#------------------------------------------------------------------------------
#$Date: 2016-03-25 11:04:14 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179774 $
#$URL: svn://www.crystallography.net/cod/cif/7/00/70/7007023.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7007023
loop_
_publ_author_name
'Liu, Fenghui'
'Chen, Wanzhi'
'Wang, Daqi'
_publ_section_title
;
 Synthesis and characterization of amidate bridged dimeric and
 oligomeric platinum complexes having short platinum-platinum
 interactions.
;
_journal_issue                   28
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              3445
_journal_page_last               3453
_journal_paper_doi               10.1039/b516410a
_journal_year                    2006
_chemical_formula_sum            'C22 H50 N12 O21 Pt2'
_chemical_formula_weight         1208.92
_chemical_name_systematic
;
?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                94.157(6)
_cell_angle_beta                 94.387(6)
_cell_angle_gamma                118.081(7)
_cell_formula_units_Z            2
_cell_length_a                   12.795(7)
_cell_length_b                   13.271(7)
_cell_length_c                   14.866(8)
_cell_measurement_temperature    293(2)
_cell_volume                     2204(2)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.893
_diffrn_measured_fraction_theta_max 0.893
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0912
_diffrn_reflns_av_sigmaI/netI    0.0969
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       10
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       15
_diffrn_reflns_limit_l_min       -14
_diffrn_reflns_number            6266
_diffrn_reflns_theta_full        22.00
_diffrn_reflns_theta_max         22.00
_diffrn_reflns_theta_min         4.57
_exptl_absorpt_coefficient_mu    6.426
_exptl_absorpt_correction_T_max  0.6619
_exptl_absorpt_correction_T_min  0.4080
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   sadabs
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.822
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       plate
_exptl_crystal_F_000             1180
_exptl_crystal_size_max          0.17
_exptl_crystal_size_mid          0.12
_exptl_crystal_size_min          0.07
_refine_diff_density_max         1.884
_refine_diff_density_min         -1.669
_refine_diff_density_rms         0.203
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.060
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     572
_refine_ls_number_reflns         4829
_refine_ls_number_restraints     2043
_refine_ls_restrained_S_all      0.927
_refine_ls_R_factor_all          0.1011
_refine_ls_R_factor_gt           0.0651
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1037P)²+6.5525P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1622
_refine_ls_wR_factor_ref         0.1858
_reflns_number_gt                3245
_reflns_number_total             4829
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b516410a.txt
_cod_data_source_block           pt2ac
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_cell_volume        2203(2)
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7007023
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
C1 C 0.214(2) -0.1770(19) 0.1266(14) 0.069(3) Uani 1 1 d U B .
C2 C 0.209(2) -0.263(2) 0.0504(14) 0.077(4) Uani 1 1 d U . .
C3 C 0.327(2) -0.236(2) 0.0232(17) 0.110(7) Uani 1 1 d U . .
H3A H 0.3726 -0.2486 0.0710 0.165 Uiso 1 1 calc R . .
H3B H 0.3676 -0.1573 0.0121 0.165 Uiso 1 1 calc R . .
H3C H 0.3164 -0.2852 -0.0312 0.165 Uiso 1 1 calc R . .
C4 C 0.163(3) -0.378(2) 0.0860(17) 0.108(7) Uani 1 1 d U . .
H4A H 0.1571 -0.4346 0.0392 0.162 Uiso 1 1 calc R . .
H4B H 0.0854 -0.4003 0.1044 0.162 Uiso 1 1 calc R . .
H4C H 0.2167 -0.3719 0.1373 0.162 Uiso 1 1 calc R . .
C5 C 0.124(2) -0.270(2) -0.0313(15) 0.101(6) Uani 1 1 d U . .
H5A H 0.1605 -0.1999 -0.0588 0.151 Uiso 1 1 calc R . .
H5B H 0.0505 -0.2797 -0.0112 0.151 Uiso 1 1 calc R . .
H5C H 0.1079 -0.3338 -0.0750 0.151 Uiso 1 1 calc R . .
C6 C 0.122(2) -0.2061(19) 0.3546(14) 0.068(4) Uani 1 1 d U B .
C7 C 0.0702(18) -0.3048(17) 0.4079(12) 0.074(4) Uani 1 1 d DU . .
C11 C 0.486(5) 0.214(4) 0.374(3) 0.085(4) Uani 0.50(3) 1 d PDU A 1
H11 H 0.5517 0.1968 0.3833 0.101 Uiso 0.50(3) 1 calc PR A 1
C12 C 0.479(4) 0.229(2) 0.275(2) 0.086(4) Uani 0.50(3) 1 d PDU A 1
H12 H 0.4073 0.2377 0.2651 0.103 Uiso 0.50(3) 1 calc PR A 1
C13 C 0.572(4) 0.342(2) 0.265(2) 0.091(4) Uani 0.50(3) 1 d PRDU A 1
H13A H 0.5517 0.3559 0.2043 0.109 Uiso 0.50(3) 1 calc PR A 1
H13B H 0.6432 0.3341 0.2622 0.109 Uiso 0.50(3) 1 calc PR A 1
C14 C 0.611(5) 0.451(3) 0.323(2) 0.097(5) Uani 0.50(3) 1 d PDU A 1
H14A H 0.5573 0.4816 0.3079 0.116 Uiso 0.50(3) 1 calc PR A 1
H14B H 0.6904 0.5067 0.3108 0.116 Uiso 0.50(3) 1 calc PR A 1
C15 C 0.614(4) 0.435(4) 0.421(2) 0.089(5) Uani 0.50(3) 1 d PDU A 1
H15A H 0.6924 0.4441 0.4414 0.107 Uiso 0.50(3) 1 calc PR A 1
H15B H 0.6067 0.4961 0.4538 0.107 Uiso 0.50(3) 1 calc PR A 1
C16 C 0.530(4) 0.332(4) 0.445(2) 0.088(4) Uani 0.50(3) 1 d PRDU A 1
H16A H 0.4606 0.3403 0.4550 0.106 Uiso 0.50(3) 1 calc PR A 1
H16B H 0.5620 0.3213 0.5023 0.106 Uiso 0.50(3) 1 calc PR A 1
C17 C 0.128(3) 0.159(2) 0.297(2) 0.079(4) Uani 0.56(2) 1 d PDU B 1
H17 H 0.2105 0.1897 0.3251 0.094 Uiso 0.56(2) 1 calc PR B 1
C18 C 0.151(3) 0.179(2) 0.205(2) 0.083(3) Uani 0.56(2) 1 d PRDU B 1
H18 H 0.0650 0.1409 0.1841 0.100 Uiso 0.56(2) 1 calc PR B 1
C19 C 0.170(2) 0.2774(17) 0.1579(13) 0.087(4) Uani 1 1 d DU . .
