#------------------------------------------------------------------------------
#$Date: 2016-03-25 12:19:48 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179810 $
#$URL: svn://www.crystallography.net/cod/cif/7/01/06/7010680.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7010680
loop_
_publ_author_name
'Chérioux, Frédéric'
'Maisse-François, Aline'
'Neels, Antonia'
'Stoeckli-Evans, Helen'
'Süss-Fink, Georg'
_publ_section_title
;
 Nucleophilic addition reactions on the electron-deficient cluster
 dication [H4Ru4(C6H6)4]2+: synthesis and structural characterisation
 of the water-soluble cluster cations [H3Ru4(C6H6)4(CO)]+and
 [H3Ru4(C6H6)4(OH)]2+†
;
_journal_issue                   14
_journal_name_full
'Journal of the Chemical Society, Dalton Transactions'
_journal_page_first              2184
_journal_paper_doi               10.1039/b102108g
_journal_year                    2001
_chemical_formula_sum            'C24 H46 Cl2 O10 Ru4'
_chemical_formula_weight         969.79
_chemical_name_systematic
; 
? 
;
_space_group_IT_number           8
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  'C -2y'
_symmetry_space_group_name_H-M   'C 1 m 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 106.534(12)
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   9.4441(10)
_cell_length_b                   16.2936(13)
_cell_length_c                   11.2913(12)
_cell_measurement_reflns_used    6062
_cell_measurement_temperature    153(2)
_cell_measurement_theta_max      26.05
_cell_measurement_theta_min      1.65
_cell_volume                     1665.6(3)
_computing_cell_refinement       'CELL, Stoe & Cie Company, Germany'
_computing_data_collection       'EXPOSE, Stoe & Cie Company, Germany'
_computing_data_reduction        'INTEGRATE, Stoe & Cie Company, Germany'
_computing_molecular_graphics    'PLATON97 (Spek, 1997)'
_computing_publication_material  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      153(2)
_diffrn_detector_area_resol_mean 0.81\%A
_diffrn_measured_fraction_theta_full 0.988
_diffrn_measured_fraction_theta_max 0.988
_diffrn_measurement_device_type  'IPDS, Stoe & Cie Company, Germany'
_diffrn_measurement_method       'Phi oscillation scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0507
_diffrn_reflns_av_sigmaI/netI    0.0694
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_k_min       -19
_diffrn_reflns_limit_l_max       13
_diffrn_reflns_limit_l_min       -13
_diffrn_reflns_number            6545
_diffrn_reflns_theta_full        25.94
_diffrn_reflns_theta_max         25.94
_diffrn_reflns_theta_min         1.88
_diffrn_standards_decay_%        0
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    1.987
_exptl_absorpt_correction_type   none
_exptl_crystal_colour            plate
_exptl_crystal_density_diffrn    1.934
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             960
_exptl_crystal_size_max          0.30
_exptl_crystal_size_mid          0.25
_exptl_crystal_size_min          0.05
_refine_diff_density_max         0.876
_refine_diff_density_min         -1.087
_refine_diff_density_rms         0.171
_refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881'
_refine_ls_abs_structure_Flack   -0.03(7)
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.952
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     193
_refine_ls_number_reflns         3255
_refine_ls_number_restraints     2
_refine_ls_restrained_S_all      0.952
_refine_ls_R_factor_all          0.0435
_refine_ls_R_factor_gt           0.0345
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0393P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0734
_refine_ls_wR_factor_ref         0.0755
_reflns_number_gt                2810
_reflns_number_total             3255
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b102108g.txt
_cod_data_source_block           compound4a
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_crystal_density_meas' value 'none' was changed to '?' - the
value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 3008 2015-01-20 13:52:24Z robertas 
;
_cod_original_sg_symbol_H-M      'C m'
_cod_database_code               7010680
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'x, -y, z'
'x+1/2, y+1/2, z'
'x+1/2, -y+1/2, z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
C1 C -0.2165(10) 0.2161(5) -0.1915(8) 0.033(2) Uani 1 1 d . . .
H1 H -0.1277 0.2431 -0.1482 0.039 Uiso 1 1 calc R . .
C2 C -0.2496(12) 0.2034(5) -0.3228(8) 0.037(2) Uani 1 1 d . . .
H2 H -0.1834 0.2222 -0.3664 0.044 Uiso 1 1 calc R . .
C3 C -0.3800(11) 0.1631(5) -0.3855(9) 0.033(2) Uani 1 1 d . . .
H3 H -0.4054 0.1579 -0.4728 0.040 Uiso 1 1 calc R . .
C4 C -0.4746(9) 0.1300(6) -0.3208(8) 0.037(2) Uani 1 1 d . . .
H4 H -0.5601 0.0998 -0.3631 0.045 Uiso 1 1 calc R . .
C5 C -0.4388(9) 0.1430(6) -0.1879(8) 0.031(2) Uani 1 1 d . . .
H5 H -0.5002 0.1200 -0.1429 0.038 Uiso 1 1 calc R . .
C6 C -0.3158(9) 0.1885(6) -0.1266(7) 0.026(2) Uani 1 1 d . . .
H6 H -0.2981 0.2012 -0.0415 0.032 Uiso 1 1 calc R . .
C7 C -0.1855(9) 0.0435(5) 0.1302(7) 0.0238(18) Uani 1 1 d . . .
H7 H -0.2734 0.0728 0.1271 0.029 Uiso 1 1 calc R . .
C8 C -0.0517(9) 0.0869(5) 0.1348(7) 0.0217(17) Uani 1 1 d . . .
H8 H -0.0505 0.1452 0.1360 0.026 Uiso 1 1 calc R . .
C9 C 0.0788(8) 0.0427(5) 0.1376(7) 0.0234(17) Uani 1 1 d . . .
H9 H 0.1667 0.0717 0.1394 0.028 Uiso 1 1 calc R . .
C10 C 0.2450(12) 0.0000 -0.1088(11) 0.026(3) Uani 1 2 d S . .
H10 H 0.2934 0.0000 -0.0226 0.031 Uiso 1 2 calc SR . .
C11 C 0.2103(8) 0.0750(5) -0.1704(7) 0.0272(18) Uani 1 1 d . . .
H11 H 0.2274 0.1251 -0.1256 0.033 Uiso 1 1 calc R . .
C12 C 0.1471(8) 0.0754(5) -0.3056(7) 0.0251(18) Uani 1 1 d . . .
H12 H 0.1227 0.1256 -0.3495 0.030 Uiso 1 1 calc R . .
C13 C 0.1237(12) 0.0000 -0.3683(10) 0.023(2) Uani 1 2 d S . .
H13 H 0.0909 0.0000 -0.4560 0.028 Uiso 1 2 calc SR . .
Cl1 Cl 0.4467(2) 0.16751(12) 0.09581(17) 0.0270(4) Uani 1 1 d . . .
