Uani 1 1 d . . .
Ru3 Ru 0.40719(2) 0.496944(12) 0.283587(18) 0.01786(6) Uani 1 1 d . . .
Ru4 Ru 0.69515(2) 0.545194(14) 0.276707(18) 0.01844(6) Uani 1 1 d . . .
P1 P 0.18099(7) 0.69626(4) 0.03700(6) 0.01453(13) Uani 1 1 d . . .
P2 P 0.32621(7) 0.59739(4) -0.15156(6) 0.01566(13) Uani 1 1 d . . .
O1 O 0.3538(2) 0.56295(10) -0.02866(16) 0.0176(4) Uani 1 1 d . . .
C11 C 0.4989(3) 0.73520(17) 0.0893(2) 0.0198(6) Uani 1 1 d . . .
O11 O 0.5514(2) 0.79615(12) 0.07233(19) 0.0345(5) Uani 1 1 d . . .
C21 C 0.6568(3) 0.7474(2) 0.4154(2) 0.0242(6) Uani 1 1 d . . .
O21 O 0.7133(2) 0.81097(14) 0.4310(2) 0.0362(5) Uani 1 1 d . . .
C22 C 0.4018(3) 0.67950(18) 0.4408(2) 0.0242(6) Uani 1 1 d . . .
O22 O 0.3161(2) 0.70005(15) 0.47783(19) 0.0353(5) Uani 1 1 d . . .
C23 C 0.6818(3) 0.59452(19) 0.5300(3) 0.0249(6) Uani 1 1 d . . .
O23 O 0.7634(2) 0.56716(15) 0.61966(18) 0.0372(6) Uani 1 1 d . . .
C31 C 0.3028(3) 0.41564(18) 0.1637(3) 0.0258(6) Uani 1 1 d . . .
O31 O 0.2346(2) 0.37316(13) 0.0850(2) 0.0383(5) Uani 1 1 d . . .
C32 C 0.5082(4) 0.4286(2) 0.4208(3) 0.0352(7) Uani 1 1 d . . .
O32 O 0.5653(3) 0.38757(18) 0.5044(2) 0.0561(7) Uani 1 1 d . . .
C33 C 0.2546(3) 0.52117(17) 0.3386(3) 0.0291(7) Uani 1 1 d . . .
O33 O 0.1611(3) 0.53256(16) 0.3714(2) 0.0474(6) Uani 1 1 d . . .
C41 C 0.8374(3) 0.6328(2) 0.3261(2) 0.0287(7) Uani 1 1 d . . .
O41 O 0.9266(3) 0.68374(17) 0.3565(2) 0.0462(6) Uani 1 1 d . . .
C42 C 0.7517(3) 0.4868(2) 0.1632(3) 0.0304(7) Uani 1 1 d . . .
O42 O 0.7859(3) 0.45370(17) 0.0944(2) 0.0514(7) Uani 1 1 d . . .
C43 C 0.8134(4) 0.4779(2) 0.4101(3) 0.0326(7) Uani 1 1 d . . .
O43 O 0.8899(3) 0.43703(17) 0.4882(2) 0.0517(7) Uani 1 1 d . . .
C51 C 0.0257(3) 0.63080(17) 0.0422(2) 0.0194(5) Uani 1 1 d . . .
H51 H 0.0691 0.5968 0.1172 0.023 Uiso 1 1 calc R . .
C52 C -0.0832(3) 0.69177(19) 0.0608(3) 0.0257(6) Uani 1 1 d . . .
H52A H -0.1492 0.7170 -0.0166 0.031 Uiso 1 1 calc R . .
H52B H -0.1464 0.6629 0.0958 0.031 Uiso 1 1 calc R . .
C53 C 0.0116(3) 0.75845(19) 0.1463(3) 0.0299(7) Uani 1 1 d . . .
H53A H 0.0643 0.7346 0.2276 0.036 Uiso 1 1 calc R . .
H53B H -0.0531 0.8045 0.1517 0.036 Uiso 1 1 calc R . .
C54 C 0.1258(3) 0.79140(17) 0.0988(2) 0.0201(6) Uani 1 1 d . . .
H54 H 0.0708 0.8289 0.0295 0.024 Uiso 1 1 calc R . .
C55 C -0.0416(3) 0.5693(2) -0.0614(3) 0.0358(8) Uani 1 1 d . . .
H55A H -0.0887 0.6000 -0.1369 0.054 Uiso 1 1 calc R . .
H55B H -0.1171 0.5351 -0.0481 0.054 Uiso 1 1 calc R . .
H55C H 0.0376 0.5334 -0.0655 0.054 Uiso 1 1 calc R . .
C56 C 0.2530(3) 0.84198(18) 0.1899(3) 0.0257(6) Uani 1 1 d . . .
H56A H 0.3121 0.8062 0.2577 0.039 Uiso 1 1 calc R . .
H56B H 0.2112 0.8885 0.2190 0.039 Uiso 1 1 calc R . .
H56C H 0.3174 0.8637 0.1517 0.039 Uiso 1 1 calc R . .
C61 C 0.5014(3) 0.62441(17) -0.1672(2) 0.0212(6) Uani 1 1 d . . .
H61 H 0.5846 0.6143 -0.0873 0.025 Uiso 1 1 calc R . .
C62 C 0.5148(3) 0.55720(19) -0.2531(3) 0.0266(7) Uani 1 1 d . . .
H62A H 0.4767 0.5792 -0.3361 0.032 Uiso 1 1 calc R . .
