#------------------------------------------------------------------------------
#$Date: 2016-03-25 11:39:42 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179801 $
#$URL: svn://www.crystallography.net/cod/cif/7/00/97/7009718.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7009718
loop_
_publ_author_name
'Carlucci, Lucia'
'Ciani, Gianfranco'
'Proserpio, Davide M.'
'Rizzato, Silvia'
_publ_section_title
;
 New examples of self-catenation in two three-dimensional polymeric
 co-ordination networks †
;
_journal_issue                   21
_journal_name_full
'Journal of the Chemical Society, Dalton Transactions'
_journal_page_first              3821
_journal_paper_doi               10.1039/b003092i
_journal_year                    2000
_chemical_formula_sum            'C12 H16 Ag F6 N4 Sb'
_chemical_formula_weight         559.91
_space_group_IT_number           9
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  'C -2yc'
_symmetry_space_group_name_H-M   'C 1 c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_cell_angle_alpha                90.00
_cell_angle_beta                 116.022(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            16
_cell_length_a                   16.9700(10)
_cell_length_b                   29.369(2)
_cell_length_c                   16.5520(10)
_cell_measurement_reflns_used    8192
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      25
_cell_measurement_theta_min      2
_cell_volume                     7413.1(8)
_computing_molecular_graphics    SCHAKAL
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    SIR97
_diffrn_ambient_temperature      293(2)
_diffrn_detector_type            CCD_plate
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device       SMART
_diffrn_measurement_method       omega-scan
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0261
_diffrn_reflns_av_sigmaI/netI    0.0272
_diffrn_reflns_limit_h_max       20
_diffrn_reflns_limit_h_min       -20
_diffrn_reflns_limit_k_max       34
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       19
_diffrn_reflns_limit_l_min       -19
_diffrn_reflns_number            41931
_diffrn_reflns_theta_full        25.05
_diffrn_reflns_theta_max         25.05
_diffrn_reflns_theta_min         1.50
_diffrn_standards_decay_%        0
_exptl_absorpt_coefficient_mu    2.572
_exptl_absorpt_correction_T_max  1.00
_exptl_absorpt_correction_T_min  0.78
_exptl_absorpt_correction_type   sadabs
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    2.007
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       cubic-like
_exptl_crystal_F_000             4288
_exptl_crystal_size_max          0.15
_exptl_crystal_size_mid          0.12
_exptl_crystal_size_min          0.13
_refine_diff_density_max         0.720
_refine_diff_density_min         -0.645
_refine_diff_density_rms         0.112
_refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881'
_refine_ls_abs_structure_Flack   0.02(3)
_refine_ls_extinction_coef       0.00034(3)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_all   0.963
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     677
_refine_ls_number_reflns         13079
_refine_ls_number_restraints     1462
_refine_ls_restrained_S_all      1.020
_refine_ls_R_factor_all          0.0575
_refine_ls_R_factor_obs          0.0466
_refine_ls_shift/su_max          0.005
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0939P)²] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_all         0.1312
_refine_ls_wR_factor_obs         0.1253
_reflns_number_observed          10296
_reflns_number_total             13079
_reflns_observed_criterion       >2sigma(I)
_cod_data_source_file            b003092i.txt
_cod_data_source_block           1
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      'C c (#9)'
_cod_database_code               7009718
#BEGIN Tags that were not found in dictionaries:
_exptl_absorpt_correction_nazim  3.2
_diffrn_measurement_domega       0.30
_diffrn_measurement_rtime        20
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'x, -y, z+1/2'
'x+1/2, y+1/2, z'
'x+1/2, -y+1/2, z+1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag -0.94694(5) -0.14397(2) -0.71648(5) 0.0673(2) Uani 1 1 d . . .
Ag2 Ag -0.53089(5) -0.61103(3) -0.20003(5) 0.0726(2) Uani 1 1 d . . .
Ag3 Ag -1.05331(5) -0.35316(2) -0.54658(5) 0.0722(2) Uani 1 1 d . . .
Ag4 Ag -0.96980(5) -0.60050(3) -0.57086(5) 0.0700(2) Uani 1 1 d . . .
N11 N -0.6110(5) -0.1220(3) -0.5999(5) 0.0648(19) Uani 1 1 d . . .
C12 C -0.6481(7) -0.1145(4) -0.5462(6) 0.081(3) Uani 1 1 d D . .
C13 C -0.7391(7) -0.1211(4) -0.5774(7) 0.080(3) Uani 1 1 d . . .
H13 H -0.7645 -0.1147 -0.5390 0.096 Uiso 1 1 calc R . .
N14 N -0.7897(5) -0.1360(3) -0.6596(6) 0.0670(19) Uani 1 1 d . . .
C15 C -0.7494(7) -0.1443(4) -0.7110(7) 0.079(3) Uani 1 1 d . . .
H15 H -0.7817 -0.1560 -0.7684 0.095 Uiso 1 1 calc R . .
C16 C -0.6638(6) -0.1363(4) -0.6831(7) 0.081(3) Uani 1 1 d . . .
H16 H -0.6399 -0.1409 -0.7234 0.098 Uiso 1 1 calc R . .
C1A C -0.5950(10) -0.0924(4) -0.4563(7) 0.119(5) Uiso 1 1 d D . .
H1A1 H -0.6297 -0.0685 -0.4471 0.143 Uiso 1 1 calc R . .
H1A2 H -0.5435 -0.0784 -0.4568 0.143 Uiso 1 1 calc R . .
C1B C -0.5664(18) -0.1256(8) -0.3791(8) 0.226(13) Uiso 1 1 d D . .
H1B1 H -0.6170 -0.1368 -0.3735 0.340 Uiso 1 1 calc R . .
H1B2 H -0.5280 -0.1105 -0.3244 0.340 Uiso 1 1 calc R . .
H1B3 H -0.5361 -0.1506 -0.3901 0.340 Uiso 1 1 calc R . .
N21 N -0.9650(5) -0.0662(2) -0.6926(5) 0.0636(18) Uani 1 1 d . . .
C22 C -1.0313(6) -0.0500(3) -0.6763(7) 0.081(3) Uani 1 1 d D . .
C23 C -1.0418(9) -0.0026(4) -0.6719(9) 0.089(3) Uani 1 1 d . . .
H23 H -1.0901 0.0076 -0.6644 0.107 Uiso 1 1 calc R . .
N24 N -0.9897(5) 0.0278(3) -0.6775(6) 0.070(2) Uani 1 1 d . . .
