#------------------------------------------------------------------------------
#$Date: 2016-03-25 11:37:32 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179799 $
#$URL: svn://www.crystallography.net/cod/cif/7/00/95/7009584.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7009584
loop_
_publ_author_name
'Ang, How Ghee'
'Ang, Siau Gek'
'Wang, Xiao'
_publ_section_title
;
 Formation of new cluster derivatives of triphospholene via ligand
 substitution and cleavage of P--P bond(s)
;
_journal_issue                   19
_journal_name_full
'Journal of the Chemical Society, Dalton Transactions'
_journal_page_first              3429
_journal_paper_doi               10.1039/b002140g
_journal_year                    2000
_chemical_formula_sum            'C54 H25 O22 Os6 P3'
_chemical_formula_weight         2259.85
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL
_cell_angle_alpha                108.455(9)
_cell_angle_beta                 100.079(12)
_cell_angle_gamma                98.27(2)
_cell_formula_units_Z            2
_cell_length_a                   12.9826(12)
_cell_length_b                   15.074(4)
_cell_length_c                   17.282(2)
_cell_measurement_temperature    293(2)
_cell_volume                     3085.9(10)
_computing_cell_refinement       'Siemens XSCANS'
_computing_data_collection       'Siemens XSCANS'
_computing_data_reduction        'Siemens SHELXTL'
_computing_molecular_graphics    'Siemens SHELXTL'
_computing_publication_material  'Siemens SHELXTL'
_computing_structure_refinement  'SHELXL-93 (Sheldrick, 1993)'
_computing_structure_solution    'SHELXS-86 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measurement_device       'Siemens P4'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0311
_diffrn_reflns_av_sigmaI/netI    0.0739
_diffrn_reflns_limit_h_max       17
_diffrn_reflns_limit_h_min       -17
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_k_min       -19
_diffrn_reflns_limit_l_max       22
_diffrn_reflns_limit_l_min       -16
_diffrn_reflns_number            19944
_diffrn_reflns_theta_max         29.30
_diffrn_reflns_theta_min         1.82
_exptl_absorpt_coefficient_mu    12.456
_exptl_absorpt_correction_type   Semiempirical
_exptl_crystal_colour            Yellow
_exptl_crystal_density_diffrn    2.432
_exptl_crystal_description       'Rectangular block '
_exptl_crystal_F_000             2052
_exptl_crystal_size_max          0.39
_exptl_crystal_size_mid          0.28
_exptl_crystal_size_min          0.14
_refine_diff_density_max         6.840
_refine_diff_density_min         -3.048
_refine_diff_density_rms         0.287
_refine_ls_extinction_coef       0.00008(5)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_all   1.031
_refine_ls_goodness_of_fit_obs   1.101
_refine_ls_matrix_type           full
_refine_ls_number_parameters     767
_refine_ls_number_reflns         14222
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.031
_refine_ls_restrained_S_obs      1.101
_refine_ls_R_factor_all          0.0949
_refine_ls_R_factor_obs          0.0625
_refine_ls_shift/esd_max         0.746
_refine_ls_shift/esd_mean        0.012
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0897P)²+27.4507P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_all         0.1846
_refine_ls_wR_factor_obs         0.1625
_reflns_number_observed          9826
_reflns_number_total             14222
_reflns_observed_criterion       >2sigma(I)
_cod_data_source_file            b002140g.txt
_cod_data_source_block           cluster3
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 

The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value 'calc
w=1/[\s^2^(Fo^2^)+(0.0897P)^2^+27.4507P] where P=(Fo^2^+2Fc^2^)/3'
was changed to 'calc'. New tag '_refine_ls_weighting_details' was
created. The value of the new tag was set to
'w=1/[\s^2^(Fo^2^)+(0.0897P)^2^+27.4507P] where P=(Fo^2^+2Fc^2^)/3'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_original_cell_volume        3085.8(9)
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7009584
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_thermal_displace_type
_atom_site_occupancy
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_group
Os1 Os 0.70763(5) 0.35335(4) 0.54217(4) 0.0439(2) Uani 1 d . .
C11 C 0.8532(14) 0.4048(11) 0.5432(9) 0.049(4) Uani 1 d . .
O11 O 0.9393(10) 0.4407(9) 0.5445(8) 0.072(3) Uani 1 d . .
C12 C 0.6672(16) 0.4621(13) 0.5242(12) 0.067(5) Uani 1 d . .
O12 O 0.6440(17) 0.5286(13) 0.5167(12) 0.117(6) Uani 1 d . .
C13 C 0.5574(16) 0.3158(13) 0.5496(11) 0.065(5) Uani 1 d . .
O13 O 0.4686(11) 0.3024(11) 0.5511(8) 0.081(4) Uani 1 d . .
Os2 Os 0.76605(5) 0.22853(4) 0.63345(4) 0.0456(2) Uani 1 d . .
C21 C 0.7736(13) 0.1017(13) 0.5662(10) 0.057(4) Uani 1 d . .
O21 O 0.7799(10) 0.0257(8) 0.5320(7) 0.062(3) Uani 1 d . .
C22 C 0.8065(14) 0.2207(11) 0.7411(11) 0.055(4) Uani 1 d . .
O22 O 0.8351(12) 0.2185(10) 0.8074(9) 0.082(4) Uani 1 d . .
C23 C 0.9140(14) 0.2809(13) 0.6310(11) 0.059(4) Uani 1 d . .
O23 O 0.9986(10) 0.2974(10) 0.6296(9) 0.074(4) Uani 1 d . .
C24 C 0.6140(13) 0.1800(14) 0.6164(12) 0.065(5) Uani 1 d . .
O24 O 0.5283(10) 0.1380(11) 0.6014(10) 0.083(4) Uani 1 d . .
Os3 Os 0.75013(7) 0.42151(5) 0.72373(4) 0.0614(2) Uani 1 d . .
C31 C 0.7074(24) 0.5382(16) 0.7332(17) 0.105(9) Uani 1 d . .
O31 O 0.6847(22) 0.6119(13) 0.7423(15) 0.159(10) Uani 1 d . .
C32 C 0.6073(17) 0.3562(14) 0.7279(11) 0.064(5) Uani 1 d . .
O32 O 0.5286(13) 0.3238(11) 0.7364(9) 0.085(4) Uani 1 d . .
C33 C 0.8828(30) 0.4678(17) 0.7173(16) 0.131(11) Uani 1 d . .
O33 O 0.9775(20) 0.5005(15) 0.7239(12) 0.150(9) Uani 1 d . .
C34 C 0.8020(21) 0.4355(16) 0.8378(14) 0.091(7) Uani 1 d . .
O34 O 0.8361(19) 0.4439(14) 0.9070(10) 0.138(8) Uani 1 d . .
P1 P 0.6665(3) 0.2428(2) 0.4030(2) 0.0347(7) Uani 1 d . .
