#------------------------------------------------------------------------------
#$Date: 2016-03-25 11:14:35 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179781 $
#$URL: svn://www.crystallography.net/cod/cif/7/00/77/7007775.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7007775
loop_
_publ_author_name
'Pedrido, Rosa'
'Romero, M José'
'Bermejo, Manuel R.'
'González-Noya, Ana M'
'Maneiro, Marcelino'
'Rodríguez, M Jesús'
'Zaragoza, Guillermo'
_publ_section_title
;
 Influence of the metal size in the structure of the complexes derived
 from a pentadentate [N(3)O(2)] hydrazone.
;
_journal_issue                   44
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              5304
_journal_page_last               5314
_journal_paper_doi               10.1039/b610010d
_journal_year                    2006
_chemical_formula_moiety         'C18 H17 N3 O5 PB1'
_chemical_formula_sum            'C18 H17 N3 O5 Pb'
_chemical_formula_weight         562.55
_chemical_name_systematic
;
?
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 99.856(2)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   9.4577(13)
_cell_length_b                   16.264(2)
_cell_length_c                   12.6521(18)
_cell_measurement_reflns_used    1967
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      23.27
_cell_measurement_theta_min      2.5
_cell_volume                     1917.4(4)
_computing_cell_refinement       'BRUKER SMART'
_computing_data_collection       'BRUKER SMART'
_computing_data_reduction        'BRUKER SAINT'
_computing_molecular_graphics    'Ortep-3 for Windows (Farrugia, 1997)'
_computing_publication_material  'WinGX publication routines (Farrugia, 1999)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'DIRDIF99 (Beurskens, 1999)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'Smart-CCD-1000 BRUKER'
_diffrn_measurement_method       'omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0000
_diffrn_reflns_av_sigmaI/netI    0.0425
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       20
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       16
_diffrn_reflns_limit_l_min       0
_diffrn_reflns_number            4238
_diffrn_reflns_theta_full        27.14
_diffrn_reflns_theta_max         27.14
_diffrn_reflns_theta_min         2.06
_exptl_absorpt_coefficient_mu    8.830
_exptl_absorpt_correction_T_max  1
_exptl_absorpt_correction_T_min  0.521259
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'BRUKER SADABS'
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.942
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             1072
_exptl_crystal_size_max          0.23
_exptl_crystal_size_mid          0.1
_exptl_crystal_size_min          0.05
_refine_diff_density_max         0.944
_refine_diff_density_min         -0.595
_refine_diff_density_rms         0.122
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.061
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     250
_refine_ls_number_reflns         4238
_refine_ls_number_restraints     1
_refine_ls_restrained_S_all      1.061
_refine_ls_R_factor_all          0.0564
_refine_ls_R_factor_gt           0.0324
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0289P)²+0.4249P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0638
_refine_ls_wR_factor_ref         0.0696
_reflns_number_gt                2978
_reflns_number_total             4238
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b610010d.txt
_cod_data_source_block           pbdaphs
_cod_original_sg_symbol_H-M      P21/n
_cod_database_code               7007775
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Pb1 Pb 0.10028(2) 0.096033(12) 0.345020(16) 0.04357(8) Uani 1 1 d . . .
O2 O -0.0214(4) -0.0355(2) 0.3166(3) 0.0526(10) Uani 1 1 d . . .
C7 C 0.0148(6) -0.0911(3) 0.3859(4) 0.0429(13) Uani 1 1 d . . .
N1 N 0.1213(5) -0.0852(3) 0.4708(4) 0.0451(11) Uani 1 1 d . . .
N2 N 0.1965(4) -0.0129(2) 0.4738(3) 0.0387(10) Uani 1 1 d . . .
C9 C 0.3023(5) -0.0028(3) 0.5517(4) 0.0409(12) Uani 1 1 d . . .
C10 C 0.3872(5) 0.0729(3) 0.5496(4) 0.0394(12) Uani 1 1 d . . .
N3 N 0.3391(4) 0.1288(3) 0.4737(3) 0.0387(10) Uani 1 1 d . . .
C14 C 0.4125(5) 0.1991(3) 0.4705(4) 0.0421(13) Uani 1 1 d . . .
C15 C 0.3529(7) 0.2588(4) 0.3843(5) 0.0538(15) Uani 1 1 d . . .
