#------------------------------------------------------------------------------
#$Date: 2016-03-25 11:22:20 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179787 $
#$URL: svn://www.crystallography.net/cod/cif/7/00/83/7008360.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7008360
loop_
_publ_author_name
'Yucesan, Gundog'
'Golub, Vladimir'
'O'Connor, C J'
'Zubieta, Jon'
_publ_section_title
;
 Solid state coordination chemistry of the
 copper(ii)-terpyridine/oxovanadium organophosphonate system:
 hydrothermal syntheses, structural characterization and magnetic
 properties.
;
_journal_issue                   13
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              2241
_journal_page_last               2251
_journal_paper_doi               10.1039/b502073e
_journal_year                    2005
_chemical_formula_sum            'C30 H22 Cu2 N6 O17 V6'
_chemical_formula_weight         1171.26
_chemical_name_systematic
;
?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                99.3440(10)
_cell_angle_beta                 98.7790(10)
_cell_angle_gamma                94.0670(10)
_cell_formula_units_Z            2
_cell_length_a                   8.8569(6)
_cell_length_b                   10.7058(7)
_cell_length_c                   20.4918(14)
_cell_measurement_reflns_used    12232
_cell_measurement_temperature    92(2)
_cell_measurement_theta_max      31.51
_cell_measurement_theta_min      1.94
_cell_volume                     1885.6(2)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL and CrystalMaker 6.x'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      92(2)
_diffrn_detector_area_resol_mean '512 x 512'
_diffrn_measured_fraction_theta_full 0.975
_diffrn_measured_fraction_theta_max 0.975
_diffrn_measurement_device_type  'APEX CCD area detector'
_diffrn_measurement_method       'Phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0257
_diffrn_reflns_av_sigmaI/netI    0.0420
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_k_min       -15
_diffrn_reflns_limit_l_max       30
_diffrn_reflns_limit_l_min       -29
_diffrn_reflns_number            24446
_diffrn_reflns_theta_full        31.51
_diffrn_reflns_theta_max         31.51
_diffrn_reflns_theta_min         1.94
_diffrn_standards_decay_%        0.001
_exptl_absorpt_coefficient_mu    2.608
_exptl_absorpt_correction_T_max  0.7805
_exptl_absorpt_correction_T_min  0.4218
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'SADABS SHELXL-97 (Sheldrick, 1997)'
_exptl_crystal_colour            green
_exptl_crystal_density_diffrn    2.063
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       parallepiped
_exptl_crystal_F_000             1152
_exptl_crystal_size_max          0.40
_exptl_crystal_size_mid          0.16
_exptl_crystal_size_min          0.10
_refine_diff_density_max         1.026
_refine_diff_density_min         -0.659
_refine_diff_density_rms         0.127
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.027
_refine_ls_hydrogen_treatment    refall
_refine_ls_matrix_type           full
_refine_ls_number_parameters     550
_refine_ls_number_reflns         12232
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.027
_refine_ls_R_factor_all          0.0527
_refine_ls_R_factor_gt           0.0388
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.001
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0504P)²+0.3365P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0932
_refine_ls_wR_factor_ref         0.0993
_reflns_number_gt                9714
_reflns_number_total             12232
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b502073e.txt
_cod_data_source_block           compound_7
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7008360
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Cu1 Cu 0.85867(3) 0.78224(2) 1.075179(12) 0.00959(6) Uani 1 1 d . . .
Cu2 Cu 0.84267(3) 0.27856(2) 0.567659(12) 0.01018(6) Uani 1 1 d . . .
V1 V 0.65937(4) 1.17167(3) 1.273692(17) 0.01027(7) Uani 1 1 d . . .
V2 V 0.77492(4) 1.09236(3) 1.126301(18) 0.01088(7) Uani 1 1 d . . .
V3 V 0.91090(4) 0.76407(3) 0.926020(17) 0.01005(7) Uani 1 1 d . . .
