#------------------------------------------------------------------------------
#$Date: 2016-03-25 11:04:14 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179774 $
#$URL: svn://www.crystallography.net/cod/cif/7/00/70/7007033.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7007033
loop_
_publ_author_name
'Kitadai, Kunihiko'
'Takahashi, Masashi'
'Takeda, Masuo'
'Bhargava, Suresh K.'
'Privér, Steven H'
'Bennett, Martin A.'
_publ_section_title
;
 Synthesis, structures and reactions of cyclometallated gold complexes
 containing (2-diphenylarsino-n-methyl)phenyl (n = 5, 6).
;
_journal_issue                   21
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              2560
_journal_page_last               2571
_journal_paper_doi               10.1039/b516538e
_journal_year                    2006
_chemical_formula_sum            'C50 H32 As2 Au2 F10'
_chemical_formula_weight         1366.53
_chemical_name_systematic
;
?
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 95.7420(10)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   13.7505(8)
_cell_length_b                   21.7158(12)
_cell_length_c                   14.9318(8)
_cell_measurement_temperature    293(2)
_cell_volume                     4436.3(4)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0498
_diffrn_reflns_av_sigmaI/netI    0.0561
_diffrn_reflns_limit_h_max       18
_diffrn_reflns_limit_h_min       -17
_diffrn_reflns_limit_k_max       27
_diffrn_reflns_limit_k_min       -28
_diffrn_reflns_limit_l_max       19
_diffrn_reflns_limit_l_min       -12
_diffrn_reflns_number            32838
_diffrn_reflns_theta_full        28.30
_diffrn_reflns_theta_max         28.30
_diffrn_reflns_theta_min         1.49
_exptl_absorpt_coefficient_mu    8.164
_exptl_absorpt_correction_type   empirical
_exptl_absorpt_process_details   'SADABS Sheldrick 1996'
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    2.046
_exptl_crystal_density_meas      0
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             2584
_exptl_crystal_size_max          0.27
_exptl_crystal_size_mid          0.25
_exptl_crystal_size_min          0.23
_refine_diff_density_max         1.653
_refine_diff_density_min         -0.901
_refine_diff_density_rms         0.141
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.959
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     578
_refine_ls_number_reflns         11013
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      0.959
_refine_ls_R_factor_all          0.0598
_refine_ls_R_factor_gt           0.0374
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0415P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0821
_refine_ls_wR_factor_ref         0.0911
_reflns_number_gt                7802
_reflns_number_total             11013
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b516538e.txt
_cod_data_source_block           compound6
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      P2(1)/c
_cod_database_code               7007033
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
As1 As 0.21549(4) 0.41412(3) 0.67105(3) 0.04217(13) Uani 1 1 d . . .
As2 As 0.20304(4) 0.58297(2) 0.88820(3) 0.04055(13) Uani 1 1 d . . .
Au1 Au 0.279942(14) 0.445810(9) 0.820827(13) 0.03568(6) Uani 1 1 d . . .
Au2 Au 0.254192(14) 0.554525(9) 0.743927(13) 0.03646(6) Uani 1 1 d . . .
C1 C 0.3223(3) 0.4826(2) 0.9474(3) 0.0366(11) Uani 1 1 d . . .
C2 C 0.3856(4) 0.4505(2) 1.0111(4) 0.0447(13) Uani 1 1 d . . .
C3 C 0.4076(4) 0.4707(3) 1.0986(4) 0.0498(14) Uani 1 1 d . . .
C4 C 0.3645(5) 0.5245(3) 1.1248(4) 0.0636(17) Uani 1 1 d . . .
C5 C 0.3039(5) 0.5580(3) 1.0646(4) 0.0576(16) Uani 1 1 d . . .
C6 C 0.2824(4) 0.5370(2) 0.9771(3) 0.0420(12) Uani 1 1 d . . .
C7 C 0.4753(5) 0.4346(3) 1.1650(4) 0.073(2) Uani 1 1 d . . .
C8 C 0.2425(5) 0.3308(3) 0.6363(4) 0.0527(15) Uani 1 1 d . . .
C9 C 0.3376(5) 0.3126(3) 0.6378(4) 0.0640(17) Uani 1 1 d . . .
C10 C 0.3608(6) 0.2522(3) 0.6188(5) 0.079(2) Uani 1 1 d . . .
C11 C 0.2862(8) 0.2109(3) 0.5989(5) 0.093(3) Uani 1 1 d . . .
C12 C 0.1922(8) 0.2295(3) 0.5955(6) 0.102(3) Uani 1 1 d . . .
