#------------------------------------------------------------------------------
#$Date: 2016-03-25 11:23:56 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179788 $
#$URL: svn://www.crystallography.net/cod/cif/7/00/84/7008490.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7008490
loop_
_publ_author_name
'Jones, Peter G.'
'Wölper, Christoph'
_publ_section_title
;
 New stoichiometries from an old system: amine complexes of silver
 chloride.
;
_journal_issue                   10
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              1762
_journal_page_last               1763
_journal_paper_doi               10.1039/b503634h
_journal_year                    2005
_chemical_formula_sum            'C24 H52 Ag3 Cl3 N4'
_chemical_formula_weight         826.66
_chemical_name_systematic
;
?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                93.265(4)
_cell_angle_beta                 91.424(4)
_cell_angle_gamma                99.097(4)
_cell_formula_units_Z            4
_cell_length_a                   10.2950(12)
_cell_length_b                   11.6318(14)
_cell_length_c                   26.616(3)
_cell_measurement_reflns_used    6646
_cell_measurement_temperature    133(2)
_cell_measurement_theta_max      30.4
_cell_measurement_theta_min      2.5
_cell_volume                     3140.2(6)
_computing_cell_refinement       'BRUKER SAINT'
_computing_data_collection       'BRUKER SMART'
_computing_data_reduction        'BRUKER SAINT'
_computing_molecular_graphics    'SIEMENS XP'
_computing_publication_material  SHELXL-97
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      133(2)
_diffrn_detector_area_resol_mean 8.192
_diffrn_measured_fraction_theta_full 0.884
_diffrn_measured_fraction_theta_max 0.874
_diffrn_measurement_device_type  'Bruker SMART 1000 CCD'
_diffrn_measurement_method       'ω & φ scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0000
_diffrn_reflns_av_sigmaI/netI    0.0657
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_k_min       -16
_diffrn_reflns_limit_l_max       37
_diffrn_reflns_limit_l_min       0
_diffrn_reflns_number            22152
_diffrn_reflns_theta_full        30.00
_diffrn_reflns_theta_max         30.63
_diffrn_reflns_theta_min         0.77
_exptl_absorpt_coefficient_mu    2.127
_exptl_absorpt_correction_T_max  0.8316
_exptl_absorpt_correction_T_min  0.5722
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   TWINABS
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.749
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       needle
_exptl_crystal_F_000             1664
_exptl_crystal_size_max          0.46
_exptl_crystal_size_mid          0.20
_exptl_crystal_size_min          0.09
_refine_diff_density_max         0.990
_refine_diff_density_min         -0.775
_refine_diff_density_rms         0.149
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.059
_refine_ls_hydrogen_treatment    riding
_refine_ls_matrix_type           full
_refine_ls_number_parameters     614
_refine_ls_number_reflns         22152
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.059
_refine_ls_R_factor_all          0.0786
_refine_ls_R_factor_gt           0.0454
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0481P)²+4.3760P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1123
_refine_ls_wR_factor_ref         0.1211
_reflns_number_gt                15083
_reflns_number_total             22152
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b503634h.txt
_cod_data_source_block           bonham5
_cod_database_code               7008490
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag14 Ag 0.14274(4) 0.66047(4) 0.245452(14) 0.02579(10) Uani 1 1 d . . .
Cl11 Cl 0.46495(11) -0.03874(11) 0.25492(5) 0.0237(3) Uani 1 1 d . . .
Ag13 Ag 0.27138(4) 0.42777(4) 0.213144(15) 0.02732(10) Uani 1 1 d . . .
Cl13 Cl 0.48191(11) 0.47207(11) 0.25782(5) 0.0237(3) Uani 1 1 d . . .
Ag12 Ag 0.15170(4) 0.16326(4) 0.243061(14) 0.02613(10) Uani 1 1 d . . .
Cl14 Cl -0.02183(11) 0.62695(10) 0.17938(4) 0.0206(2) Uani 1 1 d . . .
Ag11 Ag 0.26072(4) -0.07012(4) 0.208274(15) 0.02540(10) Uani 1 1 d . . .
Cl12 Cl -0.02645(11) 0.13839(10) 0.18175(4) 0.0208(2) Uani 1 1 d . . .
Ag22 Ag -0.12622(4) 0.74022(4) 0.274064(14) 0.02493(10) Uani 1 1 d . . .
Cl22 Cl 0.04649(11) 0.91489(11) 0.27803(4) 0.0231(3) Uani 1 1 d . . .
Ag21 Ag -0.12388(4) 0.26528(3) 0.264137(14) 0.02422(9) Uani 1 1 d . . .
Cl21 Cl 0.08967(11) 0.41245(11) 0.28911(5) 0.0248(3) Uani 1 1 d . . .
N10 N -0.1572(4) 0.5704(3) 0.31574(14) 0.0219(9) Uani 1 1 d . . .
H10A H -0.2441 0.5376 0.3102 0.026 Uiso 1 1 calc R . .
H10B H -0.1081 0.5207 0.2997 0.026 Uiso 1 1 calc R . .
C11 C -0.1281(5) 0.5679(4) 0.37057(19) 0.0239(11) Uani 1 1 d . . .
H11 H -0.0302 0.5813 0.3758 0.029 Uiso 1 1 calc R . .
C12 C -0.1807(7) 0.4515(5) 0.3915(2) 0.0458(17) Uani 1 1 d . . .
H12A H -0.1398 0.3895 0.3740 0.055 Uiso 1 1 calc R . .
H12B H -0.2769 0.4334 0.3846 0.055 Uiso 1 1 calc R . .
C13 C -0.1530(8) 0.4511(6) 0.4479(2) 0.056(2) Uani 1 1 d . . .
H13A H -0.1922 0.3748 0.4600 0.067 Uiso 1 1 calc R . .
H13B H -0.0567 0.4617 0.4547 0.067 Uiso 1 1 calc R . .