C25 C -0.9201(8) 0.0103(3) -0.6882(8) 0.078(3) Uani 1 1 d . . .
H25 H -0.8778 0.0303 -0.6886 0.094 Uiso 1 1 calc R . .
C26 C -0.9104(7) -0.0344(3) -0.6983(8) 0.076(3) Uani 1 1 d . . .
H26 H -0.8639 -0.0438 -0.7097 0.091 Uiso 1 1 calc R . .
C2A C -1.0902(8) -0.0830(4) -0.6582(5) 0.114(4) Uiso 1 1 d D . .
H2A1 H -1.0543 -0.1058 -0.6153 0.137 Uiso 1 1 calc R . .
H2A2 H -1.1226 -0.0667 -0.6314 0.137 Uiso 1 1 calc R . .
C2B C -1.1542(4) -0.10652(14) -0.7427(4) 0.205(11) Uiso 1 1 d D . .
H2B1 H -1.2094 -0.0908 -0.7663 0.308 Uiso 1 1 calc R . .
H2B2 H -1.1624 -0.1374 -0.7291 0.308 Uiso 1 1 calc R . .
H2B3 H -1.1314 -0.1063 -0.7866 0.308 Uiso 1 1 calc R . .
N31A N -1.0411(4) -0.12750(14) -1.0620(4) 0.064(4) Uiso 0.60(2) 1 d PRD . 1
C32A C -1.0228(4) -0.17073(14) -1.0240(4) 0.045(4) Uiso 0.60(2) 1 d PRD . 1
C33A C -1.0016(4) -0.17650(14) -0.9334(4) 0.054(4) Uiso 0.60(2) 1 d PRD . 1
H33A H -0.9894 -0.2054 -0.9080 0.064 Uiso 0.60(2) 1 calc PR . 1
N34A N -0.9986(4) -0.13905(14) -0.8808(4) 0.062(5) Uiso 0.60(2) 1 d PRD . 1
C35A C -1.0169(4) -0.09582(14) -0.9188(4) 0.080(5) Uiso 0.60(2) 1 d PRD . 1
H35A H -1.0149 -0.0708 -0.8836 0.096 Uiso 0.60(2) 1 calc PR . 1
C36A C -1.0381(4) -0.09005(14) -1.0094(4) 0.087(6) Uiso 0.60(2) 1 d PRD . 1
H36A H -1.0503 -0.0611 -1.0348 0.104 Uiso 0.60(2) 1 calc PR . 1
C3A1 C -1.0282(5) -0.2083(3) -1.0879(6) 0.122(12) Uiso 0.60(2) 1 d PD . 1
H3A1 H -1.0818 -0.2047 -1.1429 0.146 Uiso 0.60(2) 1 calc PR . 1
H3A2 H -0.9793 -0.2054 -1.1031 0.146 Uiso 0.60(2) 1 calc PR . 1
C3B1 C -1.0268(8) -0.25529(18) -1.0514(7) 0.145(6) Uiso 0.50 1 d PD . 1
H3B1 H -0.9879 -0.2558 -0.9883 0.218 Uiso 0.50 1 calc PR . 1
H3B2 H -1.0068 -0.2767 -1.0821 0.218 Uiso 0.50 1 calc PR . 1
H3B3 H -1.0849 -0.2634 -1.0603 0.218 Uiso 0.50 1 calc PR . 1
N31B N -1.0201(8) -0.12815(18) -1.0517(7) 0.063(7) Uiso 0.40(2) 1 d PRD . 2
C32B C -1.0223(8) -0.17150(18) -1.0190(7) 0.25(5) Uiso 0.40(2) 1 d PRD . 2
C33B C -1.0028(8) -0.17756(18) -0.9289(7) 0.32(6) Uiso 0.40(2) 1 d PRD . 2
H33B H -1.0042 -0.2066 -0.9070 0.379 Uiso 0.40(2) 1 calc PR . 2
N34B N -0.9811(8) -0.14026(18) -0.8715(7) 0.057(7) Uiso 0.40(2) 1 d PRD . 2
C35B C -0.9789(8) -0.09691(18) -0.9041(7) 0.055(6) Uiso 0.40(2) 1 d PRD . 2
H35B H -0.9644 -0.0720 -0.8657 0.066 Uiso 0.40(2) 1 calc PR . 2
C36B C -0.9984(8) -0.09085(18) -0.9942(7) 0.065(7) Uiso 0.40(2) 1 d PRD . 2
H36B H -0.9970 -0.0618 -1.0161 0.079 Uiso 0.40(2) 1 calc PR . 2
C3A2 C -1.0473(9) -0.2080(2) -1.0901(8) 0.16(3) Uiso 0.40(2) 1 d PD . 2
H3A3 H -1.1096 -0.2058 -1.1293 0.195 Uiso 0.40(2) 1 calc PR . 2
H3A4 H -1.0162 -0.2026 -1.1263 0.195 Uiso 0.40(2) 1 calc PR . 2
C3B2 C -1.0268(8) -0.25529(18) -1.0514(7) 0.145(6) Uiso 0.50 1 d PD . 2
H3B4 H -0.9726 -0.2549 -0.9975 0.218 Uiso 0.50 1 calc PR . 2
H3B5 H -1.0215 -0.2755 -1.0944 0.218 Uiso 0.50 1 calc PR . 2
H3B6 H -1.0732 -0.2656 -1.0376 0.218 Uiso 0.50 1 calc PR . 2
N41 N -0.9808(5) -0.2094(2) -0.6618(5) 0.0636(19) Uani 1 1 d . . .
C42 C -0.9447(6) -0.2495(3) -0.6688(6) 0.062(2) Uani 1 1 d D . .
C43 C -0.9691(7) -0.2881(3) -0.6374(8) 0.074(3) Uani 1 1 d . . .
H43 H -0.9463 -0.3158 -0.6447 0.089 Uiso 1 1 calc R . .
N44 N -1.0206(5) -0.2889(2) -0.5990(5) 0.0595(17) Uani 1 1 d . . .
C45 C -1.0543(8) -0.2496(3) -0.5919(9) 0.078(3) Uani 1 1 d . . .
H45 H -1.0912 -0.2479 -0.5639 0.093 Uiso 1 1 calc R . .
C46 C -1.0342(7) -0.2107(3) -0.6265(8) 0.076(3) Uani 1 1 d . . .
H46 H -1.0615 -0.1836 -0.6239 0.091 Uiso 1 1 calc R . .
