#------------------------------------------------------------------------------
#$Date: 2016-03-25 11:04:14 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179774 $
#$URL: svn://www.crystallography.net/cod/cif/7/00/70/7007034.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7007034
loop_
_publ_author_name
'Kitadai, Kunihiko'
'Takahashi, Masashi'
'Takeda, Masuo'
'Bhargava, Suresh K.'
'Privér, Steven H'
'Bennett, Martin A.'
_publ_section_title
;
 Synthesis, structures and reactions of cyclometallated gold complexes
 containing (2-diphenylarsino-n-methyl)phenyl (n = 5, 6).
;
_journal_issue                   21
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              2560
_journal_page_last               2571
_journal_paper_doi               10.1039/b516538e
_journal_year                    2006
_chemical_formula_sum            'C50 H32 As2 Au2 F10'
_chemical_formula_weight         1366.53
_chemical_name_systematic
;
?
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 97.678(2)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   12.0980(9)
_cell_length_b                   20.5775(16)
_cell_length_c                   18.6526(15)
_cell_measurement_temperature    293(2)
_cell_volume                     4601.9(6)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.994
_diffrn_measured_fraction_theta_max 0.994
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0432
_diffrn_reflns_av_sigmaI/netI    0.0514
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       -16
_diffrn_reflns_limit_k_max       27
_diffrn_reflns_limit_k_min       -24
_diffrn_reflns_limit_l_max       21
_diffrn_reflns_limit_l_min       -24
_diffrn_reflns_number            33783
_diffrn_reflns_theta_full        28.35
_diffrn_reflns_theta_max         28.35
_diffrn_reflns_theta_min         1.48
_exptl_absorpt_coefficient_mu    7.871
_exptl_absorpt_correction_type   empirical
_exptl_absorpt_process_details   'SADABS Sheldrick 1996'
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.972
_exptl_crystal_density_meas      0
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             2584
_exptl_crystal_size_max          0.40
_exptl_crystal_size_mid          0.26
_exptl_crystal_size_min          0.22
_refine_diff_density_max         1.963
_refine_diff_density_min         -1.093
_refine_diff_density_rms         0.122
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.975
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     579
_refine_ls_number_reflns         11431
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      0.975
_refine_ls_R_factor_all          0.0685
_refine_ls_R_factor_gt           0.0405
_refine_ls_shift/su_max          0.130
_refine_ls_shift/su_mean         0.002
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0583P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0954
_refine_ls_wR_factor_ref         0.1093
_reflns_number_gt                7707
_reflns_number_total             11431
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b516538e.txt
_cod_data_source_block           compound7
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      P2(1)/c
_cod_database_code               7007034
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
As1 As 0.51908(4) 0.35705(2) 0.27579(3) 0.04987(13) Uani 1 1 d . . .
As2 As 0.23746(4) 0.38600(3) 0.08485(3) 0.05805(14) Uani 1 1 d . . .
Au1 Au 0.387711(18) 0.272484(10) 0.243518(12) 0.05692(8) Uani 1 1 d . . .
Au2 Au 0.209750(18) 0.424177(12) 0.201314(14) 0.06787(9) Uani 1 1 d . . .
C1 C 0.2846(4) 0.1941(2) 0.2259(3) 0.0560(12) Uani 1 1 d . . .
C2 C 0.3033(5) 0.1461(3) 0.1788(3) 0.0645(14) Uani 1 1 d . . .
C3 C 0.2391(6) 0.0920(3) 0.1678(4) 0.0748(17) Uani 1 1 d . . .
C4 C 0.1541(6) 0.0816(3) 0.2060(5) 0.084(2) Uani 1 1 d . . .
C5 C 0.1317(5) 0.1285(3) 0.2557(4) 0.0799(19) Uani 1 1 d . . .
C6 C 0.1978(5) 0.1824(3) 0.2644(4) 0.0697(16) Uani 1 1 d . . .
C7 C 0.5148(4) 0.3811(2) 0.3759(3) 0.0534(12) Uani 1 1 d . . .
C8 C 0.4135(5) 0.3782(3) 0.4011(3) 0.0663(15) Uani 1 1 d . . .
C9 C 0.4029(7) 0.3961(3) 0.4702(4) 0.086(2) Uani 1 1 d . . .
C10 C 0.4932(7) 0.4170(3) 0.5154(4) 0.083(2) Uani 1 1 d . . .