C14 C -0.2093(6) 0.5473(6) 0.4761(2) 0.0428(16) Uani 1 1 d . . .
H14A H -0.1857 0.5481 0.5124 0.051 Uiso 1 1 calc R . .
H14B H -0.3065 0.5323 0.4722 0.051 Uiso 1 1 calc R . .
C15 C -0.1571(5) 0.6647(5) 0.45651(19) 0.0322(13) Uani 1 1 d . . .
H15A H -0.0616 0.6843 0.4648 0.039 Uiso 1 1 calc R . .
H15B H -0.2011 0.7252 0.4735 0.039 Uiso 1 1 calc R . .
C16 C -0.1800(5) 0.6657(5) 0.39962(18) 0.0276(12) Uani 1 1 d . . .
H16A H -0.2756 0.6592 0.3920 0.033 Uiso 1 1 calc R . .
H16B H -0.1365 0.7413 0.3881 0.033 Uiso 1 1 calc R . .
N20 N 0.3199(4) 0.6935(3) 0.29273(14) 0.0199(9) Uani 1 1 d . . .
H20A H 0.3770 0.6463 0.2804 0.024 Uiso 1 1 calc R . .
H20B H 0.3588 0.7695 0.2895 0.024 Uiso 1 1 calc R . .
C21 C 0.3055(5) 0.6755(4) 0.34756(17) 0.0206(11) Uani 1 1 d . . .
H21 H 0.2551 0.5957 0.3511 0.025 Uiso 1 1 calc R . .
C22 C 0.4393(5) 0.6831(5) 0.3744(2) 0.0298(13) Uani 1 1 d . . .
H22A H 0.4937 0.7590 0.3686 0.036 Uiso 1 1 calc R . .
H22B H 0.4848 0.6205 0.3602 0.036 Uiso 1 1 calc R . .
C23 C 0.4260(5) 0.6711(5) 0.4309(2) 0.0378(15) Uani 1 1 d . . .
H23A H 0.3796 0.5921 0.4369 0.045 Uiso 1 1 calc R . .
H23B H 0.5148 0.6804 0.4473 0.045 Uiso 1 1 calc R . .
C24 C 0.3512(5) 0.7611(6) 0.4543(2) 0.0411(16) Uani 1 1 d . . .
H24A H 0.4010 0.8402 0.4511 0.049 Uiso 1 1 calc R . .
H24B H 0.3404 0.7488 0.4906 0.049 Uiso 1 1 calc R . .
C25 C 0.2158(5) 0.7506(6) 0.4277(2) 0.0438(16) Uani 1 1 d . . .
H25A H 0.1638 0.6735 0.4334 0.053 Uiso 1 1 calc R . .
H25B H 0.1683 0.8114 0.4424 0.053 Uiso 1 1 calc R . .
C26 C 0.2276(5) 0.7640(5) 0.3710(2) 0.0309(13) Uani 1 1 d . . .
H26A H 0.1386 0.7529 0.3548 0.037 Uiso 1 1 calc R . .
H26B H 0.2719 0.8437 0.3652 0.037 Uiso 1 1 calc R . .
N30 N 0.1250(4) 0.3942(4) 0.15096(14) 0.0207(9) Uani 1 1 d . . .
H30A H 0.0639 0.3320 0.1591 0.025 Uiso 1 1 calc R . .
H30B H 0.0822 0.4578 0.1509 0.025 Uiso 1 1 calc R . .
C31 C 0.1615(4) 0.3692(4) 0.09785(17) 0.0172(10) Uani 1 1 d . . .
H31 H 0.1913 0.2914 0.0954 0.021 Uiso 1 1 calc R . .
C32 C 0.2748(4) 0.4614(4) 0.08405(17) 0.0199(10) Uani 1 1 d . . .
H32A H 0.2490 0.5396 0.0889 0.024 Uiso 1 1 calc R . .
H32B H 0.3521 0.4590 0.1066 0.024 Uiso 1 1 calc R . .
C33 C 0.3119(4) 0.4415(5) 0.02977(18) 0.0241(11) Uani 1 1 d . . .
H33A H 0.3455 0.3664 0.0257 0.029 Uiso 1 1 calc R . .
H33B H 0.3833 0.5044 0.0215 0.029 Uiso 1 1 calc R . .
C34 C 0.1936(5) 0.4394(4) -0.00676(18) 0.0240(11) Uani 1 1 d . . .
H34A H 0.1658 0.5172 -0.0054 0.029 Uiso 1 1 calc R . .
H34B H 0.2193 0.4214 -0.0416 0.029 Uiso 1 1 calc R . .
C35 C 0.0800(5) 0.3486(4) 0.00695(18) 0.0248(11) Uani 1 1 d . . .
H35A H 0.1042 0.2700 0.0011 0.030 Uiso 1 1 calc R . .
H35B H 0.0025 0.3531 -0.0152 0.030 Uiso 1 1 calc R . .
C36 C 0.0435(4) 0.3654(4) 0.06174(18) 0.0229(11) Uani 1 1 d . . .
H36A H 0.0073 0.4391 0.0665 0.027 Uiso 1 1 calc R . .
H36B H -0.0260 0.3006 0.0697 0.027 Uiso 1 1 calc R . .
N40 N 0.1021(4) -0.1013(3) 0.15106(14) 0.0183(8) Uani 1 1 d . . .
H40A H 0.0535 -0.1729 0.1562 0.022 Uiso 1 1 calc R . .
H40B H 0.0483 -0.0466 0.1577 0.022 Uiso 1 1 calc R . .
C41 C 0.1292(4) -0.1003(4) 0.09648(17) 0.0194(10) Uani 1 1 d . . .
H41 H 0.0460 -0.1331 0.0770 0.023 Uiso 1 1 calc R . .
C42 C 0.2320(5) -0.1770(4) 0.08402(18) 0.0229(11) Uani 1 1 d . . .
H42A H 0.1981 -0.2582 0.0919 0.028 Uiso 1 1 calc R . .
