#------------------------------------------------------------------------------
#$Date: 2016-02-16 03:10:39 +0200 (Tue, 16 Feb 2016) $
#$Revision: 176453 $
#$URL: svn://www.crystallography.net/cod/cif/7/01/13/7011386.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7011386
loop_
_publ_author_name
'Liu, C. W.'
'Shang, Iu-Jie'
'Hung, Chiu-Mine'
'Wang, Ju-Chung'
'Keng, Tai-Chiun'
_publ_section_title
;
 Novel silver diselenophosphate clusters: structures of
 Ag10(µ10-Se)[Se2P(OEt)2]8 and {Ag[Se2P(OPri)2]}6Metal dialkyl
 diselenophosphates. Part 5. For preceding paper see ref. 1.
;
_journal_issue                   9
_journal_name_full
'Journal of the Chemical Society, Dalton Transactions'
_journal_page_first              1974
_journal_paper_doi               10.1039/b111095k
_journal_year                    2002
_chemical_formula_sum            'C34 H85 Ag10 O16.5 P8 Se17'
_chemical_formula_weight         3426.80
_chemical_name_systematic
; 
? 
;
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 107.8720(10)
_cell_angle_gamma                90.00
_cell_formula_units_Z            8
_cell_length_a                   49.153(3)
_cell_length_b                   14.9447(9)
_cell_length_c                   25.3060(15)
_cell_measurement_temperature    298(2)
_cell_volume                     17692.2(18)
_computing_cell_refinement       'Siemens XSCANS'
_computing_data_collection       'Siemens XSCANS'
_computing_data_reduction        'Siemens SHELXTL'
_computing_molecular_graphics    'Siemens SHELXTL'
_computing_publication_material  'Siemens SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      298(2)
_diffrn_measured_fraction_theta_full 0.778
_diffrn_measured_fraction_theta_max 0.778
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0430
_diffrn_reflns_av_sigmaI/netI    0.0385
_diffrn_reflns_limit_h_max       57
_diffrn_reflns_limit_h_min       -35
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_k_min       -17
_diffrn_reflns_limit_l_max       6
_diffrn_reflns_limit_l_min       -30
_diffrn_reflns_number            24371
_diffrn_reflns_theta_full        24.97
_diffrn_reflns_theta_max         24.97
_diffrn_reflns_theta_min         2.11
_exptl_absorpt_coefficient_mu    9.348
_exptl_absorpt_correction_T_max  0.5128
_exptl_absorpt_correction_T_min  0.2620
_exptl_absorpt_correction_type   empirical
_exptl_crystal_colour            YELLOW
_exptl_crystal_density_diffrn    2.573
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       NUGGET
_exptl_crystal_F_000             12712
_exptl_crystal_size_max          0.4
_exptl_crystal_size_mid          0.4
_exptl_crystal_size_min          0.44
_refine_diff_density_max         2.210
_refine_diff_density_min         -1.708
_refine_diff_density_rms         0.127
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.036
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     767
_refine_ls_number_reflns         12086
_refine_ls_number_restraints     13
_refine_ls_restrained_S_all      1.039
_refine_ls_R_factor_all          0.0917
_refine_ls_R_factor_gt           0.0714
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0677P)²+354.4878P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1703
_refine_ls_wR_factor_ref         0.1857
_reflns_number_gt                9086
_reflns_number_total             12086
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b111095k.txt
_cod_data_source_block           ag10
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_cell_volume        17692.0(18)
_cod_original_sg_symbol_H-M      C2/c
_cod_original_formula_sum        'C34 H85 Ag10 O16.50 P8 Se17'
_cod_database_code               7011386
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.17506(3) 0.18881(9) 0.10014(6) 0.1066(4) Uani 1 1 d . A .
Ag2 Ag 0.18327(3) 0.43852(9) 0.15994(6) 0.1053(4) Uani 1 1 d . A .
Ag3 Ag 0.13627(3) 0.17685(11) 0.17244(7) 0.1227(5) Uani 1 1 d . A .
Ag4 Ag 0.13764(4) 0.36793(9) 0.20751(7) 0.1139(5) Uani 1 1 d . . .
Ag5 Ag 0.16406(4) 0.35209(10) 0.03035(7) 0.1184(5) Uani 1 1 d . . .
Ag6 Ag 0.13720(3) 0.52751(13) 0.07043(6) 0.1273(6) Uani 1 1 d . A .
Ag7 Ag 0.07998(4) 0.17899(15) 0.07465(6) 0.1456(7) Uani 1 1 d . . .
Ag8 Ag 0.09111(5) 0.36005(13) -0.01168(8) 0.1617(8) Uani 1 1 d . . .
Ag9 Ag 0.12215(5) 0.18779(12) 0.00318(8) 0.1470(7) Uani 1 1 d . A .
Ag10 Ag 0.08894(10) 0.4368(3) 0.10102(15) 0.1390(13) Uani 0.50 1 d P A 1
Ag11 Ag 0.07337(7) 0.3756(2) 0.07626(12) 0.1018(8) Uani 0.50 1 d P A 2
Se1 Se 0.13040(3) 0.32062(9) 0.09149(5) 0.0710(4) Uani 1 1 d . A .
Se2 Se 0.16133(4) 0.03491(10) 0.14583(7) 0.0969(5) Uani 1 1 d . . .
Se3 Se 0.19079(4) 0.58478(10) 0.10701(7) 0.0902(5) Uani 1 1 d . . .
Se4 Se 0.21353(4) 0.29132(11) 0.17587(7) 0.0887(5) Uani 1 1 d . . .
Se5 Se 0.09586(4) 0.04796(11) 0.01966(8) 0.1081(6) Uani 1 1 d . A .
Se6 Se 0.17030(4) 0.50651(11) 0.24738(6) 0.1020(6) Uani 1 1 d . A .
Se7 Se 0.10934(5) 0.59730(14) 0.13460(8) 0.1131(6) Uani 1 1 d . . .
Se8 Se 0.16959(4) 0.23669(13) 0.27042(6) 0.1050(6) Uani 1 1 d . A .