V4 V 0.67312(4) 0.69824(4) 0.776386(17) 0.01176(8) Uani 1 1 d . . .
V5 V 0.78093(4) 0.59224(3) 0.634966(17) 0.01131(7) Uani 1 1 d . . .
V6 V 0.90460(4) 0.26629(3) 0.419900(17) 0.01103(7) Uani 1 1 d . . .
O1 O 0.6515(2) 1.02541(15) 1.28335(8) 0.0189(3) Uani 1 1 d . . .
O2 O 0.75908(19) 1.26823(16) 1.34637(8) 0.0198(3) Uani 1 1 d . . .
O3 O 0.7491(2) 1.18841(16) 1.20638(9) 0.0253(4) Uani 1 1 d . . .
O4 O 0.90578(18) 1.18452(17) 1.08976(8) 0.0191(3) Uani 1 1 d . . .
O5 O 0.6111(2) 1.06494(19) 1.07735(9) 0.0279(4) Uani 1 1 d . . .
O6 O 0.8350(2) 0.95612(15) 1.14081(8) 0.0191(3) Uani 1 1 d . . .
O7 O 0.86883(18) 0.85302(15) 0.99517(7) 0.0136(3) Uani 1 1 d . . .
O8 O 0.9108(2) 0.61858(16) 0.93661(9) 0.0254(4) Uani 1 1 d . . .
O9 O 0.7662(2) 0.77761(18) 0.85481(8) 0.0224(4) Uani 1 1 d . . .
O10 O 0.5962(2) 0.56239(18) 0.78241(9) 0.0261(4) Uani 1 1 d . . .
O11 O 0.5350(2) 0.79397(18) 0.74336(9) 0.0242(4) Uani 1 1 d . . .
O12 O 0.80622(19) 0.67793(15) 0.72266(8) 0.0167(3) Uani 1 1 d . . .
O13 O 0.6087(2) 0.60178(19) 0.59891(9) 0.0251(4) Uani 1 1 d . . .
O14 O 0.8054(2) 0.44237(16) 0.63783(8) 0.0231(4) Uani 1 1 d . . .
O15 O 0.84964(18) 0.34933(15) 0.48769(7) 0.0141(3) Uani 1 1 d . . .
O16 O 0.9208(2) 0.12261(17) 0.43154(9) 0.0246(4) Uani 1 1 d . . .
O17 O 1.0832(2) 0.33396(19) 0.40726(8) 0.0242(4) Uani 1 1 d . . .
N1 N 0.6381(2) 0.70872(17) 1.05542(9) 0.0112(3) Uani 1 1 d . . .
N2 N 0.8684(2) 0.65630(16) 1.13326(8) 0.0106(3) Uani 1 1 d . . .
N3 N 1.0860(2) 0.80490(17) 1.11140(9) 0.0125(3) Uani 1 1 d . . .
N4 N 0.6226(2) 0.20361(17) 0.54852(9) 0.0119(3) Uani 1 1 d . . .
N5 N 0.8529(2) 0.15832(17) 0.62878(9) 0.0114(3) Uani 1 1 d . . .
N6 N 1.0692(2) 0.30621(17) 0.60486(9) 0.0134(3) Uani 1 1 d . . .
C1 C 0.5253(2) 0.7466(2) 1.01391(10) 0.0135(4) Uani 1 1 d . . .
H1 H 0.5486 0.8132 0.9904 0.016 Uiso 1 1 calc R . .
C2 C 0.3746(2) 0.6908(2) 1.00429(11) 0.0143(4) Uani 1 1 d . . .
H2 H 0.2963 0.7185 0.9744 0.017 Uiso 1 1 calc R . .
C3 C 0.3409(2) 0.5943(2) 1.03899(11) 0.0139(4) Uani 1 1 d . . .
H3 H 0.2391 0.5546 1.0329 0.017 Uiso 1 1 calc R . .
