#------------------------------------------------------------------------------
#$Date: 2016-03-25 11:22:20 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179787 $
#$URL: svn://www.crystallography.net/cod/cif/7/00/83/7008344.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7008344
loop_
_publ_author_name
'Cowley, Andrew R.'
'Downs, Anthony J.'
'Himmel, Hans-Jorg'
'Marchant, Sarah'
'Parsons, Simon'
'Yeoman, Justin A.'
_publ_section_title
;
 1,1,3,3-Tetramethylguanidine-gallane, (Me2N)2CN(H).GaH3: an unusually
 strongly bound gallane adduct.
;
_journal_issue                   9
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              1591
_journal_page_last               1597
_journal_paper_doi               10.1039/b501818h
_journal_year                    2005
_chemical_absolute_configuration ad
_chemical_formula_moiety         'C18 H56 Ga7 N13'
_chemical_formula_sum            'C18 H56 Ga7 N13'
_chemical_formula_weight         942.80
_space_group_IT_number           143
_symmetry_cell_setting           rhombohedral
_symmetry_Int_Tables_number      143
_symmetry_space_group_name_Hall  'P 3'
_symmetry_space_group_name_H-M   'P 3'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                120.00
_cell_formula_units_Z            3
_cell_length_a                   19.7013(2)
_cell_length_b                   19.7013(2)
_cell_length_c                   8.8318(2)
_cell_measurement_reflns_used    6963
_cell_measurement_temperature    150(2)
_cell_measurement_theta_max      28.5
_cell_measurement_theta_min      2
_cell_volume                     2968.72(8)
_computing_cell_refinement       SAINT
_computing_data_collection       SMART
_computing_data_reduction        SAINT
_computing_molecular_graphics    XP
_computing_publication_material  'XCIF, ENCIFER, PLATON'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      150(2)
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device_type  'Bruker Smart Apex CCD'
_diffrn_measurement_method       omega
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0676
_diffrn_reflns_av_sigmaI/netI    0.0613
_diffrn_reflns_limit_h_max       23
_diffrn_reflns_limit_h_min       -23
_diffrn_reflns_limit_k_max       23
_diffrn_reflns_limit_k_min       -23
_diffrn_reflns_limit_l_max       10
_diffrn_reflns_limit_l_min       -10
_diffrn_reflns_number            28333
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         24.99
_diffrn_reflns_theta_min         1.19
_diffrn_source                   'fine-focus sealed tube'
_diffrn_source_type              'sealed tube'
_exptl_absorpt_coefficient_mu    4.719
_exptl_absorpt_correction_T_max  0.650
_exptl_absorpt_correction_T_min  0.424
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'Sadabs v 2004/1'
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.582
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       needle
_exptl_crystal_F_000             1416
_exptl_crystal_recrystallization_method 'decomposition product'
_exptl_crystal_size_max          0.35
_exptl_crystal_size_mid          0.09
_exptl_crystal_size_min          0.09
_refine_diff_density_max         2.198
_refine_diff_density_min         -0.736
_refine_diff_density_rms         0.196
_refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881'
_refine_ls_abs_structure_Flack   0.43(5)
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.165
_refine_ls_hydrogen_treatment    'riding or variable metric rigid group'
_refine_ls_matrix_type           full
_refine_ls_number_parameters     370
_refine_ls_number_reflns         6995
_refine_ls_number_restraints     409
_refine_ls_restrained_S_all      1.145
_refine_ls_R_factor_all          0.0661
_refine_ls_R_factor_gt           0.0638
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0853P)²+11.8493P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1623
_refine_ls_wR_factor_ref         0.1643
_reflns_number_gt                6766
_reflns_number_total             6995
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b501818h.txt
_cod_data_source_block           COMPOUND6
_cod_depositor_comments
;
The following automatic conversions were performed:
'_exptl_absorpt_correction_type' value 'Multiscan' changed to 'multi-scan'
according to '/home/adriana/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1555 2011-01-17 13:19:09Z saulius 
;
_cod_database_code               7008344
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-y, x-y, z'
'-x+y, -x, z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ga1 Ga 0.59323(11) 0.22778(10) 0.00640(19) 0.0273(4) Uani 1 1 d DU . .
H1 H 0.535(2) 0.1930(13) 0.091(3) 0.041 Uiso 1 1 calc RD . .
Ga2 Ga 0.48284(12) 0.27051(14) -0.1855(2) 0.0379(5) Uani 1 1 d DU . .
H21 H 0.419(2) 0.211(2) -0.1507(13) 0.057 Uiso 1 1 calc RD . .