Se9 Se 0.11176(4) 0.52442(14) -0.03641(7) 0.1040(6) Uani 1 1 d . A .
Se10 Se 0.08525(5) 0.13763(12) 0.17909(8) 0.1066(6) Uani 1 1 d . A .
Se11 Se 0.03002(4) 0.24624(14) 0.02702(9) 0.1106(6) Uani 1 1 d . A .
Se12 Se 0.04780(4) 0.49738(15) 0.00864(8) 0.1152(6) Uani 1 1 d . . .
Se13 Se 0.08226(5) 0.38764(13) 0.19303(9) 0.1149(6) Uani 1 1 d . A .
Se14 Se 0.06442(5) 0.24273(16) -0.08436(7) 0.1265(7) Uani 1 1 d . A .
Se15 Se 0.21603(6) 0.39514(14) 0.04310(11) 0.1358(8) Uani 1 1 d . A .
Se16 Se 0.19219(7) 0.11457(19) 0.02223(10) 0.1644(11) Uani 1 1 d . . .
Se17 Se 0.14307(6) 0.26832(18) -0.07158(8) 0.1343(8) Uani 1 1 d . A .
P1 P 0.21026(11) 0.2455(3) 0.25450(16) 0.0928(13) Uani 1 1 d . A .
P2 P 0.06982(11) 0.5686(3) -0.03869(17) 0.0935(13) Uani 1 1 d . A .
P3 P 0.12483(10) -0.0270(2) 0.08716(19) 0.0900(12) Uani 1 1 d . A .
P4 P 0.07158(11) 0.2554(3) 0.21310(19) 0.0989(14) Uani 1 1 d . . .
P5 P 0.14211(11) 0.6156(3) 0.21015(17) 0.0912(12) Uani 1 1 d . A .
P6 P 0.20948(11) 0.5347(3) 0.0467(2) 0.1004(14) Uani 1 1 d . A .
P7 P 0.17666(12) 0.1737(4) -0.0568(2) 0.1140(17) Uani 1 1 d . A .
P8 P 0.02790(13) 0.2278(4) -0.0587(2) 0.1208(18) Uani 1 1 d . . .
O1 O 0.1337(3) -0.1119(9) 0.0627(7) 0.147(5) Uani 1 1 d . . .
O2 O 0.0505(3) 0.5701(13) -0.1004(6) 0.167(7) Uani 1 1 d D . .
O3 O 0.2311(3) 0.3081(14) 0.2965(6) 0.180(8) Uani 1 1 d D . .
O4 O 0.1596(4) 0.6977(9) 0.2003(7) 0.147(5) Uani 1 1 d . . .
O5 O 0.1038(4) -0.0639(10) 0.1172(7) 0.150(6) Uani 1 1 d . . .
O6 O 0.1301(4) 0.6568(10) 0.2557(7) 0.170(7) Uani 1 1 d . . .
O7 O 0.1902(5) 0.5770(12) -0.0106(6) 0.187(8) Uani 1 1 d . . .
O8 O 0.2383(5) 0.5856(12) 0.0570(11) 0.208(11) Uani 1 1 d . . .
O9 O 0.1698(5) 0.1013(15) -0.1024(7) 0.211(9) Uani 1 1 d . . .
O10 O 0.0720(4) 0.6696(10) -0.0279(9) 0.180(8) Uani 1 1 d D . .
O11 O 0.2214(5) 0.1474(13) 0.2653(9) 0.204(10) Uani 1 1 d D . .
O12 O 0.2072(6) 0.2122(18) -0.0659(12) 0.256(13) Uani 1 1 d D . .
O13 O 0.0395(4) 0.2498(14) 0.2073(11) 0.194(8) Uani 1 1 d D A .
O14 O 0.0134(7) 0.141(2) -0.0823(10) 0.255(13) Uani 1 1 d D A .
O15 O 0.0045(6) 0.282(3) -0.0969(8) 0.301(19) Uani 1 1 d D A .
O16 O 0.0790(6) 0.2460(13) 0.2749(7) 0.215(11) Uani 1 1 d D A .
C1 C 0.1139(8) 0.6144(19) 0.2842(11) 0.184(13) Uani 1 1 d . A .
H1A H 0.1070 0.5591 0.2645 0.221 Uiso 1 1 calc R . .
H1B H 0.1268 0.5977 0.3202 0.221 Uiso 1 1 calc R . .
C2 C 0.1864(7) 0.560(3) -0.0611(11) 0.218(16) Uani 1 1 d . A .
H2A H 0.1799 0.4980 -0.0662 0.262 Uiso 1 1 calc R . .
H2B H 0.2053 0.5599 -0.0656 0.262 Uiso 1 1 calc R . .
C3 C 0.1829(8) 0.732(2) 0.2313(16) 0.239(18) Uani 1 1 d . A .
H3A H 0.1811 0.7274 0.2684 0.287 Uiso 1 1 calc R . .
H3B H 0.1974 0.6893 0.2301 0.287 Uiso 1 1 calc R . .
C4 C 0.1705(7) 0.602(2) -0.1023(11) 0.218(16) Uani 1 1 d . . .
H4A H 0.1713 0.5747 -0.1360 0.326 Uiso 1 1 calc R A .
H4B H 0.1770 0.6630 -0.1009 0.326 Uiso 1 1 calc R . .
H4C H 0.1512 0.6013 -0.1011 0.326 Uiso 1 1 calc R . .
C5 C 0.1104(6) -0.1146(18) 0.1590(13) 0.183(12) Uani 1 1 d . A .
H5A H 0.1245 -0.0846 0.1892 0.220 Uiso 1 1 calc R . .
H5B H 0.1191 -0.1685 0.1502 0.220 Uiso 1 1 calc R . .
C6 C 0.1950(7) 0.807(2) 0.2320(17) 0.29(3) Uani 1 1 d . . .
H6A H 0.2128 0.8075 0.2615 0.433 Uiso 1 1 calc R A .
H6B H 0.1829 0.8538 0.2380 0.433 Uiso 1 1 calc R . .
H6C H 0.1985 0.8162 0.1972 0.433 Uiso 1 1 calc R . .