C4 C 0.4574(2) 0.5562(2) 1.08287(10) 0.0133(4) Uani 1 1 d . . .
H4 H 0.4362 0.4913 1.1077 0.016 Uiso 1 1 calc R . .
C5 C 0.6053(2) 0.61467(19) 1.08960(10) 0.0109(4) Uani 1 1 d . . .
C6 C 0.7409(2) 0.58210(19) 1.13357(10) 0.0107(4) Uani 1 1 d . . .
C7 C 0.7460(3) 0.4862(2) 1.17211(11) 0.0151(4) Uani 1 1 d . . .
H7 H 0.6565 0.4319 1.1723 0.018 Uiso 1 1 calc R . .
C8 C 0.8857(3) 0.4720(2) 1.21029(11) 0.0173(4) Uani 1 1 d . . .
H8 H 0.8915 0.4078 1.2374 0.021 Uiso 1 1 calc R . .
C9 C 1.0174(3) 0.5506(2) 1.20933(11) 0.0152(4) Uani 1 1 d . . .
H9 H 1.1128 0.5418 1.2356 0.018 Uiso 1 1 calc R . .
C10 C 1.0043(2) 0.6428(2) 1.16845(10) 0.0114(4) Uani 1 1 d . . .
C11 C 1.1290(2) 0.7336(2) 1.15858(11) 0.0129(4) Uani 1 1 d . . .
C12 C 1.2772(3) 0.7477(2) 1.19415(12) 0.0180(4) Uani 1 1 d . . .
H12 H 1.3063 0.6955 1.2263 0.022 Uiso 1 1 calc R . .
C13 C 1.3823(3) 0.8402(2) 1.18164(13) 0.0217(5) Uani 1 1 d . . .
H13 H 1.4842 0.8525 1.2058 0.026 Uiso 1 1 calc R . .
C14 C 1.3381(3) 0.9139(2) 1.13403(12) 0.0200(5) Uani 1 1 d . . .
H14 H 1.4085 0.9775 1.1250 0.024 Uiso 1 1 calc R . .
C15 C 1.1878(3) 0.8929(2) 1.09949(11) 0.0154(4) Uani 1 1 d . . .
H15 H 1.1568 0.9428 1.0664 0.019 Uiso 1 1 calc R . .
C16 C 0.5095(2) 0.2391(2) 0.50615(11) 0.0142(4) Uani 1 1 d . . .
H16 H 0.5332 0.3023 0.4807 0.017 Uiso 1 1 calc R . .
C17 C 0.3582(3) 0.1861(2) 0.49840(11) 0.0151(4) Uani 1 1 d . . .
H17 H 0.2797 0.2124 0.4680 0.018 Uiso 1 1 calc R . .
C18 C 0.3245(3) 0.0940(2) 0.53589(11) 0.0154(4) Uani 1 1 d . . .
H18 H 0.2224 0.0558 0.5312 0.019 Uiso 1 1 calc R . .
C19 C 0.4417(2) 0.0583(2) 0.58049(11) 0.0146(4) Uani 1 1 d . . .
H19 H 0.4205 -0.0038 0.6070 0.018 Uiso 1 1 calc R . .
C20 C 0.5891(2) 0.1145(2) 0.58556(10) 0.0123(4) Uani 1 1 d . . .
C21 C 0.7251(2) 0.0858(2) 0.63109(10) 0.0124(4) Uani 1 1 d . . .
C22 C 0.7298(3) -0.0035(2) 0.67325(11) 0.0166(4) Uani 1 1 d . . .
H22 H 0.6406 -0.0569 0.6748 0.020 Uiso 1 1 calc R . .
C23 C 0.8693(3) -0.0124(2) 0.71324(11) 0.0184(4) Uani 1 1 d . . .
H23 H 0.8749 -0.0723 0.7428 0.022 Uiso 1 1 calc R . .