H42B H 0.3124 -0.1497 0.1053 0.028 Uiso 1 1 calc R . .
C43 C 0.2671(5) -0.1747(4) 0.02889(19) 0.0275(12) Uani 1 1 d . . .
H43A H 0.1897 -0.2113 0.0076 0.033 Uiso 1 1 calc R . .
H43B H 0.3391 -0.2205 0.0228 0.033 Uiso 1 1 calc R . .
C44 C 0.3104(5) -0.0495(5) 0.0143(2) 0.0292(12) Uani 1 1 d . . .
H44A H 0.3939 -0.0162 0.0326 0.035 Uiso 1 1 calc R . .
H44B H 0.3262 -0.0496 -0.0223 0.035 Uiso 1 1 calc R . .
C45 C 0.2068(5) 0.0253(5) 0.0267(2) 0.0344(14) Uani 1 1 d . . .
H45A H 0.1264 -0.0030 0.0055 0.041 Uiso 1 1 calc R . .
H45B H 0.2393 0.1067 0.0187 0.041 Uiso 1 1 calc R . .
C46 C 0.1724(5) 0.0229(5) 0.08201(19) 0.0272(12) Uani 1 1 d . . .
H46A H 0.2502 0.0591 0.1032 0.033 Uiso 1 1 calc R . .
H46B H 0.1008 0.0690 0.0883 0.033 Uiso 1 1 calc R . .
N50 N 0.3353(4) 0.2038(4) 0.28690(16) 0.0284(10) Uani 1 1 d . . .
H50A H 0.3849 0.1461 0.2795 0.034 Uiso 1 1 calc R . .
H50B H 0.3810 0.2725 0.2767 0.034 Uiso 1 1 calc R . .
C51 C 0.3233(6) 0.2157(6) 0.3431(2) 0.0421(16) Uani 1 1 d . . .
H51 H 0.2488 0.2588 0.3508 0.051 Uiso 1 1 calc R . .
C52 C 0.4490(8) 0.2830(7) 0.3686(3) 0.074(3) Uani 1 1 d . . .
H52A H 0.4667 0.3620 0.3558 0.089 Uiso 1 1 calc R . .
H52B H 0.5240 0.2426 0.3601 0.089 Uiso 1 1 calc R . .
C53 C 0.4375(9) 0.2933(7) 0.4257(3) 0.079(3) Uani 1 1 d . . .
H53A H 0.5220 0.3331 0.4415 0.094 Uiso 1 1 calc R . .
H53B H 0.3685 0.3406 0.4345 0.094 Uiso 1 1 calc R . .
C54 C 0.4034(6) 0.1746(6) 0.4454(2) 0.0512(18) Uani 1 1 d . . .
H54A H 0.3903 0.1830 0.4820 0.061 Uiso 1 1 calc R . .
H54B H 0.4780 0.1314 0.4402 0.061 Uiso 1 1 calc R . .
C55 C 0.2816(8) 0.1053(8) 0.4202(2) 0.077(3) Uani 1 1 d . . .
H55A H 0.2043 0.1422 0.4292 0.093 Uiso 1 1 calc R . .
H55B H 0.2678 0.0254 0.4322 0.093 Uiso 1 1 calc R . .
C56 C 0.2943(7) 0.0992(6) 0.3626(2) 0.059(2) Uani 1 1 d . . .
H56A H 0.3655 0.0545 0.3536 0.071 Uiso 1 1 calc R . .
H56B H 0.2111 0.0572 0.3466 0.071 Uiso 1 1 calc R . .
N60 N -0.3349(4) 0.7420(4) 0.23809(15) 0.0219(9) Uani 1 1 d . . .
H60A H -0.3919 0.6787 0.2479 0.026 Uiso 1 1 calc R . .
H60B H -0.3654 0.8084 0.2498 0.026 Uiso 1 1 calc R . .
C61 C -0.3335(4) 0.7383(4) 0.18184(18) 0.0201(10) Uani 1 1 d . . .
H61 H -0.2812 0.6767 0.1705 0.024 Uiso 1 1 calc R . .
C62 C -0.2627(4) 0.8550(4) 0.16530(17) 0.0191(10) Uani 1 1 d . . .
H62A H -0.3127 0.9179 0.1757 0.023 Uiso 1 1 calc R . .
H62B H -0.1741 0.8730 0.1819 0.023 Uiso 1 1 calc R . .
C63 C -0.2500(5) 0.8501(5) 0.1083(2) 0.0285(12) Uani 1 1 d . . .
H63A H -0.1939 0.7916 0.0982 0.034 Uiso 1 1 calc R . .
H63B H -0.2071 0.9270 0.0979 0.034 Uiso 1 1 calc R . .
C64 C -0.3852(5) 0.8177(4) 0.08153(19) 0.0250(11) Uani 1 1 d . . .
H64A H -0.3741 0.8101 0.0447 0.030 Uiso 1 1 calc R . .
H64B H -0.4377 0.8808 0.0886 0.030 Uiso 1 1 calc R . .
C65 C -0.4591(4) 0.7027(4) 0.09903(18) 0.0220(11) Uani 1 1 d . . .
H65A H -0.5483 0.6868 0.0829 0.026 Uiso 1 1 calc R . .
H65B H -0.4119 0.6380 0.0884 0.026 Uiso 1 1 calc R . .
C66 C -0.4701(4) 0.7081(4) 0.15617(17) 0.0187(10) Uani 1 1 d . . .
H66A H -0.5141 0.6319 0.1668 0.022 Uiso 1 1 calc R . .
H66B H -0.5242 0.7680 0.1666 0.022 Uiso 1 1 calc R . .
N70 N -0.2312(4) 0.3807(3) 0.21587(13) 0.0170(8) Uani 1 1 d . . .
H70A H -0.3010 0.4015 0.2332 0.020 Uiso 1 1 calc R . .
H70B H -0.1746 0.4480 0.2103 0.020 Uiso 1 1 calc R . .