C7 C 0.0911(7) 0.655(3) 0.2934(12) 0.236(18) Uani 1 1 d . . .
H7A H 0.0824 0.6144 0.3129 0.354 Uiso 1 1 calc R A .
H7B H 0.0774 0.6707 0.2585 0.354 Uiso 1 1 calc R . .
H7C H 0.0973 0.7077 0.3152 0.354 Uiso 1 1 calc R . .
C8 C 0.0845(8) -0.141(2) 0.1789(14) 0.223(16) Uani 1 1 d . . .
H8A H 0.0909 -0.1804 0.2105 0.335 Uiso 1 1 calc R A .
H8B H 0.0705 -0.1718 0.1494 0.335 Uiso 1 1 calc R . .
H8C H 0.0761 -0.0886 0.1891 0.335 Uiso 1 1 calc R . .
C9 C 0.1591(7) -0.1988(19) 0.0165(12) 0.206(14) Uani 1 1 d . . .
H9A H 0.1748 -0.1853 0.0027 0.310 Uiso 1 1 calc R A .
H9B H 0.1430 -0.2181 -0.0136 0.310 Uiso 1 1 calc R . .
H9C H 0.1646 -0.2456 0.0437 0.310 Uiso 1 1 calc R . .
C10 C 0.1522(8) -0.127(2) 0.0393(17) 0.25(2) Uani 1 1 d . A .
H10A H 0.1699 -0.1089 0.0665 0.299 Uiso 1 1 calc R . .
H10B H 0.1484 -0.0823 0.0101 0.299 Uiso 1 1 calc R . .
C11 C 0.0115(9) 0.0549(19) -0.0659(15) 0.222(16) Uani 1 1 d D . .
H11A H 0.0285 0.0235 -0.0675 0.267 Uiso 1 1 calc R A .
H11B H 0.0120 0.0562 -0.0273 0.267 Uiso 1 1 calc R . .
C12 C -0.0108(8) 0.007(2) -0.0934(14) 0.243(19) Uani 1 1 d . A .
H12A H -0.0093 -0.0520 -0.0779 0.365 Uiso 1 1 calc R . .
H12B H -0.0116 0.0034 -0.1317 0.365 Uiso 1 1 calc R . .
H12C H -0.0280 0.0350 -0.0908 0.365 Uiso 1 1 calc R . .
C13 C 0.2362(9) 0.016(3) 0.2710(17) 0.30(3) Uani 1 1 d D . .
H13A H 0.2485 -0.0294 0.2641 0.449 Uiso 1 1 calc R A .
H13B H 0.2166 0.0007 0.2527 0.449 Uiso 1 1 calc R . .
H13C H 0.2393 0.0210 0.3102 0.449 Uiso 1 1 calc R . .
C14 C 0.1457(8) 0.061(2) -0.1299(15) 0.26(2) Uani 1 1 d . A .
H14A H 0.1312 0.1070 -0.1412 0.313 Uiso 1 1 calc R . .
H14B H 0.1404 0.0231 -0.1036 0.313 Uiso 1 1 calc R . .
C15 C 0.1993(7) 0.283(3) -0.1043(16) 0.44(6) Uani 1 1 d D A .
H15A H 0.1903 0.3320 -0.0909 0.526 Uiso 1 1 calc R . .
H15B H 0.1873 0.2634 -0.1404 0.526 Uiso 1 1 calc R . .
C16 C 0.2291(7) 0.304(3) -0.1038(14) 0.236(18) Uani 1 1 d D . .
H16A H 0.2286 0.3508 -0.1301 0.355 Uiso 1 1 calc R A .
H16B H 0.2378 0.2517 -0.1135 0.355 Uiso 1 1 calc R . .
H16C H 0.2401 0.3238 -0.0673 0.355 Uiso 1 1 calc R . .
C17 C 0.2429(6) 0.104(3) 0.2491(14) 0.35(4) Uani 1 1 d D A .
H17A H 0.2620 0.1256 0.2682 0.416 Uiso 1 1 calc R . .
H17B H 0.2394 0.1038 0.2093 0.416 Uiso 1 1 calc R . .
C18 C 0.0505(9) 0.523(3) -0.1479(12) 0.41(4) Uani 1 1 d D A .
H18A H 0.0686 0.5354 -0.1540 0.487 Uiso 1 1 calc R . .
H18B H 0.0507 0.4598 -0.1385 0.487 Uiso 1 1 calc R . .
C19 C 0.0315(8) 0.532(2) -0.1941(11) 0.25(2) Uani 1 1 d . . .
H19A H 0.0347 0.4894 -0.2200 0.381 Uiso 1 1 calc R A .
H19B H 0.0325 0.5915 -0.2077 0.381 Uiso 1 1 calc R . .
H19C H 0.0131 0.5222 -0.1897 0.381 Uiso 1 1 calc R . .
C20 C 0.1437(10) 0.011(2) -0.1745(13) 0.30(3) Uani 1 1 d . . .
H20A H 0.1247 -0.0126 -0.1887 0.457 Uiso 1 1 calc R A .
H20B H 0.1572 -0.0374 -0.1646 0.457 Uiso 1 1 calc R . .
H20C H 0.1478 0.0472 -0.2025 0.457 Uiso 1 1 calc R . .
C21 C 0.0577(6) 0.8117(15) -0.0055(12) 0.177(11) Uani 1 1 d . . .
H21A H 0.0499 0.8391 0.0210 0.266 Uiso 1 1 calc R A .
H21B H 0.0452 0.8229 -0.0424 0.266 Uiso 1 1 calc R . .
H21C H 0.0762 0.8365 -0.0017 0.266 Uiso 1 1 calc R . .
C22 C -0.0300(7) 0.386(3) -0.1512(13) 0.27(2) Uani 1 1 d . A .
H22A H -0.0434 0.4292 -0.1462 0.399 Uiso 1 1 calc R . .
H22B H -0.0401 0.3370 -0.1733 0.399 Uiso 1 1 calc R . .
H22C H -0.0177 0.4132 -0.1697 0.399 Uiso 1 1 calc R . .
