#------------------------------------------------------------------------------
#$Date: 2016-03-25 13:08:46 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179828 $
#$URL: svn://www.crystallography.net/cod/cif/7/01/24/7012476.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7012476
loop_
_publ_author_name
'Birte Ahrens'
'Jacqueline M. Cole'
'Jonathan P. Hickey'
'James N. Martin'
'Martin J. Mays'
'Paul R. Raithby'
'Simon J. Teat'
'Anthony D. Woods'
_publ_section_title
;
 Reaction of metallophosphanide anions with MLnX (X = halide) species
 as a simple route to heterometallic transition metal complexes
;
_journal_issue                   7
_journal_name_full               'Dalton Trans.'
_journal_page_first              1389
_journal_page_last               1395
_journal_paper_doi               10.1039/b211243d
_journal_year                    2003
_chemical_formula_sum            'C40 H25 Au O10 Os3 P2'
_chemical_formula_weight         1495.11
_chemical_name_systematic
;
?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                94.6710(10)
_cell_angle_beta                 103.7790(10)
_cell_angle_gamma                111.1270(10)
_cell_formula_units_Z            2
_cell_length_a                   10.0320(2)
_cell_length_b                   13.9040(2)
_cell_length_c                   16.4300(4)
_cell_measurement_temperature    180(2)
_cell_volume                     2040.47(7)
_computing_cell_refinement       DENZO
_computing_data_collection       'Bruker Nonius control software'
_computing_data_reduction        DENZO
_computing_molecular_graphics    'SHELXTL (Sheldrick, 1991)'
_computing_publication_material  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-93 (Sheldrick, 1993)'
_diffrn_ambient_temperature      180(2)
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.997
_diffrn_measurement_device_type  'Bruker Nonius Kappa CCD Diffractometer'
_diffrn_measurement_method       'Combined phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71070
_diffrn_reflns_av_R_equivalents  0.0666
_diffrn_reflns_av_sigmaI/netI    0.0468
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_k_min       -17
_diffrn_reflns_limit_l_max       20
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_number            26465
_diffrn_reflns_theta_full        26.37
_diffrn_reflns_theta_max         26.37
_diffrn_reflns_theta_min         3.40
_exptl_absorpt_coefficient_mu    13.028
_exptl_absorpt_correction_T_max  0.4624
_exptl_absorpt_correction_T_min  0.1213
_exptl_absorpt_correction_type   SORTAV
_exptl_crystal_colour            Orange
_exptl_crystal_density_diffrn    2.433
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Block
_exptl_crystal_F_000             1364
_exptl_crystal_size_max          0.28
_exptl_crystal_size_mid          0.12
_exptl_crystal_size_min          0.07
_refine_diff_density_max         2.168
_refine_diff_density_min         -3.752
_refine_diff_density_rms         0.236
_refine_ls_extinction_coef       0.00106(11)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.067
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     506
_refine_ls_number_reflns         8336
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.067
_refine_ls_R_factor_all          0.0368
_refine_ls_R_factor_gt           0.0333
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0525P)²+1.4713P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0857
_refine_ls_wR_factor_ref         0.0880
_reflns_number_gt                7673
_reflns_number_total             8336
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b211243d.txt
_cod_data_source_block           for_complex_10
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7012476
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Os1 Os 0.25475(2) 0.263620(15) 0.226222(13) 0.01990(8) Uani 1 1 d . . .
Os2 Os 0.46405(2) 0.160680(15) 0.218152(13) 0.02043(8) Uani 1 1 d . . .
Os3 Os 0.41296(2) 0.294339(18) 0.098130(14) 0.02704(8) Uani 1 1 d . . .
Au1 Au 0.17578(2) 0.049517(15) 0.226240(13) 0.02279(8) Uani 1 1 d . . .
P2 P 0.02695(15) -0.11237(10) 0.24653(9) 0.0218(3) Uani 1 1 d . . .
P1 P 0.48597(15) 0.29381(10) 0.32578(9) 0.0205(3) Uani 1 1 d . . .
C11 C 0.1541(7) 0.2505(5) 0.3116(4) 0.0323(13) Uani 1 1 d . . .
O11 O 0.0902(6) 0.2494(4) 0.3612(3) 0.0510(13) Uani 1 1 d . . .
C12 C 0.2805(7) 0.4040(5) 0.2200(4) 0.0321(13) Uani 1 1 d . . .