C13 C 0.1697(6) 0.2892(3) 0.6156(5) 0.078(2) Uani 1 1 d . . .
C14 C 0.0747(4) 0.4225(3) 0.6527(4) 0.0495(14) Uani 1 1 d . . .
C15 C 0.0230(5) 0.4205(4) 0.7262(5) 0.074(2) Uani 1 1 d . . .
C16 C -0.0784(6) 0.4273(4) 0.7162(6) 0.090(2) Uani 1 1 d . . .
C17 C -0.1249(6) 0.4365(3) 0.6350(7) 0.084(2) Uani 1 1 d . . .
C18 C -0.0755(7) 0.4384(4) 0.5609(6) 0.089(3) Uani 1 1 d . . .
C19 C 0.0251(6) 0.4308(4) 0.5692(5) 0.079(2) Uani 1 1 d . . .
C20 C 0.2743(4) 0.4665(2) 0.5892(3) 0.0424(12) Uani 1 1 d . . .
C21 C 0.2975(5) 0.4477(3) 0.5045(4) 0.0555(16) Uani 1 1 d . . .
C22 C 0.3492(5) 0.4867(3) 0.4552(4) 0.0598(16) Uani 1 1 d . . .
C23 C 0.3800(4) 0.5434(3) 0.4862(4) 0.0540(15) Uani 1 1 d . . .
C24 C 0.3541(4) 0.5618(3) 0.5698(4) 0.0457(13) Uani 1 1 d . . .
C25 C 0.3007(4) 0.5243(2) 0.6232(3) 0.0405(12) Uani 1 1 d . . .
C26 C 0.4395(5) 0.5845(3) 0.4304(4) 0.0716(19) Uani 1 1 d . . .
C27 C 0.2188(4) 0.6695(3) 0.9173(3) 0.0445(12) Uani 1 1 d . . .
C28 C 0.3082(5) 0.6933(3) 0.9520(4) 0.0574(15) Uani 1 1 d . . .
C29 C 0.3188(6) 0.7557(3) 0.9661(4) 0.0707(19) Uani 1 1 d . . .
C30 C 0.2423(6) 0.7941(3) 0.9457(5) 0.0691(19) Uani 1 1 d . . .
C31 C 0.1536(5) 0.7710(3) 0.9109(4) 0.0658(18) Uani 1 1 d . . .
C32 C 0.1417(5) 0.7089(3) 0.8982(4) 0.0563(15) Uani 1 1 d . . .
C33 C 0.0662(4) 0.5712(2) 0.9005(4) 0.0438(13) Uani 1 1 d . . .
C34 C 0.0302(5) 0.5776(3) 0.9830(4) 0.0631(17) Uani 1 1 d . . .
C35 C -0.0697(6) 0.5750(3) 0.9885(6) 0.077(2) Uani 1 1 d . . .
C36 C -0.1310(5) 0.5670(3) 0.9132(6) 0.076(2) Uani 1 1 d . . .
C37 C -0.0959(6) 0.5607(4) 0.8321(6) 0.083(2) Uani 1 1 d . . .
C38 C 0.0036(5) 0.5632(3) 0.8258(5) 0.0684(19) Uani 1 1 d . . .
C39 C 0.3076(4) 0.3525(2) 0.8578(3) 0.0425(12) Uani 1 1 d . . .
C40 C 0.2360(4) 0.3085(3) 0.8634(4) 0.0533(14) Uani 1 1 d . . .
C41 C 0.2545(6) 0.2464(3) 0.8697(5) 0.0699(19) Uani 1 1 d . . .
C42 C 0.3471(6) 0.2258(3) 0.8719(5) 0.071(2) Uani 1 1 d . . .
C43 C 0.4214(5) 0.2668(3) 0.8673(4) 0.0662(18) Uani 1 1 d . . .
C44 C 0.4008(4) 0.3281(3) 0.8605(4) 0.0525(14) Uani 1 1 d . . .
C45 C 0.2284(5) 0.6444(3) 0.6972(4) 0.0528(15) Uani 1 1 d . . .
C46 C 0.2917(6) 0.6916(3) 0.7184(4) 0.0615(17) Uani 1 1 d . . .
C47 C 0.2696(8) 0.7531(4) 0.7008(6) 0.087(3) Uani 1 1 d . . .
C48 C 0.1789(9) 0.7663(4) 0.6600(7) 0.102(4) Uani 1 1 d . . .