C71 C -0.2805(4) 0.3215(4) 0.16670(16) 0.0162(10) Uani 1 1 d . . .
H71 H -0.2044 0.2944 0.1496 0.019 Uiso 1 1 calc R . .
C72 C -0.3818(5) 0.2143(4) 0.17509(18) 0.0227(11) Uani 1 1 d . . .
H72A H -0.3412 0.1615 0.1963 0.027 Uiso 1 1 calc R . .
H72B H -0.4564 0.2388 0.1934 0.027 Uiso 1 1 calc R . .
C73 C -0.4326(5) 0.1495(4) 0.1266(2) 0.0284(12) Uani 1 1 d . . .
H73A H -0.5031 0.0847 0.1336 0.034 Uiso 1 1 calc R . .
H73B H -0.3605 0.1154 0.1105 0.034 Uiso 1 1 calc R . .
C74 C -0.4875(5) 0.2302(4) 0.08986(19) 0.0265(12) Uani 1 1 d . . .
H74A H -0.5118 0.1865 0.0571 0.032 Uiso 1 1 calc R . .
H74B H -0.5680 0.2548 0.1036 0.032 Uiso 1 1 calc R . .
C75 C -0.3867(5) 0.3374(4) 0.08197(18) 0.0232(11) Uani 1 1 d . . .
H75A H -0.4268 0.3904 0.0607 0.028 Uiso 1 1 calc R . .
H75B H -0.3112 0.3135 0.0640 0.028 Uiso 1 1 calc R . .
C76 C -0.3374(4) 0.4023(4) 0.13226(17) 0.0179(10) Uani 1 1 d . . .
H76A H -0.2690 0.4695 0.1261 0.021 Uiso 1 1 calc R . .
H76B H -0.4113 0.4326 0.1488 0.021 Uiso 1 1 calc R . .
N80 N -0.1993(4) 0.0949(3) 0.29715(15) 0.0228(9) Uani 1 1 d . . .
H80A H -0.2804 0.0673 0.2820 0.027 Uiso 1 1 calc R . .
H80B H -0.1442 0.0433 0.2874 0.027 Uiso 1 1 calc R . .
C81 C -0.2143(5) 0.0883(4) 0.35232(18) 0.0229(11) Uani 1 1 d . . .
H81 H -0.2762 0.1424 0.3632 0.028 Uiso 1 1 calc R . .
C82 C -0.2740(5) -0.0348(5) 0.3655(2) 0.0295(13) Uani 1 1 d . . .
H82A H -0.3628 -0.0560 0.3493 0.035 Uiso 1 1 calc R . .
H82B H -0.2186 -0.0911 0.3522 0.035 Uiso 1 1 calc R . .
C83 C -0.2838(6) -0.0429(5) 0.4225(2) 0.0366(14) Uani 1 1 d . . .
H83A H -0.3486 0.0054 0.4350 0.044 Uiso 1 1 calc R . .
H83B H -0.3159 -0.1248 0.4299 0.044 Uiso 1 1 calc R . .
C84 C -0.1517(6) -0.0018(5) 0.4497(2) 0.0397(15) Uani 1 1 d . . .
H84A H -0.0892 -0.0550 0.4399 0.048 Uiso 1 1 calc R . .
H84B H -0.1626 -0.0039 0.4865 0.048 Uiso 1 1 calc R . .
C85 C -0.0957(6) 0.1227(5) 0.4367(2) 0.0384(15) Uani 1 1 d . . .
H85A H -0.1546 0.1769 0.4491 0.046 Uiso 1 1 calc R . .
H85B H -0.0083 0.1469 0.4538 0.046 Uiso 1 1 calc R . .
C86 C -0.0825(5) 0.1299(5) 0.37978(19) 0.0295(12) Uani 1 1 d . . .
H86A H -0.0500 0.2116 0.3721 0.035 Uiso 1 1 calc R . .
H86B H -0.0175 0.0812 0.3679 0.035 Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N20 Ag14 Cl14 168.13(11) . . ?
N20 Ag14 Ag22 124.56(11) . . ?
Cl14 Ag14 Ag22 65.73(3) . . ?
N20 Ag14 Ag13 80.22(11) . . ?
Cl14 Ag14 Ag13 94.32(3) . . ?
Ag22 Ag14 Ag13 141.892(17) . . ?
N30 Ag13 Cl13 160.38(11) . . ?
N30 Ag13 Cl21 95.55(10) . . ?
Cl13 Ag13 Cl21 104.04(4) . . ?
N30 Ag13 Ag14 87.36(11) . . ?
Cl13 Ag13 Ag14 100.85(3) . . ?
Cl21 Ag13 Ag14 61.87(3) . . ?
N30 Ag13 Ag12 84.89(10) . . ?
Cl13 Ag13 Ag12 104.46(3) . . ?
Cl21 Ag13 Ag12 64.13(3) . . ?
Ag14 Ag13 Ag12 124.249(18) . . ?
N50 Ag12 Cl12 168.49(12) . . ?
N50 Ag12 Ag11 84.16(12) . . ?
Cl12 Ag12 Ag11 95.71(3) . . ?
N50 Ag12 Ag13 76.52(11) . . ?
Cl12 Ag12 Ag13 94.49(3) . . ?
Ag11 Ag12 Ag13 126.005(18) . . ?
N50 Ag12 Ag21 127.34(12) . . ?
Cl12 Ag12 Ag21 57.92(3) . . ?
Ag11 Ag12 Ag21 141.938(16) . . ?
Ag13 Ag12 Ag21 86.069(15) . . ?
N40 Ag11 Cl11 167.02(10) . . ?
N40 Ag11 Cl22 83.84(10) . 1_545 ?
Cl11 Ag11 Cl22 109.10(4) . 1_545 ?
N40 Ag11 Ag12 87.34(11) . . ?
Cl11 Ag11 Ag12 99.70(3) . . ?
Cl22 Ag11 Ag12 61.32(3) 1_545 . ?