O12 O 0.2941(6) 0.4893(4) 0.2171(4) 0.0509(13) Uani 1 1 d . . .
C13 C 0.0676(7) 0.1982(5) 0.1362(4) 0.0291(13) Uani 1 1 d . . .
O13 O -0.0454(5) 0.1624(4) 0.0865(3) 0.0443(12) Uani 1 1 d . . .
C21 C 0.6651(7) 0.2102(5) 0.2126(4) 0.0349(14) Uani 1 1 d . . .
O21 O 0.7835(5) 0.2368(5) 0.2096(3) 0.0548(14) Uani 1 1 d . . .
C22 C 0.4859(6) 0.0671(4) 0.2940(4) 0.0280(12) Uani 1 1 d . . .
O22 O 0.5057(5) 0.0097(3) 0.3368(3) 0.0383(10) Uani 1 1 d . . .
C23 C 0.3862(6) 0.0512(5) 0.1172(4) 0.0302(13) Uani 1 1 d . . .
O23 O 0.3481(5) -0.0142(4) 0.0600(3) 0.0400(11) Uani 1 1 d . . .
C31 C 0.3416(8) 0.3822(6) 0.0310(5) 0.0446(17) Uani 1 1 d . . .
O31 O 0.3042(7) 0.4348(5) -0.0094(4) 0.078(2) Uani 1 1 d . . .
C32 C 0.5493(8) 0.2726(7) 0.0424(5) 0.0501(19) Uani 1 1 d . . .
O32 O 0.6350(7) 0.2608(7) 0.0131(4) 0.094(3) Uani 1 1 d . . .
C33 C 0.5769(7) 0.4221(5) 0.1685(4) 0.0380(15) Uani 1 1 d . . .
O33 O 0.6705(6) 0.5004(4) 0.1976(3) 0.0592(15) Uani 1 1 d . . .
C34 C 0.2437(7) 0.1694(5) 0.0304(4) 0.0325(13) Uani 1 1 d . . .
O34 O 0.1443(5) 0.0979(4) -0.0124(3) 0.0407(11) Uani 1 1 d . . .
C201 C -0.1710(6) -0.1408(4) 0.2150(3) 0.0260(12) Uani 1 1 d . . .
C202 C -0.2769(7) -0.2409(5) 0.2104(4) 0.0368(15) Uani 1 1 d . . .
H202 H -0.2464 -0.2970 0.2213 0.044 Uiso 1 1 calc R . .
C203 C -0.4282(7) -0.2580(6) 0.1898(5) 0.0473(18) Uani 1 1 d . . .
H203 H -0.5008 -0.3259 0.1865 0.057 Uiso 1 1 calc R . .
C204 C -0.4709(7) -0.1789(7) 0.1746(4) 0.0479(19) Uani 1 1 d . . .
H204 H -0.5740 -0.1916 0.1604 0.057 Uiso 1 1 calc R . .
C205 C -0.3679(8) -0.0788(7) 0.1792(5) 0.053(2) Uani 1 1 d . . .
H205 H -0.3997 -0.0233 0.1684 0.064 Uiso 1 1 calc R . .
C206 C -0.2188(7) -0.0611(5) 0.1997(4) 0.0379(15) Uani 1 1 d . . .
H206 H -0.1475 0.0075 0.2034 0.045 Uiso 1 1 calc R . .
C211 C 0.0469(6) -0.2235(4) 0.1930(4) 0.0246(11) Uani 1 1 d . . .
C212 C 0.0271(7) -0.3157(5) 0.2256(4) 0.0342(14) Uani 1 1 d . . .
H212 H 0.0037 -0.3213 0.2782 0.041 Uiso 1 1 calc R . .
C213 C 0.0413(8) -0.3984(5) 0.1823(5) 0.0452(17) Uani 1 1 d . . .
H213 H 0.0270 -0.4609 0.2049 0.054 Uiso 1 1 calc R . .
C214 C 0.0757(8) -0.3916(6) 0.1066(5) 0.0439(17) Uani 1 1 d . . .
H214 H 0.0877 -0.4487 0.0779 0.053 Uiso 1 1 calc R . .
C215 C 0.0932(7) -0.3022(6) 0.0719(4) 0.0400(15) Uani 1 1 d . . .
H215 H 0.1143 -0.2989 0.0186 0.048 Uiso 1 1 calc R . .