C11 C 0.5943(7) 0.4198(3) 0.4914(4) 0.090(2) Uani 1 1 d . . .
C12 C 0.6063(6) 0.4012(3) 0.4215(3) 0.0745(16) Uani 1 1 d . . .
C13 C 0.6727(4) 0.3332(2) 0.2718(3) 0.0537(12) Uani 1 1 d . . .
C14 C 0.7000(6) 0.2690(3) 0.2664(4) 0.0743(17) Uani 1 1 d . . .
C15 C 0.8096(7) 0.2512(4) 0.2645(4) 0.093(2) Uani 1 1 d . . .
C16 C 0.8912(6) 0.2973(4) 0.2671(4) 0.091(2) Uani 1 1 d . . .
C17 C 0.8635(5) 0.3607(4) 0.2721(4) 0.0842(19) Uani 1 1 d . . .
C18 C 0.7556(5) 0.3800(3) 0.2739(3) 0.0654(14) Uani 1 1 d . . .
C19 C 0.4980(4) 0.4388(2) 0.2238(3) 0.0469(11) Uani 1 1 d . . .
C20 C 0.4983(4) 0.4965(3) 0.2623(3) 0.0558(12) Uani 1 1 d . . .
C21 C 0.4763(5) 0.5551(3) 0.2259(3) 0.0661(15) Uani 1 1 d . . .
C22 C 0.4550(5) 0.5569(3) 0.1512(3) 0.0650(15) Uani 1 1 d . . .
C23 C 0.4564(5) 0.4991(2) 0.1141(3) 0.0584(13) Uani 1 1 d . . .
C24 C 0.4771(4) 0.4393(2) 0.1494(3) 0.0456(10) Uani 1 1 d . . .
C25 C 0.4300(7) 0.6199(3) 0.1113(4) 0.102(3) Uani 1 1 d . . .
C26 C 0.4787(4) 0.3785(2) 0.1057(2) 0.0464(10) Uani 1 1 d . . .
C27 C 0.5805(4) 0.3507(2) 0.0976(3) 0.0550(12) Uani 1 1 d . . .
C28 C 0.5881(5) 0.2942(2) 0.0568(3) 0.0578(13) Uani 1 1 d . . .
C29 C 0.4904(6) 0.2666(3) 0.0250(4) 0.0696(16) Uani 1 1 d . . .
C30 C 0.3889(5) 0.2928(3) 0.0319(3) 0.0613(14) Uani 1 1 d . . .
C31 C 0.3811(4) 0.3486(2) 0.0727(3) 0.0497(11) Uani 1 1 d . . .
C32 C 0.7004(6) 0.2664(3) 0.0485(4) 0.093(2) Uani 1 1 d . . .
C33 C 0.1306(4) 0.3192(3) 0.0506(3) 0.0593(13) Uani 1 1 d . . .
C34 C 0.0954(6) 0.3103(4) -0.0209(4) 0.096(2) Uani 1 1 d . . .
C35 C 0.0185(7) 0.2593(5) -0.0418(5) 0.114(3) Uani 1 1 d . . .
C36 C -0.0205(6) 0.2236(4) 0.0092(5) 0.093(2) Uani 1 1 d . . .
C37 C 0.0139(6) 0.2331(4) 0.0807(5) 0.102(3) Uani 1 1 d . . .
C38 C 0.0889(5) 0.2818(3) 0.1022(4) 0.0800(18) Uani 1 1 d . . .
C39 C 0.2137(5) 0.4539(3) 0.0125(4) 0.0757(18) Uani 1 1 d . . .
C40 C 0.1514(6) 0.5066(4) 0.0256(5) 0.103(3) Uani 1 1 d . . .
C41 C 0.1257(8) 0.5558(5) -0.0244(8) 0.142(5) Uani 1 1 d . . .
C42 C 0.1668(9) 0.5470(7) -0.0910(8) 0.151(5) Uani 1 1 d . . .
C43 C 0.2320(9) 0.4964(5) -0.1047(5) 0.123(3) Uani 1 1 d . . .
C44 C 0.2544(6) 0.4488(4) -0.0531(4) 0.095(2) Uani 1 1 d . . .
C45 C 0.1752(4) 0.4649(3) 0.2960(4) 0.0656(15) Uani 1 1 d . . .
C46 C 0.1457(5) 0.4292(3) 0.3526(4) 0.0741(18) Uani 1 1 d . . .