C49 C 0.1126(7) 0.7228(5) 0.6362(6) 0.102(3) Uani 1 1 d . . .
C50 C 0.1376(6) 0.6623(3) 0.6553(4) 0.0676(19) Uani 1 1 d . . .
F1 F 0.1424(3) 0.32718(18) 0.8597(3) 0.0902(13) Uani 1 1 d . . .
F2 F 0.1811(4) 0.20660(19) 0.8718(4) 0.125(2) Uani 1 1 d . . .
F3 F 0.3664(4) 0.16560(17) 0.8773(3) 0.1124(17) Uani 1 1 d . . .
F4 F 0.5136(3) 0.2454(2) 0.8698(3) 0.1071(16) Uani 1 1 d . . .
F5 F 0.4768(3) 0.36641(18) 0.8518(3) 0.0833(12) Uani 1 1 d . . .
F6 F 0.3810(3) 0.67898(18) 0.7594(3) 0.0845(12) Uani 1 1 d . . .
F7 F 0.3324(5) 0.7980(2) 0.7256(4) 0.142(2) Uani 1 1 d . . .
F8 F 0.1551(5) 0.8264(2) 0.6423(4) 0.172(3) Uani 1 1 d . . .
F9 F 0.0243(4) 0.7362(3) 0.5937(4) 0.162(3) Uani 1 1 d . . .
F10 F 0.0690(3) 0.6189(3) 0.6331(3) 0.1024(15) Uani 1 1 d . . .
H2 H 0.4138 0.4141 0.9935 0.054 Uiso 1 1 calc R . .
H4 H 0.3767 0.5381 1.1839 0.076 Uiso 1 1 calc R . .
H5 H 0.2772 0.5948 1.0825 0.069 Uiso 1 1 calc R . .
H7A H 0.5294 0.4601 1.1872 0.109 Uiso 1 1 calc R . .
H7B H 0.4989 0.3991 1.1357 0.109 Uiso 1 1 calc R . .
H7C H 0.4404 0.4217 1.2143 0.109 Uiso 1 1 calc R . .
H9 H 0.3874 0.3410 0.6518 0.077 Uiso 1 1 calc R . .
H10 H 0.4256 0.2400 0.6195 0.095 Uiso 1 1 calc R . .
H11 H 0.3004 0.1699 0.5876 0.112 Uiso 1 1 calc R . .
H12 H 0.1422 0.2015 0.5795 0.123 Uiso 1 1 calc R . .
H13 H 0.1047 0.3012 0.6150 0.094 Uiso 1 1 calc R . .
H15 H 0.0556 0.4146 0.7831 0.089 Uiso 1 1 calc R . .
H16 H -0.1134 0.4253 0.7663 0.107 Uiso 1 1 calc R . .
H17 H -0.1924 0.4418 0.6289 0.101 Uiso 1 1 calc R . .
H18 H -0.1091 0.4447 0.5045 0.107 Uiso 1 1 calc R . .
H19 H 0.0588 0.4315 0.5182 0.095 Uiso 1 1 calc R . .
H21 H 0.2781 0.4092 0.4820 0.067 Uiso 1 1 calc R . .
H22 H 0.3639 0.4742 0.3985 0.072 Uiso 1 1 calc R . .
H24 H 0.3731 0.6007 0.5911 0.055 Uiso 1 1 calc R . .
H26A H 0.4872 0.5602 0.4037 0.107 Uiso 1 1 calc R . .
H26B H 0.4720 0.6155 0.4683 0.107 Uiso 1 1 calc R . .
H26C H 0.3969 0.6039 0.3839 0.107 Uiso 1 1 calc R . .
H28 H 0.3611 0.6671 0.9657 0.069 Uiso 1 1 calc R . .
H29 H 0.3788 0.7715 0.9896 0.085 Uiso 1 1 calc R . .
H30 H 0.2498 0.8363 0.9554 0.083 Uiso 1 1 calc R . .
H31 H 0.1014 0.7976 0.8959 0.079 Uiso 1 1 calc R . .
H32 H 0.0809 0.6933 0.8764 0.068 Uiso 1 1 calc R . .
H34 H 0.0728 0.5836 1.0347 0.076 Uiso 1 1 calc R . .
H35 H -0.0944 0.5788 1.0440 0.092 Uiso 1 1 calc R . .
H36 H -0.1981 0.5658 0.9169 0.091 Uiso 1 1 calc R . .
H37 H -0.1388 0.5547 0.7807 0.100 Uiso 1 1 calc R . .