C101 C 0.5225(10) 0.1937(11) 0.3742(8) 0.041(3) Uani 1 d . .
C102 C 0.4516(12) 0.2461(13) 0.3515(11) 0.057(4) Uani 1 d . .
H10A H 0.4778(12) 0.3037(13) 0.3455(11) 0.068 Uiso 1 calc R .
C103 C 0.3420(12) 0.2145(15) 0.3375(12) 0.068(5) Uani 1 d . .
H10B H 0.2956(12) 0.2521(15) 0.3247(12) 0.082 Uiso 1 calc R .
C104 C 0.3011(13) 0.1251(16) 0.3427(13) 0.078(6) Uani 1 d . .
H10C H 0.2276(13) 0.1020(16) 0.3309(13) 0.094 Uiso 1 calc R .
C105 C 0.3707(13) 0.0732(14) 0.3654(13) 0.069(5) Uani 1 d . .
H10D H 0.3436(13) 0.0146(14) 0.3693(13) 0.083 Uiso 1 calc R .
C106 C 0.4817(12) 0.1052(11) 0.3827(10) 0.052(4) Uani 1 d . .
H10E H 0.5279(12) 0.0695(11) 0.3995(10) 0.062 Uiso 1 calc R .
P2 P 0.7368(3) 0.1131(3) 0.3730(2) 0.0369(7) Uani 1 d . .
C201 C 0.8817(10) 0.1629(11) 0.4046(8) 0.042(3) Uani 1 d . .
C202 C 0.9453(12) 0.1059(12) 0.4341(9) 0.050(4) Uani 1 d . .
H20A H 0.9130(12) 0.0472(12) 0.4351(9) 0.060 Uiso 1 calc R .
C203 C 1.0560(13) 0.1380(15) 0.4617(10) 0.062(5) Uani 1 d . .
H20B H 1.0970(13) 0.1010(15) 0.4824(10) 0.075 Uiso 1 calc R .
C204 C 1.1038(13) 0.2206(16) 0.4588(11) 0.076(6) Uani 1 d . .
H20C H 1.1778(13) 0.2407(16) 0.4778(11) 0.091 Uiso 1 calc R .
C205 C 1.0437(13) 0.2791(14) 0.4273(11) 0.068(5) Uani 1 d . .
H20D H 1.0785(13) 0.3357(14) 0.4239(11) 0.081 Uiso 1 calc R .
C206 C 0.9315(12) 0.2505(12) 0.4013(10) 0.058(4) Uani 1 d . .
H20E H 0.8910(12) 0.2888(12) 0.3823(10) 0.070 Uiso 1 calc R .
P3 P 0.7037(2) 0.0895(2) 0.2370(2) 0.0330(7) Uani 1 d . .
C301 C 0.5604(9) 0.0358(10) 0.2072(8) 0.038(3) Uani 1 d . .
C302 C 0.4824(10) 0.0716(12) 0.1715(10) 0.050(4) Uani 1 d . .
H30A H 0.4999(10) 0.1310(12) 0.1662(10) 0.060 Uiso 1 calc R .
C303 C 0.3781(11) 0.0213(13) 0.1432(11) 0.058(4) Uani 1 d . .
H30B H 0.3265(11) 0.0471(13) 0.1183(11) 0.070 Uiso 1 calc R .
C304 C 0.3486(11) -0.0647(13) 0.1506(11) 0.058(4) Uani 1 d . .
H30C H 0.2780(11) -0.0987(13) 0.1294(11) 0.070 Uiso 1 calc R .
C305 C 0.4235(11) -0.1012(11) 0.1895(10) 0.050(4) Uani 1 d . .
H30D H 0.4035(11) -0.1588(11) 0.1976(10) 0.060 Uiso 1 calc R .
C306 C 0.5309(10) -0.0516(11) 0.2174(10) 0.046(3) Uani 1 d . .
H30E H 0.5823(10) -0.0771(11) 0.2427(10) 0.055 Uiso 1 calc R .
C4 C 0.7060(9) 0.2150(9) 0.2433(8) 0.035(3) Uani 1 d . .
C401 C 0.7322(11) 0.2462(10) 0.1736(8) 0.045(3) Uani 1 d . .
C402 C 0.6598(14) 0.2273(14) 0.1003(10) 0.063(5) Uani 1 d . .
H40A H 0.5912(14) 0.1921(14) 0.0916(10) 0.076 Uiso 1 calc R .
C403 C 0.6866(20) 0.2596(19) 0.0391(13) 0.089(7) Uani 1 d . .
H40B H 0.6354(20) 0.2454(19) -0.0105(13) 0.107 Uiso 1 calc R .
C404 C 0.7823(22) 0.3099(16) 0.0480(13) 0.090(7) Uani 1 d . .
H40C H 0.7972(22) 0.3335(16) 0.0066(13) 0.108 Uiso 1 calc R .
C405 C 0.8605(24) 0.3275(19) 0.1200(13) 0.141(15) Uani 1 d . .
H40D H 0.9289(24) 0.3625(19) 0.1276(13) 0.169 Uiso 1 calc R .
C406 C 0.8345(17) 0.2915(18) 0.1810(11) 0.100(9) Uani 1 d . .
H40E H 0.8877(17) 0.2985(18) 0.2274(11) 0.120 Uiso 1 calc R .
C5 C 0.6885(9) 0.2798(10) 0.3123(8) 0.039(3) Uani 1 d . .
C501 C 0.6850(11) 0.3790(10) 0.3154(9) 0.041(3) Uani 1 d . .
C502 C 0.5963(14) 0.3971(12) 0.2683(13) 0.066(5) Uani 1 d . .
H50A H 0.5371(14) 0.3479(12) 0.2379(13) 0.079 Uiso 1 calc R .
C503 C 0.5971(18) 0.4880(17) 0.2671(17) 0.092(7) Uani 1 d . .
H50B H 0.5398(18) 0.4994(17) 0.2339(17) 0.110 Uiso 1 calc R .
C504 C 0.6828(20) 0.5626(14) 0.3151(15) 0.081(6) Uani 1 d . .
H50C H 0.6803(20) 0.6247(14) 0.3174(15) 0.098 Uiso 1 calc R .
C505 C 0.7706(17) 0.5453(13) 0.3590(12) 0.071(5) Uani 1 d . .
H50D H 0.8304(17) 0.5946(13) 0.3872(12) 0.085 Uiso 1 calc R .
C506 C 0.7713(13) 0.4557(13) 0.3617(10) 0.058(4) Uani 1 d . .
H50E H 0.8299(13) 0.4455(13) 0.3947(10) 0.069 Uiso 1 calc R .
Os4 Os 0.79484(4) -0.00638(4) 0.14764(3) 0.03649(14) Uani 1 d . .
C41 C 0.8214(10) 0.0600(12) 0.0747(9) 0.045(3) Uani 1 d . .