C47 C 0.1251(5) 0.4563(4) 0.4168(4) 0.0827(19) Uani 1 1 d . . .
C48 C 0.1307(6) 0.5221(4) 0.4241(5) 0.094(2) Uani 1 1 d . . .
C49 C 0.1592(6) 0.5597(4) 0.3697(5) 0.086(2) Uani 1 1 d . . .
C50 C 0.1805(5) 0.5299(3) 0.3065(4) 0.0775(18) Uani 1 1 d . . .
F1 F 0.3870(4) 0.15266(19) 0.1383(2) 0.0985(13) Uani 1 1 d . . .
F2 F 0.2624(4) 0.0449(2) 0.1204(3) 0.1135(15) Uani 1 1 d . . .
F3 F 0.0932(4) 0.02692(19) 0.2000(3) 0.1169(16) Uani 1 1 d . . .
F4 F 0.0469(4) 0.1202(3) 0.2946(3) 0.1288(18) Uani 1 1 d . . .
F5 F 0.1723(4) 0.22603(19) 0.3135(3) 0.1055(15) Uani 1 1 d . . .
F6 F 0.1381(3) 0.36375(18) 0.3484(3) 0.0953(12) Uani 1 1 d . . .
F7 F 0.0993(4) 0.4194(3) 0.4712(3) 0.1236(17) Uani 1 1 d . . .
F8 F 0.1127(4) 0.5496(3) 0.4872(3) 0.139(2) Uani 1 1 d . . .
F9 F 0.1670(4) 0.6239(2) 0.3774(3) 0.1263(18) Uani 1 1 d . . .
F10 F 0.2077(4) 0.56984(19) 0.2539(3) 0.1082(14) Uani 1 1 d . . .
H8 H 0.3511 0.3639 0.3706 0.080 Uiso 1 1 calc R . .
H9 H 0.3335 0.3940 0.4864 0.103 Uiso 1 1 calc R . .
H10 H 0.4858 0.4294 0.5625 0.100 Uiso 1 1 calc R . .
H11 H 0.6562 0.4342 0.5223 0.108 Uiso 1 1 calc R . .
H12 H 0.6760 0.4024 0.4057 0.089 Uiso 1 1 calc R . .
H14 H 0.6447 0.2374 0.2639 0.089 Uiso 1 1 calc R . .
H15 H 0.8280 0.2075 0.2615 0.112 Uiso 1 1 calc R . .
H16 H 0.9650 0.2853 0.2655 0.109 Uiso 1 1 calc R . .
H17 H 0.9193 0.3920 0.2744 0.101 Uiso 1 1 calc R . .
H18 H 0.7381 0.4238 0.2766 0.078 Uiso 1 1 calc R . .
H20 H 0.5133 0.4960 0.3125 0.067 Uiso 1 1 calc R . .
H21 H 0.4759 0.5935 0.2522 0.079 Uiso 1 1 calc R . .
H23 H 0.4432 0.4998 0.0638 0.070 Uiso 1 1 calc R . .
H25A H 0.4961 0.6352 0.0934 0.154 Uiso 1 1 calc R . .
H25B H 0.4057 0.6516 0.1435 0.154 Uiso 1 1 calc R . .
H25C H 0.3722 0.6130 0.0714 0.154 Uiso 1 1 calc R . .
H27 H 0.6456 0.3701 0.1199 0.066 Uiso 1 1 calc R . .
H29 H 0.4936 0.2288 -0.0020 0.084 Uiso 1 1 calc R . .
H30 H 0.3244 0.2731 0.0091 0.074 Uiso 1 1 calc R . .
H32A H 0.7110 0.2265 0.0751 0.139 Uiso 1 1 calc R . .
H32B H 0.7575 0.2968 0.0669 0.139 Uiso 1 1 calc R . .
H32C H 0.7046 0.2582 -0.0017 0.139 Uiso 1 1 calc R . .
H34 H 0.1211 0.3369 -0.0554 0.116 Uiso 1 1 calc R . .
H35 H -0.0045 0.2509 -0.0905 0.136 Uiso 1 1 calc R . .
H36 H -0.0728 0.1912 -0.0047 0.111 Uiso 1 1 calc R . .
H37 H -0.0130 0.2068 0.1150 0.123 Uiso 1 1 calc R . .
H38 H 0.1113 0.2895 0.1511 0.096 Uiso 1 1 calc R . .
