#------------------------------------------------------------------------------
#$Date: 2025-01-07 17:50:09 +0200 (Tue, 07 Jan 2025) $
#$Revision: 297185 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/01/29/7012949.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7012949
loop_
_publ_author_name
'Lassahn, Paul-Gerhard'
'Lozan, Vasile'
'Wu, Biao'
'Weller, Andrew S.'
'Janiak, Christoph'
_publ_section_title
;
 Dihalogeno(diphosphane)metal(II) complexes (metal = Co, Ni, Pd) as
 pre-catalysts for the vinyl/addition polymerization of norbornene --
 elucidation of the activation process with B(C6F5)3/AlEt3 or
 Ag[closo-1-CB11H12] and evidence for the in situ formation of
 “naked” Pd2+ as a highly active species
;
_journal_coden_ASTM              DTARAF
_journal_issue                   23
_journal_name_full               'Dalton Transactions'
_journal_page_first              4437
_journal_page_last               4450
_journal_paper_doi               10.1039/b302937a
_journal_year                    2003
_chemical_formula_moiety         'Pd{Ph2P(CH2)3PPh2}(CB11H12), [CB11H12O0.22]'
_chemical_formula_sum            'C29 H50 B22 O0.22 P2 Pd'
_chemical_formula_weight         808.37
_chemical_name_systematic
; 
[(1,3-(diphenylphosphino)propane)palladium(II)-
1-carbadodecaboranyl][1-carbadodecaboranyl] 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                102.1920(10)
_cell_angle_beta                 98.5030(10)
_cell_angle_gamma                107.0250(10)
_cell_formula_units_Z            2
_cell_length_a                   10.9600(8)
_cell_length_b                   11.4034(9)
_cell_length_c                   18.4232(14)
_cell_measurement_temperature    213(2)
_cell_volume                     2097.1(3)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      213(2)
_diffrn_measured_fraction_theta_full 0.939
_diffrn_measured_fraction_theta_max 0.939
_diffrn_measurement_device_type  'Bruker AXS CCD'
_diffrn_measurement_method       'ω scan'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0416
_diffrn_reflns_av_sigmaI/netI    0.0879
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_k_min       -15
_diffrn_reflns_limit_l_max       24
_diffrn_reflns_limit_l_min       -23
_diffrn_reflns_number            19180
_diffrn_reflns_theta_full        28.32
_diffrn_reflns_theta_max         28.32
_diffrn_reflns_theta_min         1.94
_exptl_absorpt_coefficient_mu    0.543
_exptl_absorpt_correction_T_max  0.9578
_exptl_absorpt_correction_T_min  0.9181
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.280
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       isometric
_exptl_crystal_F_000             824
_exptl_crystal_size_max          0.16
_exptl_crystal_size_mid          0.12
_exptl_crystal_size_min          0.08
_refine_diff_density_max         1.152
_refine_diff_density_min         -1.241
_refine_diff_density_rms         0.092
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.038
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     493
_refine_ls_number_reflns         9809
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.038
_refine_ls_R_factor_all          0.0971
_refine_ls_R_factor_gt           0.0522
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0389P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0933
_refine_ls_wR_factor_ref         0.1090
_reflns_number_gt                5954
_reflns_number_total             9809
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b302937a.txt
_cod_data_source_block           lass1
_cod_depositor_comments
;
The following automatic conversions were performed:
'_exptl_absorpt_correction_type' value 'Multi-scan' changed to
'multi-scan' according to
'/home/saulius/struct/CIF-dictionaries/cif_core.dic' dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7012949
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Pd Pd 0.92998(3) 0.56958(3) 0.733599(16) 0.03449(10) Uani 1 1 d . . .
P1 P 1.04839(10) 0.57289(10) 0.84567(5) 0.0378(2) Uani 1 1 d . . .
P2 P 0.95971(9) 0.38696(8) 0.67846(5) 0.0306(2) Uani 1 1 d . . .
C1 C 1.0142(4) 0.4224(4) 0.8693(2) 0.0463(10) Uani 1 1 d . . .
H1C H 1.0622 0.4366 0.9214 0.056 Uiso 1 1 calc R . .
H1D H 0.9205 0.3879 0.8677 0.056 Uiso 1 1 calc R . .
C2 C 1.0524(4) 0.3248(4) 0.8150(2) 0.0513(11) Uani 1 1 d . . .
H2C H 1.1434 0.3635 0.8120 0.062 Uiso 1 1 calc R . .
H2D H 1.0480 0.2521 0.8362 0.062 Uiso 1 1 calc R . .
C3 C 0.9667(4) 0.2769(3) 0.7355(2) 0.0447(10) Uani 1 1 d . . .
H3C H 0.8771 0.2352 0.7396 0.054 Uiso 1 1 calc R . .
H3D H 0.9948 0.2107 0.7066 0.054 Uiso 1 1 calc R . .
C111 C 1.0104(4) 0.6778(4) 0.9207(2) 0.0443(10) Uani 1 1 d . . .
C112 C 1.1058(5) 0.7875(4) 0.9666(2) 0.0602(12) Uani 1 1 d . . .
H112 H 1.1927 0.8080 0.9608 0.072 Uiso 1 1 calc R . .
C113 C 1.0704(6) 0.8682(5) 1.0222(3) 0.0781(16) Uani 1 1 d . . .
H113 H 1.1339 0.9430 1.0546 0.094 Uiso 1 1 calc R . .
C114 C 0.9431(7) 0.8372(6) 1.0290(3) 0.0790(17) Uani 1 1 d . . .
H114 H 0.9198 0.8921 1.0658 0.095 Uiso 1 1 calc R . .
C115 C 0.8492(6) 0.7287(6) 0.9836(3) 0.0814(17) Uani 1 1 d . . .
H115 H 0.7622 0.7088 0.9894 0.098 Uiso 1 1 calc R . .
C116 C 0.8827(5) 0.6486(5) 0.9293(2) 0.0642(13) Uani 1 1 d . . .
H116 H 0.8183 0.5735 0.8978 0.077 Uiso 1 1 calc R . .
C121 C 1.2209(4) 0.6297(3) 0.8484(2) 0.0402(9) Uani 1 1 d . . .
C122 C 1.3090(4) 0.6073(4) 0.9012(2) 0.0543(11) Uani 1 1 d . . .
H122 H 1.2792 0.5670 0.9379 0.065 Uiso 1 1 calc R . .
C123 C 1.4398(5) 0.6437(5) 0.9003(3) 0.0643(13) Uani 1 1 d . . .
H123 H 1.4991 0.6279 0.9362 0.077 Uiso 1 1 calc R . .
C124 C 1.4838(4) 0.7028(4) 0.8472(3) 0.0647(13) Uani 1 1 d . . .
H124 H 1.5733 0.7272 0.8468 0.078 Uiso 1 1 calc R . .
C125 C 1.3986(4) 0.7271(4) 0.7946(3) 0.0600(12) Uani 1 1 d . . .
H125 H 1.4295 0.7679 0.7583 0.072 Uiso 1 1 calc R . .
C126 C 1.2668(4) 0.6909(4) 0.7953(2) 0.0481(10) Uani 1 1 d . . .