H62B H 0.6212 0.5416 -0.2293 0.032 Uiso 1 1 calc R . .
C63 C 0.4235(3) 0.48046(18) -0.2478(3) 0.0284(7) Uani 1 1 d . . .
H63A H 0.4124 0.4417 -0.3142 0.034 Uiso 1 1 calc R . .
H63B H 0.4739 0.4507 -0.1706 0.034 Uiso 1 1 calc R . .
C64 C 0.2699(3) 0.51251(16) -0.2594(2) 0.0208(6) Uani 1 1 d . . .
H64 H 0.2160 0.5360 -0.3417 0.025 Uiso 1 1 calc R . .
C65 C 0.5212(3) 0.71269(19) -0.2041(3) 0.0284(7) Uani 1 1 d . . .
H65A H 0.4412 0.7253 -0.2823 0.043 Uiso 1 1 calc R . .
H65B H 0.6185 0.7175 -0.2099 0.043 Uiso 1 1 calc R . .
H65C H 0.5165 0.7521 -0.1440 0.043 Uiso 1 1 calc R . .
C66 C 0.1695(3) 0.44754(19) -0.2353(3) 0.0267(6) Uani 1 1 d . . .
H66A H 0.2163 0.4292 -0.1516 0.040 Uiso 1 1 calc R . .
H66B H 0.1565 0.3997 -0.2886 0.040 Uiso 1 1 calc R . .
H66C H 0.0716 0.4723 -0.2505 0.040 Uiso 1 1 calc R . .
C71 C 0.1912(3) 0.68024(16) -0.1978(2) 0.0162(5) Uani 1 1 d . . .
C72 C 0.1448(3) 0.70469(17) -0.3187(2) 0.0217(6) Uani 1 1 d . . .
H72 H 0.1894 0.6792 -0.3671 0.026 Uiso 1 1 calc R . .
C73 C 0.0362(3) 0.76461(17) -0.3686(3) 0.0262(6) Uani 1 1 d . . .
H73 H 0.0090 0.7816 -0.4495 0.031 Uiso 1 1 calc R . .
C74 C -0.0318(4) 0.7991(2) -0.3006(3) 0.0331(7) Uani 1 1 d . . .
H74 H -0.1091 0.8390 -0.3353 0.040 Uiso 1 1 calc R . .
C75 C 0.0109(3) 0.77653(18) -0.1807(3) 0.0275(7) Uani 1 1 d . . .
H75 H -0.0388 0.8010 -0.1354 0.033 Uiso 1 1 calc R . .
C76 C 0.1248(3) 0.71889(15) -0.1255(2) 0.0173(5) Uani 1 1 d . . .
H112 H 0.4144 0.6998 0.2555 0.050 Uiso 1 1 d . . .
H113 H 0.2959 0.5646 0.1567 0.050 Uiso 1 1 d . . .
H114 H 0.5998 0.6022 0.1341 0.050 Uiso 1 1 d . . .
H134 H 0.5550 0.4605 0.2351 0.050 Uiso 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ru Ru -1.2594 0.8363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C11 Ru1 O1 105.68(9) . . ?
C11 Ru1 P1 90.96(8) . . ?
O1 Ru1 P1 85.61(6) . . ?
C11 Ru1 Ru2 101.57(8) . . ?
O1 Ru1 Ru2 144.68(5) . . ?
P1 Ru1 Ru2 116.20(3) . . ?
C11 Ru1 Ru4 101.48(8) . . ?
O1 Ru1 Ru4 96.28(5) . . ?
P1 Ru1 Ru4 166.340(19) . . ?
Ru2 Ru1 Ru4 56.06(2) . . ?
C11 Ru1 Ru3 155.01(8) . . ?
O1 Ru1 Ru3 91.91(5) . . ?
P1 Ru1 Ru3 108.29(2) . . ?
Ru2 Ru1 Ru3 55.983(11) . . ?
Ru4 Ru1 Ru3 58.195(15) . . ?
C11 Ru1 H112 86.76(8) . . ?
O1 Ru1 H112 162.30(5) . . ?
P1 Ru1 H112 81.56(3) . . ?
Ru2 Ru1 H112 38.299(10) . . ?
Ru4 Ru1 H112 93.42(3) . . ?
Ru3 Ru1 H112 80.688(16) . . ?
C11 Ru1 H113 165.61(8) . . ?
O1 Ru1 H113 78.30(5) . . ?
P1 Ru1 H113 75.41(2) . . ?
Ru2 Ru1 H113 80.89(2) . . ?
Ru4 Ru1 H113 91.679(18) . . ?
Ru3 Ru1 H113 34.783(16) . . ?
H112 Ru1 H113 86.67(2) . . ?
C11 Ru1 H114 78.15(8) . . ?
O1 Ru1 H114 77.49(5) . . ?
P1 Ru1 H114 156.42(2) . . ?
Ru2 Ru1 H114 86.68(3) . . ?
Ru4 Ru1 H114 35.359(12) . . ?
Ru3 Ru1 H114 88.79(2) . . ?
H112 Ru1 H114 118.09(3) . . ?
H113 Ru1 H114 116.231(16) . . ?
C23 Ru2 C21 94.74(12) . . ?
C23 Ru2 C22 97.49(11) . . ?
C21 Ru2 C22 96.13(12) . . ?
C23 Ru2 Ru4 85.27(8) . . ?
C21 Ru2 Ru4 104.62(9) . . ?