Ag12 Cl12 Ag21 76.93(3) . . ?
N10 Ag22 N60 102.30(14) . . ?
N10 Ag22 Cl22 134.17(10) . . ?
N60 Ag22 Cl22 121.72(10) . . ?
N10 Ag22 Ag14 83.57(10) . . ?
N60 Ag22 Ag14 139.39(10) . . ?
Cl22 Ag22 Ag14 71.71(3) . . ?
Ag22 Cl22 Ag11 120.12(5) . 1_565 ?
N80 Ag21 N70 130.17(14) . . ?
N80 Ag21 Cl21 128.65(10) . . ?
N70 Ag21 Cl21 99.49(10) . . ?
N80 Ag21 Cl12 88.98(11) . . ?
N70 Ag21 Cl12 96.22(10) . . ?
Cl21 Ag21 Cl12 98.96(4) . . ?
N80 Ag21 Ag12 87.50(11) . . ?
N70 Ag21 Ag12 129.29(9) . . ?
Cl21 Ag21 Ag12 65.52(3) . . ?
Cl12 Ag21 Ag12 45.14(2) . . ?
Ag21 Cl21 Ag13 112.47(5) . . ?
C11 N10 Ag22 122.6(3) . . ?
N10 C11 C16 110.8(4) . . ?
N10 C11 C12 113.0(4) . . ?
C16 C11 C12 110.3(4) . . ?
C11 C12 C13 112.4(5) . . ?
C14 C13 C12 111.1(5) . . ?
C13 C14 C15 110.8(5) . . ?
C14 C15 C16 112.0(5) . . ?
C11 C16 C15 113.1(4) . . ?
C21 N20 Ag14 117.2(3) . . ?
N20 C21 C26 109.7(4) . . ?
N20 C21 C22 111.2(4) . . ?
C26 C21 C22 111.1(4) . . ?
C21 C22 C23 111.6(4) . . ?
C24 C23 C22 111.6(5) . . ?
C23 C24 C25 109.6(5) . . ?
C26 C25 C24 111.6(5) . . ?
C21 C26 C25 110.9(4) . . ?
C31 N30 Ag13 122.2(3) . . ?
N30 C31 C32 109.5(4) . . ?
N30 C31 C36 110.8(4) . . ?
C32 C31 C36 110.8(4) . . ?
C33 C32 C31 111.2(4) . . ?
C32 C33 C34 111.4(4) . . ?
C35 C34 C33 110.4(4) . . ?
C34 C35 C36 112.1(4) . . ?
C31 C36 C35 111.9(4) . . ?
C41 N40 Ag11 121.6(3) . . ?
N40 C41 C46 110.2(4) . . ?
N40 C41 C42 110.0(4) . . ?
C46 C41 C42 111.4(4) . . ?
C41 C42 C43 111.9(4) . . ?
C42 C43 C44 110.8(4) . . ?
C45 C44 C43 110.9(4) . . ?
C44 C45 C46 111.8(4) . . ?
C41 C46 C45 111.0(5) . . ?
C51 N50 Ag12 116.0(3) . . ?
C56 C51 N50 109.3(5) . . ?
C56 C51 C52 110.0(5) . . ?
N50 C51 C52 111.3(5) . . ?
C51 C52 C53 111.2(6) . . ?
C54 C53 C52 110.1(6) . . ?
C53 C54 C55 112.7(6) . . ?
C54 C55 C56 110.4(6) . . ?
C51 C56 C55 111.9(6) . . ?
C61 N60 Ag22 112.0(3) . . ?
N60 C61 C66 113.9(4) . . ?
N60 C61 C62 109.3(4) . . ?
C66 C61 C62 110.4(4) . . ?
C63 C62 C61 110.3(4) . . ?
C62 C63 C64 110.9(4) . . ?
C63 C64 C65 111.2(4) . . ?
C66 C65 C64 111.0(4) . . ?
C65 C66 C61 110.3(4) . . ?
C71 N70 Ag21 112.5(3) . . ?
N70 C71 C76 112.5(4) . . ?
N70 C71 C72 109.9(4) . . ?
C76 C71 C72 110.8(4) . . ?
C73 C72 C71 112.1(4) . . ?
C72 C73 C74 111.7(4) . . ?
C75 C74 C73 111.1(4) . . ?
C74 C75 C76 111.3(4) . . ?
C71 C76 C75 110.6(4) . . ?
C81 N80 Ag21 120.7(3) . . ?
N80 C81 C86 109.9(4) . . ?
N80 C81 C82 111.2(4) . . ?
C86 C81 C82 111.8(4) . . ?
C83 C82 C81 111.2(5) . . ?
C84 C83 C82 111.7(5) . . ?
C83 C84 C85 110.6(5) . . ?
C86 C85 C84 110.8(5) . . ?
C81 C86 C85 110.7(4) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag14 N20 2.160(4) . ?
Ag14 Cl14 2.3833(11) . ?
Ag14 Ag22 3.1534(6) . ?
Ag14 Ag13 3.2779(7) . ?
Cl11 Ag11 2.3815(12) . ?
Ag13 N30 2.186(4) . ?
Ag13 Cl13 2.4136(12) . ?
Ag13 Cl21 2.7826(13) . ?
Ag13 Ag12 3.2784(7) . ?
Ag12 N50 2.169(4) . ?
Ag12 Cl12 2.3958(11) . ?
Ag12 Ag11 3.1961(7) . ?
Ag12 Ag21 3.2923(6) . ?
Ag11 N40 2.178(4) . ?
Ag11 Cl22 2.9086(13) 1_545 ?
Cl12 Ag21 2.8639(13) . ?
Ag22 N10 2.302(4) . ?
Ag22 N60 2.334(4) . ?
Ag22 Cl22 2.4748(13) . ?
Cl22 Ag11 2.9087(13) 1_565 ?
Ag21 N80 2.247(4) . ?
Ag21 N70 2.296(4) . ?
Ag21 Cl21 2.6102(13) . ?