H38 H 0.0276 0.5592 0.7700 0.082 Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
As As 0.0499 2.0058 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Au Au -2.0133 8.8022 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
As1 Au1 Au2 80.285(15) . . ?
As2 Au2 Au1 83.031(15) . . ?
C1 Au1 As1 172.43(14) . . ?
C1 Au1 Au2 93.70(13) . . ?
C1 Au1 C39 95.98(19) . . ?
C1 C6 As2 115.9(4) . . ?
C2 C1 Au1 121.4(4) . . ?
C2 C3 C7 121.2(6) . . ?
C3 C2 C1 122.9(5) . . ?
C4 C3 C2 118.3(5) . . ?
C4 C3 C7 120.5(5) . . ?
C4 C5 C6 120.1(6) . . ?
C5 C4 C3 120.8(5) . . ?
C5 C6 As2 122.3(4) . . ?
C5 C6 C1 121.7(5) . . ?
C6 As2 Au2 106.78(16) . . ?
C6 As2 C27 107.9(2) . . ?
C6 As2 C33 111.1(2) . . ?
C6 C1 Au1 122.1(4) . . ?
C6 C1 C2 116.2(5) . . ?
C8 As1 Au1 116.92(18) . . ?
C8 As1 C14 105.5(3) . . ?
C8 C9 C10 120.8(7) . . ?
C8 C13 C12 119.9(8) . . ?
C9 C8 As1 118.5(5) . . ?
C11 C10 C9 118.7(7) . . ?
C11 C12 C13 120.7(8) . . ?
C12 C11 C10 120.3(7) . . ?
C13 C8 As1 121.8(5) . . ?
C13 C8 C9 119.6(6) . . ?
C14 As1 Au1 111.85(17) . . ?
C14 C15 C16 120.4(7) . . ?
C14 C19 C18 119.8(7) . . ?
C15 C14 As1 118.5(5) . . ?
C15 C14 C19 118.8(6) . . ?
C16 C17 C18 120.9(8) . . ?
C17 C16 C15 119.9(8) . . ?
C17 C18 C19 120.1(8) . . ?
C19 C14 As1 122.7(5) . . ?
C20 As1 Au1 106.43(16) . . ?
C20 As1 C8 106.4(2) . . ?
C20 As1 C14 109.6(2) . . ?
C20 C25 Au2 120.7(4) . . ?
C20 C25 C24 116.8(5) . . ?
C21 C20 As1 123.8(4) . . ?
C21 C22 C23 122.4(6) . . ?
C22 C21 C20 119.0(5) . . ?
C22 C23 C24 117.6(6) . . ?
C22 C23 C26 120.7(6) . . ?
C23 C24 C25 122.8(5) . . ?
C24 C23 C26 121.7(6) . . ?
C24 C25 Au2 122.4(4) . . ?
C25 Au2 As2 176.20(14) . . ?
C25 Au2 Au1 93.19(14) . . ?
C25 Au2 C45 93.5(2) . . ?
C25 C20 As1 114.7(4) . . ?
C25 C20 C21 121.3(5) . . ?
C27 As2 Au2 114.39(15) . . ?
C27 C32 C31 120.4(6) . . ?
C28 C27 As2 121.4(4) . . ?
C29 C28 C27 120.0(6) . . ?
C29 C30 C31 120.0(6) . . ?
C30 C29 C28 120.3(7) . . ?
C32 C27 As2 119.5(4) . . ?
C32 C27 C28 119.0(5) . . ?
C32 C31 C30 120.1(7) . . ?
C33 As2 Au2 115.23(16) . . ?
C33 As2 C27 101.3(2) . . ?
C33 C34 C35 119.6(7) . . ?
C33 C38 C37 120.1(7) . . ?
C34 C33 As2 120.8(5) . . ?
C35 C36 C37 120.6(7) . . ?
C36 C35 C34 119.8(6) . . ?
C36 C37 C38 120.1(7) . . ?
C38 C33 As2 119.1(4) . . ?
C38 C33 C34 119.7(6) . . ?
C39 Au1 As1 90.48(14) . . ?
C39 Au1 Au2 168.83(14) . . ?
C40 C39 Au1 124.5(4) . . ?
C40 C39 C44 113.4(5) . . ?
C41 C40 C39 123.8(6) . . ?
C41 C42 C43 119.6(6) . . ?
C42 C41 C40 119.7(7) . . ?
C42 C43 C44 119.4(6) . . ?
C43 C44 C39 124.1(6) . . ?
C44 C39 Au1 120.9(4) . . ?