H19A H 0.1232 0.2514 0.0983 0.104 Uiso 1 1 calc R B 1
H19B H 0.2536 0.3214 0.1499 0.104 Uiso 1 1 calc R B 1
C20 C 0.133(3) 0.351(2) 0.213(2) 0.090(4) Uani 0.56(2) 1 d PDU B 1
H20A H 0.0524 0.3308 0.1876 0.108 Uiso 0.56(2) 1 calc PR B 1
H20B H 0.1837 0.4298 0.2029 0.108 Uiso 0.56(2) 1 calc PR B 1
C21 C 0.132(3) 0.352(2) 0.322(2) 0.087(5) Uani 0.56(2) 1 d PRDU B 1
H21A H 0.2105 0.4069 0.3523 0.104 Uiso 0.56(2) 1 calc PR B 1
H21B H 0.0757 0.3768 0.3405 0.104 Uiso 0.56(2) 1 calc PR B 1
C22 C 0.098(4) 0.236(3) 0.351(3) 0.081(5) Uani 0.56(2) 1 d PDU B 1
H22A H 0.1353 0.2479 0.4129 0.098 Uiso 0.56(2) 1 calc PR B 1
H22B H 0.0123 0.1969 0.3523 0.098 Uiso 0.56(2) 1 calc PR B 1
C11' C 0.442(4) 0.227(2) 0.386(3) 0.086(4) Uani 0.50(3) 1 d PDU A 2
H11' H 0.3787 0.2424 0.3606 0.103 Uiso 0.50(3) 1 calc PR A 2
C12' C 0.499(4) 0.215(3) 0.303(2) 0.088(4) Uani 0.50(3) 1 d PDU A 2
H12' H 0.5573 0.1961 0.3326 0.106 Uiso 0.50(3) 1 calc PR A 2
C13' C 0.584(5) 0.334(3) 0.282(3) 0.091(4) Uani 0.50(3) 1 d PDU A 2
H13C H 0.5430 0.3555 0.2355 0.109 Uiso 0.50(3) 1 calc PR A 2
H13D H 0.6504 0.3310 0.2564 0.109 Uiso 0.50(3) 1 calc PR A 2
C14' C 0.631(4) 0.424(4) 0.364(3) 0.087(5) Uani 0.50(3) 1 d PDU A 2
H14C H 0.7000 0.4222 0.3944 0.104 Uiso 0.50(3) 1 calc PR A 2
H14D H 0.6609 0.4983 0.3412 0.104 Uiso 0.50(3) 1 calc PR A 2
C15' C 0.553(5) 0.422(4) 0.435(3) 0.091(5) Uani 0.50(3) 1 d PDU A 2
H15C H 0.6014 0.4793 0.4859 0.109 Uiso 0.50(3) 1 calc PR A 2
H15D H 0.4936 0.4410 0.4097 0.109 Uiso 0.50(3) 1 calc PR A 2
C16' C 0.492(4) 0.306(4) 0.468(3) 0.088(4) Uani 0.50(3) 1 d PDU A 2
H16C H 0.5488 0.2915 0.5037 0.106 Uiso 0.50(3) 1 calc PR A 2
H16D H 0.4301 0.3007 0.5037 0.106 Uiso 0.50(3) 1 calc PR A 2
C17' C 0.051(5) 0.120(4) 0.267(3) 0.081(4) Uani 0.44(2) 1 d PDU B 2
H17' H -0.0307 0.0754 0.2356 0.097 Uiso 0.44(2) 1 calc PR B 2
C18' C 0.135(5) 0.165(5) 0.196(4) 0.083(3) Uani 0.44(2) 1 d PDU B 2
H18' H 0.2066 0.1982 0.2407 0.100 Uiso 0.44(2) 1 calc PR B 2
C20' C 0.175(4) 0.373(3) 0.219(3) 0.090(4) Uani 0.44(2) 1 d PDU B 2
H20C H 0.1703 0.4307 0.1853 0.108 Uiso 0.44(2) 1 calc PR B 2
H20D H 0.2472 0.4090 0.2621 0.108 Uiso 0.44(2) 1 calc PR B 2
C21' C 0.064(4) 0.314(4) 0.269(3) 0.082(5) Uani 0.44(2) 1 d PDU B 2
H21C H 0.0592 0.3723 0.3084 0.098 Uiso 0.44(2) 1 calc PR B 2
H21D H -0.0058 0.2791 0.2240 0.098 Uiso 0.44(2) 1 calc PR B 2
C22' C 0.060(6) 0.222(4) 0.325(3) 0.081(5) Uani 0.44(2) 1 d PDU B 2
H22C H -0.0082 0.1971 0.3589 0.097 Uiso 0.44(2) 1 calc PR B 2
H22D H 0.1316 0.2543 0.3690 0.097 Uiso 0.44(2) 1 calc PR B 2
N1 N 0.3043(16) -0.1323(15) 0.1857(11) 0.069(3) Uani 1 1 d U . .
H1 H 0.3589 -0.1518 0.1801 0.082 Uiso 1 1 calc R . .
O2 O 0.2395(15) -0.1436(13) 0.3635(9) 0.079(3) Uani 1 1 d U . .
N3 N 0.3764(16) 0.1045(14) 0.4002(11) 0.075(3) Uani 1 1 d DU . .
H3D H 0.3157 0.1188 0.4095 0.090 Uiso 1 1 calc R A 1
H3E H 0.3976 0.0820 0.4510 0.090 Uiso 1 1 calc R A 1
N4 N 0.4410(17) 0.1158(15) 0.2271(12) 0.088(3) Uani 1 1 d DU . .
H4D H 0.5060 0.1081 0.2189 0.105 Uiso 1 1 calc R A 1
H4E H 0.4035 0.1103 0.1718 0.105 Uiso 1 1 calc R A 1
N5 N 0.0814(15) 0.0409(13) 0.3179(11) 0.070(3) Uani 1 1 d DU . .