H22 H 0.4747(3) 0.2984(10) -0.307(4) 0.057 Uiso 1 1 calc RD . .
Ga3 Ga 0.6667 0.3333 -0.2861(3) 0.0308(7) Uani 1 3 d SDU . .
H3 H 0.6667 0.3333 -0.428(5) 0.046 Uiso 1 3 calc SRD . .
N11 N 0.6510(8) 0.1732(7) -0.0215(12) 0.041(3) Uani 1 1 d DU . .
C21 C 0.6431(10) 0.1183(7) 0.0655(13) 0.035(3) Uani 1 1 d DU . .
N31 N 0.6434(11) 0.0531(8) 0.0217(16) 0.050(3) Uani 1 1 d DU . .
N41 N 0.6311(9) 0.1186(7) 0.2220(12) 0.042(3) Uani 1 1 d DU . .
C51 C 0.6828(12) 0.0180(10) 0.102(2) 0.056(5) Uani 1 1 d DU . .
H51A H 0.7396 0.0512 0.0908 0.085 Uiso 1 1 calc R . .
H51B H 0.6660 -0.0342 0.0608 0.085 Uiso 1 1 calc R . .
H51C H 0.6691 0.0133 0.2102 0.085 Uiso 1 1 calc R . .
C61 C 0.6230(12) 0.0259(11) -0.1306(18) 0.051(5) Uani 1 1 d DU . .
H61A H 0.6079 0.0597 -0.1851 0.076 Uiso 1 1 calc R . .
H61B H 0.5790 -0.0280 -0.1302 0.076 Uiso 1 1 calc R . .
H61C H 0.6681 0.0276 -0.1809 0.076 Uiso 1 1 calc R . .
C71 C 0.5798(12) 0.0483(9) 0.307(2) 0.047(4) Uani 1 1 d DU . .
H71A H 0.5435 0.0074 0.2378 0.070 Uiso 1 1 calc R . .
H71B H 0.5500 0.0601 0.3812 0.070 Uiso 1 1 calc R . .
H71C H 0.6114 0.0300 0.3603 0.070 Uiso 1 1 calc R . .
C81 C 0.6619(13) 0.1929(9) 0.3048(18) 0.053(6) Uani 1 1 d DU . .
H81A H 0.7193 0.2207 0.3026 0.079 Uiso 1 1 calc R . .
H81B H 0.6437 0.1822 0.4100 0.079 Uiso 1 1 calc R . .
H81C H 0.6431 0.2254 0.2569 0.079 Uiso 1 1 calc R . .
N91 N 0.6667 0.3333 0.0691(15) 0.020(3) Uani 1 3 d SDU . .
H91 H 0.6667 0.3333 0.1744 0.023 Uiso 1 3 calc SR . .
N101 N 0.5687(4) 0.2475(5) -0.1974(9) 0.030(2) Uani 1 1 d DU . .
C111 C 0.5388(9) 0.1774(7) -0.2968(16) 0.047(3) Uani 1 1 d DU . .
H11A H 0.5820 0.1683 -0.3231 0.070 Uiso 1 1 calc R . .
H11B H 0.5169 0.1862 -0.3895 0.070 Uiso 1 1 calc R . .
H11C H 0.4979 0.1315 -0.2434 0.070 Uiso 1 1 calc R . .
Ga4 Ga 0.40824(9) 0.77271(9) -0.11226(17) 0.0174(3) Uani 1 1 d DU . .
H4 H 0.467(2) 0.8068(12) -0.197(3) 0.026 Uiso 1 1 calc RD . .
Ga5 Ga 0.51590(10) 0.72602(12) 0.07938(19) 0.0283(4) Uani 1 1 d DU . .
H51 H 0.5219(2) 0.6959(11) 0.200(4) 0.042 Uiso 1 1 calc RD . .
H52 H 0.580(2) 0.785(2) 0.0484(11) 0.042 Uiso 1 1 calc RD . .
Ga6 Ga 0.3333 0.6667 0.1800(3) 0.0206(6) Uani 1 3 d SDU . .
H6 H 0.3333 0.6667 0.322(5) 0.031 Uiso 1 3 calc SRD . .
N12 N 0.3501(6) 0.8275(6) -0.0881(11) 0.022(2) Uani 1 1 d DU . .
C22 C 0.3614(9) 0.8841(7) -0.1742(12) 0.028(2) Uani 1 1 d DU . .
N32 N 0.3614(10) 0.9493(8) -0.1292(16) 0.047(3) Uani 1 1 d DU . .
N42 N 0.3737(8) 0.8824(6) -0.3301(12) 0.037(3) Uani 1 1 d DU . .