C4A C -0.8804(9) -0.2482(4) -0.7091(11) 0.117(5) Uiso 1 1 d D . .
H4A1 H -0.8305 -0.2296 -0.6713 0.141 Uiso 1 1 calc R . .
H4A2 H -0.9082 -0.2338 -0.7677 0.141 Uiso 1 1 calc R . .
C4B C -0.8484(14) -0.2948(6) -0.7192(16) 0.183(9) Uiso 1 1 d D . .
H4B1 H -0.8437 -0.3138 -0.6701 0.274 Uiso 1 1 calc R . .
H4B2 H -0.7920 -0.2921 -0.7191 0.274 Uiso 1 1 calc R . .
H4B3 H -0.8892 -0.3081 -0.7749 0.274 Uiso 1 1 calc R . .
N51 N -1.0133(6) -0.4269(3) -0.5733(5) 0.072(2) Uani 1 1 d . . .
C52 C -0.9349(5) -0.4440(3) -0.5242(6) 0.061(2) Uani 1 1 d D . .
C53 C -0.9261(6) -0.4910(3) -0.5208(6) 0.064(2) Uani 1 1 d . . .
H53 H -0.8716 -0.5031 -0.4830 0.077 Uiso 1 1 calc R . .
N54 N -0.9891(5) -0.5194(3) -0.5671(5) 0.0631(18) Uani 1 1 d . . .
C55 C -1.0683(7) -0.5009(4) -0.6205(8) 0.084(3) Uani 1 1 d . . .
H55 H -1.1157 -0.5195 -0.6545 0.100 Uiso 1 1 calc R . .
C56 C -1.0773(7) -0.4543(4) -0.6237(7) 0.091(4) Uani 1 1 d . . .
H56 H -1.1307 -0.4417 -0.6631 0.109 Uiso 1 1 calc R . .
C5A C -0.8599(6) -0.4137(3) -0.4650(6) 0.085(3) Uiso 1 1 d D . .
H5A1 H -0.8288 -0.4281 -0.4067 0.102 Uiso 1 1 calc R . 1
H5A2 H -0.8832 -0.3851 -0.4560 0.102 Uiso 1 1 calc R . 1
C5B1 C -0.7960(13) -0.4043(10) -0.5039(15) 0.118(10) Uiso 0.66(5) 1 d PD . 1
H5B1 H -0.7551 -0.3813 -0.4687 0.178 Uiso 0.66(5) 1 calc PR . 1
H5B2 H -0.8274 -0.3939 -0.5647 0.178 Uiso 0.66(5) 1 calc PR . 1
H5B3 H -0.7648 -0.4318 -0.5029 0.178 Uiso 0.66(5) 1 calc PR . 1
C5B2 C -0.7734(7) -0.4274(11) -0.462(3) 0.090(14) Uiso 0.34(5) 1 d PD . 2
H5B4 H -0.7800 -0.4312 -0.5227 0.135 Uiso 0.34(5) 1 calc PR . 2
H5B5 H -0.7543 -0.4556 -0.4303 0.135 Uiso 0.34(5) 1 calc PR . 2
H5B6 H -0.7306 -0.4042 -0.4326 0.135 Uiso 0.34(5) 1 calc PR . 2
N61 N -1.3869(5) -0.3686(3) -0.6652(5) 0.0646(18) Uani 1 1 d . . .
C62 C -1.3555(7) -0.3523(4) -0.7177(7) 0.081(3) Uani 1 1 d D . .
C63 C -1.2662(7) -0.3481(4) -0.6862(8) 0.084(3) Uani 1 1 d . . .
H63 H -1.2457 -0.3347 -0.7241 0.101 Uiso 1 1 calc R . .
N64 N -1.2081(5) -0.3615(3) -0.6074(6) 0.071(2) Uani 1 1 d . . .
C65 C -1.2434(7) -0.3776(4) -0.5546(7) 0.082(3) Uani 1 1 d . . .
H65 H -1.2066 -0.3856 -0.4956 0.098 Uiso 1 1 calc R . .
C66 C -1.3328(6) -0.3824(4) -0.5857(7) 0.076(3) Uani 1 1 d . . .
H66 H -1.3547 -0.3959 -0.5489 0.092 Uiso 1 1 calc R . .
C6A C -1.4153(13) -0.3292(7) -0.8050(9) 0.163(7) Uiso 1 1 d D . .
H6A1 H -1.4736 -0.3268 -0.8082 0.195 Uiso 1 1 calc R . .
H6A2 H -1.3941 -0.2986 -0.8055 0.195 Uiso 1 1 calc R . .
C6B C -1.421(3) -0.3545(13) -0.8864(8) 0.34(2) Uiso 1 1 d D . .
H6B1 H -1.3635 -0.3651 -0.8756 0.503 Uiso 1 1 calc R . .
H6B2 H -1.4428 -0.3345 -0.9374 0.503 Uiso 1 1 calc R . .
H6B3 H -1.4597 -0.3801 -0.8981 0.503 Uiso 1 1 calc R . .
N71 N -0.9741(5) -0.3863(3) -0.2154(6) 0.071(2) Uani 1 1 d . . .
C72 C -0.9429(6) -0.3485(3) -0.2375(6) 0.066(2) Uani 1 1 d D . .
C73 C -0.9621(7) -0.3409(3) -0.3300(6) 0.069(2) Uani 1 1 d . . .
H73 H -0.9420 -0.3146 -0.3462 0.082 Uiso 1 1 calc R . .
N74 N -1.0078(5) -0.3708(2) -0.3919(5) 0.0643(18) Uani 1 1 d . . .
C75 C -1.0351(7) -0.4075(3) -0.3654(7) 0.069(2) Uani 1 1 d . . .
H75 H -1.0664 -0.4294 -0.4079 0.083 Uiso 1 1 calc R . .
C76 C -1.0191(7) -0.4143(3) -0.2779(6) 0.071(2) Uani 1 1 d . . .
H76 H -1.0417 -0.4402 -0.2632 0.085 Uiso 1 1 calc R . .
C7A C -0.8861(6) -0.3142(4) -0.1692(7) 0.092(3) Uiso 1 1 d D . .
H7A1 H -0.8872 -0.3205 -0.1122 0.111 Uiso 1 1 calc R . .
H7A2 H -0.9104 -0.2841 -0.1884 0.111 Uiso 1 1 calc R . .
C7B C -0.7923(7) -0.3146(7) -0.1557(13) 0.174(8) Uiso 1 1 d D . .