O41 O 0.8410(10) 0.0944(10) 0.0277(8) 0.067(3) Uani 1 d . .
C42 C 0.9358(11) 0.0611(11) 0.2201(9) 0.044(3) Uani 1 d . .
O42 O 1.0167(7) 0.1038(9) 0.2586(6) 0.058(3) Uani 1 d . .
C43 C 0.6572(12) -0.0710(12) 0.0722(10) 0.057(4) Uani 1 d . .
O43 O 0.5753(9) -0.1005(10) 0.0255(8) 0.077(4) Uani 1 d . .
Os5 Os 0.80671(5) -0.17125(5) 0.20184(4) 0.0486(2) Uani 1 d . .
C51 C 0.7553(15) -0.1537(12) 0.3034(10) 0.060(4) Uani 1 d . .
O51 O 0.7303(12) -0.1457(10) 0.3635(8) 0.083(4) Uani 1 d . .
C52 C 0.6590(16) -0.2254(12) 0.1355(12) 0.061(4) Uani 1 d . .
O52 O 0.5734(10) -0.2560(9) 0.1025(9) 0.079(4) Uani 1 d . .
C53 C 0.9507(14) -0.1027(13) 0.2672(10) 0.061(4) Uani 1 d . .
O53 O 1.0344(10) -0.0676(11) 0.3099(8) 0.079(4) Uani 1 d . .
C54 C 0.8394(18) -0.2954(15) 0.1862(12) 0.075(5) Uani 1 d . .
O54 O 0.8649(18) -0.3662(12) 0.1798(12) 0.124(7) Uani 1 d . .
Os6 Os 0.87098(5) -0.16806(5) 0.05070(4) 0.0520(2) Uani 1 d . .
C61 C 0.9213(18) -0.2832(15) 0.0230(13) 0.079(6) Uani 1 d . .
O61 O 0.9565(16) -0.3495(12) 0.0092(13) 0.125(7) Uani 1 d . .
C62 C 0.8948(13) -0.1297(14) -0.0399(11) 0.062(4) Uani 1 d . .
O62 O 0.9070(13) -0.1085(14) -0.0963(11) 0.107(5) Uani 1 d . .
C63 C 0.7286(17) -0.2352(16) -0.0174(12) 0.083(6) Uani 1 d . .
O63 O 0.6494(14) -0.2764(15) -0.0599(11) 0.126(7) Uani 1 d . .
C64 C 1.0129(13) -0.0943(11) 0.1173(10) 0.050(4) Uani 1 d . .
O64 O 1.0955(9) -0.0545(9) 0.1541(8) 0.070(3) Uani 1 d . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Os Os -1.2165 7.6030 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C12 Os1 C11 89.1(8) . . ?
C12 Os1 C13 86.1(8) . . ?
C11 Os1 C13 173.3(7) . . ?
C12 Os1 P1 101.2(6) . . ?
C11 Os1 P1 95.5(4) . . ?
C13 Os1 P1 90.1(5) . . ?
C12 Os1 Os3 98.8(6) . . ?
C11 Os1 Os3 92.7(4) . . ?
C13 Os1 Os3 83.5(5) . . ?
P1 Os1 Os3 158.44(9) . . ?
C12 Os1 Os2 158.3(6) . . ?
C11 Os1 Os2 94.8(5) . . ?
C13 Os1 Os2 88.0(5) . . ?
P1 Os1 Os2 99.69(9) . . ?
Os3 Os1 Os2 59.67(2) . . ?
O11 C11 Os1 176.1(14) . . ?
O12 C12 Os1 177.4(19) . . ?
O13 C13 Os1 172.5(17) . . ?
C22 Os2 C21 99.2(7) . . ?
C22 Os2 C24 96.0(8) . . ?
C21 Os2 C24 87.4(8) . . ?
C22 Os2 C23 94.3(7) . . ?
C21 Os2 C23 91.5(7) . . ?
C24 Os2 C23 169.7(8) . . ?
C22 Os2 Os3 84.8(5) . . ?
C21 Os2 Os3 176.0(5) . . ?
C24 Os2 Os3 92.2(6) . . ?
C23 Os2 Os3 88.2(5) . . ?
C22 Os2 Os1 144.7(5) . . ?
C21 Os2 Os1 116.1(5) . . ?
C24 Os2 Os1 87.3(6) . . ?
C23 Os2 Os1 84.0(5) . . ?
Os3 Os2 Os1 59.93(3) . . ?
O21 C21 Os2 175.0(15) . . ?
O22 C22 Os2 177.1(16) . . ?
O23 C23 Os2 169.8(17) . . ?
O24 C24 Os2 169.5(17) . . ?
C33 Os3 C31 92.7(13) . . ?
C33 Os3 C34 90.7(12) . . ?
C31 Os3 C34 102.4(11) . . ?
C33 Os3 C32 173.7(11) . . ?
C31 Os3 C32 93.5(10) . . ?
C34 Os3 C32 88.8(9) . . ?
C33 Os3 Os2 90.9(8) . . ?
C31 Os3 Os2 154.2(9) . . ?
C34 Os3 Os2 103.1(7) . . ?
C32 Os3 Os2 83.1(5) . . ?
C33 Os3 Os1 83.6(8) . . ?
C31 Os3 Os1 94.7(8) . . ?
C34 Os3 Os1 162.2(8) . . ?
C32 Os3 Os1 95.1(5) . . ?
Os2 Os3 Os1 60.40(2) . . ?
O31 C31 Os3 177.0(28) . . ?
O32 C32 Os3 174.8(16) . . ?
O33 C33 Os3 171.4(26) . . ?
O34 C34 Os3 178.3(25) . . ?
C101 P1 C5 102.7(6) . . ?
C101 P1 P2 103.5(5) . . ?
C5 P1 P2 98.5(5) . . ?
C101 P1 Os1 107.0(4) . . ?
C5 P1 Os1 122.3(5) . . ?
P2 P1 Os1 120.3(2) . . ?
C102 C101 C106 119.1(13) . . ?
C102 C101 P1 120.3(12) . . ?
C106 C101 P1 120.4(10) . . ?
C101 C102 C103 121.2(16) . . ?
C102 C103 C104 119.8(16) . . ?
C105 C104 C103 119.1(16) . . ?
C104 C105 C106 122.0(17) . . ?
C105 C106 C101 118.6(14) . . ?
C201 P2 P3 101.0(4) . . ?
C201 P2 P1 103.3(5) . . ?
P3 P2 P1 93.1(2) . . ?
C206 C201 C202 119.6(13) . . ?
C206 C201 P2 125.2(11) . . ?
C202 C201 P2 115.2(12) . . ?
C203 C202 C201 120.0(16) . . ?
C204 C203 C202 120.8(16) . . ?
C203 C204 C205 121.2(15) . . ?
C206 C205 C204 119.5(19) . . ?