C216 C 0.0800(6) -0.2171(5) 0.1144(4) 0.0298(13) Uani 1 1 d . . .
H216 H 0.0931 -0.1553 0.0908 0.036 Uiso 1 1 calc R . .
C221 C 0.0714(6) -0.1224(4) 0.3586(3) 0.0222(11) Uani 1 1 d . . .
C222 C -0.0196(6) -0.1160(4) 0.4095(4) 0.0263(12) Uani 1 1 d . . .
H222 H -0.1105 -0.1088 0.3847 0.032 Uiso 1 1 calc R . .
C223 C 0.0202(7) -0.1201(5) 0.4951(4) 0.0329(13) Uani 1 1 d . . .
H223 H -0.0423 -0.1148 0.5290 0.039 Uiso 1 1 calc R . .
C224 C 0.1533(6) -0.1320(4) 0.5319(4) 0.0294(12) Uani 1 1 d . . .
H224 H 0.1805 -0.1359 0.5906 0.035 Uiso 1 1 calc R . .
C225 C 0.2440(7) -0.1379(5) 0.4829(4) 0.0314(13) Uani 1 1 d . . .
H225 H 0.3344 -0.1457 0.5079 0.038 Uiso 1 1 calc R . .
C226 C 0.2048(6) -0.1327(4) 0.3969(4) 0.0293(12) Uani 1 1 d . . .
H226 H 0.2692 -0.1362 0.3637 0.035 Uiso 1 1 calc R . .
C101 C 0.6448(6) 0.4192(4) 0.3571(4) 0.0256(12) Uani 1 1 d . . .
C102 C 0.7879(7) 0.4214(5) 0.3680(4) 0.0344(14) Uani 1 1 d . . .
H102 H 0.8017 0.3586 0.3543 0.041 Uiso 1 1 calc R . .
C103 C 0.9112(7) 0.5167(5) 0.3995(4) 0.0409(16) Uani 1 1 d . . .
H103 H 1.0089 0.5185 0.4068 0.049 Uiso 1 1 calc R . .
C104 C 0.8923(8) 0.6078(5) 0.4198(5) 0.0450(17) Uani 1 1 d . . .
H104 H 0.9768 0.6722 0.4408 0.054 Uiso 1 1 calc R . .
C105 C 0.7509(8) 0.6059(5) 0.4099(4) 0.0455(17) Uani 1 1 d . . .
H105 H 0.7375 0.6686 0.4245 0.055 Uiso 1 1 calc R . .
C106 C 0.6285(7) 0.5114(4) 0.3782(4) 0.0348(14) Uani 1 1 d . . .
H106 H 0.5311 0.5103 0.3710 0.042 Uiso 1 1 calc R . .
C111 C 0.4792(6) 0.2629(4) 0.4322(3) 0.0210(11) Uani 1 1 d . . .
C112 C 0.3753(6) 0.1680(4) 0.4403(3) 0.0252(11) Uani 1 1 d . . .
H112 H 0.3064 0.1199 0.3905 0.030 Uiso 1 1 calc R . .
C113 C 0.3708(7) 0.1426(5) 0.5202(4) 0.0310(13) Uani 1 1 d . . .
H113 H 0.2993 0.0776 0.5245 0.037 Uiso 1 1 calc R . .
C114 C 0.4707(7) 0.2123(5) 0.5933(4) 0.0336(14) Uani 1 1 d . . .
H114 H 0.4676 0.1952 0.6478 0.040 Uiso 1 1 calc R . .
C115 C 0.5738(7) 0.3056(5) 0.5869(4) 0.0369(14) Uani 1 1 d . . .
H115 H 0.6427 0.3531 0.6370 0.044 Uiso 1 1 calc R . .
C116 C 0.5776(7) 0.3310(4) 0.5074(4) 0.0296(13) Uani 1 1 d . . .
H116 H 0.6491 0.3964 0.5040 0.036 Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Au Au -2.0133 8.8022 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Os Os -1.2165 7.6030 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C12 Os1 C11 95.9(3) . . ?
C12 Os1 C13 96.7(3) . . ?
C11 Os1 C13 91.8(2) . . ?
C12 Os1 P1 99.26(18) . . ?
C11 Os1 P1 92.86(18) . . ?
C13 Os1 P1 162.78(18) . . ?
C12 Os1 Au1 172.30(18) . . ?