H7B1 H -0.7669 -0.3439 -0.1341 0.261 Uiso 1 1 calc R . .
H7B2 H -0.7596 -0.2917 -0.1126 0.261 Uiso 1 1 calc R . .
H7B3 H -0.7906 -0.3083 -0.2119 0.261 Uiso 1 1 calc R . .
N81 N -0.6639(4) -0.6104(2) -0.3191(4) 0.0492(15) Uani 1 1 d . . .
C82 C -0.6811(5) -0.5906(3) -0.3985(6) 0.063(2) Uani 1 1 d D . .
C83 C -0.7655(5) -0.5902(3) -0.4680(6) 0.062(2) Uani 1 1 d . . .
H83 H -0.7765 -0.5758 -0.5220 0.074 Uiso 1 1 calc R . .
N84 N -0.8307(5) -0.6103(3) -0.4574(5) 0.0605(18) Uani 1 1 d . . .
C85 C -0.8137(6) -0.6288(4) -0.3831(7) 0.075(3) Uani 1 1 d . . .
H85 H -0.8595 -0.6424 -0.3755 0.090 Uiso 1 1 calc R . .
C86 C -0.7304(6) -0.6300(4) -0.3115(6) 0.067(2) Uani 1 1 d . . .
H86 H -0.7216 -0.6447 -0.2583 0.081 Uiso 1 1 calc R . .
C8A C -0.6090(6) -0.5666(3) -0.4115(9) 0.095(3) Uiso 1 1 d D . .
H8A1 H -0.5535 -0.5723 -0.3596 0.114 Uiso 1 1 calc R . .
H8A2 H -0.6052 -0.5791 -0.4638 0.114 Uiso 1 1 calc R . .
C8B C -0.6231(11) -0.5159(3) -0.4236(13) 0.134(6) Uiso 1 1 d D . .
H8B1 H -0.6765 -0.5100 -0.4764 0.201 Uiso 1 1 calc R . .
H8B2 H -0.5748 -0.5023 -0.4302 0.201 Uiso 1 1 calc R . .
H8B3 H -0.6269 -0.5032 -0.3720 0.201 Uiso 1 1 calc R . .
Sb1 Sb -0.72690(6) -0.25823(4) -0.39680(6) 0.1111(3) Uani 1 1 d D . .
F11 F -0.7716(7) -0.2091(3) -0.4684(7) 0.241(7) Uiso 1 1 d D . .
F12 F -0.6164(5) -0.2443(5) -0.3832(11) 0.240(7) Uiso 1 1 d D . .
F13 F -0.8368(5) -0.2755(5) -0.4137(12) 0.244(7) Uiso 1 1 d D . .
F14 F -0.7380(14) -0.2927(4) -0.4937(7) 0.269(8) Uiso 1 1 d D . .
F15 F -0.7110(12) -0.2250(4) -0.2969(6) 0.237(7) Uiso 1 1 d D . .
F16 F -0.6804(7) -0.3087(3) -0.3231(7) 0.227(6) Uiso 1 1 d D . .
Sb2 Sb -0.82848(5) -0.48675(3) -0.73735(5) 0.0844(2) Uani 1 1 d D . .
F21 F -0.7692(5) -0.4805(2) -0.8066(5) 0.129(3) Uiso 1 1 d D . .
F22 F -0.9321(5) -0.4942(4) -0.8386(5) 0.142(6) Uiso 0.666(18) 1 d PD . .
F23 F -0.7235(5) -0.4820(4) -0.6360(5) 0.148(6) Uiso 0.666(18) 1 d PD . .
F24 F -0.8124(8) -0.5491(2) -0.7373(8) 0.141(6) Uiso 0.666(18) 1 d PD . .
F25 F -0.8446(8) -0.4255(2) -0.7372(8) 0.146(6) Uiso 0.666(18) 1 d PD . .
F26 F -0.8863(5) -0.4945(3) -0.6673(5) 0.187(5) Uiso 1 1 d D . .
F22B F -0.7653(8) -0.4398(4) -0.6659(8) 0.22(2) Uiso 0.334(18) 1 d PD . .
F23B F -0.8891(8) -0.5353(4) -0.8074(8) 0.179(16) Uiso 0.334(18) 1 d PD . .
F24B F -0.9133(7) -0.4479(5) -0.8106(8) 0.37(4) Uiso 0.334(18) 1 d PD . .
F25B F -0.7438(7) -0.5273(4) -0.6650(8) 0.62(11) Uiso 0.334(18) 1 d PD . .
Sb3 Sb -1.29441(6) -0.49471(3) -0.88107(6) 0.0954(3) Uani 1 1 d D . .
F31 F -1.1775(5) -0.4948(3) -0.8514(7) 0.189(5) Uiso 1 1 d D . .
F32 F -1.2765(7) -0.4514(5) -0.7941(9) 0.223(6) Uiso 1 1 d D . .
F33 F -1.3137(7) -0.4497(5) -0.9629(9) 0.223(6) Uiso 1 1 d D . .
F34 F -1.3139(8) -0.5405(6) -0.9621(13) 0.306(11) Uiso 1 1 d D . .
F35 F -1.2735(7) -0.5327(5) -0.7855(9) 0.233(7) Uiso 1 1 d D . .
F36 F -1.4124(5) -0.4947(3) -0.9079(7) 0.183(5) Uiso 1 1 d D . .
Sb4 Sb -0.70438(7) -0.23696(3) -0.89963(7) 0.1070(3) Uani 1 1 d D . .
F41 F -0.6212(7) -0.2251(4) -0.9414(8) 0.155(6) Uiso 0.721(15) 1 d PD . .
F42 F -0.7905(7) -0.2245(5) -1.0144(6) 0.182(7) Uiso 0.721(15) 1 d PD . .
F43 F -0.7022(9) -0.1760(3) -0.8724(10) 0.178(7) Uiso 0.721(15) 1 d PD . .
F44 F -0.6169(8) -0.2477(6) -0.7879(6) 0.247(12) Uiso 0.721(15) 1 d PD . .
F45 F -0.7045(10) -0.2970(3) -0.9296(11) 0.206(8) Uiso 0.721(15) 1 d PD . .
F46 F -0.7878(8) -0.2476(5) -0.8620(9) 0.235(11) Uiso 0.721(15) 1 d PD . .
F41B F -0.7701(18) -0.1859(7) -0.908(2) 0.121(11) Uiso 0.279(15) 1 d PD . .