C22 Ru2 Ru4 158.80(9) . . ?
C23 Ru2 Ru3 95.01(10) . . ?
C21 Ru2 Ru3 164.12(9) . . ?
C22 Ru2 Ru3 95.00(9) . . ?
Ru4 Ru2 Ru3 63.800(14) . . ?
C23 Ru2 Ru1 148.14(9) . . ?
C21 Ru2 Ru1 101.22(9) . . ?
C22 Ru2 Ru1 107.88(8) . . ?
Ru4 Ru2 Ru1 64.158(18) . . ?
Ru3 Ru2 Ru1 64.446(16) . . ?
C23 Ru2 H112 173.49(8) . . ?
C21 Ru2 H112 83.88(8) . . ?
C22 Ru2 H112 76.38(8) . . ?
Ru4 Ru2 H112 101.234(17) . . ?
Ru3 Ru2 H112 87.77(2) . . ?
Ru1 Ru2 H112 38.108(15) . . ?
C33 Ru3 C32 90.87(13) . . ?
C33 Ru3 C31 98.85(12) . . ?
C32 Ru3 C31 101.82(14) . . ?
C33 Ru3 Ru2 89.69(9) . . ?
C32 Ru3 Ru2 96.02(11) . . ?
C31 Ru3 Ru2 160.04(9) . . ?
C33 Ru3 Ru4 147.66(9) . . ?
C32 Ru3 Ru4 90.53(10) . . ?
C31 Ru3 Ru4 112.45(9) . . ?
Ru2 Ru3 Ru4 58.040(13) . . ?
C33 Ru3 Ru1 106.94(9) . . ?
C32 Ru3 Ru1 148.74(10) . . ?
C31 Ru3 Ru1 100.55(9) . . ?
Ru2 Ru3 Ru1 59.572(19) . . ?
Ru4 Ru3 Ru1 60.67(2) . . ?
C33 Ru3 H113 83.70(9) . . ?
C32 Ru3 H113 174.58(10) . . ?
C31 Ru3 H113 78.99(9) . . ?
Ru2 Ru3 H113 84.10(3) . . ?
Ru4 Ru3 H113 94.11(2) . . ?
Ru1 Ru3 H113 34.781(9) . . ?
C33 Ru3 H134 173.31(8) . . ?
C32 Ru3 H134 84.22(10) . . ?
C31 Ru3 H134 77.79(9) . . ?
Ru2 Ru3 H134 95.334(15) . . ?
Ru4 Ru3 H134 37.348(11) . . ?
Ru1 Ru3 H134 79.471(17) . . ?
H113 Ru3 H134 101.17(2) . . ?
C41 Ru4 C43 91.89(14) . . ?
C41 Ru4 C42 102.05(13) . . ?
C43 Ru4 C42 94.82(13) . . ?
C41 Ru4 Ru2 82.28(8) . . ?
C43 Ru4 Ru2 99.65(9) . . ?
C42 Ru4 Ru2 164.78(9) . . ?
C41 Ru4 Ru3 140.44(8) . . ?
C43 Ru4 Ru3 95.02(10) . . ?
C42 Ru4 Ru3 116.05(10) . . ?
Ru2 Ru4 Ru3 58.159(16) . . ?
C41 Ru4 Ru1 100.24(9) . . ?
C43 Ru4 Ru1 153.88(9) . . ?
C42 Ru4 Ru1 104.99(9) . . ?
Ru2 Ru4 Ru1 59.785(17) . . ?
Ru3 Ru4 Ru1 61.139(17) . . ?
C41 Ru4 H114 87.77(9) . . ?
C43 Ru4 H114 170.04(9) . . ?
C42 Ru4 H114 75.54(9) . . ?
Ru2 Ru4 H114 90.174(18) . . ?
Ru3 Ru4 H114 91.55(3) . . ?
Ru1 Ru4 H114 35.324(16) . . ?
C41 Ru4 H134 177.31(8) . . ?
C43 Ru4 H134 86.92(10) . . ?
C42 Ru4 H134 80.47(10) . . ?
Ru2 Ru4 H134 95.529(17) . . ?
Ru3 Ru4 H134 37.424(9) . . ?
Ru1 Ru4 H134 79.90(2) . . ?
H114 Ru4 H134 93.81(3) . . ?
C76 P1 C51 104.16(12) . . ?
C76 P1 C54 104.73(12) . . ?
C51 P1 C54 94.70(12) . . ?
C76 P1 Ru1 113.19(9) . . ?
C51 P1 Ru1 116.22(9) . . ?
C54 P1 Ru1 121.18(9) . . ?
O1 P2 C71 113.65(11) . . ?
O1 P2 C64 108.71(11) . . ?
C71 P2 C64 110.88(12) . . ?
O1 P2 C61 112.25(11) . . ?
C71 P2 C61 112.67(12) . . ?
C64 P2 C61 97.45(13) . . ?
P2 O1 Ru1 121.88(10) . . ?
O11 C11 Ru1 176.1(2) . . ?
O21 C21 Ru2 176.7(2) . . ?
O22 C22 Ru2 177.4(2) . . ?
O23 C23 Ru2 177.3(3) . . ?
O31 C31 Ru3 173.6(3) . . ?
O32 C32 Ru3 177.9(3) . . ?
O33 C33 Ru3 177.3(3) . . ?
O41 C41 Ru4 177.8(3) . . ?
O42 C42 Ru4 178.4(3) . . ?
O43 C43 Ru4 176.7(3) . . ?