C45 Au2 As2 90.24(15) . . ?
C45 Au2 Au1 173.27(15) . . ?
C45 C46 C47 123.9(8) . . ?
C46 C45 Au2 122.9(5) . . ?
C46 C45 C50 114.6(6) . . ?
C47 C48 F8 118.6(11) . . ?
C48 C47 C46 117.4(9) . . ?
C48 C49 C50 117.9(9) . . ?
C48 C49 F9 122.2(10) . . ?
C49 C48 C47 122.7(8) . . ?
C49 C48 F8 118.7(11) . . ?
C49 C50 C45 123.5(9) . . ?
C50 C45 Au2 121.6(5) . . ?
F1 C40 C39 118.2(5) . . ?
F1 C40 C41 118.0(6) . . ?
F2 C41 C40 120.2(7) . . ?
F2 C41 C42 120.1(6) . . ?
F3 C42 C41 120.5(7) . . ?
F3 C42 C43 119.8(7) . . ?
F4 C43 C42 118.9(6) . . ?
F4 C43 C44 121.8(7) . . ?
F5 C44 C39 119.0(5) . . ?
F5 C44 C43 116.8(6) . . ?
F6 C46 C45 119.0(6) . . ?
F6 C46 C47 117.1(7) . . ?
F7 C47 C46 121.9(9) . . ?
F7 C47 C48 120.7(8) . . ?
F9 C49 C50 119.9(11) . . ?
F10 C50 C45 119.2(6) . . ?
F10 C50 C49 117.3(8) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
As1 C8 1.929(6) . ?
As1 C14 1.936(6) . ?
As1 C20 1.907(5) . ?
As2 C6 1.914(5) . ?
As2 C27 1.937(5) . ?
As2 C33 1.926(6) . ?
Au1 As1 2.4216(6) . ?
Au1 Au2 2.6336(3) . ?
Au1 C1 2.081(5) . ?
Au1 C39 2.124(5) . ?
Au2 As2 2.4125(6) . ?
Au2 C25 2.078(5) . ?
Au2 C45 2.090(6) . ?
C1 C2 1.408(7) . ?
C1 C6 1.392(7) . ?
C2 C3 1.383(7) . ?
C3 C7 1.509(8) . ?
C4 C3 1.383(9) . ?
C4 C5 1.371(8) . ?
C6 C5 1.388(7) . ?
C8 C13 1.361(9) . ?
C9 C8 1.364(9) . ?
C9 C10 1.385(8) . ?
C11 C10 1.373(11) . ?
C12 C11 1.349(11) . ?
C13 C12 1.373(10) . ?
C14 C15 1.366(8) . ?
C14 C19 1.374(8) . ?
C15 C16 1.396(9) . ?
C17 C16 1.328(11) . ?
C18 C17 1.356(12) . ?
C18 C19 1.386(11) . ?
C21 C20 1.397(7) . ?
C21 C22 1.368(8) . ?
C23 C22 1.370(8) . ?
C23 C24 1.391(8) . ?
C23 C26 1.515(8) . ?
C25 C20 1.390(7) . ?
C25 C24 1.398(7) . ?
C27 C28 1.385(8) . ?
C27 C32 1.369(8) . ?
C28 C29 1.377(8) . ?
C30 C29 1.354(9) . ?
C30 C31 1.373(9) . ?
C32 C31 1.370(8) . ?
C33 C34 1.379(8) . ?
C33 C38 1.350(8) . ?
C34 C35 1.386(10) . ?
C36 C35 1.347(11) . ?
C36 C37 1.355(10) . ?
C38 C37 1.382(9) . ?
C39 C40 1.381(7) . ?
C39 C44 1.385(8) . ?
C40 C41 1.373(8) . ?
C42 C41 1.347(10) . ?
C43 C42 1.362(10) . ?
C44 C43 1.364(8) . ?
C45 C46 1.362(9) . ?
C45 C50 1.395(9) . ?
C46 C47 1.388(9) . ?
C47 C48 1.363(13) . ?
C48 F8 1.366(8) . ?
C49 C48 1.336(13) . ?
C49 C50 1.381(10) . ?
C49 F9 1.344(10) . ?
C50 F10 1.350(8) . ?
F1 C40 1.346(7) . ?
F2 C41 1.332(8) . ?
F3 C42 1.335(7) . ?
F4 C43 1.346(7) . ?
F5 C44 1.352(7) . ?
F6 C46 1.345(8) . ?
F7 C47 1.331(10) . ?