N10 C11 1.486(6) . ?
C11 C16 1.513(7) . ?
C11 C12 1.518(7) . ?
C12 C13 1.522(8) . ?
C13 C14 1.512(8) . ?
C14 C15 1.513(8) . ?
C15 C16 1.528(7) . ?
N20 C21 1.494(6) . ?
C21 C26 1.518(7) . ?
C21 C22 1.523(6) . ?
C22 C23 1.526(7) . ?
C23 C24 1.510(8) . ?
C24 C25 1.532(7) . ?
C25 C26 1.531(7) . ?
N30 C31 1.496(6) . ?
C31 C32 1.521(6) . ?
C31 C36 1.524(6) . ?
C32 C33 1.518(6) . ?
C33 C34 1.536(6) . ?
C34 C35 1.513(7) . ?
C35 C36 1.525(7) . ?
N40 C41 1.486(6) . ?
C41 C46 1.507(6) . ?
C41 C42 1.519(6) . ?
C42 C43 1.521(6) . ?
C43 C44 1.530(7) . ?
C44 C45 1.511(7) . ?
C45 C46 1.523(7) . ?
N50 C51 1.505(7) . ?
C51 C56 1.468(9) . ?
C51 C52 1.524(8) . ?
C52 C53 1.527(10) . ?
C53 C54 1.497(9) . ?
C54 C55 1.499(9) . ?
C55 C56 1.540(8) . ?
N60 C61 1.496(6) . ?
C61 C66 1.528(6) . ?
C61 C62 1.530(6) . ?
C62 C63 1.525(7) . ?
C63 C64 1.530(6) . ?
C64 C65 1.534(6) . ?
C65 C66 1.526(6) . ?
N70 C71 1.483(5) . ?
C71 C76 1.521(6) . ?
C71 C72 1.525(6) . ?
C72 C73 1.496(7) . ?
C73 C74 1.550(7) . ?
C74 C75 1.519(7) . ?
C75 C76 1.533(6) . ?
N80 C81 1.486(6) . ?
C81 C86 1.521(7) . ?
C81 C82 1.530(7) . ?
C82 C83 1.529(7) . ?
C83 C84 1.521(8) . ?
C84 C85 1.534(8) . ?
C85 C86 1.531(7) . ?
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_site_symmetry_A
N40 H40A Cl14 0.92 2.45 3.351(4) 165.2 1_545
N40 H40B Cl12 0.92 2.45 3.340(4) 161.5 .
N20 H20A Cl13 0.92 2.49 3.383(4) 162.5 .
N20 H20B Cl11 0.92 2.56 3.450(4) 164.1 1_565
N30 H30A Cl12 0.92 2.41 3.291(4) 159.6 .
N30 H30B Cl14 0.92 2.48 3.362(4) 162.0 .
N50 H50A Cl11 0.92 2.48 3.382(5) 165.9 .
N50 H50B Cl13 0.92 2.47 3.385(4) 171.2 .
N10 H10B Cl21 0.92 2.57 3.429(4) 155.3 .
N60 H60A Cl13 0.92 2.58 3.472(4) 164.6 1_455
N60 H60B Cl11 0.92 2.68 3.540(4) 155.4 1_465
N70 H70A Cl13 0.92 2.59 3.481(4) 164.4 1_455
N70 H70B Cl14 0.92 2.59 3.501(4) 170.7 .
N80 H80A Cl11 0.92 2.77 3.679(4) 168.0 1_455
N80 H80B Cl22 0.92 2.66 3.559(4) 166.9 1_545
C46 H46B Cl12 0.99 2.97 3.711(5) 132.5 .
C21 H21 Cl21 1.00 2.91 3.723(5) 138.8 .
C52 H52A Cl13 0.99 2.97 3.768(7) 138.8 .
C56 H56B Cl22 0.99 2.75 3.689(6) 158.7 1_545
C61 H61 Cl14 1.00 2.83 3.645(5) 139.5 .
C71 H71 Cl12 1.00 2.92 3.653(5) 130.8 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
N20 Ag14 Ag13 N30 -168.38(14) . . . . ?
Cl14 Ag14 Ag13 N30 0.99(10) . . . . ?
Ag22 Ag14 Ag13 N30 56.12(10) . . . . ?
N20 Ag14 Ag13 Cl13 -6.35(11) . . . . ?
Cl14 Ag14 Ag13 Cl13 163.02(4) . . . . ?
Ag22 Ag14 Ag13 Cl13 -141.85(4) . . . . ?
N20 Ag14 Ag13 Cl21 93.89(11) . . . . ?
Cl14 Ag14 Ag13 Cl21 -96.74(4) . . . . ?
Ag22 Ag14 Ag13 Cl21 -41.61(4) . . . . ?
N20 Ag14 Ag13 Ag12 109.63(10) . . . . ?
Cl14 Ag14 Ag13 Ag12 -81.00(3) . . . . ?
Ag22 Ag14 Ag13 Ag12 -25.87(3) . . . . ?
N30 Ag13 Ag12 N50 165.45(16) . . . . ?
Cl13 Ag13 Ag12 N50 2.98(13) . . . . ?
Cl21 Ag13 Ag12 N50 -95.85(13) . . . . ?
Ag14 Ag13 Ag12 N50 -111.27(13) . . . . ?
N30 Ag13 Ag12 Cl12 -7.28(11) . . . . ?
Cl13 Ag13 Ag12 Cl12 -169.74(4) . . . . ?
Cl21 Ag13 Ag12 Cl12 91.43(4) . . . . ?
Ag14 Ag13 Ag12 Cl12 76.01(3) . . . . ?
N30 Ag13 Ag12 Ag11 93.13(11) . . . . ?
Cl13 Ag13 Ag12 Ag11 -69.34(4) . . . . ?
Cl21 Ag13 Ag12 Ag11 -168.17(3) . . . . ?
Ag14 Ag13 Ag12 Ag11 176.412(16) . . . . ?