Ru1 Ru -0.24882(5) 0.08437(3) -0.22995(5) 0.01211(13) Uani 1 1 d . . .
H1RU H -0.0724 0.0918 -0.2292 0.020 Uiso 1 1 d . . .
Ru2 Ru -0.10013(8) 0.0000 -0.02165(7) 0.01214(19) Uani 1 2 d S . .
Ru3 Ru 0.00609(8) 0.0000 -0.22219(6) 0.01138(18) Uani 1 2 d S . .
O1 O -0.1967(8) 0.0000 -0.3344(7) 0.026(2) Uani 1 2 d S . .
H1O H -0.2301 0.0000 -0.4226 0.020 Uiso 1 2 d S . .
O2 O -0.2341(9) 0.0000 -0.5918(7) 0.027(2) Uani 1 2 d S . .
O3 O -0.0933(6) 0.1499(4) -0.5672(5) 0.0347(15) Uani 1 1 d . . .
O4 O -0.2550(7) 0.2542(3) -0.7542(5) 0.0308(14) Uani 1 1 d . . .
O5 O 0.2011(7) -0.1473(4) -0.5627(5) 0.0351(14) Uani 1 1 d . . .
O6 O 0.3455(10) 0.0000 -0.5631(7) 0.0318(19) Uani 1 2 d S . .
O7 O 0.4850(8) 0.0000 -0.7570(7) 0.0276(18) Uani 1 2 d S . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ru Ru -1.2594 0.8363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C6 C1 C2 120.3(8) . . ?
C6 C1 Ru1 73.6(5) . . ?
C2 C1 Ru1 71.2(5) . . ?
C3 C2 C1 119.4(9) . . ?
C3 C2 Ru1 73.2(5) . . ?
C1 C2 Ru1 70.5(5) . . ?
C2 C3 C4 120.9(8) . . ?
C2 C3 Ru1 70.2(5) . . ?
C4 C3 Ru1 70.5(5) . . ?
C3 C4 C5 118.8(8) . . ?
C3 C4 Ru1 72.5(5) . . ?
C5 C4 Ru1 70.2(4) . . ?
C6 C5 C4 120.6(8) . . ?
C6 C5 Ru1 73.8(5) . . ?
C4 C5 Ru1 71.3(4) . . ?
C5 C6 C1 119.6(7) . . ?
C5 C6 Ru1 69.9(5) . . ?
C1 C6 Ru1 69.3(4) . . ?
C7 C7 C8 119.5(5) 2 . ?
C7 C7 Ru2 71.3(2) 2 . ?
C8 C7 Ru2 71.0(4) . . ?
C9 C8 C7 120.0(7) . . ?
C9 C8 Ru2 70.9(4) . . ?
C7 C8 Ru2 71.0(4) . . ?
C9 C9 C8 120.5(5) 2 . ?
C9 C9 Ru2 71.5(2) 2 . ?
C8 C9 Ru2 71.5(4) . . ?
C11 C10 C11 121.8(11) 2 . ?
C11 C10 Ru3 70.3(5) 2 . ?
C11 C10 Ru3 70.3(5) . . ?
C10 C11 C12 119.2(8) . . ?
C10 C11 Ru3 73.3(6) . . ?
C12 C11 Ru3 70.3(4) . . ?
C13 C12 C11 118.6(8) . . ?
C13 C12 Ru3 72.6(5) . . ?
C11 C12 Ru3 70.8(4) . . ?
C12 C13 C12 122.2(10) 2 . ?
C12 C13 Ru3 70.6(5) 2 . ?
C12 C13 Ru3 70.6(5) . . ?
O1 Ru1 C1 139.4(3) . . ?
O1 Ru1 C5 142.5(3) . . ?
C1 Ru1 C5 67.0(3) . . ?
O1 Ru1 C2 107.3(3) . . ?
C1 Ru1 C2 38.2(3) . . ?
C5 Ru1 C2 80.1(4) . . ?
O1 Ru1 C4 109.3(3) . . ?
C1 Ru1 C4 79.9(4) . . ?
C5 Ru1 C4 38.5(3) . . ?
C2 Ru1 C4 67.2(4) . . ?
O1 Ru1 C3 96.1(3) . . ?
C1 Ru1 C3 67.0(3) . . ?
C5 Ru1 C3 67.5(3) . . ?
C2 Ru1 C3 36.6(4) . . ?
C4 Ru1 C3 36.9(4) . . ?
O1 Ru1 C6 174.5(3) . . ?
C1 Ru1 C6 37.2(3) . . ?
C5 Ru1 C6 36.3(3) . . ?
C2 Ru1 C6 67.6(3) . . ?
C4 Ru1 C6 67.1(3) . . ?
C3 Ru1 C6 78.5(3) . . ?
O1 Ru1 Ru2 90.5(2) . . ?
C1 Ru1 Ru2 108.2(2) . . ?
C5 Ru1 Ru2 106.4(2) . . ?
C2 Ru1 Ru2 141.4(3) . . ?
C4 Ru1 Ru2 139.1(3) . . ?
C3 Ru1 Ru2 173.2(2) . . ?
C6 Ru1 Ru2 94.8(2) . . ?
O1 Ru1 Ru1 45.56(15) . 2 ?
C1 Ru1 Ru1 168.1(2) . 2 ?
C5 Ru1 Ru1 115.7(2) . 2 ?
C2 Ru1 Ru1 151.6(2) . 2 ?
C4 Ru1 Ru1 109.6(3) . 2 ?
C3 Ru1 Ru1 124.9(2) . 2 ?
C6 Ru1 Ru1 139.0(2) . 2 ?
Ru2 Ru1 Ru1 59.900(14) . 2 ?
O1 Ru1 Ru3 45.8(2) . . ?
C1 Ru1 Ru3 114.3(2) . . ?
C5 Ru1 Ru3 165.9(2) . . ?
C2 Ru1 Ru3 109.8(3) . . ?
C4 Ru1 Ru3 154.2(2) . . ?
C3 Ru1 Ru3 126.5(2) . . ?
C6 Ru1 Ru3 137.1(2) . . ?
Ru2 Ru1 Ru3 59.49(2) . . ?
Ru1 Ru1 Ru3 60.030(14) 2 . ?
C9 Ru2 C9 36.9(4) . 2 ?
C9 Ru2 C8 37.6(3) . . ?
C9 Ru2 C8 67.2(3) 2 . ?
C9 Ru2 C8 67.2(3) . 2 ?
C9 Ru2 C8 37.6(3) 2 2 ?
C8 Ru2 C8 79.8(5) . 2 ?
C9 Ru2 C7 68.2(3) . . ?
C9 Ru2 C7 80.3(3) 2 . ?
C8 Ru2 C7 38.0(3) . . ?