O3 O 0.2527(5) 0.2373(3) 0.3166(4) 0.0832(16) Uani 1 1 d . . .
C11 C 0.5142(6) 0.0866(3) 0.6234(4) 0.0472(14) Uani 1 1 d . . .
H11 H 0.5481 0.0472 0.6747 0.057 Uiso 1 1 calc R . .
C12 C 0.5865(6) 0.1583(4) 0.6188(5) 0.0590(17) Uani 1 1 d . . .
H12 H 0.6700 0.1683 0.6676 0.071 Uiso 1 1 calc R . .
C13 C 0.5363(6) 0.2164(4) 0.5417(5) 0.0528(15) Uani 1 1 d . . .
H13 H 0.5847 0.2657 0.5380 0.063 Uiso 1 1 calc R . .
C6 C -0.0675(6) -0.1694(3) 0.3787(4) 0.0467(14) Uani 1 1 d . . .
C1 C -0.0260(7) -0.2361(4) 0.4442(5) 0.0542(15) Uani 1 1 d . . .
C2 C -0.1104(7) -0.3084(4) 0.4371(6) 0.0696(19) Uani 1 1 d . . .
H2 H -0.0837 -0.3525 0.4830 0.084 Uiso 1 1 calc R . .
C3 C -0.2322(8) -0.3122(4) 0.3612(6) 0.0705(19) Uani 1 1 d . . .
H3 H -0.2885 -0.3594 0.3559 0.085 Uiso 1 1 calc R . .
C4 C -0.2723(7) -0.2484(5) 0.2936(6) 0.071(2) Uani 1 1 d . . .
H4 H -0.3545 -0.2528 0.2417 0.085 Uiso 1 1 calc R . .
C5 C -0.1913(6) -0.1764(4) 0.3012(5) 0.0593(17) Uani 1 1 d . . .
H5 H -0.2198 -0.1329 0.2547 0.071 Uiso 1 1 calc R . .
O4 O 0.2608(4) 0.0434(2) 0.2448(3) 0.0549(10) Uani 1 1 d . . .
O5 O 0.0768(5) 0.0916(3) 0.1319(3) 0.0688(12) Uani 1 1 d . . .
C17 C 0.1979(7) 0.0600(4) 0.1496(5) 0.0562(16) Uani 1 1 d . . .
C18 C 0.2756(9) 0.0400(5) 0.0591(6) 0.102(3) Uani 1 1 d . . .
H18A H 0.2094 0.0169 0.0006 0.153 Uiso 1 1 calc R . .
H18B H 0.3504 0.0009 0.0830 0.153 Uiso 1 1 calc R . .
H18C H 0.3168 0.0892 0.0356 0.153 Uiso 1 1 calc R . .
C8 C 0.3400(6) -0.0624(4) 0.6418(4) 0.0552(15) Uani 1 1 d . . .
H6A H 0.3249 -0.0372 0.7075 0.083 Uiso 1 1 calc R . .
H6B H 0.4389 -0.0780 0.6477 0.083 Uiso 1 1 calc R . .
H6C H 0.2804 -0.1103 0.6281 0.083 Uiso 1 1 calc R . .
C16 C 0.4160(8) 0.3408(4) 0.3805(5) 0.078(2) Uani 1 1 d . . .
H16A H 0.3631 0.3713 0.3217 0.117 Uiso 1 1 calc R . .
H16B H 0.5141 0.3357 0.3709 0.117 Uiso 1 1 calc R . .
H16C H 0.4121 0.3692 0.4464 0.117 Uiso 1 1 calc R . .
O1 O 0.0952(6) -0.2378(3) 0.5207(5) 0.0866(15) Uani 1 1 d D . .
H1B H 0.126(8) -0.191(2) 0.523(6) 0.104 Uiso 1 1 d D . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pb Pb -3.3944 10.1111 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O4 Pb1 O2 86.07(14) . . ?
O4 Pb1 N2 83.90(13) . . ?
O2 Pb1 N2 65.03(13) . . ?
O4 Pb1 N3 80.63(13) . . ?
O2 Pb1 N3 127.73(13) . . ?
N2 Pb1 N3 63.42(13) . . ?
O4 Pb1 O5 51.84(13) . . ?
O2 Pb1 O5 82.59(13) . . ?