C52 C 0.3348(18) 0.9942(15) -0.216(3) 0.086(7) Uani 1 1 d DU . .
H52A H 0.3791 1.0468 -0.2353 0.128 Uiso 1 1 calc R . .
H52B H 0.2945 0.9985 -0.1583 0.128 Uiso 1 1 calc R . .
H52C H 0.3127 0.9678 -0.3123 0.128 Uiso 1 1 calc R . .
C62 C 0.3870(14) 0.9784(12) 0.021(2) 0.064(6) Uani 1 1 d DU . .
H62A H 0.3429 0.9518 0.0912 0.096 Uiso 1 1 calc R . .
H62B H 0.4063 1.0350 0.0229 0.096 Uiso 1 1 calc R . .
H62C H 0.4291 0.9685 0.0505 0.096 Uiso 1 1 calc R . .
C72 C 0.4283(14) 0.9503(10) -0.418(2) 0.062(6) Uani 1 1 d DU . .
H72A H 0.4062 0.9480 -0.5187 0.093 Uiso 1 1 calc R . .
H72B H 0.4780 0.9506 -0.4288 0.093 Uiso 1 1 calc R . .
H72C H 0.4377 0.9982 -0.3664 0.093 Uiso 1 1 calc R . .
C82 C 0.3421(9) 0.8080(7) -0.4119(14) 0.027(3) Uani 1 1 d DU . .
H82A H 0.3834 0.7948 -0.4257 0.041 Uiso 1 1 calc R . .
H82B H 0.3226 0.8130 -0.5110 0.041 Uiso 1 1 calc R . .
H82C H 0.2989 0.7665 -0.3536 0.041 Uiso 1 1 calc R . .
N92 N 0.3333 0.6667 -0.1748(18) 0.026(3) Uani 1 3 d SDU . .
H92 H 0.3333 0.6667 -0.2801 0.031 Uiso 1 3 calc SR . .
N102 N 0.4320(5) 0.7521(5) 0.0916(9) 0.0239(19) Uani 1 1 d DU . .
C112 C 0.4629(8) 0.8226(7) 0.1887(15) 0.042(3) Uani 1 1 d DU . .
H11D H 0.5122 0.8642 0.1460 0.064 Uiso 1 1 calc R . .
H11E H 0.4724 0.8097 0.2908 0.064 Uiso 1 1 calc R . .
H11F H 0.4247 0.8405 0.1935 0.064 Uiso 1 1 calc R . .
Ga7 Ga -0.00469(10) 0.09206(9) 0.60650(19) 0.0252(3) Uani 1 1 d DU . .
H7 H -0.0447(14) 0.1090(6) 0.521(3) 0.038 Uiso 1 1 calc RD . .
Ga8 Ga -0.16152(10) 0.00041(11) 0.7971(2) 0.0313(4) Uani 1 1 d DU . .
H81 H -0.1918(11) -0.0360(13) 0.917(4) 0.047 Uiso 1 1 calc RD . .
H82 H -0.1895(10) 0.0433(15) 0.7652(12) 0.047 Uiso 1 1 calc RD . .
Ga9 Ga 0.0000 0.0000 0.8987(3) 0.0223(6) Uani 1 3 d SDU . .
H9 H 0.0000 0.0000 1.040(5) 0.033 Uiso 1 3 calc SRD . .
N13 N 0.1038(5) 0.1749(5) 0.6303(10) 0.027(2) Uani 1 1 d DU . .
C23 C 0.1351(8) 0.2334(7) 0.5422(12) 0.036(3) Uani 1 1 d DU . .
N33 N 0.1859(8) 0.3080(6) 0.5825(14) 0.049(4) Uani 1 1 d DU . .
N43 N 0.1219(11) 0.2274(7) 0.3856(11) 0.052(4) Uani 1 1 d DU . .
C53 C 0.2541(12) 0.3611(11) 0.494(2) 0.067(6) Uani 1 1 d DU . .
H53A H 0.2689 0.3307 0.4275 0.100 Uiso 1 1 calc R . .
H53B H 0.2977 0.3937 0.5616 0.100 Uiso 1 1 calc R . .
H53C H 0.2416 0.3947 0.4317 0.100 Uiso 1 1 calc R . .
C63 C 0.1902(9) 0.3321(9) 0.7354(17) 0.039(4) Uani 1 1 d DU . .
H63A H 0.1373 0.3073 0.7786 0.058 Uiso 1 1 calc R . .
H63B H 0.2138 0.3892 0.7395 0.058 Uiso 1 1 calc R . .