C8 Ru2 C7 67.8(3) 2 . ?
C9 Ru2 C7 80.3(3) . 2 ?
C9 Ru2 C7 68.2(3) 2 2 ?
C8 Ru2 C7 67.8(3) . 2 ?
C8 Ru2 C7 38.0(3) 2 2 ?
C7 Ru2 C7 37.4(4) . 2 ?
C9 Ru2 Ru3 107.5(2) . . ?
C9 Ru2 Ru3 107.5(2) 2 . ?
C8 Ru2 Ru3 128.6(2) . . ?
C8 Ru2 Ru3 128.6(2) 2 . ?
C7 Ru2 Ru3 161.3(2) . . ?
C7 Ru2 Ru3 161.3(2) 2 . ?
C9 Ru2 Ru1 161.2(2) . 2 ?
C9 Ru2 Ru1 129.0(2) 2 2 ?
C8 Ru2 Ru1 161.3(2) . 2 ?
C8 Ru2 Ru1 107.7(2) 2 2 ?
C7 Ru2 Ru1 128.0(2) . 2 ?
C7 Ru2 Ru1 107.1(2) 2 2 ?
Ru3 Ru2 Ru1 60.45(2) . 2 ?
C9 Ru2 Ru1 129.0(2) . . ?
C9 Ru2 Ru1 161.2(2) 2 . ?
C8 Ru2 Ru1 107.7(2) . . ?
C8 Ru2 Ru1 161.3(2) 2 . ?
C7 Ru2 Ru1 107.1(2) . . ?
C7 Ru2 Ru1 128.0(2) 2 . ?
Ru3 Ru2 Ru1 60.45(2) . . ?
Ru1 Ru2 Ru1 60.20(3) 2 . ?
O1 Ru3 C12 108.6(3) . 2 ?
O1 Ru3 C12 108.6(3) . . ?
C12 Ru3 C12 67.5(5) 2 . ?
O1 Ru3 C11 141.4(2) . 2 ?
C12 Ru3 C11 38.9(3) 2 2 ?
C12 Ru3 C11 80.4(3) . 2 ?
O1 Ru3 C11 141.4(2) . . ?
C12 Ru3 C11 80.4(3) 2 . ?
C12 Ru3 C11 38.9(3) . . ?
C11 Ru3 C11 66.9(5) 2 . ?
O1 Ru3 C13 97.0(4) . . ?
C12 Ru3 C13 36.8(2) 2 . ?
C12 Ru3 C13 36.8(2) . . ?
C11 Ru3 C13 67.5(3) 2 . ?
C11 Ru3 C13 67.5(3) . . ?
O1 Ru3 C10 175.0(4) . . ?
C12 Ru3 C10 67.4(3) 2 . ?
C12 Ru3 C10 67.4(3) . . ?
C11 Ru3 C10 36.4(2) 2 . ?
C11 Ru3 C10 36.4(2) . . ?
C13 Ru3 C10 78.0(4) . . ?
O1 Ru3 Ru2 90.8(2) . . ?
C12 Ru3 Ru2 139.8(2) 2 . ?
C12 Ru3 Ru2 139.8(2) . . ?
C11 Ru3 Ru2 106.2(2) 2 . ?
C11 Ru3 Ru2 106.2(2) . . ?
C13 Ru3 Ru2 172.2(3) . . ?
C10 Ru3 Ru2 94.2(3) . . ?
O1 Ru3 Ru1 45.50(15) . 2 ?
C12 Ru3 Ru1 109.7(2) 2 2 ?
C12 Ru3 Ru1 153.1(2) . 2 ?
C11 Ru3 Ru1 114.9(2) 2 2 ?
C11 Ru3 Ru1 166.3(2) . 2 ?
C13 Ru3 Ru1 126.2(2) . 2 ?
C10 Ru3 Ru1 138.0(2) . 2 ?
Ru2 Ru3 Ru1 60.06(2) . 2 ?
O1 Ru3 Ru1 45.50(15) . . ?
C12 Ru3 Ru1 153.1(2) 2 . ?
C12 Ru3 Ru1 109.7(2) . . ?
C11 Ru3 Ru1 166.3(2) 2 . ?
C11 Ru3 Ru1 114.9(2) . . ?
C13 Ru3 Ru1 126.2(2) . . ?
C10 Ru3 Ru1 138.0(2) . . ?
Ru2 Ru3 Ru1 60.06(2) . . ?
Ru1 Ru3 Ru1 59.94(3) 2 . ?
Ru1 O1 Ru1 88.9(3) . 2 ?
Ru1 O1 Ru3 88.7(3) . . ?
Ru1 O1 Ru3 88.7(3) 2 . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
C1 C6 1.418(12) . ?
C1 C2 1.440(12) . ?
C1 Ru1 2.194(8) . ?
C2 C3 1.397(14) . ?
C2 Ru1 2.203(8) . ?
C3 C4 1.412(14) . ?
C3 Ru1 2.242(8) . ?
C4 C5 1.456(12) . ?
C4 Ru1 2.215(8) . ?
C5 C6 1.387(12) . ?
C5 Ru1 2.200(7) . ?
C6 Ru1 2.250(8) . ?
C7 C7 1.416(17) 2 ?
C7 C8 1.436(11) . ?
C7 Ru2 2.208(7) . ?
C8 C9 1.419(11) . ?
C8 Ru2 2.208(7) . ?
C9 C9 1.393(16) 2 ?
C9 Ru2 2.201(8) . ?
C10 C11 1.399(10) 2 ?
C10 C11 1.399(10) . ?
C10 Ru3 2.255(11) . ?
C11 C12 1.472(11) . ?
C11 Ru3 2.217(7) . ?
C12 C13 1.403(10) . ?
C12 Ru3 2.210(7) . ?
C13 C12 1.403(10) 2 ?
C13 Ru3 2.235(10) . ?
Ru1 O1 1.963(5) . ?
Ru1 Ru2 2.7411(9) . ?
Ru1 Ru1 2.7494(11) 2 ?
Ru1 Ru3 2.7519(8) . ?
Ru2 C9 2.201(8) 2 ?
Ru2 C8 2.208(7) 2 ?
Ru2 C7 2.208(7) 2 ?
Ru2 Ru3 2.7252(10) . ?
Ru2 Ru1 2.7411(9) 2 ?
Ru3 O1 1.973(8) . ?
Ru3 C12 2.210(7) 2 ?
Ru3 C11 2.217(7) 2 ?
Ru3 Ru1 2.7519(8) 2 ?
O1 Ru1 1.963(5) 2 ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C6 C1 C2 C3 -0.4(13) . . . . ?
Ru1 C1 C2 C3 56.6(7) . . . . ?
C6 C1 C2 Ru1 -57.0(7) . . . . ?
C1 C2 C3 C4 -4.2(13) . . . . ?