C52 C51 C55 116.2(2) . . ?
C52 C51 P1 105.27(19) . . ?
C55 C51 P1 115.26(18) . . ?
C52 C51 H51 106.5 . . ?
C55 C51 H51 106.5 . . ?
P1 C51 H51 106.5 . . ?
C53 C52 C51 106.5(2) . . ?
C53 C52 H52A 110.4 . . ?
C51 C52 H52A 110.4 . . ?
C53 C52 H52B 110.4 . . ?
C51 C52 H52B 110.4 . . ?
H52A C52 H52B 108.6 . . ?
C52 C53 C54 108.7(2) . . ?
C52 C53 H53A 110.0 . . ?
C54 C53 H53A 110.0 . . ?
C52 C53 H53B 110.0 . . ?
C54 C53 H53B 110.0 . . ?
H53A C53 H53B 108.3 . . ?
C56 C54 C53 114.3(2) . . ?
C56 C54 P1 116.46(19) . . ?
C53 C54 P1 103.55(18) . . ?
C56 C54 H54 107.4 . . ?
C53 C54 H54 107.4 . . ?
P1 C54 H54 107.4 . . ?
C51 C55 H55A 109.5 . . ?
C51 C55 H55B 109.5 . . ?
H55A C55 H55B 109.5 . . ?
C51 C55 H55C 109.5 . . ?
H55A C55 H55C 109.5 . . ?
H55B C55 H55C 109.5 . . ?
C54 C56 H56A 109.5 . . ?
C54 C56 H56B 109.5 . . ?
H56A C56 H56B 109.5 . . ?
C54 C56 H56C 109.5 . . ?
H56A C56 H56C 109.5 . . ?
H56B C56 H56C 109.5 . . ?
C65 C61 C62 113.5(2) . . ?
C65 C61 P2 118.7(2) . . ?
C62 C61 P2 103.59(18) . . ?
C65 C61 H61 106.8 . . ?
C62 C61 H61 106.8 . . ?
P2 C61 H61 106.8 . . ?
C63 C62 C61 109.1(2) . . ?
C63 C62 H62A 109.9 . . ?
C61 C62 H62A 109.9 . . ?
C63 C62 H62B 109.9 . . ?
C61 C62 H62B 109.9 . . ?
H62A C62 H62B 108.3 . . ?
C64 C63 C62 106.6(2) . . ?
C64 C63 H63A 110.4 . . ?
C62 C63 H63A 110.4 . . ?
C64 C63 H63B 110.4 . . ?
C62 C63 H63B 110.4 . . ?
H63A C63 H63B 108.6 . . ?
C63 C64 C66 115.1(2) . . ?
C63 C64 P2 100.43(18) . . ?
C66 C64 P2 113.95(19) . . ?
C63 C64 H64 109.0 . . ?
C66 C64 H64 109.0 . . ?
P2 C64 H64 109.0 . . ?
C61 C65 H65A 109.5 . . ?
C61 C65 H65B 109.5 . . ?
H65A C65 H65B 109.5 . . ?
C61 C65 H65C 109.5 . . ?
H65A C65 H65C 109.5 . . ?
H65B C65 H65C 109.5 . . ?
C64 C66 H66A 109.5 . . ?
C64 C66 H66B 109.5 . . ?
H66A C66 H66B 109.5 . . ?
C64 C66 H66C 109.5 . . ?
H66A C66 H66C 109.5 . . ?
H66B C66 H66C 109.5 . . ?
C72 C71 C76 119.0(2) . . ?
C72 C71 P2 115.1(2) . . ?
C76 C71 P2 125.82(19) . . ?
C73 C72 C71 121.7(3) . . ?
C73 C72 H72 119.1 . . ?
C71 C72 H72 119.1 . . ?
C74 C73 C72 119.2(3) . . ?
C74 C73 H73 120.4 . . ?
C72 C73 H73 120.4 . . ?
C73 C74 C75 120.7(3) . . ?
C73 C74 H74 119.6 . . ?
C75 C74 H74 119.6 . . ?
C74 C75 C76 121.8(3) . . ?
C74 C75 H75 119.1 . . ?
C76 C75 H75 119.1 . . ?
C75 C76 C71 117.5(2) . . ?
C75 C76 P1 118.9(2) . . ?
C71 C76 P1 123.65(19) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ru1 C11 1.840(3) . ?
Ru1 O1 2.1399(18) . ?
Ru1 P1 2.2971(9) . ?
Ru1 Ru2 2.8948(9) . ?
Ru1 Ru4 3.0149(9) . ?
Ru1 Ru3 3.0288(5) . ?
Ru1 H112 1.8380(3) . ?
Ru1 H113 1.8438(3) . ?
Ru1 H114 1.8472(4) . ?
Ru2 C23 1.881(3) . ?
Ru2 C21 1.903(3) . ?
Ru2 C22 1.909(3) . ?
Ru2 Ru4 2.7791(5) . ?
Ru2 Ru3 2.7827(6) . ?
Ru2 H112 1.8458(6) . ?
Ru3 C33 1.893(3) . ?
Ru3 C32 1.909(3) . ?
Ru3 C31 1.918(3) . ?
Ru3 Ru4 2.9391(6) . ?
Ru3 H113 1.8439(5) . ?
Ru3 H134 1.8511(4) . ?
Ru4 C41 1.896(3) . ?
Ru4 C43 1.907(3) . ?
Ru4 C42 1.918(3) . ?