C205 C206 C201 118.7(17) . . ?
C301 P3 C4 102.9(6) . . ?
C301 P3 P2 99.7(4) . . ?
C4 P3 P2 98.6(4) . . ?
C301 P3 Os4 110.5(4) . . ?
C4 P3 Os4 120.5(4) . . ?
P2 P3 Os4 121.4(2) . . ?
C302 C301 C306 118.1(12) . . ?
C302 C301 P3 125.1(11) . . ?
C306 C301 P3 116.7(10) . . ?
C301 C302 C303 121.0(15) . . ?
C304 C303 C302 121.6(15) . . ?
C303 C304 C305 119.2(14) . . ?
C304 C305 C306 119.8(15) . . ?
C301 C306 C305 120.1(13) . . ?
C5 C4 C401 119.7(12) . . ?
C5 C4 P3 120.5(10) . . ?
C401 C4 P3 119.8(10) . . ?
C402 C401 C406 117.4(15) . . ?
C402 C401 C4 122.9(13) . . ?
C406 C401 C4 119.6(13) . . ?
C401 C402 C403 120.9(19) . . ?
C404 C403 C402 122.3(21) . . ?
C403 C404 C405 119.1(17) . . ?
C404 C405 C406 118.6(20) . . ?
C401 C406 C405 121.3(20) . . ?
C4 C5 C501 120.4(12) . . ?
C4 C5 P1 119.6(10) . . ?
C501 C5 P1 120.0(10) . . ?
C506 C501 C502 118.2(14) . . ?
C506 C501 C5 121.4(13) . . ?
C502 C501 C5 120.3(13) . . ?
C503 C502 C501 119.8(18) . . ?
C502 C503 C504 120.5(20) . . ?
C505 C504 C503 120.2(18) . . ?
C504 C505 C506 120.2(18) . . ?
C505 C506 C501 120.9(17) . . ?
C41 Os4 C43 88.9(7) . . ?
C41 Os4 C42 88.5(6) . . ?
C43 Os4 C42 177.4(7) . . ?
C41 Os4 P3 104.0(4) . . ?
C43 Os4 P3 87.7(5) . . ?
C42 Os4 P3 93.4(4) . . ?
C41 Os4 Os6 91.4(4) . . ?
C43 Os4 Os6 85.1(5) . . ?
C42 Os4 Os6 94.5(4) . . ?
P3 Os4 Os6 162.93(9) . . ?
C41 Os4 Os5 150.6(4) . . ?
C43 Os4 Os5 91.0(6) . . ?
C42 Os4 Os5 90.9(5) . . ?
P3 Os4 Os5 105.43(8) . . ?
Os6 Os4 Os5 59.37(2) . . ?
O41 C41 Os4 174.7(14) . . ?
O42 C42 Os4 175.2(14) . . ?
O43 C43 Os4 172.6(17) . . ?
C54 Os5 C51 98.4(8) . . ?
C54 Os5 C53 93.7(9) . . ?
C51 Os5 C53 91.1(7) . . ?
C54 Os5 C52 93.0(8) . . ?
C51 Os5 C52 89.2(7) . . ?
C53 Os5 C52 173.2(7) . . ?
C54 Os5 Os6 91.2(6) . . ?
C51 Os5 Os6 170.3(5) . . ?
C53 Os5 Os6 89.5(5) . . ?
C52 Os5 Os6 89.0(5) . . ?
C54 Os5 Os4 150.9(6) . . ?
C51 Os5 Os4 110.6(5) . . ?
C53 Os5 Os4 86.7(6) . . ?
C52 Os5 Os4 86.8(5) . . ?
Os6 Os5 Os4 59.72(2) . . ?
O51 C51 Os5 176.1(16) . . ?
O52 C52 Os5 175.5(17) . . ?
O53 C53 Os5 173.8(17) . . ?
O54 C54 Os5 175.9(22) . . ?
C62 Os6 C61 99.6(9) . . ?
C62 Os6 C63 87.6(8) . . ?
C61 Os6 C63 91.2(10) . . ?
C62 Os6 C64 90.2(7) . . ?
C61 Os6 C64 91.5(8) . . ?
C63 Os6 C64 176.7(9) . . ?
C62 Os6 Os5 161.4(6) . . ?
C61 Os6 Os5 99.0(7) . . ?
C63 Os6 Os5 91.3(6) . . ?
C64 Os6 Os5 90.1(4) . . ?
C62 Os6 Os4 100.6(6) . . ?
C61 Os6 Os4 159.5(7) . . ?
C63 Os6 Os4 93.3(6) . . ?
C64 Os6 Os4 84.8(4) . . ?
Os5 Os6 Os4 60.90(2) . . ?
O61 C61 Os6 176.4(21) . . ?
O62 C62 Os6 178.1(18) . . ?
O63 C63 Os6 176.1(19) . . ?
O64 C64 Os6 177.6(13) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Os1 C12 1.89(2) . ?
Os1 C11 1.93(2) . ?
Os1 C13 1.99(2) . ?
Os1 P1 2.367(3) . ?
Os1 Os3 2.8974(10) . ?
Os1 Os2 2.9111(9) . ?
C11 O11 1.16(2) . ?
C12 O12 1.13(2) . ?
C13 O13 1.15(2) . ?
Os2 C22 1.89(2) . ?
Os2 C21 1.92(2) . ?
Os2 C24 1.94(2) . ?
Os2 C23 1.98(2) . ?
Os2 Os3 2.8898(11) . ?
C21 O21 1.13(2) . ?
C22 O22 1.15(2) . ?
C23 O23 1.10(2) . ?
C24 O24 1.14(2) . ?
Os3 C33 1.80(4) . ?
Os3 C31 1.89(2) . ?
Os3 C34 1.90(2) . ?
Os3 C32 1.99(2) . ?
C31 O31 1.16(3) . ?
C32 O32 1.12(2) . ?
C33 O33 1.23(4) . ?
C34 O34 1.16(2) . ?
P1 C101 1.827(13) . ?
P1 C5 1.875(13) . ?
P1 P2 2.226(5) . ?
C101 C102 1.38(2) . ?
C101 C106 1.42(2) . ?
C102 C103 1.39(2) . ?
C103 C104 1.41(3) . ?
C104 C105 1.36(3) . ?
C105 C106 1.40(2) . ?
P2 C201 1.838(14) . ?
P2 P3 2.217(5) . ?
C201 C206 1.41(2) . ?
C201 C202 1.42(2) . ?
C202 C203 1.39(2) . ?
C203 C204 1.33(3) . ?
C204 C205 1.43(3) . ?
C205 C206 1.41(2) . ?
P3 C301 1.830(12) . ?
P3 C4 1.856(12) . ?
P3 Os4 2.365(3) . ?
C301 C302 1.36(2) . ?
C301 C306 1.39(2) . ?
C302 C303 1.37(2) . ?