H126 H 1.2081 0.7078 0.7596 0.058 Uiso 1 1 calc R . .
C211 C 0.8283(3) 0.2894(3) 0.59741(19) 0.0339(8) Uani 1 1 d . . .
C212 C 0.8556(4) 0.2064(3) 0.5405(2) 0.0437(10) Uani 1 1 d . . .
H212 H 0.9420 0.2068 0.5429 0.052 Uiso 1 1 calc R . .
C213 C 0.7562(4) 0.1230(4) 0.4800(2) 0.0511(11) Uani 1 1 d . . .
H213 H 0.7751 0.0670 0.4415 0.061 Uiso 1 1 calc R . .
C214 C 0.6295(4) 0.1224(4) 0.4765(2) 0.0554(12) Uani 1 1 d . . .
H214 H 0.5620 0.0660 0.4355 0.066 Uiso 1 1 calc R . .
C215 C 0.6017(4) 0.2036(4) 0.5325(2) 0.0545(11) Uani 1 1 d . . .
H215 H 0.5152 0.2028 0.5297 0.065 Uiso 1 1 calc R . .
C216 C 0.7005(4) 0.2870(4) 0.5932(2) 0.0447(10) Uani 1 1 d . . .
H216 H 0.6806 0.3421 0.6317 0.054 Uiso 1 1 calc R . .
C221 C 1.1058(3) 0.4343(3) 0.64298(18) 0.0311(8) Uani 1 1 d . . .
C222 C 1.2119(4) 0.3939(4) 0.6607(2) 0.0428(9) Uani 1 1 d . . .
H222 H 1.2071 0.3343 0.6894 0.051 Uiso 1 1 calc R . .
C223 C 1.3242(4) 0.4419(4) 0.6359(2) 0.0537(11) Uani 1 1 d . . .
H223 H 1.3961 0.4150 0.6479 0.064 Uiso 1 1 calc R . .
C224 C 1.3319(4) 0.5285(4) 0.5939(2) 0.0518(11) Uani 1 1 d . . .
H224 H 1.4096 0.5620 0.5782 0.062 Uiso 1 1 calc R . .
C225 C 1.2261(4) 0.5670(4) 0.5746(2) 0.0486(10) Uani 1 1 d . . .
H225 H 1.2309 0.6250 0.5447 0.058 Uiso 1 1 calc R . .
C226 C 1.1135(4) 0.5201(3) 0.5992(2) 0.0380(9) Uani 1 1 d . . .
H226 H 1.0415 0.5464 0.5862 0.046 Uiso 1 1 calc R . .
C1A C 0.7994(4) 0.9319(4) 0.6793(3) 0.0538(11) Uani 1 1 d . . .
H1A H 0.7874 1.0270 0.6915 0.065 Uiso 1 1 calc R . .
B2A B 0.9348(4) 0.9193(4) 0.7300(3) 0.0477(12) Uani 1 1 d . . .
H2A H 1.0121 0.9979 0.7744 0.057 Uiso 1 1 calc R . .
B3A B 0.7753(5) 0.8506(4) 0.7462(3) 0.0503(13) Uani 1 1 d . . .
H3A H 0.7498 0.8847 0.8010 0.060 Uiso 1 1 calc R . .
B4A B 0.6610(4) 0.8024(4) 0.6574(3) 0.0481(12) Uani 1 1 d . . .
H4A H 0.5602 0.8058 0.6541 0.058 Uiso 1 1 calc R . .
B5A B 0.7495(4) 0.8403(4) 0.5876(3) 0.0475(12) Uani 1 1 d . . .
H5A H 0.7057 0.8685 0.5386 0.057 Uiso 1 1 calc R . .
B6A B 0.9183(4) 0.9130(4) 0.6321(3) 0.0487(12) Uani 1 1 d . . .
H6A H 0.9842 0.9880 0.6124 0.058 Uiso 1 1 calc R . .
B7A B 0.8807(4) 0.7620(4) 0.7363(2) 0.0400(11) Uani 1 1 d . . .
H7A H 0.9247 0.7347 0.7856 0.048 Uiso 1 1 calc R . .
B8A B 0.7101(4) 0.6883(4) 0.6933(3) 0.0422(11) Uani 1 1 d . . .
H8A H 0.6426 0.6150 0.7133 0.051 Uiso 1 1 calc R . .
B9A B 0.6953(4) 0.6816(4) 0.5938(3) 0.0410(11) Uani 1 1 d . . .
H9A H 0.6178 0.6037 0.5491 0.049 Uiso 1 1 calc R . .
B10A B 0.8563(4) 0.7506(4) 0.5785(3) 0.0411(11) Uani 1 1 d . . .
H10A H 0.8828 0.7170 0.5238 0.049 Uiso 1 1 calc R . .
B11A B 0.9720(4) 0.8007(4) 0.6672(2) 0.0399(11) Uani 1 1 d . . .
H11A H 1.0736 0.7996 0.6706 0.048 Uiso 1 1 calc R . .
B12A B 0.8324(4) 0.6618(4) 0.6449(2) 0.0341(10) Uani 1 1 d . . .
H12A H 0.8443 0.5667 0.6336 0.041 Uiso 1 1 calc R . .
C1B C 0.5223(5) 0.0689(5) 0.8212(3) 0.0834(16) Uani 1 1 d . . .
H1B H 0.5459 -0.0169 0.8282 0.100 Uiso 1 1 calc R . .
B2B B 0.4076(5) 0.0555(5) 0.7427(3) 0.0656(16) Uani 1 1 d . . .
H2B H 0.3542 -0.0349 0.6979 0.079 Uiso 1 1 calc R . .
B3B B 0.3768(6) 0.0812(6) 0.8340(3) 0.0729(17) Uani 1 1 d . . .
H3B H 0.3026 0.0069 0.8497 0.088 Uiso 1 1 calc R . .
B4B B 0.5206(6) 0.1787(6) 0.8993(3) 0.0734(18) Uani 1 1 d . . .
H4B H 0.5424 0.1699 0.9582 0.088 Uiso 1 1 calc R . .
B5B B 0.6433(6) 0.2134(6) 0.8501(4) 0.080(2) Uani 1 1 d . B .
H5B H 0.7462 0.2273 0.8762 0.096 Uiso 1 1 calc R . .
B6B B 0.5748(6) 0.1391(5) 0.7526(4) 0.0695(16) Uani 1 1 d . B .
H6B H 0.6328 0.1042 0.7139 0.083 Uiso 1 1 calc R . .
B7B B 0.3330(6) 0.1684(6) 0.7723(3) 0.0707(17) Uani 1 1 d . . .
H7B H 0.2294 0.1534 0.7469 0.085 Uiso 1 1 calc R . .
B8B B 0.4018(7) 0.2433(6) 0.8690(3) 0.0822(19) Uani 1 1 d . . .
H8B H 0.3434 0.2775 0.9077 0.099 Uiso 1 1 calc R . .
B9B B 0.5674(6) 0.3265(6) 0.8798(3) 0.0786(18) Uani 1 1 d . B .