H5D H 0.0018 0.0086 0.3175 0.084 Uiso 1 1 calc R B 1
H5E H 0.1136 0.0411 0.3739 0.084 Uiso 1 1 calc R B 1
N6 N 0.1641(16) 0.0832(15) 0.1506(11) 0.071(3) Uani 1 1 d U . .
H6A H 0.2398 0.1103 0.1384 0.085 Uiso 1 1 calc R B 1
H6B H 0.1157 0.0593 0.0976 0.085 Uiso 1 1 calc R B 1
N7 N 0.531(2) -0.0485(18) 0.3923(14) 0.087(4) Uani 1 1 d U A .
N8 N -0.100(2) -0.140(2) 0.0947(16) 0.095(5) Uani 1 1 d U B .
N9 N 0.432(3) 0.671(3) 0.282(2) 0.151(7) Uani 1 1 d U . .
N10 N 0.376(2) 0.157(3) 0.0178(19) 0.113(6) Uani 1 1 d U . .
N11 N 0.1599(19) 0.080(2) 0.5483(14) 0.073(4) Uani 1 1 d U . .
N12 N 0.702(3) 0.089(3) 0.2018(19) 0.114(6) Uani 1 1 d U . .
O1 O 0.1289(14) -0.1550(12) 0.1263(9) 0.073(3) Uani 1 1 d U . .
N2 N 0.0617(15) -0.1807(14) 0.3017(10) 0.062(3) Uani 1 1 d U . .
H2 H -0.0144 -0.2238 0.2967 0.074 Uiso 1 1 calc R B .
O3 O 0.5009(13) -0.0058(13) 0.3262(10) 0.081(3) Uani 1 1 d U . .
O4 O 0.4613(16) -0.1053(18) 0.4388(12) 0.116(5) Uani 1 1 d U . .
O5 O 0.6264(18) -0.0417(18) 0.3999(12) 0.117(5) Uani 1 1 d U . .
O6 O -0.0666(13) -0.1247(13) 0.1840(10) 0.081(3) Uani 1 1 d U . .
O7 O -0.0602(18) -0.0942(18) 0.0448(12) 0.116(6) Uani 1 1 d U . .
O8 O -0.205(2) -0.214(3) 0.0771(17) 0.201(10) Uani 1 1 d U . .
O9 O 0.483(2) 0.6155(19) 0.3075(16) 0.144(6) Uani 1 1 d U . .
O10 O 0.488(3) 0.749(2) 0.2392(19) 0.188(9) Uani 1 1 d U . .
O11 O 0.330(3) 0.647(2) 0.3013(17) 0.177(8) Uani 1 1 d U . .
O12 O 0.4002(18) 0.2385(19) 0.0698(13) 0.122(5) Uani 1 1 d U . .
O13 O 0.377(2) 0.164(2) -0.0730(16) 0.170(8) Uani 1 1 d U . .
O14 O 0.3280(19) 0.0553(19) 0.0294(12) 0.121(5) Uani 1 1 d U . .
O15 O 0.2242(16) 0.1629(15) 0.5109(10) 0.092(4) Uani 1 1 d U . .
O16 O 0.1449(15) 0.0951(15) 0.6286(11) 0.098(5) Uani 1 1 d U . .
O17 O 0.1158(16) -0.0145(16) 0.5078(11) 0.094(4) Uani 1 1 d U . .
O18 O 0.609(2) 0.036(2) 0.1536(14) 0.144(7) Uani 1 1 d U . .
O19 O 0.742(2) 0.169(2) 0.2516(17) 0.152(7) Uani 1 1 d U . .
O20 O 0.769(2) 0.036(2) 0.1871(17) 0.154(7) Uani 1 1 d U . .
O21 O 0.692(2) 0.724(2) 0.2602(15) 0.170(7) Uani 1 1 d U . .
H3 H 0.6640 0.7585 0.2290 0.204 Uiso 1 1 d R . .
H4 H 0.6317 0.6725 0.2808 0.204 Uiso 1 1 d R . .
Pt1 Pt 0.32922(6) -0.01666(6) 0.29353(5) 0.0487(3) Uani 1 1 d . A .
Pt2 Pt 0.11904(6) -0.05329(6) 0.22740(4) 0.0471(3) Uani 1 1 d . A .
C10 C -0.0520(19) -0.324(2) 0.4320(17) 0.117(4) Uani 1 1 d DU . .
H10A H -0.1070 -0.3468 0.3774 0.175 Uiso 1 1 calc R . .
H10B H -0.0435 -0.2533 0.4623 0.175 Uiso 1 1 calc R . .
H10C H -0.0817 -0.3827 0.4715 0.175 Uiso 1 1 calc R . .
C8 C 0.148(2) -0.278(2) 0.4980(14) 0.117(4) Uani 1 1 d DU . .
H8A H 0.1002 -0.2928 0.5468 0.175 Uiso 1 1 calc R . .
H8B H 0.2088 -0.1989 0.5061 0.175 Uiso 1 1 calc R . .
H8C H 0.1858 -0.3263 0.4979 0.175 Uiso 1 1 calc R . .
C9 C 0.055(2) -0.4081(19) 0.3454(15) 0.117(4) Uani 1 1 d DU . .
H9A H -0.0142 -0.4344 0.3017 0.175 Uiso 1 1 calc R . .
H9B H 0.0461 -0.4688 0.3808 0.175 Uiso 1 1 calc R . .
H9C H 0.1245 -0.3861 0.3144 0.175 Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O1 C1 N1 124(2) . . ?
O1 C1 C2 118(2) . . ?
N1 C1 C2 117(2) . . ?
C3 C2 C4 106(2) . . ?
C3 C2 C1 113(2) . . ?
C4 C2 C1 107.4(18) . . ?
C3 C2 C5 111(2) . . ?
C4 C2 C5 111(2) . . ?
C1 C2 C5 108.7(18) . . ?
C2 C3 H3A 109.5 . . ?
C2 C3 H3B 109.5 . . ?
H3A C3 H3B 109.5 . . ?
C2 C3 H3C 109.5 . . ?
H3A C3 H3C 109.5 . . ?
H3B C3 H3C 109.5 . . ?
C2 C4 H4A 109.5 . . ?