C303 C304 1.35(2) . ?
C304 C305 1.36(2) . ?
C305 C306 1.40(2) . ?
C4 C5 1.36(2) . ?
C4 C401 1.50(2) . ?
C401 C402 1.36(2) . ?
C401 C406 1.37(2) . ?
C402 C403 1.37(2) . ?
C403 C404 1.31(3) . ?
C404 C405 1.39(3) . ?
C405 C406 1.40(3) . ?
C5 C501 1.49(2) . ?
C501 C506 1.40(2) . ?
C501 C502 1.40(2) . ?
C502 C503 1.37(3) . ?
C503 C504 1.38(3) . ?
C504 C505 1.36(3) . ?
C505 C506 1.37(2) . ?
Os4 C41 1.89(2) . ?
Os4 C43 1.93(2) . ?
Os4 C42 1.951(14) . ?
Os4 Os6 2.9001(10) . ?
Os4 Os5 2.9343(11) . ?
C41 O41 1.14(2) . ?
C42 O42 1.12(2) . ?
C43 O43 1.15(2) . ?
Os5 C54 1.92(2) . ?
Os5 C51 1.94(2) . ?
Os5 C53 1.95(2) . ?
Os5 C52 1.96(2) . ?
Os5 Os6 2.8897(9) . ?
C51 O51 1.12(2) . ?
C52 O52 1.11(2) . ?
C53 O53 1.15(2) . ?
C54 O54 1.14(2) . ?
Os6 C62 1.89(2) . ?
Os6 C61 1.89(2) . ?
Os6 C63 1.94(2) . ?
Os6 C64 1.95(2) . ?
C61 O61 1.13(2) . ?
C62 O62 1.15(2) . ?
C63 O63 1.12(2) . ?
C64 O64 1.12(2) . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C12 Os1 C11 O11 15.8(190) . . . . ?
C13 Os1 C11 O11 -28.5(222) . . . . ?
P1 Os1 C11 O11 117.0(189) . . . . ?
Os3 Os1 C11 O11 -83.0(190) . . . . ?
Os2 Os1 C11 O11 -142.8(189) . . . . ?
C11 Os1 C12 O12 -88.1(437) . . . . ?
C13 Os1 C12 O12 87.2(437) . . . . ?
P1 Os1 C12 O12 176.5(436) . . . . ?
Os3 Os1 C12 O12 4.4(438) . . . . ?
Os2 Os1 C12 O12 12.6(450) . . . . ?
C12 Os1 C13 O13 8.0(120) . . . . ?
C11 Os1 C13 O13 52.3(154) . . . . ?
P1 Os1 C13 O13 -93.3(121) . . . . ?
Os3 Os1 C13 O13 107.3(121) . . . . ?
Os2 Os1 C13 O13 167.0(121) . . . . ?
C12 Os1 Os2 C22 -12.0(19) . . . . ?
C11 Os1 Os2 C22 87.7(10) . . . . ?
C13 Os1 Os2 C22 -86.1(10) . . . . ?
P1 Os1 Os2 C22 -175.9(9) . . . . ?
Os3 Os1 Os2 C22 -2.5(9) . . . . ?
C12 Os1 Os2 C21 170.4(18) . . . . ?
C11 Os1 Os2 C21 -89.9(7) . . . . ?
C13 Os1 Os2 C21 96.3(7) . . . . ?
P1 Os1 Os2 C21 6.5(5) . . . . ?
Os3 Os1 Os2 C21 179.8(5) . . . . ?
C12 Os1 Os2 C24 84.7(18) . . . . ?
C11 Os1 Os2 C24 -175.6(7) . . . . ?
C13 Os1 Os2 C24 10.5(8) . . . . ?
P1 Os1 Os2 C24 -79.2(6) . . . . ?
Os3 Os1 Os2 C24 94.1(6) . . . . ?
C12 Os1 Os2 C23 -100.9(18) . . . . ?
C11 Os1 Os2 C23 -1.2(6) . . . . ?
C13 Os1 Os2 C23 -175.0(7) . . . . ?
P1 Os1 Os2 C23 95.2(5) . . . . ?
Os3 Os1 Os2 C23 -91.4(5) . . . . ?
C12 Os1 Os2 Os3 -9.4(17) . . . . ?
C11 Os1 Os2 Os3 90.3(4) . . . . ?
C13 Os1 Os2 Os3 -83.6(5) . . . . ?
P1 Os1 Os2 Os3 -173.34(8) . . . . ?
Os3 Os1 Os2 Os3 0.0 . . . . ?
C22 Os2 C21 O21 2.2(168) . . . . ?
C24 Os2 C21 O21 -93.5(167) . . . . ?
C23 Os2 C21 O21 96.8(167) . . . . ?
Os3 Os2 C21 O21 -177.2(110) . . . . ?
Os1 Os2 C21 O21 -179.2(1000) . . . . ?
C21 Os2 C22 O22 109.9(298) . . . . ?
C24 Os2 C22 O22 -161.8(298) . . . . ?
C23 Os2 C22 O22 17.7(299) . . . . ?
Os3 Os2 C22 O22 -70.1(298) . . . . ?
Os1 Os2 C22 O22 -67.9(301) . . . . ?
C22 Os2 C23 O23 65.8(90) . . . . ?
C21 Os2 C23 O23 -33.5(90) . . . . ?
C24 Os2 C23 O23 -116.9(90) . . . . ?
Os3 Os2 C23 O23 150.4(90) . . . . ?
Os1 Os2 C23 O23 -149.6(90) . . . . ?
C22 Os2 C24 O24 -89.0(95) . . . . ?
C21 Os2 C24 O24 10.0(95) . . . . ?
C23 Os2 C24 O24 93.7(102) . . . . ?
Os3 Os2 C24 O24 -174.0(95) . . . . ?
Os1 Os2 C24 O24 126.3(95) . . . . ?
C22 Os2 Os3 C33 96.5(11) . . . . ?
C21 Os2 Os3 C33 -84.1(70) . . . . ?
C24 Os2 Os3 C33 -167.7(12) . . . . ?
C23 Os2 Os3 C33 2.0(11) . . . . ?
Os1 Os2 Os3 C33 -82.1(10) . . . . ?
C22 Os2 Os3 C31 -165.3(19) . . . . ?
C21 Os2 Os3 C31 14.1(72) . . . . ?
C24 Os2 Os3 C31 -69.5(19) . . . . ?
C23 Os2 Os3 C31 100.2(19) . . . . ?
Os1 Os2 Os3 C31 16.1(19) . . . . ?
C22 Os2 Os3 C34 5.5(9) . . . . ?
C21 Os2 Os3 C34 -175.0(69) . . . . ?
C24 Os2 Os3 C34 101.4(10) . . . . ?
C23 Os2 Os3 C34 -88.9(9) . . . . ?
Os1 Os2 Os3 C34 -173.0(8) . . . . ?