H9B H 0.6195 0.4163 0.9253 0.094 Uiso 1 1 calc R . .
B10B B 0.6030(5) 0.3018(5) 0.7880(3) 0.0623(15) Uani 1 1 d . . .
H10B H 0.6793 0.3751 0.7730 0.075 Uiso 0.78 1 calc PR A 1
O O 0.6705(4) 0.4356(4) 0.7838(3) 0.045(3) Uani 0.22 1 d P B 2
H0 H 0.6522 0.4872 0.8157 0.068 Uiso 0.22 1 calc PR B 2
B11B B 0.4559(4) 0.2029(4) 0.7214(3) 0.0552(13) Uani 1 1 d R B .
H11B H 0.4346 0.2103 0.6621 0.066 Uiso 1 1 calc R . .
B12B B 0.4516(6) 0.3205(5) 0.8001(3) 0.0657(16) Uani 1 1 d . B .
H12B H 0.4278 0.4061 0.7928 0.079 Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pd Pd -0.9988 1.0072 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
P2 Pd P1 89.48(3) . . ?
P2 Pd B7A 155.58(11) . . ?
P1 Pd B7A 113.32(11) . . ?
P2 Pd B12A 114.03(10) . . ?
P1 Pd B12A 154.84(10) . . ?
B7A Pd B12A 42.16(14) . . ?
C121 P1 C1 106.75(18) . . ?
C121 P1 C111 109.93(18) . . ?
C1 P1 C111 105.57(18) . . ?
C121 P1 Pd 110.86(13) . . ?
C1 P1 Pd 115.88(13) . . ?
C111 P1 Pd 107.66(12) . . ?
C221 P2 C211 107.01(15) . . ?
C221 P2 C3 111.62(18) . . ?
C211 P2 C3 102.28(17) . . ?
C221 P2 Pd 105.54(11) . . ?
C211 P2 Pd 112.42(12) . . ?
C3 P2 Pd 117.66(13) . . ?
C2 C1 P1 112.7(3) . . ?
C2 C1 H1C 109.1 . . ?
P1 C1 H1C 109.1 . . ?
C2 C1 H1D 109.1 . . ?
P1 C1 H1D 109.1 . . ?
H1C C1 H1D 107.8 . . ?
C3 C2 C1 113.8(3) . . ?
C3 C2 H2C 108.8 . . ?
C1 C2 H2C 108.8 . . ?
C3 C2 H2D 108.8 . . ?
C1 C2 H2D 108.8 . . ?
H2C C2 H2D 107.7 . . ?
C2 C3 P2 119.9(3) . . ?
C2 C3 H3C 107.3 . . ?
P2 C3 H3C 107.3 . . ?
C2 C3 H3D 107.3 . . ?
P2 C3 H3D 107.3 . . ?
H3C C3 H3D 106.9 . . ?
C112 C111 C116 120.4(4) . . ?
C112 C111 P1 120.8(3) . . ?
C116 C111 P1 118.8(3) . . ?
C111 C112 C113 118.6(5) . . ?
C111 C112 H112 120.7 . . ?
C113 C112 H112 120.7 . . ?
C114 C113 C112 119.6(5) . . ?
C114 C113 H113 120.2 . . ?
C112 C113 H113 120.2 . . ?
C115 C114 C113 121.6(5) . . ?
C115 C114 H114 119.2 . . ?
C113 C114 H114 119.2 . . ?
C114 C115 C116 119.3(5) . . ?
C114 C115 H115 120.3 . . ?
C116 C115 H115 120.3 . . ?
C115 C116 C111 120.5(5) . . ?
C115 C116 H116 119.8 . . ?
C111 C116 H116 119.8 . . ?
C122 C121 C126 119.1(4) . . ?
C122 C121 P1 120.3(3) . . ?
C126 C121 P1 120.5(3) . . ?
C123 C122 C121 120.4(4) . . ?
C123 C122 H122 119.8 . . ?
C121 C122 H122 119.8 . . ?
C124 C123 C122 120.1(4) . . ?
C124 C123 H123 120.0 . . ?
C122 C123 H123 120.0 . . ?
C123 C124 C125 120.7(4) . . ?
C123 C124 H124 119.6 . . ?
C125 C124 H124 119.6 . . ?
C124 C125 C126 119.5(4) . . ?
C124 C125 H125 120.3 . . ?
C126 C125 H125 120.3 . . ?
C125 C126 C121 120.2(4) . . ?
C125 C126 H126 119.9 . . ?
C121 C126 H126 119.9 . . ?
C216 C211 C212 119.1(3) . . ?
C216 C211 P2 122.5(3) . . ?
C212 C211 P2 118.2(3) . . ?
C213 C212 C211 120.3(4) . . ?
C213 C212 H212 119.8 . . ?
C211 C212 H212 119.8 . . ?
C214 C213 C212 119.8(4) . . ?
C214 C213 H213 120.1 . . ?
C212 C213 H213 120.1 . . ?
C215 C214 C213 120.2(4) . . ?
C215 C214 H214 119.9 . . ?
C213 C214 H214 119.9 . . ?
C214 C215 C216 120.3(4) . . ?
C214 C215 H215 119.8 . . ?
C216 C215 H215 119.8 . . ?
C211 C216 C215 120.2(4) . . ?
C211 C216 H216 119.9 . . ?
C215 C216 H216 119.9 . . ?
C226 C221 C222 119.5(3) . . ?
C226 C221 P2 117.4(3) . . ?
C222 C221 P2 123.1(3) . . ?
C223 C222 C221 119.6(4) . . ?
C223 C222 H222 120.2 . . ?
C221 C222 H222 120.2 . . ?
C224 C223 C222 120.5(4) . . ?
C224 C223 H223 119.7 . . ?
C222 C223 H223 119.7 . . ?
C223 C224 C225 120.3(4) . . ?
C223 C224 H224 119.8 . . ?
C225 C224 H224 119.8 . . ?
C226 C225 C224 119.7(4) . . ?
C226 C225 H225 120.2 . . ?
C224 C225 H225 120.2 . . ?
C225 C226 C221 120.4(4) . . ?
C225 C226 H226 119.8 . . ?
C221 C226 H226 119.8 . . ?
B2A C1A B3A 63.8(3) . . ?
B2A C1A B5A 114.8(3) . . ?
B3A C1A B5A 115.1(3) . . ?
B2A C1A B4A 115.9(3) . . ?
B3A C1A B4A 63.0(3) . . ?
B5A C1A B4A 62.8(3) . . ?
B2A C1A B6A 62.7(3) . . ?
B3A C1A B6A 115.8(3) . . ?
B5A C1A B6A 62.7(3) . . ?
B4A C1A B6A 115.4(3) . . ?
B2A C1A H1A 117.1 . . ?
B3A C1A H1A 116.9 . . ?
B5A C1A H1A 117.9 . . ?
B4A C1A H1A 117.2 . . ?
B6A C1A H1A 117.3 . . ?
C1A B2A B7A 102.7(3) . . ?
C1A B2A B6A 59.1(3) . . ?
B7A B2A B6A 107.2(3) . . ?
C1A B2A B11A 104.6(3) . . ?