Ru1 C2 C3 C4 51.0(7) . . . . ?
C1 C2 C3 Ru1 -55.3(7) . . . . ?
C2 C3 C4 C5 3.8(12) . . . . ?
Ru1 C3 C4 C5 54.7(7) . . . . ?
C2 C3 C4 Ru1 -50.9(7) . . . . ?
C3 C4 C5 C6 1.4(13) . . . . ?
Ru1 C4 C5 C6 57.2(8) . . . . ?
C3 C4 C5 Ru1 -55.8(7) . . . . ?
C4 C5 C6 C1 -6.0(13) . . . . ?
Ru1 C5 C6 C1 50.0(8) . . . . ?
C4 C5 C6 Ru1 -56.0(7) . . . . ?
C2 C1 C6 C5 5.6(13) . . . . ?
Ru1 C1 C6 C5 -50.3(8) . . . . ?
C2 C1 C6 Ru1 55.9(7) . . . . ?
C7 C7 C8 C9 0.9(9) 2 . . . ?
Ru2 C7 C8 C9 -53.3(6) . . . . ?
C7 C7 C8 Ru2 54.2(3) 2 . . . ?
C7 C8 C9 C9 -0.9(9) . . . 2 ?
Ru2 C8 C9 C9 -54.3(3) . . . 2 ?
C7 C8 C9 Ru2 53.4(6) . . . . ?
C11 C10 C11 C12 -5.3(16) 2 . . . ?
Ru3 C10 C11 C12 -55.2(7) . . . . ?
C11 C10 C11 Ru3 49.9(10) 2 . . . ?
C10 C11 C12 C13 0.0(12) . . . . ?
Ru3 C11 C12 C13 -56.6(7) . . . . ?
C10 C11 C12 Ru3 56.6(8) . . . . ?
C11 C12 C13 C12 5.3(15) . . . 2 ?
Ru3 C12 C13 C12 -50.4(9) . . . 2 ?
C11 C12 C13 Ru3 55.8(6) . . . . ?
C6 C1 Ru1 O1 173.1(5) . . . . ?
C2 C1 Ru1 O1 42.1(8) . . . . ?
C6 C1 Ru1 C5 27.3(5) . . . . ?
C2 C1 Ru1 C5 -103.8(6) . . . . ?
C6 C1 Ru1 C2 131.0(8) . . . . ?
C6 C1 Ru1 C4 65.3(5) . . . . ?
C2 C1 Ru1 C4 -65.7(6) . . . . ?
C6 C1 Ru1 C3 101.5(6) . . . . ?
C2 C1 Ru1 C3 -29.5(6) . . . . ?
C2 C1 Ru1 C6 -131.0(8) . . . . ?
C6 C1 Ru1 Ru2 -73.3(5) . . . . ?
C2 C1 Ru1 Ru2 155.7(5) . . . . ?
C6 C1 Ru1 Ru1 -78.3(13) . . . 2 ?
C2 C1 Ru1 Ru1 150.6(9) . . . 2 ?
C6 C1 Ru1 Ru3 -137.3(4) . . . . ?
C2 C1 Ru1 Ru3 91.6(5) . . . . ?
C6 C5 Ru1 O1 -171.1(5) . . . . ?
C4 C5 Ru1 O1 -40.0(8) . . . . ?
C6 C5 Ru1 C1 -27.9(5) . . . . ?
C4 C5 Ru1 C1 103.2(6) . . . . ?
C6 C5 Ru1 C2 -65.5(5) . . . . ?
C4 C5 Ru1 C2 65.6(6) . . . . ?
C6 C5 Ru1 C4 -131.1(8) . . . . ?
C6 C5 Ru1 C3 -101.5(6) . . . . ?
C4 C5 Ru1 C3 29.6(6) . . . . ?
C4 C5 Ru1 C6 131.1(8) . . . . ?
C6 C5 Ru1 Ru2 75.3(5) . . . . ?
C4 C5 Ru1 Ru2 -153.6(5) . . . . ?
C6 C5 Ru1 Ru1 139.3(5) . . . 2 ?
C4 C5 Ru1 Ru1 -89.6(6) . . . 2 ?
C6 C5 Ru1 Ru3 70.3(12) . . . . ?
C4 C5 Ru1 Ru3 -158.7(8) . . . . ?
C3 C2 Ru1 O1 76.6(6) . . . . ?
C1 C2 Ru1 O1 -152.8(5) . . . . ?
C3 C2 Ru1 C1 -130.6(8) . . . . ?
C3 C2 Ru1 C5 -65.4(6) . . . . ?
C1 C2 Ru1 C5 65.1(6) . . . . ?
C3 C2 Ru1 C4 -27.5(5) . . . . ?
C1 C2 Ru1 C4 103.1(6) . . . . ?
C1 C2 Ru1 C3 130.6(8) . . . . ?
C3 C2 Ru1 C6 -101.1(6) . . . . ?
C1 C2 Ru1 C6 29.5(5) . . . . ?
C3 C2 Ru1 Ru2 -169.4(4) . . . . ?
C1 C2 Ru1 Ru2 -38.8(8) . . . . ?
C3 C2 Ru1 Ru1 61.7(8) . . . 2 ?
C1 C2 Ru1 Ru1 -167.7(4) . . . 2 ?
C3 C2 Ru1 Ru3 125.0(5) . . . . ?
C1 C2 Ru1 Ru3 -104.4(5) . . . . ?
C3 C4 Ru1 O1 -74.0(6) . . . . ?
C5 C4 Ru1 O1 155.5(5) . . . . ?
C3 C4 Ru1 C1 65.0(5) . . . . ?
C5 C4 Ru1 C1 -65.5(6) . . . . ?
C3 C4 Ru1 C5 130.5(8) . . . . ?
C3 C4 Ru1 C2 27.3(5) . . . . ?
C5 C4 Ru1 C2 -103.3(6) . . . . ?
C5 C4 Ru1 C3 -130.5(8) . . . . ?
C3 C4 Ru1 C6 101.6(6) . . . . ?
C5 C4 Ru1 C6 -29.0(5) . . . . ?
C3 C4 Ru1 Ru2 171.2(4) . . . . ?
C5 C4 Ru1 Ru2 40.7(7) . . . . ?
C3 C4 Ru1 Ru1 -122.5(5) . . . 2 ?
C5 C4 Ru1 Ru1 107.0(5) . . . 2 ?
C3 C4 Ru1 Ru3 -61.3(9) . . . . ?
C5 C4 Ru1 Ru3 168.2(5) . . . . ?
C2 C3 Ru1 O1 -110.9(5) . . . . ?
C4 C3 Ru1 O1 114.1(5) . . . . ?
C2 C3 Ru1 C1 30.7(6) . . . . ?
C4 C3 Ru1 C1 -104.3(6) . . . . ?