Ru4 H114 1.8488(5) . ?
Ru4 H134 1.8479(4) . ?
P1 C76 1.861(3) . ?
P1 C51 1.862(3) . ?
P1 C54 1.872(3) . ?
P2 O1 1.5113(19) . ?
P2 C71 1.796(3) . ?
P2 C64 1.817(3) . ?
P2 C61 1.839(3) . ?
C11 O11 1.159(3) . ?
C21 O21 1.139(4) . ?
C22 O22 1.141(3) . ?
C23 O23 1.150(3) . ?
C31 O31 1.147(4) . ?
C32 O32 1.151(4) . ?
C33 O33 1.143(4) . ?
C41 O41 1.142(4) . ?
C42 O42 1.145(4) . ?
C43 O43 1.150(4) . ?
C51 C52 1.524(4) . ?
C51 C55 1.526(4) . ?
C51 H51 1.0000 . ?
C52 C53 1.521(4) . ?
C52 H52A 0.9900 . ?
C52 H52B 0.9900 . ?
C53 C54 1.535(4) . ?
C53 H53A 0.9900 . ?
C53 H53B 0.9900 . ?
C54 C56 1.526(4) . ?
C54 H54 1.0000 . ?
C55 H55A 0.9800 . ?
C55 H55B 0.9800 . ?
C55 H55C 0.9800 . ?
C56 H56A 0.9800 . ?
C56 H56B 0.9800 . ?
C56 H56C 0.9800 . ?
C61 C65 1.522(4) . ?
C61 C62 1.542(4) . ?
C61 H61 1.0000 . ?
C62 C63 1.536(4) . ?
C62 H62A 0.9900 . ?
C62 H62B 0.9900 . ?
C63 C64 1.532(4) . ?
C63 H63A 0.9900 . ?
C63 H63B 0.9900 . ?
C64 C66 1.534(4) . ?
C64 H64 1.0000 . ?
C65 H65A 0.9800 . ?
C65 H65B 0.9800 . ?
C65 H65C 0.9800 . ?
C66 H66A 0.9800 . ?
C66 H66B 0.9800 . ?
C66 H66C 0.9800 . ?
C71 C72 1.409(4) . ?
C71 C76 1.422(4) . ?
C72 C73 1.379(4) . ?
C72 H72 0.9500 . ?
C73 C74 1.363(4) . ?
C73 H73 0.9500 . ?
C74 C75 1.393(4) . ?
C74 H74 0.9500 . ?
C75 C76 1.394(4) . ?
C75 H75 0.9500 . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C11 Ru1 Ru2 C23 -113.83(18) . . . . ?
O1 Ru1 Ru2 C23 26.14(19) . . . . ?
P1 Ru1 Ru2 C23 149.29(17) . . . . ?
Ru4 Ru1 Ru2 C23 -17.67(17) . . . . ?
Ru3 Ru1 Ru2 C23 54.14(17) . . . . ?
C11 Ru1 Ru2 C21 4.79(12) . . . . ?
O1 Ru1 Ru2 C21 144.76(12) . . . . ?
P1 Ru1 Ru2 C21 -92.09(9) . . . . ?
Ru4 Ru1 Ru2 C21 100.94(9) . . . . ?
Ru3 Ru1 Ru2 C21 172.75(9) . . . . ?
C11 Ru1 Ru2 C22 105.06(12) . . . . ?
O1 Ru1 Ru2 C22 -114.97(12) . . . . ?
P1 Ru1 Ru2 C22 8.18(9) . . . . ?
Ru4 Ru1 Ru2 C22 -158.78(9) . . . . ?
Ru3 Ru1 Ru2 C22 -86.97(9) . . . . ?
C11 Ru1 Ru2 Ru4 -96.16(8) . . . . ?
O1 Ru1 Ru2 Ru4 43.82(8) . . . . ?
P1 Ru1 Ru2 Ru4 166.97(2) . . . . ?
Ru3 Ru1 Ru2 Ru4 71.810(15) . . . . ?
C11 Ru1 Ru2 Ru3 -167.97(8) . . . . ?
O1 Ru1 Ru2 Ru3 -27.99(8) . . . . ?
P1 Ru1 Ru2 Ru3 95.16(2) . . . . ?
Ru4 Ru1 Ru2 Ru3 -71.810(15) . . . . ?
C23 Ru2 Ru3 C33 95.48(12) . . . . ?
C21 Ru2 Ru3 C33 -136.8(3) . . . . ?
C22 Ru2 Ru3 C33 -2.50(12) . . . . ?
Ru4 Ru2 Ru3 C33 177.71(9) . . . . ?
Ru1 Ru2 Ru3 C33 -109.95(9) . . . . ?
C23 Ru2 Ru3 C32 4.64(13) . . . . ?
C21 Ru2 Ru3 C32 132.3(3) . . . . ?
C22 Ru2 Ru3 C32 -93.35(13) . . . . ?
Ru4 Ru2 Ru3 C32 86.86(10) . . . . ?
Ru1 Ru2 Ru3 C32 159.21(10) . . . . ?
C23 Ru2 Ru3 C31 -148.7(3) . . . . ?
C21 Ru2 Ru3 C31 -21.0(4) . . . . ?
C22 Ru2 Ru3 C31 113.3(3) . . . . ?
Ru4 Ru2 Ru3 C31 -66.5(2) . . . . ?
Ru1 Ru2 Ru3 C31 5.9(2) . . . . ?
C23 Ru2 Ru3 Ru4 -82.22(8) . . . . ?