C23 C 0.2583(7) 0.389(3) 0.3774(11) 0.27(2) Uani 1 1 d . . .
H23A H 0.2592 0.3904 0.4158 0.410 Uiso 1 1 calc R A .
H23B H 0.2533 0.4477 0.3616 0.410 Uiso 1 1 calc R . .
H23C H 0.2765 0.3722 0.3743 0.410 Uiso 1 1 calc R . .
C24 C 0.2836(7) 0.627(2) 0.0582(14) 0.223(15) Uani 1 1 d . . .
H24A H 0.3016 0.5996 0.0607 0.335 Uiso 1 1 calc R A .
H24B H 0.2859 0.6672 0.0888 0.335 Uiso 1 1 calc R . .
H24C H 0.2768 0.6594 0.0239 0.335 Uiso 1 1 calc R . .
C25 C -0.0107(6) 0.212(3) 0.1688(13) 0.239(18) Uani 1 1 d D A .
H25A H -0.0242 0.1987 0.1333 0.359 Uiso 1 1 calc R . .
H25B H -0.0186 0.2555 0.1876 0.359 Uiso 1 1 calc R . .
H25C H -0.0065 0.1580 0.1906 0.359 Uiso 1 1 calc R . .
C26 C 0.0601(8) 0.7220(19) 0.0037(12) 0.233(18) Uani 1 1 d D A .
H26A H 0.0410 0.6990 -0.0008 0.280 Uiso 1 1 calc R . .
H26B H 0.0711 0.7131 0.0422 0.280 Uiso 1 1 calc R . .
C27 C 0.2635(8) 0.559(3) 0.0598(18) 0.249(19) Uani 1 1 d . A .
H27A H 0.2619 0.5185 0.0293 0.299 Uiso 1 1 calc R . .
H27B H 0.2711 0.5258 0.0939 0.299 Uiso 1 1 calc R . .
C28 C 0.0163(7) 0.248(4) 0.1609(11) 0.30(3) Uani 1 1 d D . .
H28A H 0.0210 0.2114 0.1331 0.358 Uiso 1 1 calc R A .
H28B H 0.0127 0.3079 0.1463 0.358 Uiso 1 1 calc R . .
C29 C 0.2392(8) 0.333(3) 0.3513(10) 0.256(19) Uani 1 1 d D A .
H29A H 0.2218 0.3521 0.3579 0.307 Uiso 1 1 calc R . .
H29B H 0.2445 0.2771 0.3716 0.307 Uiso 1 1 calc R . .
C30 C 0.1019(9) 0.213(3) 0.3708(10) 0.26(2) Uani 1 1 d . A .
H30A H 0.1169 0.2425 0.3989 0.394 Uiso 1 1 calc R . .
H30B H 0.1065 0.1506 0.3698 0.394 Uiso 1 1 calc R . .
H30C H 0.0842 0.2188 0.3793 0.394 Uiso 1 1 calc R . .
C31 C -0.0128(8) 0.352(2) -0.0973(16) 0.213(15) Uani 1 1 d D . .
H31A H -0.0010 0.4012 -0.0775 0.256 Uiso 1 1 calc R A .
H31B H -0.0256 0.3357 -0.0765 0.256 Uiso 1 1 calc R . .
C32 C 0.0993(8) 0.248(4) 0.3242(14) 0.30(3) Uani 1 1 d D . .
H32A H 0.1164 0.2287 0.3158 0.357 Uiso 1 1 calc R A .
H32B H 0.1020 0.3113 0.3324 0.357 Uiso 1 1 calc R . .
C33 C 0.0233(10) 0.101(3) -0.234(2) 0.30(2) Uiso 1 1 d . . .
H0A H 0.0209 0.1434 -0.2068 0.362 Uiso 1 1 calc R . .
H0B H 0.0252 0.1333 -0.2656 0.362 Uiso 1 1 calc R . .
C34 C 0.0515(10) 0.038(3) -0.2065(18) 0.31(2) Uiso 1 1 d . . .
H0C H 0.0682 0.0754 -0.1948 0.463 Uiso 1 1 calc R . .
H0D H 0.0536 -0.0040 -0.2337 0.463 Uiso 1 1 calc R . .
H0E H 0.0493 0.0065 -0.1751 0.463 Uiso 1 1 calc R . .
O O 0.0000 0.043(3) -0.2500 0.258(16) Uiso 1 2 d S . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Se Se -0.0929 2.2259 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Se16 Ag1 Se4 117.10(11) . . ?
Se16 Ag1 Se2 98.01(9) . . ?
Se4 Ag1 Se2 112.51(7) . . ?
Se16 Ag1 Se1 129.84(8) . . ?
Se4 Ag1 Se1 90.98(6) . . ?
Se2 Ag1 Se1 108.75(7) . . ?
Se16 Ag1 Ag5 86.68(8) . . ?
Se4 Ag1 Ag5 85.19(6) . . ?
Se2 Ag1 Ag5 156.36(8) . . ?
Se1 Ag1 Ag5 53.25(5) . . ?
Se16 Ag1 Ag9 77.21(9) . . ?
Se4 Ag1 Ag9 145.84(7) . . ?
Se2 Ag1 Ag9 94.43(7) . . ?
Se1 Ag1 Ag9 59.54(6) . . ?
Ag5 Ag1 Ag9 63.87(6) . . ?
Se16 Ag1 Ag3 147.01(10) . . ?
Se4 Ag1 Ag3 92.19(6) . . ?
Se2 Ag1 Ag3 54.19(6) . . ?
Se1 Ag1 Ag3 58.96(5) . . ?
Ag5 Ag1 Ag3 112.06(6) . . ?
Ag9 Ag1 Ag3 86.84(6) . . ?
Se4 Ag2 Se3 127.65(8) . . ?
Se4 Ag2 Se6 117.32(7) . . ?
Se3 Ag2 Se6 102.12(7) . . ?
Se4 Ag2 Ag6 139.10(8) . . ?
Se3 Ag2 Ag6 55.85(6) . . ?
Se6 Ag2 Ag6 98.07(6) . . ?
Se4 Ag2 Ag4 95.79(6) . . ?