C2 C3 Ru1 C5 104.2(6) . . . . ?
C4 C3 Ru1 C5 -30.8(5) . . . . ?
C4 C3 Ru1 C2 -134.9(8) . . . . ?
C2 C3 Ru1 C4 134.9(8) . . . . ?
C2 C3 Ru1 C6 67.9(6) . . . . ?
C4 C3 Ru1 C6 -67.1(6) . . . . ?
C2 C3 Ru1 Ru2 77(2) . . . . ?
C4 C3 Ru1 Ru2 -58(2) . . . . ?
C2 C3 Ru1 Ru1 -149.3(4) . . . 2 ?
C4 C3 Ru1 Ru1 75.7(6) . . . 2 ?
C2 C3 Ru1 Ru3 -73.3(6) . . . . ?
C4 C3 Ru1 Ru3 151.7(4) . . . . ?
C5 C6 Ru1 O1 80(3) . . . . ?
C1 C6 Ru1 O1 -54(3) . . . . ?
C5 C6 Ru1 C1 134.6(8) . . . . ?
C1 C6 Ru1 C5 -134.6(8) . . . . ?
C5 C6 Ru1 C2 104.2(6) . . . . ?
C1 C6 Ru1 C2 -30.3(5) . . . . ?
C5 C6 Ru1 C4 30.6(6) . . . . ?
C1 C6 Ru1 C4 -104.0(6) . . . . ?
C5 C6 Ru1 C3 67.5(6) . . . . ?
C1 C6 Ru1 C3 -67.0(5) . . . . ?
C5 C6 Ru1 Ru2 -111.4(5) . . . . ?
C1 C6 Ru1 Ru2 114.1(5) . . . . ?
C5 C6 Ru1 Ru1 -63.4(6) . . . 2 ?
C1 C6 Ru1 Ru1 162.0(4) . . . 2 ?
C5 C6 Ru1 Ru3 -160.2(4) . . . . ?
C1 C6 Ru1 Ru3 65.2(6) . . . . ?
C8 C9 Ru2 C9 -132.5(4) . . . 2 ?
C9 C9 Ru2 C8 132.5(4) 2 . . . ?
C9 C9 Ru2 C8 29.2(3) 2 . . 2 ?
C8 C9 Ru2 C8 -103.3(6) . . . 2 ?
C9 C9 Ru2 C7 103.3(3) 2 . . . ?
C8 C9 Ru2 C7 -29.1(5) . . . . ?
C9 C9 Ru2 C7 66.4(2) 2 . . 2 ?
C8 C9 Ru2 C7 -66.0(5) . . . 2 ?
C9 C9 Ru2 Ru3 -96.03(10) 2 . . . ?
C8 C9 Ru2 Ru3 131.5(4) . . . . ?
C9 C9 Ru2 Ru1 -48.8(6) 2 . . 2 ?
C8 C9 Ru2 Ru1 178.8(5) . . . 2 ?
C9 C9 Ru2 Ru1 -161.8(2) 2 . . . ?
C8 C9 Ru2 Ru1 65.7(5) . . . . ?
C7 C8 Ru2 C9 -132.7(7) . . . . ?
C9 C8 Ru2 C9 28.7(4) . . . 2 ?
C7 C8 Ru2 C9 -104.0(5) . . . 2 ?
C9 C8 Ru2 C8 65.8(5) . . . 2 ?
C7 C8 Ru2 C8 -66.9(5) . . . 2 ?
C9 C8 Ru2 C7 132.7(7) . . . . ?
C9 C8 Ru2 C7 103.5(5) . . . 2 ?
C7 C8 Ru2 C7 -29.3(4) . . . 2 ?
C9 C8 Ru2 Ru3 -66.0(5) . . . . ?
C7 C8 Ru2 Ru3 161.3(4) . . . . ?
C9 C8 Ru2 Ru1 -178.8(5) . . . 2 ?
C7 C8 Ru2 Ru1 48.5(10) . . . 2 ?
C9 C8 Ru2 Ru1 -131.9(4) . . . . ?
C7 C8 Ru2 Ru1 95.4(5) . . . . ?
C7 C7 Ru2 C9 -103.0(3) 2 . . . ?
C8 C7 Ru2 C9 28.8(5) . . . . ?
C7 C7 Ru2 C9 -66.6(2) 2 . . 2 ?
C8 C7 Ru2 C9 65.2(5) . . . 2 ?
C7 C7 Ru2 C8 -131.8(4) 2 . . . ?
C7 C7 Ru2 C8 -29.7(3) 2 . . 2 ?
C8 C7 Ru2 C8 102.1(7) . . . 2 ?
C8 C7 Ru2 C7 131.8(4) . . . 2 ?
C7 C7 Ru2 Ru3 176.8(7) 2 . . . ?
C8 C7 Ru2 Ru3 -51.4(9) . . . . ?
C7 C7 Ru2 Ru1 65.96(15) 2 . . 2 ?
C8 C7 Ru2 Ru1 -162.2(4) . . . 2 ?
C7 C7 Ru2 Ru1 131.16(13) 2 . . . ?
C8 C7 Ru2 Ru1 -97.0(5) . . . . ?
O1 Ru1 Ru2 C9 124.6(3) . . . . ?
C1 Ru1 Ru2 C9 -18.8(4) . . . . ?
C5 Ru1 Ru2 C9 -89.4(3) . . . . ?
C2 Ru1 Ru2 C9 5.3(5) . . . . ?
C4 Ru1 Ru2 C9 -114.4(5) . . . . ?
C3 Ru1 Ru2 C9 -63(2) . . . . ?
C6 Ru1 Ru2 C9 -54.3(3) . . . . ?
Ru1 Ru1 Ru2 C9 160.0(3) 2 . . . ?
Ru3 Ru1 Ru2 C9 89.2(3) . . . . ?
O1 Ru1 Ru2 C9 89.0(7) . . . 2 ?
C1 Ru1 Ru2 C9 -54.3(7) . . . 2 ?
C5 Ru1 Ru2 C9 -124.9(7) . . . 2 ?
C2 Ru1 Ru2 C9 -30.2(8) . . . 2 ?
C4 Ru1 Ru2 C9 -149.9(7) . . . 2 ?
C3 Ru1 Ru2 C9 -99(2) . . . 2 ?
C6 Ru1 Ru2 C9 -89.8(7) . . . 2 ?
Ru1 Ru1 Ru2 C9 124.5(6) 2 . . 2 ?
Ru3 Ru1 Ru2 C9 53.7(6) . . . 2 ?
O1 Ru1 Ru2 C8 160.2(3) . . . . ?
C1 Ru1 Ru2 C8 16.9(3) . . . . ?
C5 Ru1 Ru2 C8 -53.7(3) . . . . ?
C2 Ru1 Ru2 C8 41.0(5) . . . . ?