C2 C4 H4B 109.5 . . ?
H4A C4 H4B 109.5 . . ?
C2 C4 H4C 109.5 . . ?
H4A C4 H4C 109.5 . . ?
H4B C4 H4C 109.5 . . ?
C2 C5 H5A 109.5 . . ?
C2 C5 H5B 109.5 . . ?
H5A C5 H5B 109.5 . . ?
C2 C5 H5C 109.5 . . ?
H5A C5 H5C 109.5 . . ?
H5B C5 H5C 109.5 . . ?
N2 C6 O2 119(2) . . ?
N2 C6 C7 124(2) . . ?
O2 C6 C7 117.8(17) . . ?
C6 C7 C8 110.2(19) . . ?
C6 C7 C9 105.3(16) . . ?
C8 C7 C9 115.4(17) . . ?
C6 C7 C10 109.7(17) . . ?
C8 C7 C10 106.1(16) . . ?
C9 C7 C10 110.2(16) . . ?
C12 C11 N3 115(4) . . ?
C12 C11 C16 115(3) . . ?
N3 C11 C16 115(3) . . ?
C12 C11 H11 103.2 . . ?
N3 C11 H11 103.2 . . ?
C16 C11 H11 103.2 . . ?
C13 C12 N4 132.9(19) . . ?
C13 C12 C11 108(2) . . ?
N4 C12 C11 105(3) . . ?
C13 C12 H12 102.3 . . ?
N4 C12 H12 102.3 . . ?
C11 C12 H12 102.3 . . ?
C12 C13 C14 129(2) . . ?
C12 C13 H13A 105.1 . . ?
C14 C13 H13A 105.1 . . ?
C12 C13 H13B 105.1 . . ?
C14 C13 H13B 105.1 . . ?
H13A C13 H13B 105.9 . . ?
C13 C14 C15 111(3) . . ?
C13 C14 H14A 109.5 . . ?
C15 C14 H14A 109.5 . . ?
C13 C14 H14B 109.5 . . ?
C15 C14 H14B 109.5 . . ?
H14A C14 H14B 108.0 . . ?
C16 C15 C14 118(2) . . ?
C16 C15 H15A 107.8 . . ?
C14 C15 H15A 107.8 . . ?
C16 C15 H15B 107.8 . . ?
C14 C15 H15B 107.8 . . ?
H15A C15 H15B 107.1 . . ?
C15 C16 C11 119(2) . . ?
C15 C16 H16A 107.7 . . ?
C11 C16 H16A 107.7 . . ?
C15 C16 H16B 107.7 . . ?
C11 C16 H16B 107.7 . . ?
H16A C16 H16B 107.1 . . ?
C18 C17 C22 118.7(16) . . ?
C18 C17 N5 116.6(16) . . ?
C22 C17 N5 119(3) . . ?
C18 C17 H17 98.2 . . ?
C22 C17 H17 98.2 . . ?
N5 C17 H17 98.2 . . ?
C17 C18 C19 130.1(16) . . ?
C17 C18 N6 114.2(11) . . ?
C19 C18 N6 116(2) . . ?
C17 C18 H18 91.0 . . ?
C19 C18 H18 91.0 . . ?
N6 C18 H18 91.0 . . ?
C18 C19 C20' 112(3) . . ?
C18 C19 C20 108(2) . . ?
C20' C19 C18' 117(3) . . ?
C20 C19 C18' 111(3) . . ?
C18 C19 H19A 110.0 . . ?
C20' C19 H19A 122.2 . . ?
C20 C19 H19A 110.0 . . ?
C18' C19 H19A 101.8 . . ?
C18 C19 H19B 110.0 . . ?
C20' C19 H19B 92.5 . . ?
C20 C19 H19B 110.0 . . ?
C18' C19 H19B 115.5 . . ?
H19A C19 H19B 108.4 . . ?
C19 C20 C21 122.7(14) . . ?
C19 C20 H20A 106.7 . . ?
C21 C20 H20A 106.7 . . ?
C19 C20 H20B 106.7 . . ?
C21 C20 H20B 106.7 . . ?
H20A C20 H20B 106.6 . . ?
C22 C21 C20 112(2) . . ?
C22 C21 H21A 109.2 . . ?
C20 C21 H21A 109.2 . . ?
C22 C21 H21B 109.2 . . ?
C20 C21 H21B 109.2 . . ?
H21A C21 H21B 107.9 . . ?
C17 C22 C21 118(3) . . ?
C17 C22 H22A 107.7 . . ?
C21 C22 H22A 107.7 . . ?
C17 C22 H22B 107.7 . . ?
C21 C22 H22B 107.7 . . ?
H22A C22 H22B 107.1 . . ?
C16' C11' N3 115(3) . . ?
C16' C11' C12' 131(4) . . ?
N3 C11' C12' 99(3) . . ?
C16' C11' H11' 103.0 . . ?
N3 C11' H11' 103.0 . . ?
C12' C11' H11' 103.0 . . ?
C11' C12' C13' 109(3) . . ?
C11' C12' N4 125(3) . . ?
C13' C12' N4 119(3) . . ?
C11' C12' H12' 98.6 . . ?
C13' C12' H12' 98.6 . . ?
N4 C12' H12' 98.6 . . ?
C12' C13' C14' 113(4) . . ?
C12' C13' H13C 109.0 . . ?
C14' C13' H13C 109.0 . . ?
C12' C13' H13D 109.0 . . ?
C14' C13' H13D 109.0 . . ?
H13C C13' H13D 107.8 . . ?
C15' C14' C13' 121(5) . . ?
C15' C14' H14C 107.1 . . ?
C13' C14' H14C 107.1 . . ?
C15' C14' H14D 107.1 . . ?
C13' C14' H14D 107.1 . . ?
H14C C14' H14D 106.8 . . ?
C16' C15' C14' 112(4) . . ?
C16' C15' H15C 109.3 . . ?
C14' C15' H15C 109.3 . . ?
C16' C15' H15D 109.3 . . ?
C14' C15' H15D 109.3 . . ?
H15C C15' H15D 107.9 . . ?
C11' C16' C15' 104(4) . . ?
C11' C16' H16C 110.9 . . ?
C15' C16' H16C 110.9 . . ?
C11' C16' H16D 110.9 . . ?
C15' C16' H16D 110.9 . . ?