Se3 Ag2 Ag4 136.13(7) . . ?
Se6 Ag2 Ag4 54.15(6) . . ?
Ag6 Ag2 Ag4 88.57(6) . . ?
Se4 Ag2 Ag5 78.72(6) . . ?
Se3 Ag2 Ag5 82.27(5) . . ?
Se6 Ag2 Ag5 151.51(8) . . ?
Ag6 Ag2 Ag5 60.79(5) . . ?
Ag4 Ag2 Ag5 103.37(6) . . ?
Se10 Ag3 Se2 111.45(8) . . ?
Se10 Ag3 Se8 109.88(9) . . ?
Se2 Ag3 Se8 107.72(8) . . ?
Se10 Ag3 Se1 108.54(7) . . ?
Se2 Ag3 Se1 111.42(7) . . ?
Se8 Ag3 Se1 107.76(7) . . ?
Se10 Ag3 Ag4 97.42(7) . . ?
Se2 Ag3 Ag4 150.95(8) . . ?
Se8 Ag3 Ag4 56.79(6) . . ?
Se1 Ag3 Ag4 59.55(5) . . ?
Se10 Ag3 Ag1 147.34(8) . . ?
Se2 Ag3 Ag1 57.57(6) . . ?
Se8 Ag3 Ag1 102.76(7) . . ?
Se1 Ag3 Ag1 58.50(5) . . ?
Ag4 Ag3 Ag1 99.34(6) . . ?
Se10 Ag3 Ag7 54.38(6) . . ?
Se2 Ag3 Ag7 100.19(7) . . ?
Se8 Ag3 Ag7 151.84(8) . . ?
Se1 Ag3 Ag7 63.90(6) . . ?
Ag4 Ag3 Ag7 99.26(7) . . ?
Ag1 Ag3 Ag7 95.19(7) . . ?
Se6 Ag4 Se13 116.53(8) . . ?
Se6 Ag4 Se8 99.78(8) . . ?
Se13 Ag4 Se8 123.26(8) . . ?
Se6 Ag4 Se1 116.54(7) . . ?
Se13 Ag4 Se1 94.85(8) . . ?
Se8 Ag4 Se1 106.53(7) . . ?
Se6 Ag4 Ag3 145.53(8) . . ?
Se13 Ag4 Ag3 97.86(7) . . ?
Se8 Ag4 Ag3 55.75(6) . . ?
Se1 Ag4 Ag3 59.14(5) . . ?
Se6 Ag4 Ag2 55.95(6) . . ?
Se13 Ag4 Ag2 139.28(8) . . ?
Se8 Ag4 Ag2 96.84(7) . . ?
Se1 Ag4 Ag2 64.22(5) . . ?
Ag3 Ag4 Ag2 99.57(6) . . ?
Se6 Ag4 Ag10 106.46(11) . . ?
Se13 Ag4 Ag10 51.09(9) . . ?
Se8 Ag4 Ag10 152.19(11) . . ?
Se1 Ag4 Ag10 53.17(8) . . ?
Ag3 Ag4 Ag10 96.61(10) . . ?
Ag2 Ag4 Ag10 90.40(9) . . ?
Se15 Ag5 Se1 139.01(10) . . ?
Se15 Ag5 Se17 107.69(9) . . ?
Se1 Ag5 Se17 110.21(9) . . ?
Se15 Ag5 Ag1 98.02(9) . . ?
Se1 Ag5 Ag1 62.28(5) . . ?
Se17 Ag5 Ag1 97.51(7) . . ?
Se15 Ag5 Ag9 141.88(8) . . ?
Se1 Ag5 Ag9 60.05(6) . . ?
Se17 Ag5 Ag9 53.88(7) . . ?
Ag1 Ag5 Ag9 58.29(5) . . ?
Se15 Ag5 Ag6 104.16(7) . . ?
Se1 Ag5 Ag6 64.51(5) . . ?
Se17 Ag5 Ag6 126.00(9) . . ?
Ag1 Ag5 Ag6 119.85(6) . . ?
Ag9 Ag5 Ag6 113.48(7) . . ?
Se15 Ag5 Ag2 79.08(7) . . ?
Se1 Ag5 Ag2 62.38(5) . . ?
Se17 Ag5 Ag2 172.45(8) . . ?
Ag1 Ag5 Ag2 77.92(5) . . ?
Ag9 Ag5 Ag2 118.70(6) . . ?
Ag6 Ag5 Ag2 53.50(4) . . ?
Se9 Ag6 Se7 118.09(8) . . ?
Se9 Ag6 Se3 118.45(9) . . ?
Se7 Ag6 Se3 107.76(8) . . ?
Se9 Ag6 Ag2 142.27(8) . . ?
Se7 Ag6 Ag2 97.21(7) . . ?
Se3 Ag6 Ag2 55.73(5) . . ?
Se9 Ag6 Ag10 95.34(10) . . ?
Se7 Ag6 Ag10 54.93(10) . . ?
Se3 Ag6 Ag10 145.74(10) . . ?
Ag2 Ag6 Ag10 94.47(9) . . ?
Se9 Ag6 Ag5 76.85(7) . . ?
Se7 Ag6 Ag5 148.42(9) . . ?
Se3 Ag6 Ag5 85.05(6) . . ?
Ag2 Ag6 Ag5 65.71(5) . . ?
Ag10 Ag6 Ag5 98.29(10) . . ?
Se11 Ag7 Se10 110.13(9) . . ?
Se11 Ag7 Se5 115.64(9) . . ?
Se10 Ag7 Se5 113.36(9) . . ?
Se11 Ag7 Ag11 61.79(9) . . ?
Se10 Ag7 Ag11 101.28(9) . . ?
Se5 Ag7 Ag11 142.30(11) . . ?
Se11 Ag7 Ag3 149.93(9) . . ?
Se10 Ag7 Ag3 53.84(6) . . ?
Se5 Ag7 Ag3 94.42(7) . . ?
Ag11 Ag7 Ag3 94.26(9) . . ?
Se11 Ag7 Ag9 114.54(8) . . ?
Se10 Ag7 Ag9 134.74(9) . . ?