C22 Os2 Os3 C32 -81.6(7) . . . . ?
C21 Os2 Os3 C32 97.8(69) . . . . ?
C24 Os2 Os3 C32 14.2(8) . . . . ?
C23 Os2 Os3 C32 -176.1(7) . . . . ?
Os1 Os2 Os3 C32 99.8(5) . . . . ?
C22 Os2 Os3 Os1 178.5(5) . . . . ?
C21 Os2 Os3 Os1 -2.0(69) . . . . ?
C24 Os2 Os3 Os1 -85.6(6) . . . . ?
C23 Os2 Os3 Os1 84.1(5) . . . . ?
Os1 Os2 Os3 Os1 0.0 . . . . ?
C12 Os1 Os3 C33 -88.8(12) . . . . ?
C11 Os1 Os3 C33 0.8(11) . . . . ?
C13 Os1 Os3 C33 -173.7(11) . . . . ?
P1 Os1 Os3 C33 112.9(10) . . . . ?
Os2 Os1 Os3 C33 94.7(10) . . . . ?
C12 Os1 Os3 C31 3.4(11) . . . . ?
C11 Os1 Os3 C31 93.0(10) . . . . ?
C13 Os1 Os3 C31 -81.5(10) . . . . ?
P1 Os1 Os3 C31 -154.9(9) . . . . ?
Os2 Os1 Os3 C31 -173.0(9) . . . . ?
C12 Os1 Os3 C34 -160.6(25) . . . . ?
C11 Os1 Os3 C34 -71.1(24) . . . . ?
C13 Os1 Os3 C34 114.5(24) . . . . ?
P1 Os1 Os3 C34 41.1(24) . . . . ?
Os2 Os1 Os3 C34 22.9(24) . . . . ?
C12 Os1 Os3 C32 97.4(8) . . . . ?
C11 Os1 Os3 C32 -173.1(7) . . . . ?
C13 Os1 Os3 C32 12.4(7) . . . . ?
P1 Os1 Os3 C32 -61.0(5) . . . . ?
Os2 Os1 Os3 C32 -79.1(5) . . . . ?
C12 Os1 Os3 Os2 176.5(6) . . . . ?
C11 Os1 Os3 Os2 -94.0(5) . . . . ?
C13 Os1 Os3 Os2 91.5(5) . . . . ?
P1 Os1 Os3 Os2 18.1(2) . . . . ?
Os2 Os1 Os3 Os2 0.0 . . . . ?
C33 Os3 C31 O31 -58.8(435) . . . . ?
C34 Os3 C31 O31 32.5(436) . . . . ?
C32 Os3 C31 O31 122.0(434) . . . . ?
Os2 Os3 C31 O31 -156.6(422) . . . . ?
Os1 Os3 C31 O31 -142.6(434) . . . . ?
C33 Os3 C32 O32 118.4(182) . . . . ?
C31 Os3 C32 O32 -69.5(178) . . . . ?
C34 Os3 C32 O32 32.8(177) . . . . ?
Os2 Os3 C32 O32 136.2(178) . . . . ?
Os1 Os3 C32 O32 -164.5(177) . . . . ?
C31 Os3 C33 O33 102.1(180) . . . . ?
C34 Os3 C33 O33 -0.3(180) . . . . ?
C32 Os3 C33 O33 -85.7(172) . . . . ?
Os2 Os3 C33 O33 -103.4(179) . . . . ?
Os1 Os3 C33 O33 -163.4(180) . . . . ?
C33 Os3 C34 O34 -25.1(684) . . . . ?
C31 Os3 C34 O34 -118.0(684) . . . . ?
C32 Os3 C34 O34 148.7(684) . . . . ?
Os2 Os3 C34 O34 66.0(685) . . . . ?
Os1 Os3 C34 O34 45.7(696) . . . . ?
C12 Os1 P1 C101 -80.4(8) . . . . ?
C11 Os1 P1 C101 -170.5(7) . . . . ?
C13 Os1 P1 C101 5.6(7) . . . . ?
Os3 Os1 P1 C101 77.8(5) . . . . ?
Os2 Os1 P1 C101 93.6(5) . . . . ?
C12 Os1 P1 C5 37.4(8) . . . . ?
C11 Os1 P1 C5 -52.8(7) . . . . ?
C13 Os1 P1 C5 123.4(7) . . . . ?
Os3 Os1 P1 C5 -164.4(4) . . . . ?
Os2 Os1 P1 C5 -148.6(5) . . . . ?
C12 Os1 P1 P2 162.2(6) . . . . ?
C11 Os1 P1 P2 72.0(5) . . . . ?
C13 Os1 P1 P2 -111.8(5) . . . . ?
Os3 Os1 P1 P2 -39.6(3) . . . . ?
Os2 Os1 P1 P2 -23.8(2) . . . . ?
C5 P1 C101 C102 -51.7(13) . . . . ?
P2 P1 C101 C102 -153.8(12) . . . . ?
Os1 P1 C101 C102 78.2(12) . . . . ?
C5 P1 C101 C106 134.4(12) . . . . ?
P2 P1 C101 C106 32.3(12) . . . . ?
Os1 P1 C101 C106 -95.7(12) . . . . ?
C106 C101 C102 C103 0.4(24) . . . . ?
P1 C101 C102 C103 -173.6(14) . . . . ?
C101 C102 C103 C104 -2.9(28) . . . . ?
C102 C103 C104 C105 3.0(30) . . . . ?
C103 C104 C105 C106 -0.7(30) . . . . ?
C104 C105 C106 C101 -1.7(27) . . . . ?
C102 C101 C106 C105 1.8(23) . . . . ?
P1 C101 C106 C105 175.8(13) . . . . ?
C101 P1 P2 C201 -178.6(6) . . . . ?
C5 P1 P2 C201 76.0(6) . . . . ?
Os1 P1 P2 C201 -59.4(5) . . . . ?
C101 P1 P2 P3 79.3(5) . . . . ?
C5 P1 P2 P3 -26.1(4) . . . . ?
Os1 P1 P2 P3 -161.5(2) . . . . ?
P3 P2 C201 C206 64.3(12) . . . . ?
P1 P2 C201 C206 -31.6(13) . . . . ?
P3 P2 C201 C202 -115.6(10) . . . . ?
P1 P2 C201 C202 148.4(9) . . . . ?
C206 C201 C202 C203 1.6(21) . . . . ?
P2 C201 C202 C203 -178.4(11) . . . . ?
C201 C202 C203 C204 -1.7(24) . . . . ?
C202 C203 C204 C205 -0.3(27) . . . . ?
C203 C204 C205 C206 2.2(26) . . . . ?
C204 C205 C206 C201 -2.1(23) . . . . ?
C202 C201 C206 C205 0.3(21) . . . . ?
P2 C201 C206 C205 -179.7(11) . . . . ?