H16C C16' H16D 108.9 . . ?
C18' C17' C22' 108(5) . . ?
C18' C17' N5 109(3) . . ?
C22' C17' N5 114(3) . . ?
C18' C17' H17' 108.6 . . ?
C22' C17' H17' 108.6 . . ?
N5 C17' H17' 108.6 . . ?
N6 C18' C19 118(3) . . ?
N6 C18' C17' 115(4) . . ?
C19 C18' C17' 125(4) . . ?
N6 C18' H18' 93.5 . . ?
C19 C18' H18' 93.5 . . ?
C17' C18' H18' 93.5 . . ?
C19 C20' C21' 104(3) . . ?
C19 C20' H20C 111.0 . . ?
C21' C20' H20C 111.0 . . ?
C19 C20' H20D 111.0 . . ?
C21' C20' H20D 111.0 . . ?
H20C C20' H20D 109.0 . . ?
C22' C21' C20' 116(4) . . ?
C22' C21' H21C 108.2 . . ?
C20' C21' H21C 108.2 . . ?
C22' C21' H21D 108.2 . . ?
C20' C21' H21D 108.2 . . ?
H21C C21' H21D 107.3 . . ?
C21' C22' C17' 111(4) . . ?
C21' C22' H22C 109.4 . . ?
C17' C22' H22C 109.4 . . ?
C21' C22' H22D 109.4 . . ?
C17' C22' H22D 109.4 . . ?
H22C C22' H22D 108.0 . . ?
C1 N1 Pt1 124.1(15) . . ?
C1 N1 H1 117.9 . . ?
Pt1 N1 H1 117.9 . . ?
C6 O2 Pt1 125.3(12) . . ?
C11' N3 Pt1 118.7(18) . . ?
C11 N3 Pt1 105.2(19) . . ?
C11 N3 H3D 110.7 . . ?
Pt1 N3 H3D 110.7 . . ?
C11' N3 H3E 119.1 . . ?
C11 N3 H3E 110.7 . . ?
Pt1 N3 H3E 110.7 . . ?
H3D N3 H3E 108.8 . . ?
C12 N4 Pt1 113.8(18) . . ?
C12' N4 Pt1 101.8(19) . . ?
C12 N4 H4D 108.8 . . ?
C12' N4 H4D 97.8 . . ?
Pt1 N4 H4D 108.8 . . ?
C12 N4 H4E 108.8 . . ?
C12' N4 H4E 130.4 . . ?
Pt1 N4 H4E 108.8 . . ?
H4D N4 H4E 107.7 . . ?
C17 N5 Pt2 111.5(17) . . ?
C17' N5 Pt2 107.6(19) . . ?
C17 N5 H5D 109.3 . . ?
C17' N5 H5D 77.6 . . ?
Pt2 N5 H5D 109.3 . . ?
C17 N5 H5E 109.3 . . ?
C17' N5 H5E 137.8 . . ?
Pt2 N5 H5E 109.3 . . ?
H5D N5 H5E 108.0 . . ?
C18' N6 Pt2 108(2) . . ?
C18 N6 Pt2 108.7(13) . . ?
C18' N6 H6A 116.6 . . ?
C18 N6 H6A 110.0 . . ?
Pt2 N6 H6A 110.0 . . ?
C18' N6 H6B 103.2 . . ?
C18 N6 H6B 110.0 . . ?
Pt2 N6 H6B 110.0 . . ?
H6A N6 H6B 108.3 . . ?
O5 N7 O4 119(2) . . ?
O5 N7 O3 120(2) . . ?
O4 N7 O3 121(2) . . ?
O7 N8 O8 118(3) . . ?
O7 N8 O6 132(3) . . ?
O8 N8 O6 109(2) . . ?
O10 N9 O9 116(4) . . ?
O10 N9 O11 123(4) . . ?
O9 N9 O11 121(4) . . ?
O12 N10 O14 129(3) . . ?
O12 N10 O13 121(3) . . ?
O14 N10 O13 109(3) . . ?
O17 N11 O15 119(2) . . ?
O17 N11 O16 121(2) . . ?
O15 N11 O16 120(2) . . ?
O19 N12 O18 134(4) . . ?
O19 N12 O20 118(3) . . ?
O18 N12 O20 108(3) . . ?
C1 O1 Pt2 122.0(14) . . ?
C6 N2 Pt2 127.6(17) . . ?
C6 N2 H2 116.2 . . ?
Pt2 N2 H2 116.2 . . ?
N7 O3 Pt1 126.3(15) . . ?
N8 O6 Pt2 116.7(15) . . ?
H4 O21 H3 104.0 . . ?
H4 O21 H3 104.0 . . ?
H3 O21 H4 104.0 . . ?
H3 O21 H4 104.0 . . ?
O2 Pt1 N3 93.5(6) . . ?
O2 Pt1 N1 89.9(6) . . ?
N3 Pt1 N1 172.6(7) . . ?
O2 Pt1 N4 173.1(7) . . ?
N3 Pt1 N4 85.5(7) . . ?
N1 Pt1 N4 90.4(7) . . ?
O2 Pt1 O3 97.1(6) . . ?
N3 Pt1 O3 86.5(6) . . ?
N1 Pt1 O3 86.6(6) . . ?
N4 Pt1 O3 76.0(6) . . ?
O2 Pt1 Pt2 84.0(4) . . ?
N3 Pt1 Pt2 103.9(5) . . ?
N1 Pt1 Pt2 83.0(5) . . ?
N4 Pt1 Pt2 102.9(5) . . ?
O3 Pt1 Pt2 169.5(4) . . ?
N2 Pt2 O1 90.1(6) . . ?
N2 Pt2 N5 90.7(6) . . ?
O1 Pt2 N5 170.2(6) . . ?
N2 Pt2 N6 174.1(6) . . ?
O1 Pt2 N6 93.3(6) . . ?
N5 Pt2 N6 85.2(6) . . ?
N2 Pt2 O6 82.0(6) . . ?
O1 Pt2 O6 89.2(6) . . ?
N5 Pt2 O6 81.3(7) . . ?
N6 Pt2 O6 93.1(6) . . ?
N2 Pt2 Pt1 84.3(5) . . ?
O1 Pt2 Pt1 86.3(4) . . ?
N5 Pt2 Pt1 103.5(5) . . ?