Se5 Ag7 Ag9 51.50(6) . . ?
Ag11 Ag7 Ag9 93.49(9) . . ?
Ag3 Ag7 Ag9 82.82(7) . . ?
Se14 Ag8 Ag11 115.64(13) . . ?
Se14 Ag8 Se1 125.16(10) . . ?
Ag11 Ag8 Se1 62.79(9) . . ?
Se14 Ag8 Se9 125.08(10) . . ?
Ag11 Ag8 Se9 110.32(10) . . ?
Se1 Ag8 Se9 101.52(8) . . ?
Se14 Ag8 Ag9 68.27(8) . . ?
Ag11 Ag8 Ag9 105.12(10) . . ?
Se1 Ag8 Ag9 61.03(6) . . ?
Se9 Ag8 Ag9 125.71(11) . . ?
Se14 Ag8 Ag10 138.59(15) . . ?
Ag11 Ag8 Ag10 22.97(10) . . ?
Se1 Ag8 Ag10 55.12(8) . . ?
Se9 Ag8 Ag10 89.90(11) . . ?
Ag9 Ag8 Ag10 111.49(10) . . ?
Se5 Ag9 Se17 143.05(11) . . ?
Se5 Ag9 Se1 112.88(8) . . ?
Se17 Ag9 Se1 103.87(8) . . ?
Se5 Ag9 Ag8 117.73(10) . . ?
Se17 Ag9 Ag8 79.36(9) . . ?
Se1 Ag9 Ag8 56.71(6) . . ?
Se5 Ag9 Ag1 103.12(8) . . ?
Se17 Ag9 Ag1 98.69(9) . . ?
Se1 Ag9 Ag1 59.02(6) . . ?
Ag8 Ag9 Ag1 112.73(8) . . ?
Se5 Ag9 Ag5 158.87(9) . . ?
Se17 Ag9 Ag5 55.91(7) . . ?
Se1 Ag9 Ag5 51.26(5) . . ?
Ag8 Ag9 Ag5 68.02(7) . . ?
Ag1 Ag9 Ag5 57.83(6) . . ?
Se5 Ag9 Ag7 54.32(7) . . ?
Se17 Ag9 Ag7 151.94(10) . . ?
Se1 Ag9 Ag7 63.26(6) . . ?
Ag8 Ag9 Ag7 72.79(8) . . ?
Ag1 Ag9 Ag7 95.13(7) . . ?
Ag5 Ag9 Ag7 114.24(8) . . ?
Se13 Ag10 Se7 96.32(16) . . ?
Se13 Ag10 Se12 127.28(17) . . ?
Se7 Ag10 Se12 94.72(13) . . ?
Se13 Ag10 Se1 101.83(12) . . ?
Se7 Ag10 Se1 112.62(18) . . ?
Se12 Ag10 Se1 120.60(15) . . ?
Se13 Ag10 Ag6 133.64(19) . . ?
Se7 Ag10 Ag6 54.95(11) . . ?
Se12 Ag10 Ag6 93.72(11) . . ?
Se1 Ag10 Ag6 66.43(10) . . ?
Se13 Ag10 Ag8 141.3(2) . . ?
Se7 Ag10 Ag8 120.98(15) . . ?
Se12 Ag10 Ag8 64.02(10) . . ?
Se1 Ag10 Ag8 56.63(8) . . ?
Ag6 Ag10 Ag8 71.38(9) . . ?
Se13 Ag10 Ag4 53.73(9) . . ?
Se7 Ag10 Ag4 84.74(14) . . ?
Se12 Ag10 Ag4 178.93(18) . . ?
Se1 Ag10 Ag4 58.87(8) . . ?
Ag6 Ag10 Ag4 85.22(12) . . ?
Ag8 Ag10 Ag4 115.48(12) . . ?
Se12 Ag11 Ag8 73.70(10) . . ?
Se12 Ag11 Se1 124.20(12) . . ?
Ag8 Ag11 Se1 61.28(8) . . ?
Se12 Ag11 Se13 122.47(13) . . ?
Ag8 Ag11 Se13 153.24(15) . . ?
Se1 Ag11 Se13 92.67(10) . . ?
Se12 Ag11 Se11 92.42(12) . . ?
Ag8 Ag11 Se11 88.15(11) . . ?
Se1 Ag11 Se11 115.87(12) . . ?
Se13 Ag11 Se11 110.46(11) . . ?
Se12 Ag11 Ag7 137.17(14) . . ?
Ag8 Ag11 Ag7 80.47(10) . . ?
Se1 Ag11 Ag7 66.74(8) . . ?
Se13 Ag11 Ag7 95.39(10) . . ?
Se11 Ag11 Ag7 52.66(8) . . ?
Ag5 Se1 Ag10 123.83(10) . . ?
Ag5 Se1 Ag8 77.99(8) . . ?
Ag10 Se1 Ag8 68.25(10) . . ?
Ag5 Se1 Ag11 130.01(8) . . ?
Ag8 Se1 Ag11 55.93(8) . . ?
Ag5 Se1 Ag1 64.47(5) . . ?
Ag10 Se1 Ag1 170.47(9) . . ?
Ag8 Se1 Ag1 120.20(7) . . ?
Ag11 Se1 Ag1 154.15(9) . . ?
Ag5 Se1 Ag3 126.82(7) . . ?
Ag10 Se1 Ag3 108.65(9) . . ?
Ag8 Se1 Ag3 134.57(8) . . ?
Ag11 Se1 Ag3 100.92(8) . . ?
Ag1 Se1 Ag3 62.55(5) . . ?
Ag5 Se1 Ag9 68.69(6) . . ?
Ag10 Se1 Ag9 124.36(12) . . ?
Ag8 Se1 Ag9 62.26(6) . . ?
Ag11 Se1 Ag9 101.17(9) . . ?
Ag1 Se1 Ag9 61.43(6) . . ?
Ag3 Se1 Ag9 89.84(6) . . ?
Ag5 Se1 Ag4 129.83(7) . . ?
Ag10 Se1 Ag4 67.96(9) . . ?
Ag8 Se1 Ag4 136.17(8) . . ?