O2 Pb1 O3 163.08(12) . . ?
N2 Pb1 O5 127.17(13) . . ?
N3 Pb1 O5 123.41(14) . . ?
N3 Pb1 O3 59.73(13) . . ?
O4 Pb1 C17 26.13(15) . . ?
O2 Pb1 C17 84.58(15) . . ?
N2 Pb1 C17 106.71(16) . . ?
N3 Pb1 C17 102.11(17) . . ?
O5 Pb1 C17 25.75(15) . . ?
C7 O2 Pb1 117.5(3) . . ?
O2 C7 N1 125.4(5) . . ?
O2 C7 C6 119.5(5) . . ?
N1 C7 C6 115.0(5) . . ?
C7 N1 N2 113.5(4) . . ?
C9 N2 N1 117.5(4) . . ?
C9 N2 Pb1 124.3(3) . . ?
N1 N2 Pb1 117.7(3) . . ?
N2 C9 C10 116.5(4) . . ?
N2 C9 C8 123.6(5) . . ?
C10 C9 C8 119.8(5) . . ?
N3 C10 C11 120.9(5) . . ?
N3 C10 C9 117.4(4) . . ?
C11 C10 C9 121.8(5) . . ?
C14 N3 C10 119.0(4) . . ?
C14 N3 Pb1 123.6(3) . . ?
C10 N3 Pb1 117.4(3) . . ?
N3 C14 C13 122.6(5) . . ?
N3 C14 C15 116.3(5) . . ?
C13 C14 C15 121.1(5) . . ?
O3 C15 C16 120.9(6) . . ?
O3 C15 C14 118.5(5) . . ?
C16 C15 C14 120.6(6) . . ?
C12 C11 C10 119.1(5) . . ?
C12 C11 H11 120.5 . . ?
C10 C11 H11 120.5 . . ?
C11 C12 C13 120.2(5) . . ?
C11 C12 H12 119.9 . . ?
C13 C12 H12 119.9 . . ?
C14 C13 C12 118.2(6) . . ?
C14 C13 H13 120.9 . . ?
C12 C13 H13 120.9 . . ?
C1 C6 C5 118.4(6) . . ?
C1 C6 C7 122.9(5) . . ?
C5 C6 C7 118.7(5) . . ?
O1 C1 C6 124.0(6) . . ?
O1 C1 C2 115.0(6) . . ?
C6 C1 C2 121.0(6) . . ?
C3 C2 C1 118.7(7) . . ?
C3 C2 H2 120.7 . . ?
C1 C2 H2 120.7 . . ?
C4 C3 C2 121.3(7) . . ?
C4 C3 H3 119.4 . . ?
C2 C3 H3 119.4 . . ?
C3 C4 C5 120.5(7) . . ?
C3 C4 H4 119.7 . . ?
C5 C4 H4 119.7 . . ?
C4 C5 C6 120.1(7) . . ?
C4 C5 H5 119.9 . . ?
C6 C5 H5 119.9 . . ?
C17 O4 Pb1 101.3(4) . . ?
C17 O5 Pb1 85.1(4) . . ?
O5 C17 O4 121.6(6) . . ?
O5 C17 C18 120.7(6) . . ?
O4 C17 C18 117.7(6) . . ?
O5 C17 Pb1 69.2(3) . . ?
O4 C17 Pb1 52.6(3) . . ?
C18 C17 Pb1 169.6(5) . . ?
C17 C18 H18A 109.5 . . ?
C17 C18 H18B 109.5 . . ?
H18A C18 H18B 109.5 . . ?
C17 C18 H18C 109.5 . . ?
H18A C18 H18C 109.5 . . ?
H18B C18 H18C 109.5 . . ?
C9 C8 H6A 109.5 . . ?
C9 C8 H6B 109.5 . . ?
H6A C8 H6B 109.5 . . ?
C9 C8 H6C 109.5 . . ?
H6A C8 H6C 109.5 . . ?
H6B C8 H6C 109.5 . . ?
C15 C16 H16A 109.5 . . ?
C15 C16 H16B 109.5 . . ?
H16A C16 H16B 109.5 . . ?
C15 C16 H16C 109.5 . . ?
H16A C16 H16C 109.5 . . ?
H16B C16 H16C 109.5 . . ?