C21 Ru2 Ru3 Ru4 45.5(3) . . . . ?
C22 Ru2 Ru3 Ru4 179.79(8) . . . . ?
Ru1 Ru2 Ru3 Ru4 72.35(2) . . . . ?
C23 Ru2 Ru3 Ru1 -154.57(8) . . . . ?
C21 Ru2 Ru3 Ru1 -26.9(3) . . . . ?
C22 Ru2 Ru3 Ru1 107.44(8) . . . . ?
Ru4 Ru2 Ru3 Ru1 -72.35(2) . . . . ?
C11 Ru1 Ru3 C33 108.2(2) . . . . ?
O1 Ru1 Ru3 C33 -116.44(11) . . . . ?
P1 Ru1 Ru3 C33 -30.44(10) . . . . ?
Ru2 Ru1 Ru3 C33 79.31(10) . . . . ?
Ru4 Ru1 Ru3 C33 147.34(10) . . . . ?
C11 Ru1 Ru3 C32 -14.0(3) . . . . ?
O1 Ru1 Ru3 C32 121.4(2) . . . . ?
P1 Ru1 Ru3 C32 -152.6(2) . . . . ?
Ru2 Ru1 Ru3 C32 -42.9(2) . . . . ?
Ru4 Ru1 Ru3 C32 25.2(2) . . . . ?
C11 Ru1 Ru3 C31 -149.0(2) . . . . ?
O1 Ru1 Ru3 C31 -13.72(10) . . . . ?
P1 Ru1 Ru3 C31 72.29(9) . . . . ?
Ru2 Ru1 Ru3 C31 -177.96(9) . . . . ?
Ru4 Ru1 Ru3 C31 -109.93(9) . . . . ?
C11 Ru1 Ru3 Ru2 28.91(19) . . . . ?
O1 Ru1 Ru3 Ru2 164.24(5) . . . . ?
P1 Ru1 Ru3 Ru2 -109.75(3) . . . . ?
Ru4 Ru1 Ru3 Ru2 68.03(3) . . . . ?
C11 Ru1 Ru3 Ru4 -39.12(19) . . . . ?
O1 Ru1 Ru3 Ru4 96.21(5) . . . . ?
P1 Ru1 Ru3 Ru4 -177.782(19) . . . . ?
Ru2 Ru1 Ru3 Ru4 -68.03(3) . . . . ?
C23 Ru2 Ru4 C41 -82.60(13) . . . . ?
C21 Ru2 Ru4 C41 11.08(12) . . . . ?
C22 Ru2 Ru4 C41 178.9(2) . . . . ?
Ru3 Ru2 Ru4 C41 179.45(9) . . . . ?
Ru1 Ru2 Ru4 C41 106.65(9) . . . . ?
C23 Ru2 Ru4 C43 8.02(14) . . . . ?
C21 Ru2 Ru4 C43 101.69(14) . . . . ?
C22 Ru2 Ru4 C43 -90.5(2) . . . . ?
Ru3 Ru2 Ru4 C43 -89.94(11) . . . . ?
Ru1 Ru2 Ru4 C43 -162.73(10) . . . . ?
C23 Ru2 Ru4 C42 169.7(4) . . . . ?
C21 Ru2 Ru4 C42 -96.6(4) . . . . ?
C22 Ru2 Ru4 C42 71.2(4) . . . . ?
Ru3 Ru2 Ru4 C42 71.7(4) . . . . ?
Ru1 Ru2 Ru4 C42 -1.0(4) . . . . ?
C23 Ru2 Ru4 Ru3 97.96(9) . . . . ?
C21 Ru2 Ru4 Ru3 -168.37(9) . . . . ?
C22 Ru2 Ru4 Ru3 -0.6(2) . . . . ?
Ru1 Ru2 Ru4 Ru3 -72.79(2) . . . . ?
C23 Ru2 Ru4 Ru1 170.75(9) . . . . ?
C21 Ru2 Ru4 Ru1 -95.58(9) . . . . ?
C22 Ru2 Ru4 Ru1 72.2(2) . . . . ?
Ru3 Ru2 Ru4 Ru1 72.79(2) . . . . ?
C33 Ru3 Ru4 C41 -5.2(2) . . . . ?
C32 Ru3 Ru4 C41 -97.63(18) . . . . ?
C31 Ru3 Ru4 C41 159.34(16) . . . . ?
Ru2 Ru3 Ru4 C41 -0.86(14) . . . . ?
Ru1 Ru3 Ru4 C41 69.62(14) . . . . ?
C33 Ru3 Ru4 C43 93.96(19) . . . . ?
C32 Ru3 Ru4 C43 1.48(14) . . . . ?
C31 Ru3 Ru4 C43 -101.54(14) . . . . ?
Ru2 Ru3 Ru4 C43 98.25(10) . . . . ?
Ru1 Ru3 Ru4 C43 168.73(9) . . . . ?
C33 Ru3 Ru4 C42 -168.18(19) . . . . ?
C32 Ru3 Ru4 C42 99.35(15) . . . . ?
C31 Ru3 Ru4 C42 -3.68(14) . . . . ?
Ru2 Ru3 Ru4 C42 -163.88(10) . . . . ?
Ru1 Ru3 Ru4 C42 -93.40(10) . . . . ?
C33 Ru3 Ru4 Ru2 -4.29(17) . . . . ?
C32 Ru3 Ru4 Ru2 -96.77(11) . . . . ?