N6 Pt2 Pt1 100.8(5) . . ?
O6 Pt2 Pt1 165.6(4) . . ?
C7 C10 H10A 109.5 . . ?
C7 C10 H10B 109.5 . . ?
H10A C10 H10B 109.5 . . ?
C7 C10 H10C 109.5 . . ?
H10A C10 H10C 109.5 . . ?
H10B C10 H10C 109.5 . . ?
C7 C8 H8A 109.5 . . ?
C7 C8 H8B 109.5 . . ?
H8A C8 H8B 109.5 . . ?
C7 C8 H8C 109.5 . . ?
H8A C8 H8C 109.5 . . ?
H8B C8 H8C 109.5 . . ?
C7 C9 H9A 109.5 . . ?
C7 C9 H9B 109.5 . . ?
H9A C9 H9B 109.5 . . ?
C7 C9 H9C 109.5 . . ?
H9A C9 H9C 109.5 . . ?
H9B C9 H9C 109.5 . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
C1 O1 1.25(2) . ?
C1 N1 1.26(2) . ?
C1 C2 1.53(3) . ?
C2 C3 1.47(3) . ?
C2 C4 1.50(3) . ?
C2 C5 1.53(3) . ?
C3 H3A 0.9600 . ?
C3 H3B 0.9600 . ?
C3 H3C 0.9600 . ?
C4 H4A 0.9600 . ?
C4 H4B 0.9600 . ?
C4 H4C 0.9600 . ?
C5 H5A 0.9600 . ?
C5 H5B 0.9600 . ?
C5 H5C 0.9600 . ?
C6 N2 1.23(2) . ?
C6 O2 1.32(2) . ?
C6 C7 1.48(3) . ?
C7 C8 1.521(15) . ?
C7 C9 1.524(15) . ?
C7 C10 1.538(15) . ?
C11 C12 1.502(18) . ?
C11 N3 1.57(5) . ?
C11 C16 1.65(6) . ?
C11 H11 0.9800 . ?
C12 C13 1.4330 . ?
C12 N4 1.456(17) . ?
C12 H12 0.9800 . ?
C13 C14 1.469(18) . ?
C13 H13A 0.9700 . ?
C13 H13B 0.9700 . ?
C14 C15 1.489(18) . ?
C14 H14A 0.9700 . ?
C14 H14B 0.9700 . ?
C15 C16 1.3695 . ?
C15 H15A 0.9700 . ?
C15 H15B 0.9700 . ?
C16 H16A 0.9700 . ?
C16 H16B 0.9700 . ?
C17 C18 1.4388 . ?
C17 C22 1.45(5) . ?
C17 N5 1.463(16) . ?
C17 H17 0.9800 . ?
C18 C19 1.456(16) . ?
C18 N6 1.54(4) . ?
C18 H18 0.9800 . ?
C19 C20' 1.483(18) . ?
C19 C20 1.498(17) . ?
C19 C18' 1.51(5) . ?
C19 H19A 0.9700 . ?
C19 H19B 0.9700 . ?
C20 C21 1.6126 . ?
C20 H20A 0.9700 . ?
C20 H20B 0.9700 . ?
C21 C22 1.493(17) . ?
C21 H21A 0.9700 . ?
C21 H21B 0.9700 . ?
C22 H22A 0.9700 . ?
C22 H22B 0.9700 . ?
C11' C16' 1.43(6) . ?
C11' N3 1.481(18) . ?
C11' C12' 1.504(18) . ?
C11' H11' 0.9800 . ?
C12' C13' 1.509(18) . ?
C12' N4 1.520(18) . ?
C12' H12' 0.9800 . ?
C13' C14' 1.514(18) . ?
C13' H13C 0.9700 . ?
C13' H13D 0.9700 . ?
C14' C15' 1.501(18) . ?
C14' H14C 0.9700 . ?
C14' H14D 0.9700 . ?
C15' C16' 1.495(13) . ?
C15' H15C 0.9700 . ?
C15' H15D 0.9700 . ?
C16' H16C 0.9700 . ?
C16' H16D 0.9700 . ?
C17' C18' 1.509(18) . ?
C17' C22' 1.510(18) . ?
C17' N5 1.513(17) . ?
C17' H17' 0.9800 . ?
C18' N6 1.45(6) . ?
C18' H18' 0.9800 . ?
C20' C21' 1.531(18) . ?
C20' H20C 0.9700 . ?
C20' H20D 0.9700 . ?
C21' C22' 1.507(18) . ?
C21' H21C 0.9700 . ?
C21' H21D 0.9700 . ?
C22' H22C 0.9700 . ?
C22' H22D 0.9700 . ?
N1 Pt1 2.032(16) . ?
N1 H1 0.8600 . ?
O2 Pt1 1.964(14) . ?
N3 Pt1 2.009(17) . ?
N3 H3D 0.9000 . ?
N3 H3E 0.9000 . ?
N4 Pt1 2.052(18) . ?
N4 H4D 0.9000 . ?
N4 H4E 0.9000 . ?
N5 Pt2 2.006(15) . ?
N5 H5D 0.9000 . ?
N5 H5E 0.9000 . ?
N6 Pt2 2.082(15) . ?
N6 H6A 0.9000 . ?
N6 H6B 0.9000 . ?
N7 O5 1.17(2) . ?
N7 O4 1.18(2) . ?
N7 O3 1.29(2) . ?
N8 O7 1.00(2) . ?
N8 O8 1.23(3) . ?
N8 O6 1.33(2) . ?
N9 O10 1.20(3) . ?
N9 O9 1.25(4) . ?
N9 O11 1.26(4) . ?
N10 O12 1.18(3) . ?
N10 O14 1.22(3) . ?
N10 O13 1.36(3) . ?
N11 O17 1.20(2) . ?
N11 O15 1.23(2) . ?
N11 O16 1.24(2) . ?
N12 O19 1.12(3) . ?
N12 O18 1.19(3) . ?
N12 O20 1.36(3) . ?
O1 Pt2 1.997(13) . ?
N2 Pt2 1.960(15) . ?
N2 H2 0.8600 . ?
O3 Pt1 2.147(14) . ?
O6 Pt2 2.124(15) . ?
O21 H4 0.8500 . ?
O21 H3 0.8500 . ?
O21 H3 0.8500 . ?
O21 H4 0.8500 . ?