C4 Ru1 Ru2 C8 -78.8(4) . . . . ?
C3 Ru1 Ru2 C8 . . . . . ?
Ru1 Ru1 Ru2 C7 -89.0(3) 2 . . 2 ?
Ru3 Ru1 Ru2 C7 -159.8(3) . . . 2 ?
O1 Ru1 Ru2 Ru3 35.40(18) . . . . ?
C1 Ru1 Ru2 Ru3 -108.0(2) . . . . ?
C5 Ru1 Ru2 Ru3 -178.6(2) . . . . ?
C2 Ru1 Ru2 Ru3 -83.9(4) . . . . ?
C4 Ru1 Ru2 Ru3 156.4(4) . . . . ?
C3 Ru1 Ru2 Ru3 -153(2) . . . . ?
C6 Ru1 Ru2 Ru3 -143.5(2) . . . . ?
Ru1 Ru1 Ru2 Ru3 70.816(16) 2 . . . ?
O1 Ru1 Ru2 Ru1 -35.42(18) . . . 2 ?
C1 Ru1 Ru2 Ru1 -178.8(2) . . . 2 ?
C5 Ru1 Ru2 Ru1 110.6(2) . . . 2 ?
C2 Ru1 Ru2 Ru1 -154.7(4) . . . 2 ?
C4 Ru1 Ru2 Ru1 85.6(4) . . . 2 ?
C3 Ru1 Ru2 Ru1 137(2) . . . 2 ?
C6 Ru1 Ru2 Ru1 145.7(2) . . . 2 ?
Ru3 Ru1 Ru2 Ru1 -70.816(16) . . . 2 ?
C13 C12 Ru3 O1 -76.4(6) . . . . ?
C11 C12 Ru3 O1 153.9(5) . . . . ?
C13 C12 Ru3 C12 26.6(6) . . . 2 ?
C11 C12 Ru3 C12 -103.1(5) . . . 2 ?
C13 C12 Ru3 C11 64.9(6) . . . 2 ?
C11 C12 Ru3 C11 -64.9(6) . . . 2 ?
C13 C12 Ru3 C11 129.8(8) . . . . ?
C11 C12 Ru3 C13 -129.8(8) . . . . ?
C13 C12 Ru3 C10 100.5(6) . . . . ?
C11 C12 Ru3 C10 -29.3(5) . . . . ?
C13 C12 Ru3 Ru2 168.8(5) . . . . ?
C11 C12 Ru3 Ru2 39.0(6) . . . . ?
C13 C12 Ru3 Ru1 -62.8(8) . . . 2 ?
C11 C12 Ru3 Ru1 167.5(4) . . . 2 ?
C13 C12 Ru3 Ru1 -124.7(5) . . . . ?
C11 C12 Ru3 Ru1 105.6(5) . . . . ?
C10 C11 Ru3 O1 -172.5(6) . . . . ?
C12 C11 Ru3 O1 -42.1(7) . . . . ?
C10 C11 Ru3 C12 -64.6(6) . . . 2 ?
C12 C11 Ru3 C12 65.9(6) . . . 2 ?
C10 C11 Ru3 C12 -130.4(8) . . . . ?
C10 C11 Ru3 C11 -26.5(6) . . . 2 ?
C12 C11 Ru3 C11 104.0(5) . . . 2 ?
C10 C11 Ru3 C13 -100.5(6) . . . . ?
C12 C11 Ru3 C13 29.9(5) . . . . ?
C12 C11 Ru3 C10 130.4(8) . . . . ?
C10 C11 Ru3 Ru2 74.6(6) . . . . ?
C12 C11 Ru3 Ru2 -154.9(4) . . . . ?
C10 C11 Ru3 Ru1 74.0(12) . . . 2 ?
C12 C11 Ru3 Ru1 -155.5(8) . . . 2 ?
C10 C11 Ru3 Ru1 138.6(5) . . . . ?
C12 C11 Ru3 Ru1 -90.9(5) . . . . ?
C12 C13 Ru3 O1 -111.9(5) 2 . . . ?
C12 C13 Ru3 O1 111.9(5) . . . . ?
C12 C13 Ru3 C12 -136.2(10) . . . 2 ?
C12 C13 Ru3 C12 136.2(10) 2 . . . ?
C12 C13 Ru3 C11 31.5(5) 2 . . 2 ?
C12 C13 Ru3 C11 -104.8(6) . . . 2 ?
C12 C13 Ru3 C11 104.8(6) 2 . . . ?
C12 C13 Ru3 C11 -31.5(5) . . . . ?
C12 C13 Ru3 C10 68.1(5) 2 . . . ?
C12 C13 Ru3 C10 -68.1(5) . . . . ?
C12 C13 Ru3 Ru2 68.1(5) 2 . . . ?
C12 C13 Ru3 Ru2 -68.1(5) . . . . ?
C12 C13 Ru3 Ru1 -73.6(6) 2 . . 2 ?
C12 C13 Ru3 Ru1 150.1(4) . . . 2 ?
C12 C13 Ru3 Ru1 -150.1(4) 2 . . . ?
C12 C13 Ru3 Ru1 73.6(6) . . . . ?
C11 C10 Ru3 O1 -68.2(5) 2 . . . ?
C11 C10 Ru3 O1 68.2(5) . . . . ?
C11 C10 Ru3 C12 -31.2(5) 2 . . 2 ?
C11 C10 Ru3 C12 105.2(6) . . . 2 ?
C11 C10 Ru3 C12 -105.2(6) 2 . . . ?
C11 C10 Ru3 C12 31.2(5) . . . . ?
C11 C10 Ru3 C11 136.3(11) . . . 2 ?
C11 C10 Ru3 C11 -136.3(11) 2 . . . ?
C11 C10 Ru3 C13 -68.2(5) 2 . . . ?
C11 C10 Ru3 C13 68.2(5) . . . . ?
C11 C10 Ru3 Ru2 111.8(5) 2 . . . ?
C11 C10 Ru3 Ru2 -111.8(5) . . . . ?
C11 C10 Ru3 Ru1 63.6(7) 2 . . 2 ?
C11 C10 Ru3 Ru1 -160.1(4) . . . 2 ?
C11 C10 Ru3 Ru1 160.1(4) 2 . . . ?
C11 C10 Ru3 Ru1 -63.6(7) . . . . ?
C9 Ru2 Ru3 O1 -160.6(2) . . . . ?
C9 Ru2 Ru3 O1 160.6(2) 2 . . . ?
C8 Ru2 Ru3 O1 -124.9(3) . . . . ?
C8 Ru2 Ru3 O1 124.9(3) 2 . . . ?
C7 Ru2 Ru3 O1 -87.0(7) . . . . ?
C7 Ru2 Ru3 O1 87.0(7) 2 . . . ?
Ru1 Ru2 Ru3 O1 35.203(15) 2 . . . ?