C24 C 1.0004(3) 0.0649(2) 0.71069(11) 0.0159(4) Uani 1 1 d . . .
H24 H 1.0952 0.0596 0.7385 0.019 Uiso 1 1 calc R . .
C25 C 0.9884(2) 0.1501(2) 0.66618(10) 0.0125(4) Uani 1 1 d . . .
C26 C 1.1118(2) 0.2399(2) 0.65458(11) 0.0135(4) Uani 1 1 d . . .
C27 C 1.2593(3) 0.2595(2) 0.69159(12) 0.0176(4) Uani 1 1 d . . .
H27 H 1.2882 0.2116 0.7259 0.021 Uiso 1 1 calc R . .
C28 C 1.3634(3) 0.3505(2) 0.67735(13) 0.0219(5) Uani 1 1 d . . .
H28 H 1.4647 0.3656 0.7021 0.026 Uiso 1 1 calc R . .
C29 C 1.3197(3) 0.4189(2) 0.62718(12) 0.0195(5) Uani 1 1 d . . .
H29 H 1.3895 0.4820 0.6173 0.023 Uiso 1 1 calc R . .
C30 C 1.1705(3) 0.3933(2) 0.59136(11) 0.0163(4) Uani 1 1 d . . .
H30 H 1.1399 0.4390 0.5563 0.020 Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
V V 0.3005 0.5294 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O7 Cu1 N2 158.18(7) . . ?
O7 Cu1 N1 99.54(7) . . ?
N2 Cu1 N1 80.33(7) . . ?
O7 Cu1 N3 97.31(7) . . ?
N2 Cu1 N3 80.28(7) . . ?
N1 Cu1 N3 160.37(7) . . ?
O7 Cu1 O6 97.68(6) . . ?
N2 Cu1 O6 103.91(7) . . ?
N1 Cu1 O6 98.92(7) . . ?
N3 Cu1 O6 88.71(7) . . ?
O15 Cu2 N5 160.74(7) . . ?
O15 Cu2 N4 99.34(7) . . ?
N5 Cu2 N4 80.36(7) . . ?
O15 Cu2 N6 97.87(7) . . ?
N5 Cu2 N6 80.52(7) . . ?
N4 Cu2 N6 160.71(7) . . ?
O15 Cu2 O14 101.75(7) . . ?
N5 Cu2 O14 97.45(7) . . ?
N4 Cu2 O14 95.24(7) . . ?
N6 Cu2 O14 89.71(7) . . ?
O1 V1 O3 109.31(8) . . ?
O1 V1 O2 109.77(8) . . ?
O3 V1 O2 110.37(9) . . ?
O1 V1 O11 105.55(9) . 2_677 ?
O3 V1 O11 109.97(9) . 2_677 ?
O2 V1 O11 111.74(8) . 2_677 ?
O5 V2 O6 108.87(10) . . ?
O5 V2 O4 109.34(8) . . ?
O6 V2 O4 113.57(9) . . ?
O5 V2 O3 108.46(10) . . ?
O6 V2 O3 108.86(8) . . ?
O4 V2 O3 107.63(8) . . ?
O8 V3 O7 108.98(8) . . ?
O8 V3 O4 108.55(9) . 2_777 ?
O7 V3 O4 111.27(8) . 2_777 ?
O8 V3 O9 110.28(10) . . ?
O7 V3 O9 108.58(8) . . ?
O4 V3 O9 109.18(8) 2_777 . ?
O10 V4 O12 109.10(9) . . ?
O10 V4 O9 110.21(9) . . ?
O12 V4 O9 108.98(8) . . ?
O10 V4 O11 111.68(10) . . ?
O12 V4 O11 107.95(8) . . ?
O9 V4 O11 108.86(8) . . ?
O13 V5 O14 109.17(10) . . ?
O13 V5 O17 110.17(9) . 2_766 ?
O14 V5 O17 112.89(10) . 2_766 ?