Ag11 Se1 Ag4 82.94(8) . . ?
Ag1 Se1 Ag4 103.36(6) . . ?
Ag3 Se1 Ag4 61.30(5) . . ?
Ag9 Se1 Ag4 151.00(7) . . ?
P3 Se2 Ag3 99.52(13) . . ?
P3 Se2 Ag1 109.21(13) . . ?
Ag3 Se2 Ag1 68.24(6) . . ?
P6 Se3 Ag2 103.23(14) . . ?
P6 Se3 Ag6 103.63(15) . . ?
Ag2 Se3 Ag6 68.42(6) . . ?
P1 Se4 Ag2 102.06(13) . . ?
P1 Se4 Ag1 103.84(14) . . ?
Ag2 Se4 Ag1 97.22(7) . . ?
P3 Se5 Ag9 107.93(15) . . ?
P3 Se5 Ag7 101.28(14) . . ?
Ag9 Se5 Ag7 74.17(8) . . ?
P5 Se6 Ag4 101.14(15) . . ?
P5 Se6 Ag2 102.07(12) . . ?
Ag4 Se6 Ag2 69.90(6) . . ?
P5 Se7 Ag10 121.33(16) . . ?
P5 Se7 Ag6 102.32(14) . . ?
Ag10 Se7 Ag6 70.12(10) . . ?
P1 Se8 Ag3 100.73(13) . . ?
P1 Se8 Ag4 104.42(13) . . ?
Ag3 Se8 Ag4 67.46(6) . . ?
P2 Se9 Ag6 99.97(13) . . ?
P2 Se9 Ag8 82.25(14) . . ?
Ag6 Se9 Ag8 82.83(7) . . ?
P4 Se10 Ag3 105.31(15) . . ?
P4 Se10 Ag7 105.13(14) . . ?
Ag3 Se10 Ag7 71.78(7) . . ?
P8 Se11 Ag7 99.50(18) . . ?
P8 Se11 Ag11 108.90(18) . . ?
Ag7 Se11 Ag11 65.55(9) . . ?
P2 Se12 Ag11 120.23(17) . . ?
P2 Se12 Ag10 106.04(17) . . ?
P4 Se13 Ag10 126.10(19) . . ?
P4 Se13 Ag4 100.40(16) . . ?
Ag10 Se13 Ag4 75.18(11) . . ?
P4 Se13 Ag11 102.48(16) . . ?
Ag4 Se13 Ag11 87.74(9) . . ?
P8 Se14 Ag8 98.47(18) . . ?
P6 Se15 Ag5 95.41(16) . . ?
P7 Se16 Ag1 115.55(18) . . ?
P7 Se17 Ag9 91.27(17) . . ?
P7 Se17 Ag5 95.15(15) . . ?
Ag9 Se17 Ag5 70.21(7) . . ?
O3 P1 O11 109.0(13) . . ?
O3 P1 Se4 102.8(8) . . ?
O11 P1 Se4 109.8(7) . . ?
O3 P1 Se8 111.4(7) . . ?
O11 P1 Se8 101.9(9) . . ?
Se4 P1 Se8 121.8(2) . . ?
O10 P2 O2 98.8(11) . . ?
O10 P2 Se12 114.4(7) . . ?
O2 P2 Se12 108.1(7) . . ?
O10 P2 Se9 106.5(7) . . ?
O2 P2 Se9 108.5(7) . . ?
Se12 P2 Se9 118.7(2) . . ?
O1 P3 O5 102.5(9) . . ?
O1 P3 Se2 110.7(6) . . ?
O5 P3 Se2 110.7(6) . . ?
O1 P3 Se5 108.0(7) . . ?
O5 P3 Se5 101.1(7) . . ?
Se2 P3 Se5 121.84(18) . . ?
O16 P4 O13 90.5(14) . . ?
O16 P4 Se13 109.5(8) . . ?
O13 P4 Se13 110.2(9) . . ?
O16 P4 Se10 109.5(9) . . ?
O13 P4 Se10 110.7(8) . . ?
Se13 P4 Se10 121.9(2) . . ?
O4 P5 O6 99.2(9) . . ?
O4 P5 Se7 105.2(6) . . ?
O6 P5 Se7 111.2(8) . . ?
O4 P5 Se6 110.5(6) . . ?
O6 P5 Se6 108.1(7) . . ?
Se7 P5 Se6 120.48(19) . . ?
O8 P6 O7 102.5(12) . . ?
O8 P6 Se15 110.3(8) . . ?
O7 P6 Se15 114.0(7) . . ?
O8 P6 Se3 106.0(7) . . ?
O7 P6 Se3 104.0(7) . . ?
Se15 P6 Se3 118.6(2) . . ?
O9 P7 O12 97.8(13) . . ?
O9 P7 Se16 110.5(9) . . ?
O12 P7 Se16 101.2(10) . . ?
O9 P7 Se17 110.8(8) . . ?
O12 P7 Se17 115.2(8) . . ?
Se16 P7 Se17 119.0(2) . . ?
O15 P8 O14 91.8(17) . . ?
O15 P8 Se14 107.6(14) . . ?
O14 P8 Se14 108.3(12) . . ?
O15 P8 Se11 111.9(11) . . ?
O14 P8 Se11 112.3(10) . . ?
Se14 P8 Se11 121.0(3) . . ?
C10 O1 P3 133(2) . . ?
C18 O2 P2 134.0(18) . . ?
C29 O3 P1 142(2) . . ?
C3 O4 P5 131(2) . . ?
C5 O5 P3 126(2) . . ?
C1 O6 P5 127.5(16) . . ?
C2 O7 P6 134(2) . . ?
C27 O8 P6 132(2) . . ?
C14 O9 P7 132(2) . . ?
C26 O10 P2 130.3(19) . . ?
C17 O11 P1 130(2) . . ?
C15 O12 P7 106(2) . . ?
C28 O13 P4 130(2) . . ?
C11 O14 P8 139(3) . . ?
C31 O15 P8 142(3) . . ?
C32 O16 P4 148(3) . . ?
C7 C1 O6 122(3) . . ?