Ru1 Ru2 Ru3 O1 -35.203(15) . . . . ?
C9 Ru2 Ru3 C12 78.7(4) . . . 2 ?
C9 Ru2 Ru3 C12 39.9(4) 2 . . 2 ?
C8 Ru2 Ru3 C12 114.4(4) . . . 2 ?
C8 Ru2 Ru3 C12 4.2(5) 2 . . 2 ?
C7 Ru2 Ru3 C12 152.3(8) . . . 2 ?
C7 Ru2 Ru3 C12 -33.7(8) 2 . . 2 ?
Ru1 Ru2 Ru3 C12 -85.5(3) 2 . . 2 ?
Ru1 Ru2 Ru3 C12 -155.9(3) . . . 2 ?
C9 Ru2 Ru3 C12 -39.9(4) . . . . ?
C9 Ru2 Ru3 C12 -78.7(4) 2 . . . ?
C8 Ru2 Ru3 C12 -4.2(5) . . . . ?
C8 Ru2 Ru3 C12 -114.4(4) 2 . . . ?
C7 Ru2 Ru3 C12 33.7(8) . . . . ?
C7 Ru2 Ru3 C12 -152.3(8) 2 . . . ?
Ru1 Ru2 Ru3 C12 155.9(3) 2 . . . ?
Ru1 Ru2 Ru3 C12 85.5(3) . . . . ?
C9 Ru2 Ru3 C11 54.4(3) . . . 2 ?
C9 Ru2 Ru3 C11 15.7(3) 2 . . 2 ?
C8 Ru2 Ru3 C11 90.1(4) . . . 2 ?
C8 Ru2 Ru3 C11 -20.1(4) 2 . . 2 ?
C7 Ru2 Ru3 C11 128.1(7) . . . 2 ?
C7 Ru2 Ru3 C11 -58.0(7) 2 . . 2 ?
Ru1 Ru2 Ru3 C11 -109.8(2) 2 . . 2 ?
Ru1 Ru2 Ru3 C11 179.8(2) . . . 2 ?
C9 Ru2 Ru3 C11 -15.7(3) . . . . ?
C9 Ru2 Ru3 C11 -54.4(3) 2 . . . ?
C8 Ru2 Ru3 C11 20.1(4) . . . . ?
C8 Ru2 Ru3 C11 -90.1(4) 2 . . . ?
C7 Ru2 Ru3 C11 58.0(7) . . . . ?
C7 Ru2 Ru3 C11 -128.1(7) 2 . . . ?
Ru1 Ru2 Ru3 C11 -179.8(2) 2 . . . ?
Ru1 Ru2 Ru3 C11 109.8(2) . . . . ?
C9 Ru2 Ru3 C13 19.4(2) . . . . ?
C9 Ru2 Ru3 C13 -19.4(2) 2 . . . ?
C8 Ru2 Ru3 C13 55.1(3) . . . . ?
C8 Ru2 Ru3 C13 -55.1(3) 2 . . . ?
C7 Ru2 Ru3 C13 93.0(7) . . . . ?
C7 Ru2 Ru3 C13 -93.0(7) 2 . . . ?
Ru1 Ru2 Ru3 C13 -144.797(17) 2 . . . ?
Ru1 Ru2 Ru3 C13 144.797(16) . . . . ?
C9 Ru2 Ru3 C10 19.4(2) . . . . ?
C9 Ru2 Ru3 C10 -19.4(2) 2 . . . ?
C8 Ru2 Ru3 C10 55.1(3) . . . . ?
C8 Ru2 Ru3 C10 -55.1(3) 2 . . . ?
C7 Ru2 Ru3 C10 93.0(7) . . . . ?
C7 Ru2 Ru3 C10 -93.0(7) 2 . . . ?
Ru1 Ru2 Ru3 C10 -144.797(15) 2 . . . ?
Ru1 Ru2 Ru3 C10 144.797(15) . . . . ?
C9 Ru2 Ru3 Ru1 164.2(2) . . . 2 ?
C9 Ru2 Ru3 Ru1 125.4(2) 2 . . 2 ?
C8 Ru2 Ru3 Ru1 -160.1(3) . . . 2 ?
C8 Ru2 Ru3 Ru1 89.7(3) 2 . . 2 ?
C7 Ru2 Ru3 Ru1 -122.2(7) . . . 2 ?
C7 Ru2 Ru3 Ru1 51.8(7) 2 . . 2 ?
Ru1 Ru2 Ru3 Ru1 -70.41(3) . . . 2 ?
C9 Ru2 Ru3 Ru1 -125.4(2) . . . . ?
C9 Ru2 Ru3 Ru1 -164.2(2) 2 . . . ?
C8 Ru2 Ru3 Ru1 -89.7(3) . . . . ?
C8 Ru2 Ru3 Ru1 160.1(3) 2 . . . ?
C7 Ru2 Ru3 Ru1 -51.8(7) . . . . ?
C7 Ru2 Ru3 Ru1 122.2(7) 2 . . . ?
Ru1 Ru2 Ru3 Ru1 70.41(3) 2 . . . ?
C1 Ru1 Ru3 O1 -136.3(3) . . . . ?
C5 Ru1 Ru3 O1 131.7(10) . . . . ?
C2 Ru1 Ru3 O1 -95.2(3) . . . . ?
C4 Ru1 Ru3 O1 -16.9(7) . . . . ?
C3 Ru1 Ru3 O1 -57.8(4) . . . . ?
C6 Ru1 Ru3 O1 -173.3(4) . . . . ?
Ru2 Ru1 Ru3 O1 126.1(2) . . . . ?
Ru1 Ru1 Ru3 O1 55.5(2) 2 . . . ?
O1 Ru1 Ru3 C12 18.2(5) . . . 2 ?
C1 Ru1 Ru3 C12 -118.1(6) . . . 2 ?
C5 Ru1 Ru3 C12 149.9(11) . . . 2 ?
C2 Ru1 Ru3 C12 -77.0(6) . . . 2 ?
C4 Ru1 Ru3 C12 1.3(8) . . . 2 ?
C3 Ru1 Ru3 C12 -39.6(6) . . . 2 ?
C6 Ru1 Ru3 C12 -155.1(6) . . . 2 ?
Ru2 Ru1 Ru3 C12 144.3(5) . . . 2 ?
Ru1 Ru1 Ru3 C12 73.7(5) 2 . . 2 ?
O1 Ru1 Ru3 C12 97.1(3) . . . . ?
C1 Ru1 Ru3 C12 -39.3(3) . . . . ?
C5 Ru1 Ru3 C12 -131.2(10) . . . . ?
C2 Ru1 Ru3 C12 1.9(4) . . . . ?
C4 Ru1 Ru3 C12 80.2(7) . . . . ?
C3 Ru1 Ru3 C12 39.3(4) . . . . ?