C201 P2 P3 C301 177.9(6) . . . . ?
P1 P2 P3 C301 -77.9(5) . . . . ?
C201 P2 P3 C4 -77.3(6) . . . . ?
P1 P2 P3 C4 26.9(4) . . . . ?
C201 P2 P3 Os4 56.5(5) . . . . ?
P1 P2 P3 Os4 160.7(2) . . . . ?
C4 P3 C301 C302 19.7(14) . . . . ?
P2 P3 C301 C302 121.0(13) . . . . ?
Os4 P3 C301 C302 -110.1(13) . . . . ?
C4 P3 C301 C306 -164.6(11) . . . . ?
P2 P3 C301 C306 -63.3(11) . . . . ?
Os4 P3 C301 C306 65.6(11) . . . . ?
C306 C301 C302 C303 -2.6(23) . . . . ?
P3 C301 C302 C303 173.1(12) . . . . ?
C301 C302 C303 C304 0.9(27) . . . . ?
C302 C303 C304 C305 2.1(27) . . . . ?
C303 C304 C305 C306 -3.2(25) . . . . ?
C302 C301 C306 C305 1.3(21) . . . . ?
P3 C301 C306 C305 -174.7(11) . . . . ?
C304 C305 C306 C301 1.6(23) . . . . ?
C301 P3 C4 C5 79.9(11) . . . . ?
P2 P3 C4 C5 -22.3(11) . . . . ?
Os4 P3 C4 C5 -156.7(9) . . . . ?
C301 P3 C4 C401 -102.9(10) . . . . ?
P2 P3 C4 C401 154.9(9) . . . . ?
Os4 P3 C4 C401 20.5(12) . . . . ?
C5 C4 C401 C402 -103.3(18) . . . . ?
P3 C4 C401 C402 79.5(18) . . . . ?
C5 C4 C401 C406 80.2(22) . . . . ?
P3 C4 C401 C406 -97.0(19) . . . . ?
C406 C401 C402 C403 -5.2(30) . . . . ?
C4 C401 C402 C403 178.3(17) . . . . ?
C401 C402 C403 C404 -0.1(35) . . . . ?
C402 C403 C404 C405 3.0(40) . . . . ?
C403 C404 C405 C406 -0.5(44) . . . . ?
C402 C401 C406 C405 7.7(36) . . . . ?
C4 C401 C406 C405 -175.6(23) . . . . ?
C404 C405 C406 C401 -5.0(45) . . . . ?
C401 C4 C5 C501 5.8(18) . . . . ?
P3 C4 C5 C501 -176.9(9) . . . . ?
C401 C4 C5 P1 -175.1(9) . . . . ?
P3 C4 C5 P1 2.1(15) . . . . ?
C101 P1 C5 C4 -86.8(11) . . . . ?
P2 P1 C5 C4 19.2(11) . . . . ?
Os1 P1 C5 C4 153.4(9) . . . . ?
C101 P1 C5 C501 92.2(11) . . . . ?
P2 P1 C5 C501 -161.8(9) . . . . ?
Os1 P1 C5 C501 -27.5(12) . . . . ?
C4 C5 C501 C506 -103.2(16) . . . . ?
P1 C5 C501 C506 77.8(15) . . . . ?
C4 C5 C501 C502 73.5(18) . . . . ?
P1 C5 C501 C502 -105.5(15) . . . . ?
C506 C501 C502 C503 1.4(26) . . . . ?
C5 C501 C502 C503 -175.5(17) . . . . ?
C501 C502 C503 C504 -2.9(33) . . . . ?
C502 C503 C504 C505 5.0(35) . . . . ?
C503 C504 C505 C506 -5.6(32) . . . . ?
C504 C505 C506 C501 4.1(27) . . . . ?
C502 C501 C506 C505 -2.0(24) . . . . ?
C5 C501 C506 C505 174.9(15) . . . . ?
C301 P3 Os4 C41 103.7(6) . . . . ?
C4 P3 Os4 C41 -16.0(6) . . . . ?
P2 P3 Os4 C41 -140.3(4) . . . . ?
C301 P3 Os4 C43 15.4(7) . . . . ?
C4 P3 Os4 C43 -104.4(7) . . . . ?
P2 P3 Os4 C43 131.4(6) . . . . ?
C301 P3 Os4 C42 -166.9(7) . . . . ?
C4 P3 Os4 C42 73.3(7) . . . . ?
P2 P3 Os4 C42 -50.9(5) . . . . ?
C301 P3 Os4 Os6 -49.4(6) . . . . ?
C4 P3 Os4 Os6 -169.1(5) . . . . ?
P2 P3 Os4 Os6 66.6(3) . . . . ?
C301 P3 Os4 Os5 -75.1(5) . . . . ?
C4 P3 Os4 Os5 165.2(5) . . . . ?
P2 P3 Os4 Os5 41.0(2) . . . . ?
C43 Os4 C41 O41 -91.4(136) . . . . ?
C42 Os4 C41 O41 88.1(136) . . . . ?
P3 Os4 C41 O41 -178.7(135) . . . . ?
Os6 Os4 C41 O41 -6.4(136) . . . . ?
Os5 Os4 C41 O41 -1.2(142) . . . . ?
C41 Os4 C42 O42 13.9(144) . . . . ?
C43 Os4 C42 O42 25.2(250) . . . . ?
P3 Os4 C42 O42 -90.0(144) . . . . ?
Os6 Os4 C42 O42 105.2(144) . . . . ?
Os5 Os4 C42 O42 164.5(144) . . . . ?
C41 Os4 C43 O43 -32.9(109) . . . . ?
C42 Os4 C43 O43 -44.2(214) . . . . ?
P3 Os4 C43 O43 71.1(108) . . . . ?
Os6 Os4 C43 O43 -124.4(109) . . . . ?
Os5 Os4 C43 O43 176.5(108) . . . . ?
C41 Os4 Os5 C54 -6.4(16) . . . . ?
C43 Os4 Os5 C54 83.3(15) . . . . ?
C42 Os4 Os5 C54 -95.0(14) . . . . ?
P3 Os4 Os5 C54 171.2(14) . . . . ?
Os6 Os4 Os5 C54 -0.3(14) . . . . ?
C41 Os4 Os5 C51 175.3(10) . . . . ?
C43 Os4 Os5 C51 -95.0(7) . . . . ?
C42 Os4 Os5 C51 86.6(7) . . . . ?
P3 Os4 Os5 C51 -7.2(6) . . . . ?
Os6 Os4 Os5 C51 -178.7(6) . . . . ?
C41 Os4 Os5 C53 85.3(9) . . . . ?
C43 Os4 Os5 C53 175.0(6) . . . . ?
C42 Os4 Os5 C53 -3.3(6) . . . . ?
P3 Os4 Os5 C53 -97.1(5) . . . . ?
Os6 Os4 Os5 C53 91.4(5) . . . . ?