H40 H 0.1249 0.5096 0.0700 0.124 Uiso 1 1 calc R . .
H41 H 0.0843 0.5921 -0.0147 0.170 Uiso 1 1 calc R . .
H42 H 0.1481 0.5775 -0.1273 0.181 Uiso 1 1 calc R . .
H43 H 0.2613 0.4939 -0.1483 0.148 Uiso 1 1 calc R . .
H44 H 0.2971 0.4130 -0.0623 0.114 Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
As As 0.0499 2.0058 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Au Au -2.0133 8.8022 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C1 Au1 As1 173.28(15) . . ?
C2 C1 Au1 121.9(4) . . ?
C2 C1 C6 114.5(5) . . ?
C2 C3 F2 121.1(6) . . ?
C3 C2 C1 123.5(6) . . ?
C3 C4 C5 118.3(6) . . ?
C4 C3 C2 120.9(6) . . ?
C4 C3 F2 117.9(6) . . ?
C5 C6 C1 124.0(6) . . ?
C6 C1 Au1 123.4(4) . . ?
C6 C5 C4 118.7(6) . . ?
C7 As1 Au1 109.11(15) . . ?
C7 As1 C19 104.0(2) . . ?
C7 C12 C11 119.5(6) . . ?
C8 C7 As1 117.3(4) . . ?
C9 C8 C7 120.9(6) . . ?
C10 C9 C8 120.3(7) . . ?
C10 C11 C12 120.7(7) . . ?
C11 C10 C9 119.5(7) . . ?
C12 C7 As1 123.6(4) . . ?
C12 C7 C8 119.0(5) . . ?
C13 As1 Au1 114.71(16) . . ?
C13 As1 C7 104.6(2) . . ?
C13 As1 C19 105.3(2) . . ?
C13 C14 C15 120.0(7) . . ?
C14 C13 As1 119.4(4) . . ?
C14 C13 C18 119.4(5) . . ?
C16 C15 C14 120.4(7) . . ?
C16 C17 C18 121.8(7) . . ?
C17 C16 C15 119.2(6) . . ?
C17 C18 C13 119.1(6) . . ?
C18 C13 As1 121.2(4) . . ?
C19 As1 Au1 117.95(14) . . ?
C19 C20 C21 120.1(5) . . ?
C19 C24 C23 118.5(4) . . ?
C19 C24 C26 122.0(4) . . ?
C20 C19 As1 119.5(4) . . ?
C21 C22 C25 121.3(6) . . ?
C22 C21 C20 120.8(5) . . ?
C22 C23 C24 122.3(5) . . ?
C23 C22 C21 118.0(5) . . ?
C23 C22 C25 120.6(6) . . ?
C23 C24 C26 119.5(4) . . ?
C24 C19 As1 120.3(3) . . ?
C24 C19 C20 120.2(4) . . ?
C26 C27 C28 121.8(5) . . ?
C26 C31 As2 119.4(3) . . ?
C27 C26 C24 118.8(4) . . ?
C27 C26 C31 118.7(4) . . ?
C27 C28 C32 119.9(6) . . ?
C29 C28 C27 117.6(5) . . ?
C29 C28 C32 122.4(5) . . ?
C29 C30 C31 120.5(5) . . ?
C30 C29 C28 122.0(5) . . ?
C30 C31 As2 121.3(4) . . ?
C30 C31 C26 119.3(5) . . ?
C31 As2 Au2 118.41(15) . . ?
C31 C26 C24 122.4(4) . . ?
C33 As2 Au2 111.54(17) . . ?
C33 As2 C31 104.4(2) . . ?
C33 As2 C39 104.6(3) . . ?
C33 C34 C35 118.6(7) . . ?
C34 C33 As2 121.9(5) . . ?
C34 C33 C38 121.0(6) . . ?
C35 C36 C37 121.9(7) . . ?
C36 C35 C34 119.3(8) . . ?
C36 C37 C38 119.8(7) . . ?
C37 C38 C33 119.4(7) . . ?
C38 C33 As2 117.1(5) . . ?
C39 As2 Au2 111.9(2) . . ?
C39 As2 C31 104.9(2) . . ?
C39 C40 C41 122.8(9) . . ?
C40 C39 As2 118.9(6) . . ?
C40 C39 C44 119.4(7) . . ?
C40 C41 C42 115.2(10) . . ?
C42 C43 C44 118.7(11) . . ?