F42B F -0.717(2) -0.2539(10) -0.7983(12) 0.142(13) Uiso 0.279(15) 1 d PD . .
F43B F -0.781(2) -0.2829(10) -0.9603(16) 0.161(15) Uiso 0.279(15) 1 d PD . .
F44B F -0.6788(17) -0.2265(8) -0.9939(11) 0.106(9) Uiso 0.279(15) 1 d PD . .
F45B F -0.6191(19) -0.1965(11) -0.8298(15) 0.155(15) Uiso 0.279(15) 1 d PD . .
F46B F -0.620(5) -0.281(3) -0.870(5) 0.37(6) Uiso 0.279(15) 1 d PD . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N41 Ag1 N21 132.0(3) . . ?
N41 Ag1 N34B 118.6(3) . . ?
N21 Ag1 N34B 98.5(2) . . ?
N41 Ag1 N14 110.5(3) . . ?
N21 Ag1 N14 92.5(3) . . ?
N34B Ag1 N14 97.0(4) . . ?
N41 Ag1 N34A 116.9(2) . . ?
N21 Ag1 N34A 96.8(2) . . ?
N14 Ag1 N34A 102.8(2) . . ?
N81 Ag2 N61 139.3(3) . 2_645 ?
N81 Ag2 N31A 111.7(2) . 3_546 ?
N61 Ag2 N31A 102.5(2) 2_645 3_546 ?
N81 Ag2 N31B 119.2(3) . 3_546 ?
N61 Ag2 N31B 95.2(3) 2_645 3_546 ?
N81 Ag2 N24 103.1(2) . 4_545 ?
N61 Ag2 N24 91.1(3) 2_645 4_545 ?
N31A Ag2 N24 100.6(2) 3_546 4_545 ?
N31B Ag2 N24 99.0(2) 3_546 4_545 ?
N44 Ag3 N51 123.8(3) . . ?
N44 Ag3 N64 109.7(3) . . ?
N51 Ag3 N64 100.4(3) . . ?
N44 Ag3 N74 125.4(3) . . ?
N51 Ag3 N74 91.0(3) . . ?
N64 Ag3 N74 102.1(3) . . ?
N84 Ag4 N11 137.2(3) . 3_445 ?
N84 Ag4 N71 111.5(3) . 2_544 ?
N11 Ag4 N71 100.0(3) 3_445 2_544 ?
N84 Ag4 N54 101.8(3) . . ?
N11 Ag4 N54 97.7(3) 3_445 . ?
N71 Ag4 N54 104.0(3) 2_544 . ?
C12 N11 C16 116.4(8) . . ?
C12 N11 Ag4 125.0(6) . 3 ?
C16 N11 Ag4 117.7(6) . 3 ?
N11 C12 C13 120.1(8) . . ?
N11 C12 C1A 119.0(10) . . ?
C13 C12 C1A 120.3(10) . . ?
N14 C13 C12 122.2(9) . . ?
C13 N14 C15 115.7(9) . . ?
C13 N14 Ag1 122.6(6) . . ?
C15 N14 Ag1 121.6(7) . . ?
N14 C15 C16 122.3(10) . . ?
C15 C16 N11 123.1(9) . . ?
C12 C1A C1B 112.9(5) . . ?
C26 N21 C22 115.3(7) . . ?
C26 N21 Ag1 121.0(6) . . ?
C22 N21 Ag1 123.6(5) . . ?
N21 C22 C23 119.5(8) . . ?
N21 C22 C2A 119.5(9) . . ?
C23 C22 C2A 120.8(11) . . ?
N24 C23 C22 125.0(10) . . ?
C23 N24 C25 114.1(9) . . ?
C23 N24 Ag2 121.8(7) . 4_444 ?
C25 N24 Ag2 122.8(7) . 4_444 ?
C26 C25 N24 122.9(10) . . ?
C25 C26 N21 122.8(10) . . ?
C2B C2A C22 112.2(5) . . ?
C32A N31A C36A 120.0 . . ?
C32A N31A Ag2 121.09(11) . 3_454 ?
C36A N31A Ag2 115.86(10) . 3_454 ?
N31A C32A C33A 120.0 . . ?
N31A C32A C3A1 114.8(4) . . ?
C33A C32A C3A1 125.2(4) . . ?
N34A C33A C32A 120.0 . . ?
C33A N34A C35A 120.0 . . ?
C33A N34A Ag1 122.78(11) . . ?
C35A N34A Ag1 116.91(10) . . ?
C36A C35A N34A 120.0 . . ?
N31A C36A C35A 120.0 . . ?
C3B1 C3A1 C32A 113.9(5) . . ?
C32B N31B C36B 120.0 . . ?
C32B N31B Ag2 125.35(12) . 3_454 ?
C36B N31B Ag2 114.05(13) . 3_454 ?
C33B C32B N31B 120.0 . . ?
C33B C32B C3A2 126.9(3) . . ?
N31B C32B C3A2 113.1(3) . . ?
C32B C33B N34B 120.0 . . ?
C33B N34B C35B 120.0 . . ?
C33B N34B Ag1 124.71(13) . . ?
C35B N34B Ag1 115.29(13) . . ?
C36B C35B N34B 120.0 . . ?
C35B C36B N31B 120.0 . . ?
C46 N41 C42 116.9(8) . . ?
C46 N41 Ag1 123.7(7) . . ?
C42 N41 Ag1 119.4(6) . . ?
N41 C42 C43 117.3(7) . . ?
N41 C42 C4A 117.2(8) . . ?
C43 C42 C4A 125.4(8) . . ?
N44 C43 C42 125.5(8) . . ?
C43 N44 C45 116.3(8) . . ?
C43 N44 Ag3 123.0(6) . . ?
C45 N44 Ag3 120.7(6) . . ?
N44 C45 C46 119.3(9) . . ?
N41 C46 C45 124.6(9) . . ?
C42 C4A C4B 113.1(5) . . ?
C56 N51 C52 119.2(8) . . ?
C56 N51 Ag3 117.0(7) . . ?
C52 N51 Ag3 121.9(6) . . ?
N51 C52 C53 117.8(7) . . ?
N51 C52 C5A 120.9(8) . . ?
C53 C52 C5A 120.9(8) . . ?
N54 C53 C52 124.5(8) . . ?
C53 N54 C55 116.6(8) . . ?
C53 N54 Ag4 124.2(6) . . ?
C55 N54 Ag4 119.1(6) . . ?
N54 C55 C56 119.0(10) . . ?