C11 Os1 Au1 81.18(18) . . ?
C13 Os1 Au1 76.32(17) . . ?
P1 Os1 Au1 88.03(3) . . ?
C12 Os1 Os3 81.5(2) . . ?
C11 Os1 Os3 177.28(18) . . ?
C13 Os1 Os3 89.29(17) . . ?
P1 Os1 Os3 86.82(3) . . ?
Au1 Os1 Os3 101.510(9) . . ?
C12 Os1 Os2 128.97(19) . . ?
C11 Os1 Os2 122.31(18) . . ?
C13 Os1 Os2 112.83(17) . . ?
P1 Os1 Os2 51.27(3) . . ?
Au1 Os1 Os2 57.910(7) . . ?
Os3 Os1 Os2 59.395(7) . . ?
C22 Os2 C21 95.5(3) . . ?
C22 Os2 C23 93.2(2) . . ?
C21 Os2 C23 94.8(2) . . ?
C22 Os2 P1 94.55(17) . . ?
C21 Os2 P1 99.85(18) . . ?
C23 Os2 P1 162.67(17) . . ?
C22 Os2 Au1 75.48(17) . . ?
C21 Os2 Au1 168.4(2) . . ?
C23 Os2 Au1 78.75(17) . . ?
P1 Os2 Au1 88.23(3) . . ?
C22 Os2 Os3 176.64(16) . . ?
C21 Os2 Os3 87.3(2) . . ?
C23 Os2 Os3 84.69(19) . . ?
P1 Os2 Os3 86.79(3) . . ?
Au1 Os2 Os3 101.501(9) . . ?
C22 Os2 Os1 119.43(17) . . ?
C21 Os2 Os1 133.5(2) . . ?
C23 Os2 Os1 111.41(17) . . ?
P1 Os2 Os1 51.41(3) . . ?
Au1 Os2 Os1 58.060(7) . . ?
Os3 Os2 Os1 59.236(7) . . ?
C32 Os3 C31 101.8(3) . . ?
C32 Os3 C34 94.2(3) . . ?
C31 Os3 C34 90.9(3) . . ?
C32 Os3 C33 88.5(3) . . ?
C31 Os3 C33 88.1(3) . . ?
C34 Os3 C33 177.3(3) . . ?
C32 Os3 Os1 153.4(2) . . ?
C31 Os3 Os1 104.8(2) . . ?
C34 Os3 Os1 84.62(18) . . ?
C33 Os3 Os1 93.20(19) . . ?
C32 Os3 Os2 92.0(2) . . ?
C31 Os3 Os2 166.1(2) . . ?
C34 Os3 Os2 86.04(18) . . ?
C33 Os3 Os2 94.30(18) . . ?
Os1 Os3 Os2 61.369(7) . . ?
P2 Au1 Os2 141.01(4) . . ?
P2 Au1 Os1 153.68(4) . . ?
Os2 Au1 Os1 64.030(7) . . ?
C201 P2 C211 105.8(3) . . ?
C201 P2 C221 104.8(3) . . ?
C211 P2 C221 104.6(2) . . ?
C201 P2 Au1 114.68(19) . . ?
C211 P2 Au1 114.96(19) . . ?
C221 P2 Au1 111.04(17) . . ?
C101 P1 C111 99.5(2) . . ?
C101 P1 Os2 121.7(2) . . ?
C111 P1 Os2 118.72(17) . . ?
C101 P1 Os1 124.14(19) . . ?
C111 P1 Os1 116.49(17) . . ?
Os2 P1 Os1 77.32(4) . . ?
O11 C11 Os1 174.3(6) . . ?
O12 C12 Os1 178.6(6) . . ?
O13 C13 Os1 176.0(5) . . ?
O21 C21 Os2 178.1(6) . . ?
O22 C22 Os2 175.3(5) . . ?
O23 C23 Os2 175.8(5) . . ?
O31 C31 Os3 177.5(7) . . ?
O32 C32 Os3 176.7(7) . . ?
O33 C33 Os3 169.6(6) . . ?
O34 C34 Os3 177.2(6) . . ?
C206 C201 C202 118.8(6) . . ?
C206 C201 P2 119.6(5) . . ?
C202 C201 P2 121.5(5) . . ?
C201 C202 C203 119.5(6) . . ?
C204 C203 C202 120.1(7) . . ?