B7A B2A B11A 60.7(2) . . ?
B6A B2A B11A 59.5(2) . . ?
C1A B2A B3A 58.2(3) . . ?
B7A B2A B3A 59.1(3) . . ?
B6A B2A B3A 108.3(3) . . ?
B11A B2A B3A 108.8(3) . . ?
C1A B2A H2A 125.5 . . ?
B7A B2A H2A 123.4 . . ?
B6A B2A H2A 121.5 . . ?
B11A B2A H2A 121.8 . . ?
B3A B2A H2A 121.3 . . ?
C1A B3A B7A 102.7(3) . . ?
C1A B3A B8A 104.4(3) . . ?
B7A B3A B8A 61.0(2) . . ?
C1A B3A B4A 58.7(3) . . ?
B7A B3A B4A 106.9(3) . . ?
B8A B3A B4A 59.3(3) . . ?
C1A B3A B2A 58.0(3) . . ?
B7A B3A B2A 59.3(3) . . ?
B8A B3A B2A 109.0(3) . . ?
B4A B3A B2A 107.6(3) . . ?
C1A B3A H3A 125.7 . . ?
B7A B3A H3A 123.2 . . ?
B8A B3A H3A 121.7 . . ?
B4A B3A H3A 122.1 . . ?
B2A B3A H3A 121.4 . . ?
C1A B4A B8A 104.9(3) . . ?
C1A B4A B5A 58.6(3) . . ?
B8A B4A B5A 108.6(3) . . ?
C1A B4A B3A 58.3(3) . . ?
B8A B4A B3A 60.3(3) . . ?
B5A B4A B3A 107.8(3) . . ?
C1A B4A B9A 104.6(3) . . ?
B8A B4A B9A 61.2(2) . . ?
B5A B4A B9A 59.7(3) . . ?
B3A B4A B9A 108.8(3) . . ?
C1A B4A H4A 125.1 . . ?
B8A B4A H4A 121.6 . . ?
B5A B4A H4A 121.6 . . ?
B3A B4A H4A 121.4 . . ?
B9A B4A H4A 121.9 . . ?
C1A B5A B9A 105.3(3) . . ?
C1A B5A B10A 105.1(3) . . ?
B9A B5A B10A 61.2(2) . . ?
C1A B5A B4A 58.7(3) . . ?
B9A B5A B4A 60.4(3) . . ?
B10A B5A B4A 109.3(3) . . ?
C1A B5A B6A 58.9(3) . . ?
B9A B5A B6A 109.5(3) . . ?
B10A B5A B6A 60.2(2) . . ?
B4A B5A B6A 108.8(3) . . ?
C1A B5A H5A 124.9 . . ?
B9A B5A H5A 121.4 . . ?
B10A B5A H5A 121.7 . . ?
B4A B5A H5A 121.0 . . ?
B6A B5A H5A 120.9 . . ?
C1A B6A B11A 104.5(3) . . ?
C1A B6A B2A 58.2(3) . . ?
B11A B6A B2A 60.3(3) . . ?
C1A B6A B5A 58.4(3) . . ?
B11A B6A B5A 108.1(3) . . ?
B2A B6A B5A 107.5(3) . . ?
C1A B6A B10A 104.4(3) . . ?
B11A B6A B10A 60.6(2) . . ?
B2A B6A B10A 108.5(3) . . ?
B5A B6A B10A 59.8(2) . . ?
C1A B6A H6A 125.3 . . ?
B11A B6A H6A 122.0 . . ?
B2A B6A H6A 121.5 . . ?
B5A B6A H6A 121.8 . . ?
B10A B6A H6A 122.1 . . ?
B12A B7A B3A 108.3(3) . . ?
B12A B7A B2A 108.1(3) . . ?
B3A B7A B2A 61.6(3) . . ?
B12A B7A B11A 60.6(2) . . ?
B3A B7A B11A 110.3(3) . . ?
B2A B7A B11A 60.2(3) . . ?
B12A B7A B8A 60.7(2) . . ?
B3A B7A B8A 60.2(3) . . ?
B2A B7A B8A 110.2(3) . . ?
B11A B7A B8A 110.8(3) . . ?
B12A B7A Pd 69.06(19) . . ?
B3A B7A Pd 151.3(3) . . ?
B2A B7A Pd 147.2(3) . . ?
B11A B7A Pd 93.6(2) . . ?
B8A B7A Pd 97.0(2) . . ?
B12A B7A H7A 121.9 . . ?
B3A B7A H7A 120.8 . . ?
B2A B7A H7A 121.0 . . ?
B11A B7A H7A 120.2 . . ?
B8A B7A H7A 120.1 . . ?
Pd B7A H7A 52.9 . . ?
B4A B8A B3A 60.4(3) . . ?
B4A B8A B12A 105.3(3) . . ?
B3A B8A B12A 105.1(3) . . ?
B4A B8A B7A 106.1(3) . . ?
B3A B8A B7A 58.8(2) . . ?
B12A B8A B7A 58.1(2) . . ?
B4A B8A B9A 60.0(3) . . ?
B3A B8A B9A 108.1(3) . . ?
B12A B8A B9A 58.6(2) . . ?
B7A B8A B9A 105.8(3) . . ?
B4A B8A H8A 122.4 . . ?
B3A B8A H8A 122.1 . . ?
B12A B8A H8A 124.2 . . ?
B7A B8A H8A 123.5 . . ?
B9A B8A H8A 122.0 . . ?
B12A B9A B5A 105.1(3) . . ?
B12A B9A B4A 105.4(3) . . ?
B5A B9A B4A 60.0(3) . . ?
B12A B9A B8A 60.1(2) . . ?
B5A B9A B8A 107.1(3) . . ?
B4A B9A B8A 58.8(3) . . ?
B12A B9A B10A 58.9(2) . . ?
B5A B9A B10A 59.5(2) . . ?
B4A B9A B10A 107.7(3) . . ?
B8A B9A B10A 108.4(3) . . ?
B12A B9A H9A 123.7 . . ?
B5A B9A H9A 122.8 . . ?
B4A B9A H9A 122.7 . . ?
B8A B9A H9A 121.7 . . ?
B10A B9A H9A 121.6 . . ?
B12A B10A B5A 105.0(3) . . ?
B12A B10A B6A 105.9(3) . . ?
B5A B10A B6A 60.0(3) . . ?
B12A B10A B11A 60.2(2) . . ?
B5A B10A B11A 107.2(3) . . ?
B6A B10A B11A 59.1(2) . . ?
B12A B10A B9A 59.1(2) . . ?
B5A B10A B9A 59.3(2) . . ?
B6A B10A B9A 107.8(3) . . ?
B11A B10A B9A 108.6(3) . . ?
B12A B10A H10A 123.5 . . ?
B5A B10A H10A 123.0 . . ?
B6A B10A H10A 122.4 . . ?
B11A B10A H10A 121.4 . . ?
B9A B10A H10A 121.5 . . ?
B6A B11A B2A 60.2(3) . . ?
B6A B11A B12A 105.8(3) . . ?
B2A B11A B12A 105.4(3) . . ?