N30 Ag13 Ag12 Ag21 -64.64(11) . . . . ?
Cl13 Ag13 Ag12 Ag21 132.89(3) . . . . ?
Cl21 Ag13 Ag12 Ag21 34.07(3) . . . . ?
Ag14 Ag13 Ag12 Ag21 18.649(18) . . . . ?
N50 Ag12 Ag11 N40 -168.43(15) . . . . ?
Cl12 Ag12 Ag11 N40 0.00(10) . . . . ?
Ag13 Ag12 Ag11 N40 -99.78(10) . . . . ?
Ag21 Ag12 Ag11 N40 42.45(10) . . . . ?
N50 Ag12 Ag11 Cl11 0.59(12) . . . . ?
Cl12 Ag12 Ag11 Cl11 169.03(4) . . . . ?
Ag13 Ag12 Ag11 Cl11 69.24(4) . . . . ?
Ag21 Ag12 Ag11 Cl11 -148.53(4) . . . . ?
N50 Ag12 Ag11 Cl22 107.14(12) . . . 1_545 ?
Cl12 Ag12 Ag11 Cl22 -84.43(4) . . . 1_545 ?
Ag13 Ag12 Ag11 Cl22 175.79(3) . . . 1_545 ?
Ag21 Ag12 Ag11 Cl22 -41.98(3) . . . 1_545 ?
N50 Ag12 Cl12 Ag21 -120.6(6) . . . . ?
Ag11 Ag12 Cl12 Ag21 150.59(2) . . . . ?
Ag13 Ag12 Cl12 Ag21 -82.51(2) . . . . ?
N20 Ag14 Ag22 N10 -84.30(16) . . . . ?
Cl14 Ag14 Ag22 N10 102.51(10) . . . . ?
Ag13 Ag14 Ag22 N10 38.68(10) . . . . ?
N20 Ag14 Ag22 N60 174.29(19) . . . . ?
Cl14 Ag14 Ag22 N60 1.10(15) . . . . ?
Ag13 Ag14 Ag22 N60 -62.73(15) . . . . ?
N20 Ag14 Ag22 Cl22 56.57(13) . . . . ?
Cl14 Ag14 Ag22 Cl22 -116.62(4) . . . . ?
Ag13 Ag14 Ag22 Cl22 179.55(4) . . . . ?
N10 Ag22 Cl22 Ag11 95.01(15) . . . 1_565 ?
N60 Ag22 Cl22 Ag11 -103.30(13) . . . 1_565 ?
Ag14 Ag22 Cl22 Ag11 34.06(4) . . . 1_565 ?
Ag12 Cl12 Ag21 N80 -87.49(10) . . . . ?
Ag12 Cl12 Ag21 N70 142.20(10) . . . . ?
Ag12 Cl12 Ag21 Cl21 41.53(4) . . . . ?
N50 Ag12 Ag21 N80 -101.42(17) . . . . ?
Cl12 Ag12 Ag21 N80 91.05(11) . . . . ?
Ag11 Ag12 Ag21 N80 38.62(10) . . . . ?
Ag13 Ag12 Ag21 N80 -171.15(10) . . . . ?
N50 Ag12 Ag21 N70 115.60(19) . . . . ?
Cl12 Ag12 Ag21 N70 -51.93(13) . . . . ?
Ag11 Ag12 Ag21 N70 -104.36(12) . . . . ?
Ag13 Ag12 Ag21 N70 45.87(12) . . . . ?
N50 Ag12 Ag21 Cl21 33.55(14) . . . . ?
Cl12 Ag12 Ag21 Cl21 -133.98(5) . . . . ?
Ag11 Ag12 Ag21 Cl21 173.59(4) . . . . ?
Ag13 Ag12 Ag21 Cl21 -36.18(3) . . . . ?
N50 Ag12 Ag21 Cl12 167.53(15) . . . . ?
Ag11 Ag12 Ag21 Cl12 -52.43(4) . . . . ?
Ag13 Ag12 Ag21 Cl12 97.80(4) . . . . ?
N80 Ag21 Cl21 Ag13 113.49(14) . . . . ?
N70 Ag21 Cl21 Ag13 -80.32(10) . . . . ?
Cl12 Ag21 Cl21 Ag13 17.59(5) . . . . ?
Ag12 Ag21 Cl21 Ag13 48.67(4) . . . . ?
N30 Ag13 Cl21 Ag21 31.86(12) . . . . ?
Cl13 Ag13 Cl21 Ag21 -149.19(5) . . . . ?
Ag14 Ag13 Cl21 Ag21 115.86(5) . . . . ?
Ag12 Ag13 Cl21 Ag21 -49.71(4) . . . . ?
N60 Ag22 N10 C11 -123.5(4) . . . . ?
Cl22 Ag22 N10 C11 40.7(4) . . . . ?
Ag14 Ag22 N10 C11 97.3(3) . . . . ?
Ag22 N10 C11 C16 44.4(5) . . . . ?
Ag22 N10 C11 C12 168.7(4) . . . . ?
N10 C11 C12 C13 -178.6(5) . . . . ?
C16 C11 C12 C13 -54.0(7) . . . . ?
C11 C12 C13 C14 56.8(8) . . . . ?
C12 C13 C14 C15 -55.9(8) . . . . ?
C13 C14 C15 C16 54.1(7) . . . . ?
N10 C11 C16 C15 177.9(4) . . . . ?
C12 C11 C16 C15 52.1(6) . . . . ?
C14 C15 C16 C11 -53.1(6) . . . . ?
Cl14 Ag14 N20 C21 -168.5(4) . . . . ?
Ag22 Ag14 N20 C21 43.2(4) . . . . ?
Ag13 Ag14 N20 C21 -105.1(3) . . . . ?
Ag14 N20 C21 C26 -65.8(5) . . . . ?
Ag14 N20 C21 C22 170.9(3) . . . . ?
N20 C21 C22 C23 177.0(4) . . . . ?