C1 O1 H1B 105(6) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pb1 O4 2.303(4) . ?
Pb1 O2 2.427(4) . ?
Pb1 N2 2.473(4) . ?
Pb1 N3 2.603(4) . ?
Pb1 O5 2.668(4) . ?
Pb1 O3 2.768(4) . ?
Pb1 C17 2.844(6) . ?
O2 C7 1.265(6) . ?
C7 N1 1.344(7) . ?
C7 C6 1.488(7) . ?
N1 N2 1.372(5) . ?
N2 C9 1.288(6) . ?
C9 C10 1.473(7) . ?
C9 C8 1.492(7) . ?
C10 N3 1.344(6) . ?
C10 C11 1.407(7) . ?
N3 C14 1.341(6) . ?
C14 C13 1.378(7) . ?
C14 C15 1.497(8) . ?
C15 O3 1.215(7) . ?
C15 C16 1.465(8) . ?
C11 C12 1.358(8) . ?
C11 H11 0.9300 . ?
C12 C13 1.382(8) . ?
C12 H12 0.9300 . ?
C13 H13 0.9300 . ?
C6 C1 1.380(8) . ?
C6 C5 1.397(8) . ?
C1 O1 1.368(8) . ?
C1 C2 1.417(8) . ?
C2 C3 1.368(9) . ?
C2 H2 0.9300 . ?
C3 C4 1.356(9) . ?
C3 H3 0.9300 . ?
C4 C5 1.394(8) . ?
C4 H4 0.9300 . ?
C5 H5 0.9300 . ?
O4 C17 1.277(7) . ?
O5 C17 1.240(7) . ?
C17 C18 1.499(8) . ?
C18 H18A 0.9600 . ?
C18 H18B 0.9600 . ?
C18 H18C 0.9600 . ?
C8 H6A 0.9600 . ?
C8 H6B 0.9600 . ?
C8 H6C 0.9600 . ?
C16 H16A 0.9600 . ?
C16 H16B 0.9600 . ?
C16 H16C 0.9600 . ?
O1 H1B 0.82(2) . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
O4 Pb1 O2 C7 91.5(4) . . . . ?
N2 Pb1 O2 C7 6.4(4) . . . . ?
N3 Pb1 O2 C7 16.5(4) . . . . ?
O5 Pb1 O2 C7 143.5(4) . . . . ?
C17 Pb1 O2 C7 117.6(4) . . . . ?
Pb1 O2 C7 N1 -4.3(7) . . . . ?
Pb1 O2 C7 C6 173.2(3) . . . . ?
O2 C7 N1 N2 -3.5(7) . . . . ?
C6 C7 N1 N2 178.8(4) . . . . ?
C7 N1 N2 C9 -178.8(5) . . . . ?
C7 N1 N2 Pb1 9.4(5) . . . . ?
O4 Pb1 N2 C9 92.0(4) . . . . ?
O2 Pb1 N2 C9 -179.5(4) . . . . ?
N3 Pb1 N2 C9 9.5(4) . . . . ?
O5 Pb1 N2 C9 122.6(4) . . . . ?
C17 Pb1 N2 C9 104.9(4) . . . . ?
O4 Pb1 N2 N1 -96.8(3) . . . . ?
O2 Pb1 N2 N1 -8.3(3) . . . . ?
N3 Pb1 N2 N1 -179.3(4) . . . . ?
O5 Pb1 N2 N1 -66.2(4) . . . . ?
C17 Pb1 N2 N1 -83.9(4) . . . . ?
N1 N2 C9 C10 176.3(4) . . . . ?
Pb1 N2 C9 C10 -12.4(6) . . . . ?
N1 N2 C9 C8 -4.5(7) . . . . ?
Pb1 N2 C9 C8 166.7(4) . . . . ?
N2 C9 C10 N3 6.6(7) . . . . ?
C8 C9 C10 N3 -172.6(5) . . . . ?
N2 C9 C10 C11 -173.0(5) . . . . ?
C8 C9 C10 C11 7.8(8) . . . . ?
C11 C10 N3 C14 -1.4(7) . . . . ?
C9 C10 N3 C14 179.0(4) . . . . ?
C11 C10 N3 Pb1 -178.9(4) . . . . ?
C9 C10 N3 Pb1 1.4(6) . . . . ?