O7 C2 C4 126(4) . . ?
C6 C3 O4 134(4) . . ?
O5 C5 C8 114(3) . . ?
O1 C10 C9 133(4) . . ?
C12 C11 O14 118(3) . . ?
O9 C14 C20 122(4) . . ?
O12 C15 C16 95(3) . . ?
O11 C17 C13 92(3) . . ?
C19 C18 O2 123(3) . . ?
C21 C26 O10 120(3) . . ?
O8 C27 C24 117(4) . . ?
O13 C28 C25 116(3) . . ?
C23 C29 O3 130(3) . . ?
O15 C31 C22 117(3) . . ?
C30 C32 O16 134(4) . . ?
O C33 C34 106(4) . . ?
C33 O C33 103(5) 2_554 . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 Se16 2.617(3) . ?
Ag1 Se4 2.715(2) . ?
Ag1 Se2 2.750(2) . ?
Ag1 Se1 2.907(2) . ?
Ag1 Ag5 2.963(2) . ?
Ag1 Ag9 2.978(3) . ?
Ag1 Ag3 3.026(2) . ?
Ag2 Se4 2.617(2) . ?
Ag2 Se3 2.648(2) . ?
Ag2 Se6 2.683(2) . ?
Ag2 Ag6 2.980(2) . ?
Ag2 Ag4 3.041(2) . ?
Ag2 Ag5 3.378(2) . ?
Ag3 Se10 2.630(3) . ?
Ag3 Se2 2.642(2) . ?
Ag3 Se8 2.672(2) . ?
Ag3 Se1 2.921(2) . ?
Ag3 Ag4 2.985(2) . ?
Ag3 Ag7 3.095(2) . ?
Ag4 Se6 2.625(2) . ?
Ag4 Se13 2.649(3) . ?
Ag4 Se8 2.704(2) . ?
Ag4 Se1 2.934(2) . ?
Ag4 Ag10 3.177(4) . ?
Ag5 Se15 2.557(3) . ?
Ag5 Se1 2.6312(19) . ?
Ag5 Se17 2.766(3) . ?
Ag5 Ag9 3.143(2) . ?
Ag5 Ag6 3.235(2) . ?
Ag6 Se9 2.608(2) . ?
Ag6 Se7 2.639(2) . ?
Ag6 Se3 2.652(2) . ?
Ag6 Ag10 3.032(5) . ?
Ag7 Se11 2.584(3) . ?
Ag7 Se10 2.648(2) . ?
Ag7 Se5 2.655(3) . ?
Ag7 Ag11 2.959(4) . ?
Ag7 Ag9 3.144(3) . ?
Ag8 Se14 2.588(3) . ?
Ag8 Ag11 2.638(4) . ?
Ag8 Se1 2.793(2) . ?
Ag8 Se9 2.801(3) . ?
Ag8 Ag9 2.957(3) . ?
Ag8 Ag10 3.106(4) . ?
Ag9 Se5 2.558(3) . ?
Ag9 Se17 2.698(3) . ?
Ag9 Se1 2.923(2) . ?
Ag10 Se13 2.557(4) . ?
Ag10 Se7 2.638(6) . ?
Ag10 Se12 2.734(4) . ?
Ag10 Se1 2.743(4) . ?
Ag11 Se12 2.549(3) . ?
Ag11 Se1 2.832(3) . ?
Ag11 Se13 2.857(4) . ?
Ag11 Se11 2.864(4) . ?
Se2 P3 2.155(5) . ?
Se3 P6 2.144(5) . ?
Se4 P1 2.157(5) . ?
Se5 P3 2.169(5) . ?
Se6 P5 2.160(5) . ?
Se7 P5 2.106(5) . ?
Se8 P1 2.161(6) . ?
Se9 P2 2.149(5) . ?
Se10 P4 2.155(5) . ?
Se11 P8 2.157(6) . ?
Se12 P2 2.130(5) . ?
Se13 P4 2.146(5) . ?
Se14 P8 2.100(7) . ?
Se15 P6 2.116(5) . ?
Se16 P7 2.103(6) . ?
Se17 P7 2.119(7) . ?
P1 O3 1.543(16) . ?
P1 O11 1.561(17) . ?
P2 O10 1.531(16) . ?
P2 O2 1.559(14) . ?
P3 O1 1.533(14) . ?
P3 O5 1.560(15) . ?
P4 O16 1.500(17) . ?
P4 O13 1.54(2) . ?
P5 O4 1.563(16) . ?
P5 O6 1.573(14) . ?
P6 O8 1.556(19) . ?
P6 O7 1.598(18) . ?
P7 O9 1.542(15) . ?
P7 O12 1.69(3) . ?
P8 O15 1.49(2) . ?
P8 O14 1.51(2) . ?
O1 C10 1.25(3) . ?
O2 C18 1.394(19) . ?
O3 C29 1.370(18) . ?
O4 C3 1.28(3) . ?
O5 C5 1.26(3) . ?
O6 C1 1.38(3) . ?
O7 C2 1.26(3) . ?
O8 C27 1.28(4) . ?
O9 C14 1.32(3) . ?
O10 C26 1.373(18) . ?
O11 C17 1.403(19) . ?
O12 C15 1.407(14) . ?
O13 C28 1.362(18) . ?
O14 C11 1.368(18) . ?
O15 C31 1.353(18) . ?
O16 C32 1.336(19) . ?
C1 C7 1.35(4) . ?
C2 C4 1.27(4) . ?
C3 C6 1.26(4) . ?
C5 C8 1.56(4) . ?
C9 C10 1.31(3) . ?
C11 C12 1.32(4) . ?
C13 C17 1.497(19) . ?
C14 C20 1.33(4) . ?
C15 C16 1.495(19) . ?
C18 C19 1.26(3) . ?
C21 C26 1.36(3) . ?
C22 C31 1.45(4) . ?
C23 C29 1.28(4) . ?
C24 C27 1.42(4) . ?
C25 C28 1.502(19) . ?
C30 C32 1.26(4) . ?
C33 O 1.39(5) . ?
C33 C34 1.64(5) . ?
O C33 1.39(5) 2_554 ?