C203 C204 C205 121.4(6) . . ?
C206 C205 C204 118.9(7) . . ?
C205 C206 C201 121.3(6) . . ?
C212 C211 C216 118.9(5) . . ?
C212 C211 P2 122.6(5) . . ?
C216 C211 P2 118.5(4) . . ?
C213 C212 C211 120.5(6) . . ?
C212 C213 C214 120.6(7) . . ?
C213 C214 C215 120.3(6) . . ?
C214 C215 C216 120.4(6) . . ?
C215 C216 C211 119.2(6) . . ?
C222 C221 C226 118.2(5) . . ?
C222 C221 P2 122.6(4) . . ?
C226 C221 P2 119.2(4) . . ?
C223 C222 C221 121.1(5) . . ?
C222 C223 C224 119.7(6) . . ?
C225 C224 C223 119.8(6) . . ?
C224 C225 C226 120.5(6) . . ?
C225 C226 C221 120.7(5) . . ?
C106 C101 C102 118.9(5) . . ?
C106 C101 P1 121.4(5) . . ?
C102 C101 P1 119.4(4) . . ?
C101 C102 C103 119.5(6) . . ?
C104 C103 C102 120.6(6) . . ?
C103 C104 C105 120.1(6) . . ?
C104 C105 C106 119.3(6) . . ?
C101 C106 C105 121.6(6) . . ?
C112 C111 C116 117.1(5) . . ?
C112 C111 P1 120.5(4) . . ?
C116 C111 P1 122.4(4) . . ?
C111 C112 C113 121.1(5) . . ?
C114 C113 C112 119.9(6) . . ?
C115 C114 C113 120.0(6) . . ?
C114 C115 C116 120.1(6) . . ?
C115 C116 C111 121.8(5) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Os1 C12 1.889(6) . ?
Os1 C11 1.898(6) . ?
Os1 C13 1.941(6) . ?
Os1 P1 2.3688(14) . ?
Os1 Au1 2.7910(3) . ?
Os1 Os3 2.8947(3) . ?
Os1 Os2 2.9568(3) . ?
Os2 C22 1.907(6) . ?
Os2 C21 1.909(6) . ?
Os2 C23 1.948(6) . ?
Os2 P1 2.3643(13) . ?
Os2 Au1 2.7864(3) . ?
Os2 Os3 2.8995(3) . ?
Os3 C32 1.910(7) . ?
Os3 C31 1.923(7) . ?
Os3 C34 1.949(6) . ?
Os3 C33 1.962(7) . ?
Au1 P2 2.3116(13) . ?
P2 C201 1.811(6) . ?
P2 C211 1.813(5) . ?
P2 C221 1.817(6) . ?
P1 C101 1.818(5) . ?
P1 C111 1.845(5) . ?
C11 O11 1.149(7) . ?
C12 O12 1.150(7) . ?
C13 O13 1.134(7) . ?
C21 O21 1.125(7) . ?
C22 O22 1.144(7) . ?
C23 O23 1.138(7) . ?
C31 O31 1.128(8) . ?
C32 O32 1.134(9) . ?
C33 O33 1.122(8) . ?
C34 O34 1.147(7) . ?
C201 C206 1.375(8) . ?
C201 C202 1.396(8) . ?
C202 C203 1.400(9) . ?
C203 C204 1.336(11) . ?
C204 C205 1.386(11) . ?
C205 C206 1.375(9) . ?
C211 C212 1.396(8) . ?
C211 C216 1.410(8) . ?
C212 C213 1.371(9) . ?
C213 C214 1.369(10) . ?
C214 C215 1.382(10) . ?
C215 C216 1.388(9) . ?
C221 C222 1.397(7) . ?
C221 C226 1.400(7) . ?
C222 C223 1.380(8) . ?
C223 C224 1.403(8) . ?
C224 C225 1.369(9) . ?
C225 C226 1.389(8) . ?
C101 C106 1.378(8) . ?
C101 C102 1.392(9) . ?
C102 C103 1.399(8) . ?
C103 C104 1.373(10) . ?
C104 C105 1.379(10) . ?
C105 C106 1.387(9) . ?
C111 C112 1.396(8) . ?
C111 C116 1.398(7) . ?
C112 C113 1.393(8) . ?
C113 C114 1.387(8) . ?
C114 C115 1.368(9) . ?
C115 C116 1.386(9) . ?