C41 Os4 Os5 C52 -96.8(9) . . . . ?
C43 Os4 Os5 C52 -7.1(7) . . . . ?
C42 Os4 Os5 C52 174.6(6) . . . . ?
P3 Os4 Os5 C52 80.8(5) . . . . ?
Os6 Os4 Os5 C52 -90.7(5) . . . . ?
C41 Os4 Os5 Os6 -6.1(8) . . . . ?
C43 Os4 Os5 Os6 83.6(4) . . . . ?
C42 Os4 Os5 Os6 -94.7(4) . . . . ?
P3 Os4 Os5 Os6 171.50(8) . . . . ?
Os6 Os4 Os5 Os6 0.0 . . . . ?
C54 Os5 C51 O51 42.4(240) . . . . ?
C53 Os5 C51 O51 -51.6(239) . . . . ?
C52 Os5 C51 O51 135.3(239) . . . . ?
Os6 Os5 C51 O51 -145.3(217) . . . . ?
Os4 Os5 C51 O51 -138.4(238) . . . . ?
C54 Os5 C52 O52 90.4(201) . . . . ?
C51 Os5 C52 O52 -8.0(201) . . . . ?
C53 Os5 C52 O52 -100.9(203) . . . . ?
Os6 Os5 C52 O52 -178.5(1000) . . . . ?
Os4 Os5 C52 O52 -118.7(201) . . . . ?
C54 Os5 C53 O53 -49.6(134) . . . . ?
C51 Os5 C53 O53 49.0(134) . . . . ?
C52 Os5 C53 O53 141.7(120) . . . . ?
Os6 Os5 C53 O53 -140.7(134) . . . . ?
Os4 Os5 C53 O53 159.6(134) . . . . ?
C51 Os5 C54 O54 -91.2(255) . . . . ?
C53 Os5 C54 O54 0.5(255) . . . . ?
C52 Os5 C54 O54 179.2(1000) . . . . ?
Os6 Os5 C54 O54 90.1(255) . . . . ?
Os4 Os5 C54 O54 90.4(254) . . . . ?
C54 Os5 Os6 C62 173.0(17) . . . . ?
C51 Os5 Os6 C62 0.6(35) . . . . ?
C53 Os5 Os6 C62 -93.3(17) . . . . ?
C52 Os5 Os6 C62 80.0(17) . . . . ?
Os4 Os5 Os6 C62 -6.9(16) . . . . ?
C54 Os5 Os6 C61 -4.6(9) . . . . ?
C51 Os5 Os6 C61 -177.0(32) . . . . ?
C53 Os5 Os6 C61 89.1(9) . . . . ?
C52 Os5 Os6 C61 -97.6(8) . . . . ?
Os4 Os5 Os6 C61 175.6(7) . . . . ?
C54 Os5 Os6 C63 86.8(10) . . . . ?
C51 Os5 Os6 C63 -85.6(32) . . . . ?
C53 Os5 Os6 C63 -179.5(9) . . . . ?
C52 Os5 Os6 C63 -6.2(9) . . . . ?
Os4 Os5 Os6 C63 -93.1(7) . . . . ?
C54 Os5 Os6 C64 -96.2(8) . . . . ?
C51 Os5 Os6 C64 91.4(31) . . . . ?
C53 Os5 Os6 C64 -2.5(7) . . . . ?
C52 Os5 Os6 C64 170.9(7) . . . . ?
Os4 Os5 Os6 C64 84.0(4) . . . . ?
C54 Os5 Os6 Os4 179.9(7) . . . . ?
C51 Os5 Os6 Os4 7.4(31) . . . . ?
C53 Os5 Os6 Os4 -86.4(5) . . . . ?
C52 Os5 Os6 Os4 86.9(5) . . . . ?
Os4 Os5 Os6 Os4 0.0 . . . . ?
C41 Os4 Os6 C62 -5.2(6) . . . . ?
C43 Os4 Os6 C62 83.6(7) . . . . ?
C42 Os4 Os6 C62 -93.9(7) . . . . ?
P3 Os4 Os6 C62 148.7(6) . . . . ?
Os5 Os4 Os6 C62 177.8(5) . . . . ?
C41 Os4 Os6 C61 164.4(19) . . . . ?
C43 Os4 Os6 C61 -106.7(20) . . . . ?
C42 Os4 Os6 C61 75.8(20) . . . . ?
P3 Os4 Os6 C61 -41.6(19) . . . . ?
Os5 Os4 Os6 C61 -12.6(19) . . . . ?
C41 Os4 Os6 C63 -93.4(8) . . . . ?
C43 Os4 Os6 C63 -4.5(9) . . . . ?
C42 Os4 Os6 C63 178.0(8) . . . . ?
P3 Os4 Os6 C63 60.6(7) . . . . ?
Os5 Os4 Os6 C63 89.6(7) . . . . ?
C41 Os4 Os6 C64 84.0(6) . . . . ?
C43 Os4 Os6 C64 172.8(7) . . . . ?
C42 Os4 Os6 C64 -4.7(6) . . . . ?
P3 Os4 Os6 C64 -122.1(5) . . . . ?
Os5 Os4 Os6 C64 -93.1(5) . . . . ?
C41 Os4 Os6 Os5 177.0(4) . . . . ?
C43 Os4 Os6 Os5 -94.1(5) . . . . ?
C42 Os4 Os6 Os5 88.4(4) . . . . ?
P3 Os4 Os6 Os5 -29.0(3) . . . . ?
Os5 Os4 Os6 Os5 0.0 . . . . ?
C62 Os6 C61 O61 96.3(346) . . . . ?
C63 Os6 C61 O61 -176.0(1000) . . . . ?
C64 Os6 C61 O61 5.9(346) . . . . ?
Os5 Os6 C61 O61 -84.5(346) . . . . ?
Os4 Os6 C61 O61 -73.4(351) . . . . ?
C61 Os6 C62 O62 68.8(509) . . . . ?
C63 Os6 C62 O62 -22.0(508) . . . . ?
C64 Os6 C62 O62 160.4(508) . . . . ?
Os5 Os6 C62 O62 -108.7(506) . . . . ?
Os4 Os6 C62 O62 -114.9(508) . . . . ?
C62 Os6 C63 O63 55.3(358) . . . . ?
C61 Os6 C63 O63 -44.2(358) . . . . ?
C64 Os6 C63 O63 101.5(366) . . . . ?
Os5 Os6 C63 O63 -143.3(358) . . . . ?
Os4 Os6 C63 O63 155.8(358) . . . . ?
C62 Os6 C64 O64 -81.0(356) . . . . ?
C61 Os6 C64 O64 18.6(356) . . . . ?
C63 Os6 C64 O64 -127.1(337) . . . . ?
Os5 Os6 C64 O64 117.7(355) . . . . ?
Os4 Os6 C64 O64 178.4(1000) . . . . ?