O4 Pb1 N3 C14 89.8(4) . . . . ?
O2 Pb1 N3 C14 167.4(4) . . . . ?
N2 Pb1 N3 C14 177.6(4) . . . . ?
O5 Pb1 N3 C14 59.0(4) . . . . ?
C17 Pb1 N3 C14 74.8(4) . . . . ?
O4 Pb1 N3 C10 -92.8(4) . . . . ?
O2 Pb1 N3 C10 -15.2(4) . . . . ?
N2 Pb1 N3 C10 -5.0(3) . . . . ?
O5 Pb1 N3 C10 -123.6(3) . . . . ?
C17 Pb1 N3 C10 -107.8(4) . . . . ?
C10 N3 C14 C13 0.5(8) . . . . ?
Pb1 N3 C14 C13 177.8(4) . . . . ?
C10 N3 C14 C15 -179.8(5) . . . . ?
Pb1 N3 C14 C15 -2.4(6) . . . . ?
N3 C14 C15 O3 -7.5(8) . . . . ?
C13 C14 C15 O3 172.2(6) . . . . ?
N3 C14 C15 C16 173.6(5) . . . . ?
C13 C14 C15 C16 -6.6(8) . . . . ?
N3 C10 C11 C12 1.5(8) . . . . ?
C9 C10 C11 C12 -178.8(5) . . . . ?
C10 C11 C12 C13 -0.7(9) . . . . ?
N3 C14 C13 C12 0.4(8) . . . . ?
C15 C14 C13 C12 -179.4(5) . . . . ?
C11 C12 C13 C14 -0.2(9) . . . . ?
O2 C7 C6 C1 173.1(5) . . . . ?
N1 C7 C6 C1 -9.1(8) . . . . ?
O2 C7 C6 C5 -6.1(8) . . . . ?
N1 C7 C6 C5 171.7(5) . . . . ?
C5 C6 C1 O1 177.9(6) . . . . ?
C7 C6 C1 O1 -1.3(9) . . . . ?
C5 C6 C1 C2 -3.1(8) . . . . ?
C7 C6 C1 C2 177.7(5) . . . . ?
O1 C1 C2 C3 -178.8(6) . . . . ?
C6 C1 C2 C3 2.2(9) . . . . ?
C1 C2 C3 C4 0.1(10) . . . . ?
C2 C3 C4 C5 -1.2(10) . . . . ?
C3 C4 C5 C6 0.2(9) . . . . ?
C1 C6 C5 C4 1.9(8) . . . . ?
C7 C6 C5 C4 -178.9(5) . . . . ?
O2 Pb1 O4 C17 85.7(4) . . . . ?
N2 Pb1 O4 C17 151.0(4) . . . . ?
N3 Pb1 O4 C17 -145.0(4) . . . . ?
O5 Pb1 O4 C17 2.1(4) . . . . ?
O4 Pb1 O5 C17 -2.1(4) . . . . ?
O2 Pb1 O5 C17 -92.9(4) . . . . ?
N2 Pb1 O5 C17 -42.1(4) . . . . ?
N3 Pb1 O5 C17 37.9(4) . . . . ?
Pb1 O5 C17 O4 3.5(6) . . . . ?
Pb1 O5 C17 C18 -176.4(6) . . . . ?
Pb1 O4 C17 O5 -4.1(7) . . . . ?
Pb1 O4 C17 C18 175.8(5) . . . . ?
O4 Pb1 C17 O5 176.3(6) . . . . ?
O2 Pb1 C17 O5 84.2(4) . . . . ?
N2 Pb1 C17 O5 146.1(3) . . . . ?
N3 Pb1 C17 O5 -148.4(4) . . . . ?
O2 Pb1 C17 O4 -92.1(4) . . . . ?
N2 Pb1 C17 O4 -30.2(4) . . . . ?
N3 Pb1 C17 O4 35.4(4) . . . . ?
O5 Pb1 C17 O4 -176.3(6) . . . . ?
O4 Pb1 C17 C18 -21(3) . . . . ?
O2 Pb1 C17 C18 -113(3) . . . . ?
N2 Pb1 C17 C18 -51(3) . . . . ?
N3 Pb1 C17 C18 14(3) . . . . ?
O5 Pb1 C17 C18 163(3) . . . . ?