O13 V5 O12 108.68(9) . . ?
O14 V5 O12 107.36(8) . . ?
O17 V5 O12 108.45(8) 2_766 . ?
O16 V6 O15 108.75(8) . . ?
O16 V6 O17 109.10(10) . . ?
O15 V6 O17 110.54(8) . . ?
O16 V6 O2 110.16(9) . 1_544 ?
O15 V6 O2 108.79(8) . 1_544 ?
O17 V6 O2 109.49(8) . 1_544 ?
V1 O2 V6 142.28(10) . 1_566 ?
V1 O3 V2 138.60(10) . . ?
V3 O4 V2 154.58(11) 2_777 . ?
V2 O6 Cu1 132.42(9) . . ?
V3 O7 Cu1 120.73(9) . . ?
V4 O9 V3 143.41(11) . . ?
V4 O11 V1 149.77(13) . 2_677 ?
V4 O12 V5 129.56(10) . . ?
V5 O14 Cu2 136.00(10) . . ?
V6 O15 Cu2 121.36(9) . . ?
V6 O17 V5 158.05(11) . 2_766 ?
C1 N1 C5 119.44(19) . . ?
C1 N1 Cu1 125.93(15) . . ?
C5 N1 Cu1 114.61(14) . . ?
C10 N2 C6 122.83(18) . . ?
C10 N2 Cu1 118.42(14) . . ?
C6 N2 Cu1 118.64(14) . . ?
C15 N3 C11 119.38(19) . . ?
C15 N3 Cu1 125.92(15) . . ?
C11 N3 Cu1 114.06(14) . . ?
C16 N4 C20 119.28(19) . . ?
C16 N4 Cu2 125.80(15) . . ?
C20 N4 Cu2 114.81(14) . . ?
C25 N5 C21 122.94(18) . . ?
C25 N5 Cu2 118.38(15) . . ?
C21 N5 Cu2 118.67(14) . . ?
C30 N6 C26 119.49(19) . . ?
C30 N6 Cu2 126.14(15) . . ?
C26 N6 Cu2 113.72(14) . . ?
N1 C1 C2 121.7(2) . . ?
C3 C2 C1 119.0(2) . . ?
C2 C3 C4 119.4(2) . . ?
C5 C4 C3 118.7(2) . . ?
N1 C5 C4 121.75(19) . . ?
N1 C5 C6 113.73(18) . . ?
C4 C5 C6 124.52(19) . . ?
N2 C6 C7 120.00(19) . . ?
N2 C6 C5 112.61(17) . . ?
C7 C6 C5 127.39(19) . . ?
C8 C7 C6 118.2(2) . . ?
C7 C8 C9 120.9(2) . . ?
C8 C9 C10 117.7(2) . . ?
N2 C10 C9 120.3(2) . . ?
N2 C10 C11 112.88(18) . . ?
C9 C10 C11 126.79(19) . . ?
N3 C11 C12 121.7(2) . . ?
N3 C11 C10 114.00(18) . . ?
C12 C11 C10 124.3(2) . . ?
C11 C12 C13 118.5(2) . . ?
C14 C13 C12 119.8(2) . . ?
C13 C14 C15 118.5(2) . . ?
N3 C15 C14 122.1(2) . . ?
N4 C16 C17 121.9(2) . . ?
C18 C17 C16 118.7(2) . . ?
C17 C18 C19 119.3(2) . . ?
C20 C19 C18 118.9(2) . . ?
N4 C20 C19 121.8(2) . . ?
N4 C20 C21 113.45(18) . . ?
C19 C20 C21 124.75(19) . . ?
N5 C21 C22 120.0(2) . . ?
N5 C21 C20 112.65(18) . . ?
C22 C21 C20 127.4(2) . . ?
C21 C22 C23 118.0(2) . . ?
C24 C23 C22 121.2(2) . . ?
C25 C24 C23 117.8(2) . . ?