H63C H 0.2224 0.3163 0.7935 0.058 Uiso 1 1 calc R . .
C73 C 0.1190(18) 0.2891(12) 0.300(2) 0.084(7) Uani 1 1 d DU . .
H73A H 0.1288 0.3322 0.3689 0.126 Uiso 1 1 calc R . .
H73B H 0.0671 0.2682 0.2541 0.126 Uiso 1 1 calc R . .
H73C H 0.1591 0.3084 0.2211 0.126 Uiso 1 1 calc R . .
C83 C 0.0910(8) 0.1536(8) 0.3018(15) 0.035(3) Uani 1 1 d DU . .
H83A H 0.1234 0.1299 0.3224 0.053 Uiso 1 1 calc R . .
H83B H 0.0918 0.1639 0.1931 0.053 Uiso 1 1 calc R . .
H83C H 0.0370 0.1177 0.3339 0.053 Uiso 1 1 calc R . .
N93 N 0.0000 0.0000 0.5461(18) 0.027(3) Uani 1 3 d SDU . .
H93 H 0.0000 0.0000 0.4408 0.033 Uiso 1 3 calc SR . .
N103 N -0.0467(5) 0.0605(5) 0.8105(9) 0.0284(19) Uani 1 1 d DU . .
C113 C -0.0317(9) 0.1271(7) 0.9091(15) 0.038(3) Uani 1 1 d DU . .
H11G H 0.0205 0.1491 0.9543 0.056 Uiso 1 1 calc R . .
H11H H -0.0712 0.1089 0.9895 0.056 Uiso 1 1 calc R . .
H11I H -0.0345 0.1675 0.8489 0.056 Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ga Ga 0.2307 1.6083 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N91 Ga1 N11 107.7(4) . . ?
N91 Ga1 N101 100.2(4) . . ?
N11 Ga1 N101 105.4(4) . . ?
N101 Ga2 N11 100.0(4) . 3_665 ?
N101 Ga3 N101 105.4(3) 2_655 . ?
N101 Ga3 N101 105.4(3) 2_655 3_665 ?
N101 Ga3 N101 105.4(3) . 3_665 ?
C21 N11 Ga1 122.7(9) . . ?
C21 N11 Ga2 121.0(9) . 2_655 ?
Ga1 N11 Ga2 116.2(5) . 2_655 ?
N11 C21 N31 125.6(10) . . ?
N11 C21 N41 122.8(10) . . ?
N31 C21 N41 111.6(10) . . ?
C21 N31 C61 119.5(11) . . ?
C21 N31 C51 124.8(11) . . ?
C61 N31 C51 113.6(11) . . ?
C21 N41 C71 123.1(11) . . ?
C21 N41 C81 120.5(10) . . ?
C71 N41 C81 115.9(10) . . ?
Ga1 N91 Ga1 112.1(3) 2_655 3_665 ?
Ga1 N91 Ga1 112.1(3) 2_655 . ?
Ga1 N91 Ga1 112.1(3) 3_665 . ?
C111 N101 Ga1 112.5(8) . . ?
C111 N101 Ga2 105.1(7) . . ?
Ga1 N101 Ga2 108.9(4) . . ?
C111 N101 Ga3 108.8(7) . . ?
Ga1 N101 Ga3 107.5(4) . . ?
Ga2 N101 Ga3 114.1(4) . . ?
N12 Ga4 N92 106.7(3) . . ?
N12 Ga4 N102 106.5(4) . . ?
N92 Ga4 N102 99.8(5) . . ?
N102 Ga5 N12 100.7(4) . 3_565 ?
N102 Ga6 N102 105.6(3) 3_565 . ?
N102 Ga6 N102 105.6(3) 3_565 2_665 ?
N102 Ga6 N102 105.6(3) . 2_665 ?
C22 N12 Ga4 121.9(8) . . ?
C22 N12 Ga5 123.0(7) . 2_665 ?
Ga4 N12 Ga5 115.1(4) . 2_665 ?
N12 C22 N32 125.2(10) . . ?
N12 C22 N42 121.5(10) . . ?
N32 C22 N42 113.3(10) . . ?
C22 N32 C62 119.2(11) . . ?
C22 N32 C52 126.8(13) . . ?
C62 N32 C52 113.9(12) . . ?
C22 N42 C72 124.1(11) . . ?
C22 N42 C82 121.1(9) . . ?
C72 N42 C82 114.0(10) . . ?
Ga4 N92 Ga4 112.2(4) . 3_565 ?
Ga4 N92 Ga4 112.2(4) . 2_665 ?