N51 C56 C55 122.6(9) . . ?
C5B2 C5A C52 113.4(5) . . ?
C5B2 C5A C5B1 35.6(15) . . ?
C52 C5A C5B1 113.0(5) . . ?
C62 N61 C66 118.7(8) . . ?
C62 N61 Ag2 128.7(6) . 2_444 ?
C66 N61 Ag2 111.8(6) . 2_444 ?
N61 C62 C63 119.2(9) . . ?
N61 C62 C6A 120.4(12) . . ?
C63 C62 C6A 119.3(12) . . ?
N64 C63 C62 125.3(10) . . ?
C63 N64 C65 113.5(9) . . ?
C63 N64 Ag3 127.2(7) . . ?
C65 N64 Ag3 119.0(7) . . ?
N64 C65 C66 121.6(9) . . ?
N61 C66 C65 121.4(10) . . ?
C6B C6A C62 112.7(5) . . ?
C76 N71 C72 118.5(8) . . ?
C76 N71 Ag4 116.7(6) . 2_545 ?
C72 N71 Ag4 124.2(6) . 2_545 ?
N71 C72 C73 119.0(8) . . ?
N71 C72 C7A 123.1(9) . . ?
C73 C72 C7A 117.9(9) . . ?
N74 C73 C72 120.5(8) . . ?
C73 N74 C75 117.3(8) . . ?
C73 N74 Ag3 119.7(6) . . ?
C75 N74 Ag3 122.5(6) . . ?
N74 C75 C76 122.4(9) . . ?
N71 C76 C75 122.2(9) . . ?
C72 C7A C7B 113.2(5) . . ?
C86 N81 C82 116.9(7) . . ?
C86 N81 Ag2 118.9(5) . . ?
C82 N81 Ag2 124.3(5) . . ?
N81 C82 C83 121.1(7) . . ?
N81 C82 C8A 119.9(8) . . ?
C83 C82 C8A 118.9(8) . . ?
N84 C83 C82 120.0(8) . . ?
C85 N84 C83 118.2(8) . . ?
C85 N84 Ag4 124.5(6) . . ?
C83 N84 Ag4 116.8(6) . . ?
N84 C85 C86 123.8(9) . . ?
N81 C86 C85 119.9(9) . . ?
C8B C8A C82 112.9(5) . . ?
F11 Sb1 F13 90.9(3) . . ?
F11 Sb1 F12 90.8(3) . . ?
F13 Sb1 F12 176.4(8) . . ?
F11 Sb1 F15 91.1(3) . . ?
F13 Sb1 F15 91.3(8) . . ?
F12 Sb1 F15 91.8(9) . . ?
F11 Sb1 F14 90.9(3) . . ?
F13 Sb1 F14 90.3(9) . . ?
F12 Sb1 F14 86.5(9) . . ?
F15 Sb1 F14 177.4(7) . . ?
F11 Sb1 F16 179.7(4) . . ?
F13 Sb1 F16 89.4(3) . . ?
F12 Sb1 F16 88.9(3) . . ?
F15 Sb1 F16 88.9(3) . . ?
F14 Sb1 F16 89.1(3) . . ?
F24B Sb2 F25 46.0(4) . . ?
F24B Sb2 F22B 91.4(6) . . ?
F25 Sb2 F22B 45.4(4) . . ?
F24B Sb2 F26 90.8(3) . . ?
F25 Sb2 F26 90.0(3) . . ?
F22B Sb2 F26 90.5(3) . . ?
F24B Sb2 F22 46.0(4) . . ?
F25 Sb2 F22 92.0(5) . . ?
F22B Sb2 F22 137.5(6) . . ?
F26 Sb2 F22 89.9(3) . . ?
F24B Sb2 F21 90.7(3) . . ?
F25 Sb2 F21 91.5(3) . . ?
F22B Sb2 F21 90.2(3) . . ?
F26 Sb2 F21 178.4(3) . . ?
F22 Sb2 F21 90.6(3) . . ?
F24B Sb2 F23 136.6(6) . . ?
F25 Sb2 F23 90.6(5) . . ?
F22B Sb2 F23 45.1(4) . . ?
F26 Sb2 F23 90.3(3) . . ?
F22 Sb2 F23 177.4(5) . . ?
F21 Sb2 F23 89.1(3) . . ?
F24B Sb2 F23B 90.4(6) . . ?
F25 Sb2 F23B 136.4(6) . . ?
F22B Sb2 F23B 178.2(7) . . ?
F26 Sb2 F23B 89.8(3) . . ?
F22 Sb2 F23B 44.3(4) . . ?
F21 Sb2 F23B 89.5(3) . . ?
F23 Sb2 F23B 133.1(6) . . ?
F24B Sb2 F25B 178.6(7) . . ?
F25 Sb2 F25B 135.3(6) . . ?
F22B Sb2 F25B 89.9(6) . . ?
F26 Sb2 F25B 89.4(3) . . ?
F22 Sb2 F25B 132.6(6) . . ?
F21 Sb2 F25B 89.1(3) . . ?
F23 Sb2 F25B 44.8(4) . . ?
F23B Sb2 F25B 88.3(6) . . ?
F24B Sb2 F24 134.0(6) . . ?
F25 Sb2 F24 179.7(4) . . ?
F22B Sb2 F24 134.6(6) . . ?
F26 Sb2 F24 89.8(3) . . ?
F22 Sb2 F24 87.9(5) . . ?
F21 Sb2 F24 88.7(3) . . ?
F23 Sb2 F24 89.5(5) . . ?
F23B Sb2 F24 43.6(4) . . ?
F25B Sb2 F24 44.7(4) . . ?
F23B F22 F24B 134.5(6) . . ?
F23B F22 Sb2 68.1(4) . . ?
F24B F22 Sb2 66.5(4) . . ?
F25B F23 F22B 134.8(6) . . ?
F25B F23 Sb2 67.8(4) . . ?
F22B F23 Sb2 67.0(4) . . ?
F23B F24 F25B 135.3(5) . . ?
F23B F24 Sb2 67.8(4) . . ?
F25B F24 Sb2 67.5(4) . . ?
F22B F25 F24B 134.5(5) . . ?
F22B F25 Sb2 67.5(4) . . ?
F24B F25 Sb2 67.0(4) . . ?
F23 F22B F25 134.9(5) . . ?
F23 F22B Sb2 67.9(4) . . ?
F25 F22B Sb2 67.0(4) . . ?