C26 C21 C22 C23 54.5(6) . . . . ?
C21 C22 C23 C24 -56.2(6) . . . . ?
C22 C23 C24 C25 56.7(6) . . . . ?
C23 C24 C25 C26 -57.1(7) . . . . ?
N20 C21 C26 C25 -177.8(4) . . . . ?
C22 C21 C26 C25 -54.5(6) . . . . ?
C24 C25 C26 C21 56.4(7) . . . . ?
Cl13 Ag13 N30 C31 14.4(6) . . . . ?
Cl21 Ag13 N30 C31 -168.6(3) . . . . ?
Ag14 Ag13 N30 C31 130.0(3) . . . . ?
Ag12 Ag13 N30 C31 -105.3(3) . . . . ?
Ag13 N30 C31 C32 -49.9(5) . . . . ?
Ag13 N30 C31 C36 -172.4(3) . . . . ?
N30 C31 C32 C33 -178.1(4) . . . . ?
C36 C31 C32 C33 -55.6(5) . . . . ?
C31 C32 C33 C34 56.8(5) . . . . ?
C32 C33 C34 C35 -55.7(6) . . . . ?
C33 C34 C35 C36 54.3(6) . . . . ?
N30 C31 C36 C35 176.0(4) . . . . ?
C32 C31 C36 C35 54.2(5) . . . . ?
C34 C35 C36 C31 -54.3(6) . . . . ?
Cl11 Ag11 N40 C41 -8.7(7) . . . . ?
Cl22 Ag11 N40 C41 176.0(3) 1_545 . . . ?
Ag12 Ag11 N40 C41 114.6(3) . . . . ?
Ag11 N40 C41 C46 -73.7(4) . . . . ?
Ag11 N40 C41 C42 49.5(5) . . . . ?
N40 C41 C42 C43 -177.7(4) . . . . ?
C46 C41 C42 C43 -55.2(5) . . . . ?
C41 C42 C43 C44 54.7(6) . . . . ?
C42 C43 C44 C45 -54.8(6) . . . . ?
C43 C44 C45 C46 55.7(6) . . . . ?
N40 C41 C46 C45 177.4(4) . . . . ?
C42 C41 C46 C45 55.0(5) . . . . ?
C44 C45 C46 C41 -55.9(6) . . . . ?
Cl12 Ag12 N50 C51 152.4(5) . . . . ?
Ag11 Ag12 N50 C51 -117.7(4) . . . . ?
Ag13 Ag12 N50 C51 113.1(4) . . . . ?
Ag21 Ag12 N50 C51 38.9(4) . . . . ?
Ag12 N50 C51 C56 77.8(5) . . . . ?
Ag12 N50 C51 C52 -160.6(5) . . . . ?
C56 C51 C52 C53 -57.8(9) . . . . ?
N50 C51 C52 C53 -179.1(6) . . . . ?
C51 C52 C53 C54 55.9(9) . . . . ?
C52 C53 C54 C55 -54.9(9) . . . . ?
C53 C54 C55 C56 54.1(10) . . . . ?
N50 C51 C56 C55 179.6(6) . . . . ?
C52 C51 C56 C55 57.2(8) . . . . ?
C54 C55 C56 C51 -55.6(9) . . . . ?
N10 Ag22 N60 C61 -118.3(3) . . . . ?
Cl22 Ag22 N60 C61 75.0(3) . . . . ?
Ag14 Ag22 N60 C61 -23.9(4) . . . . ?
Ag22 N60 C61 C66 165.2(3) . . . . ?
Ag22 N60 C61 C62 -70.8(4) . . . . ?
N60 C61 C62 C63 175.4(4) . . . . ?
C66 C61 C62 C63 -58.6(5) . . . . ?
C61 C62 C63 C64 57.1(5) . . . . ?
C62 C63 C64 C65 -55.5(6) . . . . ?
C63 C64 C65 C66 55.2(6) . . . . ?
C64 C65 C66 C61 -56.5(5) . . . . ?
N60 C61 C66 C65 -178.3(4) . . . . ?
C62 C61 C66 C65 58.3(5) . . . . ?
N80 Ag21 N70 C71 -63.2(3) . . . . ?
Cl21 Ag21 N70 C71 130.9(3) . . . . ?
Cl12 Ag21 N70 C71 30.7(3) . . . . ?
Ag12 Ag21 N70 C71 64.9(3) . . . . ?
Ag21 N70 C71 C76 -173.4(3) . . . . ?
Ag21 N70 C71 C72 62.7(4) . . . . ?
N70 C71 C72 C73 -178.7(4) . . . . ?
C76 C71 C72 C73 56.4(6) . . . . ?
C71 C72 C73 C74 -54.3(6) . . . . ?
C72 C73 C74 C75 53.4(6) . . . . ?
C73 C74 C75 C76 -54.3(6) . . . . ?
N70 C71 C76 C75 179.9(4) . . . . ?
C72 C71 C76 C75 -56.7(5) . . . . ?
C74 C75 C76 C71 56.6(5) . . . . ?
N70 Ag21 N80 C81 -109.8(3) . . . . ?
Cl21 Ag21 N80 C81 52.3(4) . . . . ?
Cl12 Ag21 N80 C81 153.0(3) . . . . ?
Ag12 Ag21 N80 C81 107.8(3) . . . . ?
Ag21 N80 C81 C86 -58.6(5) . . . . ?
Ag21 N80 C81 C82 177.0(3) . . . . ?
N80 C81 C82 C83 177.5(4) . . . . ?
C86 C81 C82 C83 54.1(6) . . . . ?
C81 C82 C83 C84 -54.4(6) . . . . ?
C82 C83 C84 C85 56.0(7) . . . . ?
C83 C84 C85 C86 -57.0(6) . . . . ?
N80 C81 C86 C85 -179.5(4) . . . . ?
C82 C81 C86 C85 -55.4(6) . . . . ?
C84 C85 C86 C81 56.7(6) . . . . ?