C31 Ru3 Ru4 Ru2 160.20(9) . . . . ?
Ru1 Ru3 Ru4 Ru2 70.48(2) . . . . ?
C33 Ru3 Ru4 Ru1 -74.77(17) . . . . ?
C32 Ru3 Ru4 Ru1 -167.25(11) . . . . ?
C31 Ru3 Ru4 Ru1 89.72(9) . . . . ?
Ru2 Ru3 Ru4 Ru1 -70.48(2) . . . . ?
C11 Ru1 Ru4 C41 21.57(12) . . . . ?
O1 Ru1 Ru4 C41 129.01(9) . . . . ?
P1 Ru1 Ru4 C41 -133.70(11) . . . . ?
Ru2 Ru1 Ru4 C41 -74.74(8) . . . . ?
Ru3 Ru1 Ru4 C41 -142.65(8) . . . . ?
C11 Ru1 Ru4 C43 138.0(2) . . . . ?
O1 Ru1 Ru4 C43 -114.6(2) . . . . ?
P1 Ru1 Ru4 C43 -17.3(2) . . . . ?
Ru2 Ru1 Ru4 C43 41.7(2) . . . . ?
Ru3 Ru1 Ru4 C43 -26.2(2) . . . . ?
C11 Ru1 Ru4 C42 -83.98(13) . . . . ?
O1 Ru1 Ru4 C42 23.47(11) . . . . ?
P1 Ru1 Ru4 C42 120.76(13) . . . . ?
Ru2 Ru1 Ru4 C42 179.72(10) . . . . ?
Ru3 Ru1 Ru4 C42 111.81(10) . . . . ?
C11 Ru1 Ru4 Ru2 96.31(8) . . . . ?
O1 Ru1 Ru4 Ru2 -156.25(5) . . . . ?
P1 Ru1 Ru4 Ru2 -58.96(8) . . . . ?
Ru3 Ru1 Ru4 Ru2 -67.907(19) . . . . ?
C11 Ru1 Ru4 Ru3 164.21(8) . . . . ?
O1 Ru1 Ru4 Ru3 -88.34(5) . . . . ?
P1 Ru1 Ru4 Ru3 8.95(8) . . . . ?
Ru2 Ru1 Ru4 Ru3 67.907(19) . . . . ?
C11 Ru1 P1 C76 60.57(12) . . . . ?
O1 Ru1 P1 C76 -45.08(10) . . . . ?
Ru2 Ru1 P1 C76 163.97(9) . . . . ?
Ru4 Ru1 P1 C76 -143.64(10) . . . . ?
Ru3 Ru1 P1 C76 -135.64(9) . . . . ?
C11 Ru1 P1 C51 -178.93(12) . . . . ?
O1 Ru1 P1 C51 75.42(11) . . . . ?
Ru2 Ru1 P1 C51 -75.53(10) . . . . ?
Ru4 Ru1 P1 C51 -23.14(14) . . . . ?
Ru3 Ru1 P1 C51 -15.14(10) . . . . ?
C11 Ru1 P1 C54 -65.05(13) . . . . ?
O1 Ru1 P1 C54 -170.70(11) . . . . ?
Ru2 Ru1 P1 C54 38.34(11) . . . . ?
Ru4 Ru1 P1 C54 90.73(13) . . . . ?
Ru3 Ru1 P1 C54 98.74(10) . . . . ?
C71 P2 O1 Ru1 -54.55(15) . . . . ?
C64 P2 O1 Ru1 -178.55(12) . . . . ?
C61 P2 O1 Ru1 74.79(15) . . . . ?
C11 Ru1 O1 P2 -21.88(15) . . . . ?
P1 Ru1 O1 P2 67.89(11) . . . . ?
Ru2 Ru1 O1 P2 -161.00(6) . . . . ?
Ru4 Ru1 O1 P2 -125.70(11) . . . . ?
Ru3 Ru1 O1 P2 176.09(11) . . . . ?
O1 Ru1 C11 O11 179(100) . . . . ?
P1 Ru1 C11 O11 93(4) . . . . ?
Ru2 Ru1 C11 O11 -24(4) . . . . ?
Ru4 Ru1 C11 O11 -81(4) . . . . ?
Ru3 Ru1 C11 O11 -48(4) . . . . ?
C23 Ru2 C21 O21 -137(4) . . . . ?
C22 Ru2 C21 O21 -39(4) . . . . ?
Ru4 Ru2 C21 O21 137(4) . . . . ?
Ru3 Ru2 C21 O21 95(4) . . . . ?
Ru1 Ru2 C21 O21 71(4) . . . . ?
C23 Ru2 C22 O22 17(6) . . . . ?
C21 Ru2 C22 O22 -79(6) . . . . ?
Ru4 Ru2 C22 O22 113(6) . . . . ?
Ru3 Ru2 C22 O22 112(6) . . . . ?
Ru1 Ru2 C22 O22 177(100) . . . . ?
C21 Ru2 C23 O23 20(5) . . . . ?
C22 Ru2 C23 O23 -77(5) . . . . ?
Ru4 Ru2 C23 O23 124(5) . . . . ?
Ru3 Ru2 C23 O23 -173(5) . . . . ?
Ru1 Ru2 C23 O23 140(5) . . . . ?
C33 Ru3 C31 O31 84(2) . . . . ?
C32 Ru3 C31 O31 176(2) . . . . ?
Ru2 Ru3 C31 O31 -31(2) . . . . ?