B6A B11A B7A 106.5(3) . . ?
B2A B11A B7A 59.1(2) . . ?
B12A B11A B7A 58.3(2) . . ?
B6A B11A B10A 60.3(3) . . ?
B2A B11A B10A 108.3(3) . . ?
B12A B11A B10A 58.9(2) . . ?
B7A B11A B10A 106.4(3) . . ?
B6A B11A H11A 122.2 . . ?
B2A B11A H11A 122.1 . . ?
B12A B11A H11A 123.9 . . ?
B7A B11A H11A 123.2 . . ?
B10A B11A H11A 121.7 . . ?
B7A B12A B10A 110.2(3) . . ?
B7A B12A B9A 110.5(3) . . ?
B10A B12A B9A 61.9(2) . . ?
B7A B12A B11A 61.2(2) . . ?
B10A B12A B11A 60.8(2) . . ?
B9A B12A B11A 111.4(3) . . ?
B7A B12A B8A 61.2(2) . . ?
B10A B12A B8A 111.8(3) . . ?
B9A B12A B8A 61.3(2) . . ?
B11A B12A B8A 111.7(3) . . ?
B7A B12A Pd 68.8(2) . . ?
B10A B12A Pd 146.6(3) . . ?
B9A B12A Pd 151.2(3) . . ?
B11A B12A Pd 93.7(2) . . ?
B8A B12A Pd 97.1(2) . . ?
B7A B12A H12A 120.6 . . ?
B10A B12A H12A 119.9 . . ?
B9A B12A H12A 119.7 . . ?
B11A B12A H12A 119.7 . . ?
B8A B12A H12A 119.4 . . ?
Pd B12A H12A 51.9 . . ?
B3B C1B B4B 61.7(3) . . ?
B3B C1B B5B 111.7(4) . . ?
B4B C1B B5B 61.0(4) . . ?
B3B C1B B6B 111.8(4) . . ?
B4B C1B B6B 111.4(4) . . ?
B5B C1B B6B 62.0(3) . . ?
B3B C1B B2B 61.6(3) . . ?
B4B C1B B2B 112.0(4) . . ?
B5B C1B B2B 112.5(4) . . ?
B6B C1B B2B 61.8(3) . . ?
B3B C1B H1B 119.5 . . ?
B4B C1B H1B 119.8 . . ?
B5B C1B H1B 119.3 . . ?
B6B C1B H1B 119.4 . . ?
B2B C1B H1B 119.0 . . ?
C1B B2B B3B 58.3(3) . . ?
C1B B2B B7B 105.7(4) . . ?
B3B B2B B7B 60.5(3) . . ?
C1B B2B B11B 106.0(4) . . ?
B3B B2B B11B 108.1(4) . . ?
B7B B2B B11B 59.9(3) . . ?
C1B B2B B6B 59.1(3) . . ?
B3B B2B B6B 106.9(4) . . ?
B7B B2B B6B 107.3(4) . . ?
B11B B2B B6B 59.7(3) . . ?
C1B B2B H2B 123.9 . . ?
B3B B2B H2B 121.9 . . ?
B7B B2B H2B 122.1 . . ?
B11B B2B H2B 122.0 . . ?
B6B B2B H2B 122.2 . . ?
C1B B3B B4B 59.6(3) . . ?
C1B B3B B2B 60.1(3) . . ?
B4B B3B B2B 109.0(4) . . ?
C1B B3B B8B 106.9(4) . . ?
B4B B3B B8B 60.4(4) . . ?
B2B B3B B8B 108.4(4) . . ?
C1B B3B B7B 106.7(4) . . ?
B4B B3B B7B 108.2(4) . . ?
B2B B3B B7B 60.0(3) . . ?
B8B B3B B7B 59.7(4) . . ?
C1B B3B H3B 122.8 . . ?
B4B B3B H3B 121.1 . . ?
B2B B3B H3B 121.0 . . ?
B8B B3B H3B 121.9 . . ?
B7B B3B H3B 122.2 . . ?
C1B B4B B5B 59.6(3) . . ?
C1B B4B B3B 58.8(3) . . ?
B5B B4B B3B 108.2(4) . . ?
C1B B4B B9B 107.3(4) . . ?
B5B B4B B9B 61.2(4) . . ?
B3B B4B B9B 108.4(4) . . ?
C1B B4B B8B 106.1(4) . . ?
B5B B4B B8B 108.7(4) . . ?
B3B B4B B8B 60.1(4) . . ?
B9B B4B B8B 59.8(4) . . ?
C1B B4B H4B 123.4 . . ?
B5B B4B H4B 120.9 . . ?
B3B B4B H4B 121.8 . . ?
B9B B4B H4B 121.3 . . ?
B8B B4B H4B 122.1 . . ?
C1B B5B B4B 59.5(3) . . ?
C1B B5B B6B 59.4(3) . . ?
B4B B5B B6B 108.2(4) . . ?
C1B B5B B9B 106.2(4) . . ?
B4B B5B B9B 59.8(4) . . ?
B6B B5B B9B 107.7(4) . . ?
C1B B5B B10B 106.1(4) . . ?
B4B B5B B10B 108.2(4) . . ?
B6B B5B B10B 59.5(3) . . ?
B9B B5B B10B 60.3(3) . . ?
C1B B5B H5B 123.3 . . ?
B4B B5B H5B 121.4 . . ?
B6B B5B H5B 121.8 . . ?
B9B B5B H5B 122.1 . . ?
B10B B5B H5B 122.1 . . ?
C1B B6B B10B 106.2(4) . . ?
C1B B6B B11B 106.2(4) . . ?
B10B B6B B11B 60.9(3) . . ?
C1B B6B B5B 58.6(3) . . ?
B10B B6B B5B 60.4(3) . . ?
B11B B6B B5B 108.8(4) . . ?
C1B B6B B2B 59.2(3) . . ?
B10B B6B B2B 108.6(4) . . ?
B11B B6B B2B 59.9(3) . . ?
B5B B6B B2B 107.7(4) . . ?
C1B B6B H6B 123.8 . . ?
B10B B6B H6B 121.4 . . ?
B11B B6B H6B 121.6 . . ?
B5B B6B H6B 121.6 . . ?
B2B B6B H6B 121.7 . . ?
B8B B7B B11B 108.5(4) . . ?
B8B B7B B12B 60.2(3) . . ?
B11B B7B B12B 60.7(3) . . ?
B8B B7B B2B 108.0(4) . . ?
B11B B7B B2B 60.0(3) . . ?
B12B B7B B2B 108.8(4) . . ?
B8B B7B B3B 59.8(3) . . ?
B11B B7B B3B 107.4(4) . . ?
B12B B7B B3B 107.9(4) . . ?
B2B B7B B3B 59.5(3) . . ?
B8B B7B H7B 121.6 . . ?
B11B B7B H7B 121.5 . . ?
B12B B7B H7B 121.1 . . ?
B2B B7B H7B 121.6 . . ?
B3B B7B H7B 122.4 . . ?
B9B B8B B7B 108.7(4) . . ?
B9B B8B B3B 107.8(5) . . ?