Pt1 Pt2 2.5942(17) . ?
C10 H10A 0.9600 . ?
C10 H10B 0.9600 . ?
C10 H10C 0.9600 . ?
C8 H8A 0.9600 . ?
C8 H8B 0.9600 . ?
C8 H8C 0.9600 . ?
C9 H9A 0.9600 . ?
C9 H9B 0.9600 . ?
C9 H9C 0.9600 . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
O1 C1 C2 C3 146(2) . . . . ?
N1 C1 C2 C3 -34(3) . . . . ?
O1 C1 C2 C4 -97(2) . . . . ?
N1 C1 C2 C4 83(3) . . . . ?
O1 C1 C2 C5 22(3) . . . . ?
N1 C1 C2 C5 -157(2) . . . . ?
N2 C6 C7 C8 -149(2) . . . . ?
O2 C6 C7 C8 32(2) . . . . ?
N2 C6 C7 C9 86(2) . . . . ?
O2 C6 C7 C9 -93(2) . . . . ?
N2 C6 C7 C10 -32(3) . . . . ?
O2 C6 C7 C10 148.8(18) . . . . ?
N3 C11 C12 C13 170(3) . . . . ?
C16 C11 C12 C13 33(4) . . . . ?
N3 C11 C12 N4 -44(5) . . . . ?
C16 C11 C12 N4 179(3) . . . . ?
N4 C12 C13 C14 -173(5) . . . . ?
C11 C12 C13 C14 -41(4) . . . . ?
C12 C13 C14 C15 41(6) . . . . ?
C13 C14 C15 C16 -34(5) . . . . ?
C14 C15 C16 C11 34(4) . . . . ?
C12 C11 C16 C15 -35(5) . . . . ?
N3 C11 C16 C15 -171.5(18) . . . . ?
C22 C17 C18 C19 12(3) . . . . ?
N5 C17 C18 C19 164(4) . . . . ?
C22 C17 C18 N6 -172(4) . . . . ?
N5 C17 C18 N6 -19.7(11) . . . . ?
C17 C18 C19 C20' 5(4) . . . . ?
N6 C18 C19 C20' -171(3) . . . . ?
C17 C18 C19 C20 -14(3) . . . . ?
N6 C18 C19 C20 170(2) . . . . ?
C18 C19 C20 C21 25(3) . . . . ?
C20' C19 C20 C21 -79(9) . . . . ?
C18' C19 C20 C21 34(3) . . . . ?
C19 C20 C21 C22 -35(2) . . . . ?
C18 C17 C22 C21 -20(4) . . . . ?
N5 C17 C22 C21 -172(3) . . . . ?
C20 C21 C22 C17 30(4) . . . . ?
C16' C11' C12' C13' -40(7) . . . . ?
N3 C11' C12' C13' -173(3) . . . . ?
C16' C11' C12' N4 170(4) . . . . ?
N3 C11' C12' N4 36(6) . . . . ?
C11' C12' C13' C14' 26(6) . . . . ?
N4 C12' C13' C14' 178(4) . . . . ?
C12' C13' C14' C15' -38(7) . . . . ?
C13' C14' C15' C16' 51(6) . . . . ?
N3 C11' C16' C15' 180(3) . . . . ?
C12' C11' C16' C15' 51(7) . . . . ?
C14' C15' C16' C11' -49(6) . . . . ?
C20' C19 C18' N6 -161(4) . . . . ?
C20 C19 C18' N6 -180(4) . . . . ?
C20' C19 C18' C17' 31(7) . . . . ?
C20 C19 C18' C17' 13(7) . . . . ?
C22' C17' C18' N6 163(4) . . . . ?
N5 C17' C18' N6 38(6) . . . . ?
C22' C17' C18' C19 -29(7) . . . . ?
N5 C17' C18' C19 -154(4) . . . . ?
C18 C19 C20' C21' -49(5) . . . . ?
C20 C19 C20' C21' 33(6) . . . . ?
C18' C19 C20' C21' -41(5) . . . . ?
C19 C20' C21' C22' 61(6) . . . . ?
C20' C21' C22' C17' -66(6) . . . . ?
C18' C17' C22' C21' 42(6) . . . . ?
N5 C17' C22' C21' 163(4) . . . . ?
O1 C1 N1 Pt1 1(3) . . . . ?
C2 C1 N1 Pt1 -179.4(14) . . . . ?
N2 C6 O2 Pt1 -4(3) . . . . ?
C7 C6 O2 Pt1 175.1(12) . . . . ?
C16' C11' N3 C11 -105(8) . . . . ?
C12' C11' N3 C11 38(4) . . . . ?
C16' C11' N3 Pt1 -168(3) . . . . ?
C12' C11' N3 Pt1 -25(4) . . . . ?
C12 C11 N3 C11' -91(7) . . . . ?
C16 C11 N3 C11' 46(6) . . . . ?
C12 C11 N3 Pt1 35(4) . . . . ?
C16 C11 N3 Pt1 172(2) . . . . ?
C13 C12 N4 C12' 106(9) . . . . ?
C11 C12 N4 C12' -27(6) . . . . ?
C13 C12 N4 Pt1 165.8(8) . . . . ?
C11 C12 N4 Pt1 32(4) . . . . ?
C11' C12' N4 C12 98(10) . . . . ?
C13' C12' N4 C12 -50(8) . . . . ?
C11' C12' N4 Pt1 -28(5) . . . . ?
C13' C12' N4 Pt1 -176(4) . . . . ?
C18 C17 N5 C17' -69(4) . . . . ?
C22 C17 N5 C17' 83(5) . . . . ?
C18 C17 N5 Pt2 21.7(16) . . . . ?
C22 C17 N5 Pt2 174(3) . . . . ?
C18' C17' N5 C17 62(6) . . . . ?
C22' C17' N5 C17 -58(5) . . . . ?
C18' C17' N5 Pt2 -40(5) . . . . ?
C22' C17' N5 Pt2 -161(4) . . . . ?
C19 C18' N6 C18 81(16) . . . . ?
C19 C18' N6 Pt2 174(3) . . . . ?
C17' C18' N6 Pt2 -17(5) . . . . ?
C19 C18 N6 C18' -86(18) . . . . ?
C17 C18 N6 Pt2 8.0(15) . . . . ?