C6 Ru1 Ru3 C12 -76.2(4) . . . . ?
Ru2 Ru1 Ru3 C12 -136.8(2) . . . . ?
Ru1 Ru1 Ru3 C12 152.6(2) 2 . . . ?
O1 Ru1 Ru3 C11 -126.7(10) . . . 2 ?
C1 Ru1 Ru3 C11 96.9(10) . . . 2 ?
C5 Ru1 Ru3 C11 5.0(14) . . . 2 ?
C2 Ru1 Ru3 C11 138.1(10) . . . 2 ?
C4 Ru1 Ru3 C11 -143.6(12) . . . 2 ?
C3 Ru1 Ru3 C11 175.5(10) . . . 2 ?
C6 Ru1 Ru3 C11 59.9(10) . . . 2 ?
Ru2 Ru1 Ru3 C11 -0.6(10) . . . 2 ?
Ru1 Ru1 Ru3 C11 -71.2(10) 2 . . 2 ?
O1 Ru1 Ru3 C11 138.8(3) . . . . ?
C1 Ru1 Ru3 C11 2.5(3) . . . . ?
C5 Ru1 Ru3 C11 -89.4(10) . . . . ?
C2 Ru1 Ru3 C11 43.6(4) . . . . ?
C4 Ru1 Ru3 C11 122.0(7) . . . . ?
C3 Ru1 Ru3 C11 81.1(4) . . . . ?
C6 Ru1 Ru3 C11 -34.5(4) . . . . ?
Ru2 Ru1 Ru3 C11 -95.1(2) . . . . ?
Ru1 Ru1 Ru3 C11 -165.7(2) 2 . . . ?
O1 Ru1 Ru3 C13 59.5(3) . . . . ?
C1 Ru1 Ru3 C13 -76.9(3) . . . . ?
C5 Ru1 Ru3 C13 -168.8(10) . . . . ?
C2 Ru1 Ru3 C13 -35.7(4) . . . . ?
C4 Ru1 Ru3 C13 42.6(7) . . . . ?
C3 Ru1 Ru3 C13 1.7(4) . . . . ?
C6 Ru1 Ru3 C13 -113.9(4) . . . . ?
Ru2 Ru1 Ru3 C13 -174.4(2) . . . . ?
Ru1 Ru1 Ru3 C13 114.9(2) 2 . . . ?
O1 Ru1 Ru3 C10 174.7(4) . . . . ?
C1 Ru1 Ru3 C10 38.4(4) . . . . ?
C5 Ru1 Ru3 C10 -53.5(10) . . . . ?
C2 Ru1 Ru3 C10 79.5(4) . . . . ?
C4 Ru1 Ru3 C10 157.9(7) . . . . ?
C3 Ru1 Ru3 C10 117.0(5) . . . . ?
C6 Ru1 Ru3 C10 1.4(5) . . . . ?
Ru2 Ru1 Ru3 C10 -59.2(3) . . . . ?
Ru1 Ru1 Ru3 C10 -129.8(3) 2 . . . ?
O1 Ru1 Ru3 Ru2 -126.1(2) . . . . ?
C1 Ru1 Ru3 Ru2 97.6(2) . . . . ?
C5 Ru1 Ru3 Ru2 5.7(10) . . . . ?
C2 Ru1 Ru3 Ru2 138.7(3) . . . . ?
C4 Ru1 Ru3 Ru2 -142.9(6) . . . . ?
C3 Ru1 Ru3 Ru2 176.1(3) . . . . ?
C6 Ru1 Ru3 Ru2 60.6(3) . . . . ?
Ru1 Ru1 Ru3 Ru2 -70.602(17) 2 . . . ?
O1 Ru1 Ru3 Ru1 -55.5(2) . . . 2 ?
C1 Ru1 Ru3 Ru1 168.2(2) . . . 2 ?
C5 Ru1 Ru3 Ru1 76.3(10) . . . 2 ?
C2 Ru1 Ru3 Ru1 -150.7(3) . . . 2 ?
C4 Ru1 Ru3 Ru1 -72.3(6) . . . 2 ?
C3 Ru1 Ru3 Ru1 -113.3(3) . . . 2 ?
C6 Ru1 Ru3 Ru1 131.2(3) . . . 2 ?
Ru2 Ru1 Ru3 Ru1 70.602(17) . . . 2 ?
C1 Ru1 O1 Ru1 164.1(4) . . . 2 ?
C5 Ru1 O1 Ru1 -73.8(5) . . . 2 ?
C2 Ru1 O1 Ru1 -170.2(3) . . . 2 ?
C4 Ru1 O1 Ru1 -98.9(4) . . . 2 ?
C3 Ru1 O1 Ru1 -134.5(3) . . . 2 ?
C6 Ru1 O1 Ru1 -147(3) . . . 2 ?
Ru2 Ru1 O1 Ru1 44.6(2) . . . 2 ?
Ru3 Ru1 O1 Ru1 88.7(3) . . . 2 ?
C1 Ru1 O1 Ru3 75.3(5) . . . . ?
C5 Ru1 O1 Ru3 -162.6(4) . . . . ?
C2 Ru1 O1 Ru3 101.1(3) . . . . ?
C4 Ru1 O1 Ru3 172.3(3) . . . . ?
C3 Ru1 O1 Ru3 136.8(3) . . . . ?
C6 Ru1 O1 Ru3 124(3) . . . . ?
Ru2 Ru1 O1 Ru3 -44.13(15) . . . . ?
Ru1 Ru1 O1 Ru3 -88.7(3) 2 . . . ?
C12 Ru3 O1 Ru1 -171.4(3) 2 . . . ?
C12 Ru3 O1 Ru1 -99.6(3) . . . . ?
C11 Ru3 O1 Ru1 162.2(4) 2 . . . ?
C11 Ru3 O1 Ru1 -73.3(5) . . . . ?
C13 Ru3 O1 Ru1 -135.54(15) . . . . ?
C10 Ru3 O1 Ru1 -135.54(15) . . . . ?
Ru2 Ru3 O1 Ru1 44.46(15) . . . . ?
Ru1 Ru3 O1 Ru1 88.9(3) 2 . . . ?
C12 Ru3 O1 Ru1 99.6(3) 2 . . 2 ?
C12 Ru3 O1 Ru1 171.4(3) . . . 2 ?
C11 Ru3 O1 Ru1 73.3(5) 2 . . 2 ?
C11 Ru3 O1 Ru1 -162.2(4) . . . 2 ?
C13 Ru3 O1 Ru1 135.54(15) . . . 2 ?
C10 Ru3 O1 Ru1 135.54(15) . . . 2 ?
Ru2 Ru3 O1 Ru1 -44.46(15) . . . 2 ?
Ru1 Ru3 O1 Ru1 -88.9(3) . . . 2 ?