F24 F23B F22 136.2(5) . . ?
F24 F23B Sb2 68.6(4) . . ?
F22 F23B Sb2 67.6(4) . . ?
F25 F24B F22 134.5(5) . . ?
F25 F24B Sb2 67.0(4) . . ?
F22 F24B Sb2 67.5(4) . . ?
F23 F25B F24 135.2(5) . . ?
F23 F25B Sb2 67.4(4) . . ?
F24 F25B Sb2 67.8(4) . . ?
F33 Sb3 F31 91.2(3) . . ?
F33 Sb3 F34 94.2(11) . . ?
F31 Sb3 F34 91.3(3) . . ?
F33 Sb3 F35 170.6(8) . . ?
F31 Sb3 F35 89.5(3) . . ?
F34 Sb3 F35 95.2(10) . . ?
F33 Sb3 F32 89.7(8) . . ?
F31 Sb3 F32 90.2(3) . . ?
F34 Sb3 F32 175.9(9) . . ?
F35 Sb3 F32 81.0(9) . . ?
F33 Sb3 F36 89.9(3) . . ?
F31 Sb3 F36 178.4(4) . . ?
F34 Sb3 F36 89.8(3) . . ?
F35 Sb3 F36 89.3(3) . . ?
F32 Sb3 F36 88.7(3) . . ?
F46 Sb4 F44 91.9(3) . . ?
F46 Sb4 F44B 147.4(9) . . ?
F44 Sb4 F44B 120.4(9) . . ?
F46 Sb4 F45 91.1(3) . . ?
F44 Sb4 F45 90.7(5) . . ?
F44B Sb4 F45 84.4(9) . . ?
F46 Sb4 F46B 115(2) . . ?
F44 Sb4 F46B 54(3) . . ?
F44B Sb4 F46B 84.0(15) . . ?
F45 Sb4 F46B 45(3) . . ?
F46 Sb4 F43B 65.7(10) . . ?
F44 Sb4 F43B 119.6(12) . . ?
F44B Sb4 F43B 91.9(6) . . ?
F45 Sb4 F43B 39.4(14) . . ?
F46B Sb4 F43B 85(4) . . ?
F46 Sb4 F45B 114.5(9) . . ?
F44 Sb4 F45B 53.6(12) . . ?
F44B Sb4 F45B 90.7(6) . . ?
F45 Sb4 F45B 134.5(13) . . ?
F46B Sb4 F45B 89(4) . . ?
F43B Sb4 F45B 172.9(17) . . ?
F46 Sb4 F41B 68.0(11) . . ?
F44 Sb4 F41B 114.5(10) . . ?
F44B Sb4 F41B 99.4(13) . . ?
F45 Sb4 F41B 146.8(11) . . ?
F46B Sb4 F41B 167(4) . . ?
F43B Sb4 F41B 107.4(18) . . ?
F45B Sb4 F41B 78.7(16) . . ?
F46 Sb4 F43 91.0(3) . . ?
F44 Sb4 F43 90.0(5) . . ?
F44B Sb4 F43 93.4(9) . . ?
F45 Sb4 F43 177.8(4) . . ?
F46B Sb4 F43 134(4) . . ?
F43B Sb4 F43 141.4(15) . . ?
F45B Sb4 F43 44.9(13) . . ?
F41B Sb4 F43 34.1(10) . . ?
F46 Sb4 F42B 39.0(10) . . ?
F44 Sb4 F42B 52.9(10) . . ?
F44B Sb4 F42B 171.3(15) . . ?
F45 Sb4 F42B 90.0(11) . . ?
F46B Sb4 F42B 87.3(16) . . ?
F43B Sb4 F42B 88.0(6) . . ?
F45B Sb4 F42B 88.5(6) . . ?
F41B Sb4 F42B 89.0(15) . . ?
F43 Sb4 F42B 92.1(11) . . ?
F46 Sb4 F42 90.2(3) . . ?
F44 Sb4 F42 177.7(4) . . ?
F44B Sb4 F42 57.7(9) . . ?
F45 Sb4 F42 90.3(5) . . ?
F46B Sb4 F42 126(3) . . ?
F43B Sb4 F42 62.2(12) . . ?
F45B Sb4 F42 124.5(11) . . ?
F41B Sb4 F42 65.4(10) . . ?
F43 Sb4 F42 89.0(5) . . ?
F42B Sb4 F42 129.1(11) . . ?
F46 Sb4 F41 178.2(4) . . ?
F44 Sb4 F41 89.8(3) . . ?
F44B Sb4 F41 31.0(8) . . ?
F45 Sb4 F41 89.5(3) . . ?
F46B Sb4 F41 66(2) . . ?
F43B Sb4 F41 113.9(10) . . ?
F45B Sb4 F41 66.1(9) . . ?
F41B Sb4 F41 110.7(10) . . ?
F43 Sb4 F41 88.4(3) . . ?
F42B Sb4 F41 142.7(11) . . ?
F42 Sb4 F41 88.1(3) . . ?
F44B F41 Sb4 72.5(6) . . ?
F44B F42 Sb4 60.2(5) . . ?
F41B F43 F45B 139.1(12) . . ?
F41B F43 Sb4 72.7(7) . . ?
F45B F43 Sb4 67.4(7) . . ?
F42B F44 F45B 103.1(16) . . ?
F42B F44 F46B 101(3) . . ?
F45B F44 F46B 102(2) . . ?
F42B F44 Sb4 64.4(6) . . ?
F45B F44 Sb4 63.7(7) . . ?
F46B F44 Sb4 63.3(14) . . ?
F43B F45 F46B 137(2) . . ?
F43B F45 Sb4 70.4(8) . . ?
F46B F45 Sb4 67.4(18) . . ?
F42B F46 Sb4 72.3(7) . . ?
F43 F41B Sb4 73.2(7) . . ?
F46 F42B F44 131.4(7) . . ?
F46 F42B Sb4 68.7(6) . . ?
F44 F42B Sb4 62.7(6) . . ?
F45 F43B Sb4 70.1(8) . . ?
F41 F44B F42 137.0(10) . . ?
F41 F44B Sb4 76.6(7) . . ?
F42 F44B Sb4 62.1(5) . . ?
F43 F45B F44 115.7(12) . . ?
F43 F45B Sb4 67.7(8) . . ?
F44 F45B Sb4 62.7(7) . . ?
F45 F46B F44 115(2) . . ?
F45 F46B Sb4 67.2(18) . . ?