B7B B8B B3B 60.5(3) . . ?
B9B B8B B4B 59.8(4) . . ?
B7B B8B B4B 108.1(4) . . ?
B3B B8B B4B 59.5(3) . . ?
B9B B8B B12B 60.7(3) . . ?
B7B B8B B12B 60.0(3) . . ?
B3B B8B B12B 108.4(4) . . ?
B4B B8B B12B 108.3(4) . . ?
B9B B8B H8B 121.5 . . ?
B7B B8B H8B 121.3 . . ?
B3B B8B H8B 121.8 . . ?
B4B B8B H8B 122.0 . . ?
B12B B8B H8B 121.3 . . ?
B4B B9B B8B 60.4(4) . . ?
B4B B9B B5B 59.0(4) . . ?
B8B B9B B5B 107.4(4) . . ?
B4B B9B B12B 108.2(4) . . ?
B8B B9B B12B 60.0(4) . . ?
B5B B9B B12B 107.9(4) . . ?
B4B B9B B10B 107.1(4) . . ?
B8B B9B B10B 107.7(4) . . ?
B5B B9B B10B 59.8(3) . . ?
B12B B9B B10B 60.1(3) . . ?
B4B B9B H9B 122.1 . . ?
B8B B9B H9B 121.8 . . ?
B5B B9B H9B 122.3 . . ?
B12B B9B H9B 121.5 . . ?
B10B B9B H9B 122.0 . . ?
O B10B B6B 147.1(5) . . ?
O B10B B5B 131.9(4) . . ?
B6B B10B B5B 60.1(3) . . ?
O B10B B12B 97.2(4) . . ?
B6B B10B B12B 107.8(4) . . ?
B5B B10B B12B 107.6(4) . . ?
O B10B B11B 120.5(4) . . ?
B6B B10B B11B 59.6(3) . . ?
B5B B10B B11B 107.6(4) . . ?
B12B B10B B11B 60.0(3) . . ?
O B10B B9B 103.1(4) . . ?
B6B B10B B9B 107.9(4) . . ?
B5B B10B B9B 59.8(3) . . ?
B12B B10B B9B 59.8(3) . . ?
B11B B10B B9B 107.6(4) . . ?
O B10B H10B 26.4 . . ?
B6B B10B H10B 121.8 . . ?
B5B B10B H10B 121.9 . . ?
B12B B10B H10B 121.9 . . ?
B11B B10B H10B 122.0 . . ?
B9B B10B H10B 121.9 . . ?
B10B O H0 109.5 . . ?
B6B B11B B7B 107.9(4) . . ?
B6B B11B B2B 60.4(3) . . ?
B7B B11B B2B 60.0(3) . . ?
B6B B11B B12B 107.7(4) . . ?
B7B B11B B12B 59.6(3) . . ?
B2B B11B B12B 107.9(4) . . ?
B6B B11B B10B 59.5(3) . . ?
B7B B11B B10B 107.5(4) . . ?
B2B B11B B10B 107.9(4) . . ?
B12B B11B B10B 60.0(3) . . ?
B6B B11B H11B 121.8 . . ?
B7B B11B H11B 122.0 . . ?
B2B B11B H11B 121.5 . . ?
B12B B11B H11B 121.9 . . ?
B10B B11B H11B 122.0 . . ?
B7B B12B B8B 59.7(3) . . ?
B7B B12B B9B 107.3(4) . . ?
B8B B12B B9B 59.3(3) . . ?
B7B B12B B11B 59.6(3) . . ?
B8B B12B B11B 107.2(4) . . ?
B9B B12B B11B 107.9(4) . . ?
B7B B12B B10B 107.5(4) . . ?
B8B B12B B10B 107.2(4) . . ?
B9B B12B B10B 60.1(3) . . ?
B11B B12B B10B 60.0(3) . . ?
B7B B12B H12B 122.1 . . ?
B8B B12B H12B 122.4 . . ?
B9B B12B H12B 121.9 . . ?
B11B B12B H12B 121.9 . . ?
B10B B12B H12B 121.9 . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pd P2 2.2532(9) . ?
Pd P1 2.2571(10) . ?
Pd B7A 2.401(4) . ?
Pd B12A 2.406(4) . ?
P1 C121 1.800(4) . ?
P1 C1 1.806(4) . ?
P1 C111 1.811(4) . ?
P2 C221 1.799(4) . ?
P2 C211 1.807(4) . ?
P2 C3 1.809(4) . ?
C1 C2 1.530(5) . ?
C1 H1C 0.9800 . ?
C1 H1D 0.9800 . ?
C2 C3 1.511(5) . ?
C2 H2C 0.9800 . ?
C2 H2D 0.9800 . ?
C3 H3C 0.9800 . ?
C3 H3D 0.9800 . ?
C111 C112 1.378(5) . ?
C111 C116 1.382(6) . ?
C112 C113 1.406(6) . ?
C112 H112 0.9400 . ?
C113 C114 1.367(7) . ?
C113 H113 0.9400 . ?
C114 C115 1.360(7) . ?
C114 H114 0.9400 . ?
C115 C116 1.375(6) . ?
C115 H115 0.9400 . ?
C116 H116 0.9400 . ?
C121 C122 1.383(5) . ?
C121 C126 1.388(5) . ?
C122 C123 1.375(6) . ?
C122 H122 0.9400 . ?
C123 C124 1.368(6) . ?
C123 H123 0.9400 . ?
C124 C125 1.373(6) . ?
C124 H124 0.9400 . ?
C125 C126 1.384(6) . ?
C125 H125 0.9400 . ?
C126 H126 0.9400 . ?
C211 C216 1.384(5) . ?
C211 C212 1.387(5) . ?
C212 C213 1.385(5) . ?
C212 H212 0.9400 . ?
C213 C214 1.378(6) . ?
C213 H213 0.9400 . ?
C214 C215 1.366(6) . ?
C214 H214 0.9400 . ?
C215 C216 1.385(5) . ?
C215 H215 0.9400 . ?
C216 H216 0.9400 . ?
C221 C226 1.386(5) . ?
C221 C222 1.392(5) . ?
C222 C223 1.379(5) . ?
C222 H222 0.9400 . ?
C223 C224 1.368(6) . ?
C223 H223 0.9400 . ?
C224 C225 1.381(5) . ?
C224 H224 0.9400 . ?
C225 C226 1.376(5) . ?
C225 H225 0.9400 . ?
C226 H226 0.9400 . ?
C1A B2A 1.693(6) . ?
C1A B3A 1.697(6) . ?
C1A B5A 1.701(6) . ?
C1A B4A 1.703(6) . ?
C1A B6A 1.709(6) . ?
C1A H1A 1.1100 . ?
B2A B7A 1.751(6) . ?
B2A B6A 1.770(7) . ?
B2A B11A 1.771(6) . ?
B2A B3A 1.791(7) . ?
B2A H2A 1.1100 . ?
B3A B7A 1.748(6) . ?
B3A B8A 1.773(6) . ?
B3A B4A 1.777(7) . ?
B3A H3A 1.1100 . ?
B4A B8A 1.756(6) . ?
B4A B5A 1.772(7) . ?