N5 C25 C24 120.1(2) . . ?
N5 C25 C26 112.69(18) . . ?
C24 C25 C26 127.2(2) . . ?
N6 C26 C27 121.5(2) . . ?
N6 C26 C25 114.33(18) . . ?
C27 C26 C25 124.2(2) . . ?
C26 C27 C28 118.6(2) . . ?
C29 C28 C27 120.0(2) . . ?
C28 C29 C30 118.4(2) . . ?
N6 C30 C29 122.0(2) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Cu1 O7 1.9259(15) . ?
Cu1 N2 1.9359(17) . ?
Cu1 N1 2.0091(18) . ?
Cu1 N3 2.0200(18) . ?
Cu1 O6 2.1556(16) . ?
Cu2 O15 1.9211(15) . ?
Cu2 N5 1.9337(18) . ?
Cu2 N4 2.0100(18) . ?
Cu2 N6 2.0171(19) . ?
Cu2 O14 2.1589(17) . ?
V1 O1 1.6078(17) . ?
V1 O3 1.7207(17) . ?
V1 O2 1.7424(16) . ?
V1 O11 1.7801(17) 2_677 ?
V2 O5 1.6113(18) . ?
V2 O6 1.6436(16) . ?
V2 O4 1.7945(16) . ?
V2 O3 1.8445(17) . ?
V3 O8 1.6071(18) . ?
V3 O7 1.6813(15) . ?
V3 O4 1.7705(16) 2_777 ?
V3 O9 1.8212(17) . ?
V4 O10 1.5930(18) . ?
V4 O12 1.7332(16) . ?
V4 O9 1.7427(17) . ?
V4 O11 1.7762(17) . ?
V5 O13 1.6078(17) . ?
V5 O14 1.6434(17) . ?
V5 O17 1.7963(17) 2_766 ?
V5 O12 1.8529(16) . ?
V6 O16 1.6073(18) . ?
V6 O15 1.6804(16) . ?
V6 O17 1.7653(17) . ?
V6 O2 1.8311(16) 1_544 ?
O2 V6 1.8313(16) 1_566 ?
O4 V3 1.7705(16) 2_777 ?
O11 V1 1.7801(17) 2_677 ?
O17 V5 1.7963(17) 2_766 ?
N1 C1 1.340(3) . ?
N1 C5 1.356(3) . ?
N2 C10 1.336(3) . ?
N2 C6 1.335(3) . ?
N3 C15 1.334(3) . ?
N3 C11 1.353(3) . ?
N4 C16 1.340(3) . ?
N4 C20 1.356(3) . ?
N5 C25 1.338(3) . ?
N5 C21 1.338(3) . ?
N6 C30 1.338(3) . ?
N6 C26 1.356(3) . ?
C1 C2 1.395(3) . ?
C2 C3 1.386(3) . ?
C3 C4 1.392(3) . ?
C4 C5 1.388(3) . ?
C5 C6 1.486(3) . ?
C6 C7 1.393(3) . ?
C7 C8 1.391(3) . ?
C8 C9 1.394(3) . ?
C9 C10 1.394(3) . ?
C10 C11 1.478(3) . ?
C11 C12 1.386(3) . ?
C12 C13 1.392(3) . ?
C13 C14 1.380(4) . ?
C14 C15 1.393(3) . ?
C16 C17 1.393(3) . ?
C17 C18 1.387(3) . ?
C18 C19 1.393(3) . ?
C19 C20 1.380(3) . ?
C20 C21 1.490(3) . ?
C21 C22 1.387(3) . ?
C22 C23 1.393(3) . ?
C23 C24 1.390(3) . ?
C24 C25 1.389(3) . ?
C25 C26 1.476(3) . ?
C26 C27 1.390(3) . ?
C27 C28 1.390(3) . ?
C28 C29 1.381(3) . ?
C29 C30 1.396(3) . ?