C43 C42 C41 123.4(10) . . ?
C43 C44 C39 120.4(9) . . ?
C44 C39 As2 121.6(6) . . ?
C45 Au2 As2 173.74(18) . . ?
C45 C46 C47 123.3(6) . . ?
C45 C50 C49 123.4(7) . . ?
C45 C50 F10 120.5(6) . . ?
C46 C45 Au2 123.2(4) . . ?
C48 C47 C46 118.7(7) . . ?
C48 C49 C50 118.7(7) . . ?
C49 C48 C47 120.4(6) . . ?
C50 C45 Au2 121.2(5) . . ?
C50 C45 C46 115.6(6) . . ?
F1 C2 C1 119.4(5) . . ?
F1 C2 C3 117.1(6) . . ?
F3 C4 C3 122.7(7) . . ?
F3 C4 C5 118.9(7) . . ?
F4 C5 C4 120.2(6) . . ?
F4 C5 C6 121.2(7) . . ?
F5 C6 C1 119.9(5) . . ?
F5 C6 C5 116.0(5) . . ?
F6 C46 C45 120.8(6) . . ?
F6 C46 C47 115.9(7) . . ?
F7 C47 C46 121.2(7) . . ?
F7 C47 C48 120.1(7) . . ?
F8 C48 C47 119.5(9) . . ?
F8 C48 C49 120.0(7) . . ?
F9 C49 C48 120.5(7) . . ?
F9 C49 C50 120.9(8) . . ?
F10 C50 C49 116.0(6) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
As1 C7 1.938(5) . ?
As1 C13 1.933(5) . ?
As1 C19 1.941(5) . ?
As2 C31 1.941(5) . ?
As2 C33 1.936(5) . ?
As2 C39 1.938(6) . ?
Au1 As1 2.3792(5) . ?
Au1 C1 2.038(5) . ?
Au2 As2 2.3755(6) . ?
Au2 C45 2.048(6) . ?
C1 C2 1.361(8) . ?
C1 C6 1.371(8) . ?
C2 C3 1.356(8) . ?
C2 F1 1.350(7) . ?
C3 C4 1.344(10) . ?
C5 C4 1.390(10) . ?
C6 C5 1.363(8) . ?
C6 F5 1.347(7) . ?
C7 C8 1.372(7) . ?
C7 C12 1.367(8) . ?
C8 C9 1.363(8) . ?
C10 C9 1.358(10) . ?
C10 C11 1.359(10) . ?
C12 C11 1.385(9) . ?
C13 C14 1.369(7) . ?
C13 C18 1.386(7) . ?
C14 C15 1.380(9) . ?
C15 C16 1.366(11) . ?
C17 C16 1.353(10) . ?
C17 C18 1.370(8) . ?
C19 C20 1.387(7) . ?
C19 C24 1.378(7) . ?
C20 C21 1.392(8) . ?
C21 C22 1.384(8) . ?
C22 C25 1.506(8) . ?
C23 C22 1.378(8) . ?
C24 C23 1.402(7) . ?
C24 C26 1.494(6) . ?
C27 C26 1.384(7) . ?
C27 C28 1.399(7) . ?
C28 C29 1.373(8) . ?
C28 C32 1.501(8) . ?
C29 C30 1.363(8) . ?
C31 C26 1.400(7) . ?
C31 C30 1.388(7) . ?
C33 C34 1.356(9) . ?
C33 C38 1.380(8) . ?
C34 C35 1.422(10) . ?
C36 C35 1.338(11) . ?
C36 C37 1.357(11) . ?
C38 C37 1.375(9) . ?
C39 C40 1.360(10) . ?
C39 C44 1.383(10) . ?
C40 C41 1.383(12) . ?
C42 C41 1.411(17) . ?
C43 C42 1.351(15) . ?
C44 C43 1.375(11) . ?
C45 C50 1.352(9) . ?
C46 C45 1.373(9) . ?
C46 C47 1.373(9) . ?
C48 C47 1.362(10) . ?
C48 C49 1.356(11) . ?
C48 F8 1.350(8) . ?
C50 C49 1.385(10) . ?
C50 F10 1.353(8) . ?
F2 C3 1.367(7) . ?
F3 C4 1.342(7) . ?
F4 C5 1.345(7) . ?
F6 C46 1.351(7) . ?
F7 C47 1.339(8) . ?
F9 C49 1.331(8) . ?