B4A B9A 1.778(6) . ?
B4A H4A 1.1100 . ?
B5A B9A 1.766(6) . ?
B5A B10A 1.771(6) . ?
B5A B6A 1.775(6) . ?
B5A H5A 1.1100 . ?
B6A B11A 1.756(6) . ?
B6A B10A 1.778(6) . ?
B6A H6A 1.1100 . ?
B7A B12A 1.729(6) . ?
B7A B11A 1.781(6) . ?
B7A B8A 1.786(6) . ?
B7A H7A 1.1100 . ?
B8A B12A 1.777(6) . ?
B8A B9A 1.799(6) . ?
B8A H8A 1.1100 . ?
B9A B12A 1.751(6) . ?
B9A B10A 1.800(6) . ?
B9A H9A 1.1100 . ?
B10A B12A 1.748(6) . ?
B10A B11A 1.782(6) . ?
B10A H10A 1.1100 . ?
B11A B12A 1.771(6) . ?
B11A H11A 1.1100 . ?
B12A H12A 1.1100 . ?
C1B B3B 1.687(8) . ?
C1B B4B 1.702(7) . ?
C1B B5B 1.702(8) . ?
C1B B6B 1.717(8) . ?
C1B B2B 1.718(7) . ?
C1B H1B 1.1100 . ?
B2B B3B 1.745(8) . ?
B2B B7B 1.754(8) . ?
B2B B11B 1.754(7) . ?
B2B B6B 1.763(8) . ?
B2B H2B 1.1100 . ?
B3B B4B 1.737(8) . ?
B3B B8B 1.748(9) . ?
B3B B7B 1.762(8) . ?
B3B H3B 1.1100 . ?
B4B B5B 1.726(9) . ?
B4B B9B 1.742(9) . ?
B4B B8B 1.752(9) . ?
B4B H4B 1.1100 . ?
B5B B6B 1.760(8) . ?
B5B B9B 1.765(9) . ?
B5B B10B 1.766(8) . ?
B5B H5B 1.1100 . ?
B6B B10B 1.748(8) . ?
B6B B11B 1.751(7) . ?
B6B H6B 1.1100 . ?
B7B B8B 1.747(8) . ?
B7B B11B 1.752(7) . ?
B7B B12B 1.752(8) . ?
B7B H7B 1.1100 . ?
B8B B9B 1.743(9) . ?
B8B B12B 1.756(9) . ?
B8B H8B 1.1100 . ?
B9B B12B 1.768(8) . ?
B9B B10B 1.774(8) . ?
B9B H9B 1.1100 . ?
B10B O 1.513(7) . ?
B10B B12B 1.773(8) . ?
B10B B11B 1.773(7) . ?
B10B H10B 1.1100 . ?
O H0 0.8300 . ?
B11B B12B 1.772(6) . ?
B11B H11B 1.1100 . ?
B12B H12B 1.1100 . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
P2 Pd P1 C121 78.78(13) . . . . ?
B7A Pd P1 C121 -92.19(18) . . . . ?
B12A Pd P1 C121 -81.0(3) . . . . ?
P2 Pd P1 C1 -43.07(14) . . . . ?
B7A Pd P1 C1 145.96(18) . . . . ?
B12A Pd P1 C1 157.2(3) . . . . ?
P2 Pd P1 C111 -160.94(15) . . . . ?
B7A Pd P1 C111 28.1(2) . . . . ?
B12A Pd P1 C111 39.3(3) . . . . ?
P1 Pd P2 C221 -91.14(12) . . . . ?
B7A Pd P2 C221 68.5(3) . . . . ?
B12A Pd P2 C221 79.60(16) . . . . ?
P1 Pd P2 C211 152.56(12) . . . . ?
B7A Pd P2 C211 -47.8(3) . . . . ?
B12A Pd P2 C211 -36.70(16) . . . . ?
P1 Pd P2 C3 34.14(16) . . . . ?
B7A Pd P2 C3 -166.3(3) . . . . ?
B12A Pd P2 C3 -155.12(19) . . . . ?
C121 P1 C1 C2 -58.0(3) . . . . ?
C111 P1 C1 C2 -175.0(3) . . . . ?
Pd P1 C1 C2 66.0(3) . . . . ?
P1 C1 C2 C3 -69.5(4) . . . . ?
C1 C2 C3 P2 61.6(4) . . . . ?
C221 P2 C3 C2 74.4(3) . . . . ?
C211 P2 C3 C2 -171.5(3) . . . . ?
Pd P2 C3 C2 -47.8(4) . . . . ?
C121 P1 C111 C112 4.1(4) . . . . ?
C1 P1 C111 C112 118.9(3) . . . . ?
Pd P1 C111 C112 -116.7(3) . . . . ?
C121 P1 C111 C116 -178.5(3) . . . . ?
C1 P1 C111 C116 -63.7(4) . . . . ?
Pd P1 C111 C116 60.7(3) . . . . ?
C116 C111 C112 C113 0.3(6) . . . . ?
P1 C111 C112 C113 177.7(3) . . . . ?
C111 C112 C113 C114 -0.8(7) . . . . ?
C112 C113 C114 C115 0.8(8) . . . . ?
C113 C114 C115 C116 -0.4(8) . . . . ?
C114 C115 C116 C111 0.0(7) . . . . ?
C112 C111 C116 C115 0.1(7) . . . . ?
P1 C111 C116 C115 -177.3(4) . . . . ?
C1 P1 C121 C122 -35.2(3) . . . . ?
C111 P1 C121 C122 78.9(3) . . . . ?
Pd P1 C121 C122 -162.2(3) . . . . ?
C1 P1 C121 C126 141.6(3) . . . . ?
C111 P1 C121 C126 -104.3(3) . . . . ?
Pd P1 C121 C126 14.6(3) . . . . ?
C126 C121 C122 C123 -0.9(6) . . . . ?
P1 C121 C122 C123 176.0(3) . . . . ?
C121 C122 C123 C124 0.2(7) . . . . ?
C122 C123 C124 C125 0.3(7) . . . . ?
C123 C124 C125 C126 -0.1(7) . . . . ?
C124 C125 C126 C121 -0.5(6) . . . . ?
C122 C121 C126 C125 1.0(6) . . . . ?
P1 C121 C126 C125 -175.8(3) . . . . ?
C221 P2 C211 C216 -147.6(3) . . . . ?
C3 P2 C211 C216 95.0(3) . . . . ?
Pd P2 C211 C216 -32.2(3) . . . . ?
C221 P2 C211 C212 37.8(3) . . . . ?
C3 P2 C211 C212 -79.6(3) . . . . ?
Pd P2 C211 C212 153.2(3) . . . . ?
C216 C211 C212 C213 0.4(6) . . . . ?
P2 C211 C212 C213 175.2(3) . . . . ?
C211 C212 C213 C214 -0.1(6) . . . . ?
C212 C213 C214 C215 -0.1(6) . . . . ?
C213 C214 C215 C216 -0.1(6) . . . . ?
C212 C211 C216 C215 -0.7(6) . . . . ?
P2 C211 C216 C215 -175.2(3) . . . . ?