C19 C18 N6 Pt2 -175(2) . . . . ?
N1 C1 O1 Pt2 -5(3) . . . . ?
C2 C1 O1 Pt2 175.1(14) . . . . ?
O2 C6 N2 Pt2 -1(3) . . . . ?
C7 C6 N2 Pt2 -179.9(13) . . . . ?
O5 N7 O3 Pt1 176.0(17) . . . . ?
O4 N7 O3 Pt1 5(3) . . . . ?
O7 N8 O6 Pt2 -35(4) . . . . ?
O8 N8 O6 Pt2 157(2) . . . . ?
C6 O2 Pt1 N3 108.5(17) . . . . ?
C6 O2 Pt1 N1 -78.0(17) . . . . ?
C6 O2 Pt1 O3 -164.6(16) . . . . ?
C6 O2 Pt1 Pt2 4.9(16) . . . . ?
C11' N3 Pt1 O2 -175(3) . . . . ?
C11 N3 Pt1 O2 161(2) . . . . ?
C11' N3 Pt1 N4 12(3) . . . . ?
C11 N3 Pt1 N4 -12(2) . . . . ?
C11' N3 Pt1 O3 88(3) . . . . ?
C11 N3 Pt1 O3 65(2) . . . . ?
C11' N3 Pt1 Pt2 -90(3) . . . . ?
C11 N3 Pt1 Pt2 -113.9(19) . . . . ?
C1 N1 Pt1 O2 86.5(17) . . . . ?
C1 N1 Pt1 N4 -100.4(18) . . . . ?
C1 N1 Pt1 O3 -176.4(17) . . . . ?
C1 N1 Pt1 Pt2 2.5(16) . . . . ?
C12 N4 Pt1 N3 -12(2) . . . . ?
C12' N4 Pt1 N3 7(2) . . . . ?
C12 N4 Pt1 N1 174(2) . . . . ?
C12' N4 Pt1 N1 -167(2) . . . . ?
C12 N4 Pt1 O3 -99(2) . . . . ?
C12' N4 Pt1 O3 -81(2) . . . . ?
C12 N4 Pt1 Pt2 91(2) . . . . ?
C12' N4 Pt1 Pt2 110(2) . . . . ?
N7 O3 Pt1 O2 -17.3(18) . . . . ?
N7 O3 Pt1 N3 75.8(17) . . . . ?
N7 O3 Pt1 N1 -106.8(17) . . . . ?
N7 O3 Pt1 N4 162.0(18) . . . . ?
N7 O3 Pt1 Pt2 -113(2) . . . . ?
C6 N2 Pt2 O1 89.9(18) . . . . ?
C6 N2 Pt2 N5 -99.9(18) . . . . ?
C6 N2 Pt2 O6 179.0(18) . . . . ?
C6 N2 Pt2 Pt1 3.6(17) . . . . ?
C1 O1 Pt2 N2 -78.9(16) . . . . ?
C1 O1 Pt2 N6 106.0(16) . . . . ?
C1 O1 Pt2 O6 -161.0(16) . . . . ?
C1 O1 Pt2 Pt1 5.3(16) . . . . ?
C17 N5 Pt2 N2 171.4(18) . . . . ?
C17' N5 Pt2 N2 -150(2) . . . . ?
C17 N5 Pt2 N6 -12.9(18) . . . . ?
C17' N5 Pt2 N6 25(2) . . . . ?
C17 N5 Pt2 O6 -106.8(18) . . . . ?
C17' N5 Pt2 O6 -68(2) . . . . ?
C17 N5 Pt2 Pt1 87.1(17) . . . . ?
C17' N5 Pt2 Pt1 125(2) . . . . ?
C18' N6 Pt2 O1 165(3) . . . . ?
C18 N6 Pt2 O1 173.2(17) . . . . ?
C18' N6 Pt2 N5 -5(3) . . . . ?
C18 N6 Pt2 N5 2.9(17) . . . . ?
C18' N6 Pt2 O6 76(3) . . . . ?
C18 N6 Pt2 O6 83.8(18) . . . . ?
C18' N6 Pt2 Pt1 -108(3) . . . . ?
C18 N6 Pt2 Pt1 -100.0(17) . . . . ?
N8 O6 Pt2 N2 -132.7(15) . . . . ?
N8 O6 Pt2 O1 -42.5(15) . . . . ?
N8 O6 Pt2 N5 135.4(15) . . . . ?
N8 O6 Pt2 N6 50.8(16) . . . . ?
N8 O6 Pt2 Pt1 -114.0(18) . . . . ?
O2 Pt1 Pt2 N2 -3.4(6) . . . . ?
N3 Pt1 Pt2 N2 -95.5(6) . . . . ?
N1 Pt1 Pt2 N2 87.3(6) . . . . ?
N4 Pt1 Pt2 N2 176.0(7) . . . . ?
O3 Pt1 Pt2 N2 93(2) . . . . ?
O2 Pt1 Pt2 O1 -93.8(6) . . . . ?
N3 Pt1 Pt2 O1 174.0(6) . . . . ?
N1 Pt1 Pt2 O1 -3.2(6) . . . . ?
N4 Pt1 Pt2 O1 85.6(7) . . . . ?
O3 Pt1 Pt2 O1 3(2) . . . . ?
O2 Pt1 Pt2 N5 85.9(6) . . . . ?
N3 Pt1 Pt2 N5 -6.2(6) . . . . ?
N1 Pt1 Pt2 N5 176.6(6) . . . . ?
N4 Pt1 Pt2 N5 -94.7(7) . . . . ?
O3 Pt1 Pt2 N5 -177(2) . . . . ?
O2 Pt1 Pt2 N6 173.5(6) . . . . ?
N3 Pt1 Pt2 N6 81.4(7) . . . . ?
N1 Pt1 Pt2 N6 -95.8(7) . . . . ?
N4 Pt1 Pt2 N6 -7.0(7) . . . . ?
O3 Pt1 Pt2 N6 -90(2) . . . . ?
O2 Pt1 Pt2 O6 -21.9(17) . . . . ?
N3 Pt1 Pt2 O6 -114.1(17) . . . . ?
N1 Pt1 Pt2 O6 68.7(17) . . . . ?
N4 Pt1 Pt2 O6 157.5(18) . . . . ?
O3 Pt1 Pt2 O6 75(3) . . . . ?