F44 F46B Sb4 62.5(13) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 N41 2.302(7) . ?
Ag1 N21 2.362(7) . ?
Ag1 N34B 2.371(10) . ?
Ag1 N14 2.420(8) . ?
Ag1 N34A 2.469(6) . ?
Ag2 N81 2.253(6) . ?
Ag2 N61 2.329(8) 2_645 ?
Ag2 N31A 2.415(6) 3_546 ?
Ag2 N31B 2.434(10) 3_546 ?
Ag2 N24 2.525(8) 4_545 ?
Ag3 N44 2.246(7) . ?
Ag3 N51 2.368(8) . ?
Ag3 N64 2.377(8) . ?
Ag3 N74 2.383(7) . ?
Ag4 N84 2.300(7) . ?
Ag4 N11 2.315(7) 3_445 ?
Ag4 N71 2.394(8) 2_544 ?
Ag4 N54 2.408(8) . ?
N11 C12 1.313(12) . ?
N11 C16 1.339(12) . ?
N11 Ag4 2.315(7) 3 ?
C12 C13 1.411(14) . ?
C12 C1A 1.507(5) . ?
C13 N14 1.325(13) . ?
N14 C15 1.328(13) . ?
C15 C16 1.337(14) . ?
C1A C1B 1.509(5) . ?
N21 C26 1.347(13) . ?
N21 C22 1.353(13) . ?
C22 C23 1.409(14) . ?
C22 C2A 1.516(5) . ?
C23 N24 1.286(15) . ?
N24 C25 1.369(14) . ?
N24 Ag2 2.525(8) 4_444 ?
C25 C26 1.343(15) . ?
C2A C2B 1.510(5) . ?
N31A C32A 1.3900 . ?
N31A C36A 1.3900 . ?
N31A Ag2 2.415(6) 3_454 ?
C32A C33A 1.3900 . ?
C32A C3A1 1.505(5) . ?
C33A N34A 1.3900 . ?
N34A C35A 1.3900 . ?
C35A C36A 1.3900 . ?
C3A1 C3B1 1.502(5) . ?
N31B C32B 1.3900 . ?
N31B C36B 1.3900 . ?
N31B Ag2 2.434(10) 3_454 ?
C32B C33B 1.3900 . ?
C32B C3A2 1.508(5) . ?
C33B N34B 1.3900 . ?
N34B C35B 1.3900 . ?
C35B C36B 1.3900 . ?
N41 C46 1.274(13) . ?
N41 C42 1.355(12) . ?
C42 C43 1.384(13) . ?
C42 C4A 1.508(5) . ?
C43 N44 1.286(13) . ?
N44 C45 1.318(12) . ?
C45 C46 1.386(14) . ?
C4A C4B 1.509(5) . ?
N51 C56 1.315(13) . ?
N51 C52 1.316(12) . ?
C52 C53 1.387(13) . ?
C52 C5A 1.508(5) . ?
C53 N54 1.308(12) . ?
N54 C55 1.357(13) . ?
C55 C56 1.376(15) . ?
C5A C5B2 1.505(5) . ?
C5A C5B1 1.509(5) . ?
N61 C62 1.295(13) . ?
N61 C66 1.295(12) . ?
N61 Ag2 2.329(8) 2_444 ?
C62 C63 1.374(15) . ?
C62 C6A 1.513(5) . ?
C63 N64 1.303(14) . ?
N64 C65 1.344(14) . ?
C65 C66 1.379(14) . ?
C6A C6B 1.506(5) . ?
N71 C76 1.279(12) . ?
N71 C72 1.347(12) . ?
N71 Ag4 2.394(8) 2_545 ?
C72 C73 1.436(13) . ?
C72 C7A 1.505(5) . ?
C73 N74 1.313(12) . ?
N74 C75 1.322(13) . ?
C75 C76 1.367(14) . ?
C7A C7B 1.507(5) . ?
N81 C86 1.323(12) . ?
N81 C82 1.346(11) . ?
C82 C83 1.389(12) . ?
C82 C8A 1.509(5) . ?
C83 N84 1.333(12) . ?
N84 C85 1.257(12) . ?
C85 C86 1.391(13) . ?
C8A C8B 1.506(5) . ?
Sb1 F11 1.808(7) . ?
Sb1 F13 1.832(7) . ?
Sb1 F12 1.834(7) . ?
Sb1 F15 1.835(7) . ?
Sb1 F14 1.836(7) . ?
Sb1 F16 1.860(7) . ?
Sb2 F24B 1.821(7) . ?
Sb2 F25 1.821(7) . ?
Sb2 F22B 1.828(7) . ?
Sb2 F26 1.832(7) . ?
Sb2 F22 1.834(7) . ?
Sb2 F21 1.836(6) . ?
Sb2 F23 1.840(7) . ?
Sb2 F23B 1.840(7) . ?
Sb2 F25B 1.846(7) . ?
Sb2 F24 1.851(7) . ?
F22 F23B 1.386(13) . ?
F22 F24B 1.429(13) . ?
F23 F25B 1.404(14) . ?
F23 F22B 1.408(13) . ?
F24 F23B 1.371(13) . ?
F24 F25B 1.405(14) . ?
F25 F22B 1.409(13) . ?
F25 F24B 1.423(13) . ?
Sb3 F33 1.817(7) . ?
Sb3 F31 1.823(7) . ?
Sb3 F34 1.823(7) . ?
Sb3 F35 1.838(7) . ?
Sb3 F32 1.843(7) . ?
Sb3 F36 1.851(7) . ?
Sb4 F46 1.807(7) . ?
Sb4 F44 1.820(7) . ?
Sb4 F44B 1.820(8) . ?
Sb4 F45 1.831(7) . ?
Sb4 F46B 1.833(9) . ?
Sb4 F43B 1.834(9) . ?
Sb4 F45B 1.837(8) . ?
Sb4 F41B 1.838(8) . ?
Sb4 F43 1.842(7) . ?
Sb4 F42B 1.847(8) . ?
Sb4 F42 1.855(7) . ?
Sb4 F41 1.857(7) . ?
F41 F44B 0.98(2) . ?
F42 F44B 1.77(2) . ?
F43 F41B 1.08(3) . ?
F43 F45B 1.41(4) . ?
F44 F42B 1.63(3) . ?
F44 F45B 1.65(3) . ?
F44 F46B 1.66(7) . ?
F45 F43B 1.24(4) . ?
F45 F46B 1.42(10) . ?
F46 F42B 1.22(3) . ?