Ru4 Ru3 C31 O31 -88(2) . . . . ?
Ru1 Ru3 C31 O31 -26(2) . . . . ?
C33 Ru3 C32 O32 11(9) . . . . ?
C31 Ru3 C32 O32 -88(9) . . . . ?
Ru2 Ru3 C32 O32 101(9) . . . . ?
Ru4 Ru3 C32 O32 158(9) . . . . ?
Ru1 Ru3 C32 O32 137(8) . . . . ?
C32 Ru3 C33 O33 -63(6) . . . . ?
C31 Ru3 C33 O33 39(6) . . . . ?
Ru2 Ru3 C33 O33 -159(6) . . . . ?
Ru4 Ru3 C33 O33 -155(6) . . . . ?
Ru1 Ru3 C33 O33 143(6) . . . . ?
C43 Ru4 C41 O41 45(7) . . . . ?
C42 Ru4 C41 O41 -50(7) . . . . ?
Ru2 Ru4 C41 O41 145(7) . . . . ?
Ru3 Ru4 C41 O41 146(7) . . . . ?
Ru1 Ru4 C41 O41 -158(7) . . . . ?
C41 Ru4 C42 O42 -42(10) . . . . ?
C43 Ru4 C42 O42 -135(10) . . . . ?
Ru2 Ru4 C42 O42 63(11) . . . . ?
Ru3 Ru4 C42 O42 127(10) . . . . ?
Ru1 Ru4 C42 O42 62(10) . . . . ?
C41 Ru4 C43 O43 -67(5) . . . . ?
C42 Ru4 C43 O43 35(5) . . . . ?
Ru2 Ru4 C43 O43 -149(5) . . . . ?
Ru3 Ru4 C43 O43 152(5) . . . . ?
Ru1 Ru4 C43 O43 175(5) . . . . ?
C76 P1 C51 C52 -92.31(19) . . . . ?
C54 P1 C51 C52 14.18(19) . . . . ?
Ru1 P1 C51 C52 142.46(15) . . . . ?
C76 P1 C51 C55 37.0(2) . . . . ?
C54 P1 C51 C55 143.5(2) . . . . ?
Ru1 P1 C51 C55 -88.2(2) . . . . ?
C55 C51 C52 C53 -166.7(2) . . . . ?
P1 C51 C52 C53 -37.9(3) . . . . ?
C51 C52 C53 C54 50.8(3) . . . . ?
C52 C53 C54 C56 -165.3(2) . . . . ?
C52 C53 C54 P1 -37.6(3) . . . . ?
C76 P1 C54 C56 -114.8(2) . . . . ?
C51 P1 C54 C56 139.2(2) . . . . ?
Ru1 P1 C54 C56 14.6(2) . . . . ?
C76 P1 C54 C53 118.9(2) . . . . ?
C51 P1 C54 C53 12.9(2) . . . . ?
Ru1 P1 C54 C53 -111.73(18) . . . . ?
O1 P2 C61 C65 -124.2(2) . . . . ?
C71 P2 C61 C65 5.7(3) . . . . ?
C64 P2 C61 C65 122.1(2) . . . . ?
O1 P2 C61 C62 108.96(17) . . . . ?
C71 P2 C61 C62 -121.19(18) . . . . ?
C64 P2 C61 C62 -4.81(19) . . . . ?
C65 C61 C62 C63 -153.0(3) . . . . ?
P2 C61 C62 C63 -22.9(3) . . . . ?
C61 C62 C63 C64 47.9(3) . . . . ?
C62 C63 C64 C66 -170.3(2) . . . . ?
C62 C63 C64 P2 -47.4(3) . . . . ?
O1 P2 C64 C63 -86.47(18) . . . . ?
C71 P2 C64 C63 147.89(17) . . . . ?
C61 P2 C64 C63 30.12(19) . . . . ?
O1 P2 C64 C66 37.2(2) . . . . ?
C71 P2 C64 C66 -88.4(2) . . . . ?
C61 P2 C64 C66 153.8(2) . . . . ?
O1 P2 C71 C72 -170.19(18) . . . . ?
C64 P2 C71 C72 -47.4(2) . . . . ?
C61 P2 C71 C72 60.7(2) . . . . ?
O1 P2 C71 C76 6.7(3) . . . . ?
C64 P2 C71 C76 129.5(2) . . . . ?
C61 P2 C71 C76 -122.4(2) . . . . ?
C76 C71 C72 C73 -0.4(4) . . . . ?
P2 C71 C72 C73 176.7(2) . . . . ?
C71 C72 C73 C74 -2.3(4) . . . . ?
C72 C73 C74 C75 2.2(5) . . . . ?
C73 C74 C75 C76 0.6(5) . . . . ?
C74 C75 C76 C71 -3.3(4) . . . . ?
C74 C75 C76 P1 177.0(2) . . . . ?
C72 C71 C76 C75 3.1(4) . . . . ?
P2 C71 C76 C75 -173.7(2) . . . . ?
C72 C71 C76 P1 -177.20(19) . . . . ?
P2 C71 C76 P1 6.0(3) . . . . ?
C51 P1 C76 C75 74.5(2) . . . . ?
C54 P1 C76 C75 -24.4(2) . . . . ?
Ru1 P1 C76 C75 -158.4(2) . . . . ?
C51 P1 C76 C71 -105.2(2) . . . . ?
C54 P1 C76 C71 155.9(2) . . . . ?
Ru1 P1 C76 C71 21.9(2) . . . . ?