Ga4 N92 Ga4 112.2(4) 3_565 2_665 ?
C112 N102 Ga4 111.6(7) . . ?
C112 N102 Ga5 105.7(7) . . ?
Ga4 N102 Ga5 108.9(4) . . ?
C112 N102 Ga6 109.7(7) . . ?
Ga4 N102 Ga6 107.7(4) . . ?
Ga5 N102 Ga6 113.3(4) . . ?
N93 Ga7 N13 105.5(4) . . ?
N93 Ga7 N103 99.6(5) . . ?
N13 Ga7 N103 106.3(4) . . ?
N13 Ga8 N103 100.3(4) 2 . ?
N103 Ga9 N103 105.7(3) 3 . ?
N103 Ga9 N103 105.7(3) 3 2 ?
N103 Ga9 N103 105.7(3) . 2 ?
C23 N13 Ga7 121.8(9) . . ?
C23 N13 Ga8 122.2(8) . 3 ?
Ga7 N13 Ga8 116.0(4) . 3 ?
N13 C23 N33 126.1(10) . . ?
N13 C23 N43 123.0(10) . . ?
N33 C23 N43 110.9(10) . . ?
C23 N33 C63 120.2(10) . . ?
C23 N33 C53 123.9(12) . . ?
C63 N33 C53 113.2(11) . . ?
C23 N43 C73 121.5(12) . . ?
C23 N43 C83 123.3(10) . . ?
C73 N43 C83 113.5(11) . . ?
Ga7 N93 Ga7 112.7(4) 3 . ?
Ga7 N93 Ga7 112.7(4) 3 2 ?
Ga7 N93 Ga7 112.7(4) . 2 ?
C113 N103 Ga7 113.4(8) . . ?
C113 N103 Ga8 103.3(7) . . ?
Ga7 N103 Ga8 108.3(4) . . ?
C113 N103 Ga9 110.7(7) . . ?
Ga7 N103 Ga9 107.6(4) . . ?
Ga8 N103 Ga9 113.6(4) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ga1 N91 1.928(4) . ?
Ga1 N11 1.933(8) . ?
Ga1 N101 1.953(8) . ?
Ga2 N101 1.960(8) . ?
Ga2 N11 1.972(12) 3_665 ?
Ga3 N101 1.984(8) 2_655 ?
Ga3 N101 1.984(8) . ?
Ga3 N101 1.984(8) 3_665 ?
N11 C21 1.271(12) . ?
N11 Ga2 1.972(12) 2_655 ?
C21 N31 1.346(12) . ?
C21 N41 1.403(12) . ?
N31 C61 1.429(15) . ?
N31 C51 1.457(14) . ?
N41 C71 1.450(13) . ?
N41 C81 1.469(13) . ?
N91 Ga1 1.928(4) 2_655 ?
N91 Ga1 1.928(4) 3_665 ?
N101 C111 1.487(11) . ?
Ga4 N12 1.938(8) . ?
Ga4 N92 1.940(5) . ?
Ga4 N102 1.953(8) . ?
Ga5 N102 1.964(8) . ?
Ga5 N12 1.969(9) 3_565 ?
Ga6 N102 1.987(8) 3_565 ?
Ga6 N102 1.987(8) . ?
Ga6 N102 1.987(8) 2_665 ?
N12 C22 1.274(12) . ?
N12 Ga5 1.968(9) 2_665 ?
C22 N32 1.346(12) . ?
C22 N42 1.401(12) . ?
N32 C62 1.430(15) . ?
N32 C52 1.451(14) . ?
N42 C72 1.454(13) . ?
N42 C82 1.464(13) . ?
N92 Ga4 1.940(5) 3_565 ?
N92 Ga4 1.940(5) 2_665 ?
N102 C112 1.479(11) . ?
Ga7 N93 1.936(5) . ?
Ga7 N13 1.946(8) . ?
Ga7 N103 1.950(8) . ?
Ga8 N13 1.962(10) 2 ?
Ga8 N103 1.963(8) . ?
Ga9 N103 1.993(8) 3 ?
Ga9 N103 1.993(8) . ?
Ga9 N103 1.993(8) 2 ?
N13 C23 1.267(12) . ?
N13 Ga8 1.962(10) 3 ?
C23 N33 1.349(13) . ?
C23 N43 1.402(12) . ?
N33 C63 1.419(15) . ?
N33 C53 1.453(14) . ?
N43 C73 1.454(13) . ?
N43 C83 1.465(13) . ?
N93 Ga7 1.936(5) 3 ?
N93 Ga7 1.936(5) 2 ?
N103 C113 1.477(12) . ?