C214 C215 C216 C211 0.5(6) . . . . ?
C211 P2 C221 C226 69.7(3) . . . . ?
C3 P2 C221 C226 -179.1(3) . . . . ?
Pd P2 C221 C226 -50.2(3) . . . . ?
C211 P2 C221 C222 -113.6(3) . . . . ?
C3 P2 C221 C222 -2.5(3) . . . . ?
Pd P2 C221 C222 126.5(3) . . . . ?
C226 C221 C222 C223 1.4(5) . . . . ?
P2 C221 C222 C223 -175.2(3) . . . . ?
C221 C222 C223 C224 -0.2(6) . . . . ?
C222 C223 C224 C225 -1.3(6) . . . . ?
C223 C224 C225 C226 1.5(6) . . . . ?
C224 C225 C226 C221 -0.2(6) . . . . ?
C222 C221 C226 C225 -1.2(5) . . . . ?
P2 C221 C226 C225 175.6(3) . . . . ?
B3A C1A B2A B7A 40.6(3) . . . . ?
B5A C1A B2A B7A -66.4(4) . . . . ?
B4A C1A B2A B7A 4.0(5) . . . . ?
B6A C1A B2A B7A -102.6(3) . . . . ?
B3A C1A B2A B6A 143.2(3) . . . . ?
B5A C1A B2A B6A 36.2(3) . . . . ?
B4A C1A B2A B6A 106.6(4) . . . . ?
B3A C1A B2A B11A 103.3(3) . . . . ?
B5A C1A B2A B11A -3.7(4) . . . . ?
B4A C1A B2A B11A 66.6(4) . . . . ?
B6A C1A B2A B11A -39.9(3) . . . . ?
B5A C1A B2A B3A -107.0(4) . . . . ?
B4A C1A B2A B3A -36.7(3) . . . . ?
B6A C1A B2A B3A -143.2(3) . . . . ?
B2A C1A B3A B7A -40.7(3) . . . . ?
B5A C1A B3A B7A 65.9(4) . . . . ?
B4A C1A B3A B7A 102.2(3) . . . . ?
B6A C1A B3A B7A -4.5(4) . . . . ?
B2A C1A B3A B8A -103.6(3) . . . . ?
B5A C1A B3A B8A 3.0(4) . . . . ?
B4A C1A B3A B8A 39.3(3) . . . . ?
B6A C1A B3A B8A -67.4(4) . . . . ?
B2A C1A B3A B4A -142.9(3) . . . . ?
B5A C1A B3A B4A -36.3(3) . . . . ?
B6A C1A B3A B4A -106.7(4) . . . . ?
B5A C1A B3A B2A 106.6(4) . . . . ?
B4A C1A B3A B2A 142.9(3) . . . . ?
B6A C1A B3A B2A 36.2(3) . . . . ?
B7A B2A B3A C1A -132.3(3) . . . . ?
B6A B2A B3A C1A -32.8(3) . . . . ?
B11A B2A B3A C1A -95.8(3) . . . . ?
C1A B2A B3A B7A 132.3(3) . . . . ?
B6A B2A B3A B7A 99.5(3) . . . . ?
B11A B2A B3A B7A 36.4(3) . . . . ?
C1A B2A B3A B8A 95.5(4) . . . . ?
B7A B2A B3A B8A -36.8(3) . . . . ?
B6A B2A B3A B8A 62.7(4) . . . . ?
B11A B2A B3A B8A -0.4(5) . . . . ?
C1A B2A B3A B4A 32.7(3) . . . . ?
B7A B2A B3A B4A -99.6(3) . . . . ?
B6A B2A B3A B4A -0.1(4) . . . . ?
B11A B2A B3A B4A -63.2(4) . . . . ?
B2A C1A B4A B8A -2.9(5) . . . . ?
B3A C1A B4A B8A -39.9(3) . . . . ?
B5A C1A B4A B8A 103.0(3) . . . . ?
B6A C1A B4A B8A 67.5(4) . . . . ?
B2A C1A B4A B5A -106.0(4) . . . . ?
B3A C1A B4A B5A -142.9(3) . . . . ?
B6A C1A B4A B5A -35.5(3) . . . . ?
B2A C1A B4A B3A 36.9(3) . . . . ?
B5A C1A B4A B3A 142.9(3) . . . . ?
B6A C1A B4A B3A 107.4(4) . . . . ?
B2A C1A B4A B9A -66.4(4) . . . . ?
B3A C1A B4A B9A -103.4(3) . . . . ?
B5A C1A B4A B9A 39.5(3) . . . . ?
B6A C1A B4A B9A 4.1(5) . . . . ?
B7A B3A B4A C1A -94.8(3) . . . . ?
B8A B3A B4A C1A -134.5(3) . . . . ?
B2A B3A B4A C1A -32.4(3) . . . . ?
C1A B3A B4A B8A 134.5(3) . . . . ?
B7A B3A B4A B8A 39.6(3) . . . . ?
B2A B3A B4A B8A 102.0(3) . . . . ?
C1A B3A B4A B5A 32.7(3) . . . . ?
B7A B3A B4A B5A -62.1(4) . . . . ?
B8A B3A B4A B5A -101.7(3) . . . . ?
B2A B3A B4A B5A 0.3(4) . . . . ?
C1A B3A B4A B9A 95.9(3) . . . . ?
B7A B3A B4A B9A 1.1(4) . . . . ?
B8A B3A B4A B9A -38.6(3) . . . . ?
B2A B3A B4A B9A 63.5(4) . . . . ?
B2A C1A B5A B9A 67.7(4) . . . . ?
B3A C1A B5A B9A -3.6(4) . . . . ?
B4A C1A B5A B9A -40.0(3) . . . . ?
B6A C1A B5A B9A 103.8(3) . . . . ?
B2A C1A B5A B10A 4.0(4) . . . . ?
B3A C1A B5A B10A -67.3(4) . . . . ?
B4A C1A B5A B10A -103.7(3) . . . . ?
B6A C1A B5A B10A 40.2(3) . . . . ?
B2A C1A B5A B4A 107.7(4) . . . . ?
B3A C1A B5A B4A 36.4(3) . . . . ?
B6A C1A B5A B4A 143.9(3) . . . . ?
B2A C1A B5A B6A -36.2(3) . . . . ?
B3A C1A B5A B6A -107.5(4) . . . . ?
B4A C1A B5A B6A -143.9(3) . . . . ?
B8A B4A B5A C1A -96.4(3) . . . . ?
B3A B4A B5A C1A -32.6(3) . . . . ?
B9A B4A B5A C1A -134.5(3) . . . . ?
C1A B4A B5A B9A 134.5(3) . . . . ?
B8A B4A B5A B9A 38.0(3) . . . . ?
B3A B4A B5A B9A 101.8(3) . . . . ?
C1A B4A B5A B10A 96.3(3) . . . . ?
B8A B4A B5A B10A -0.1(4) . . . . ?
B3A B4A B5A B10A 63.7(4) . . . . ?
B9A B4A B5A B10A -38.2(3) . . . . ?
C1A B4A B5A B6A 32.2(3) . . . . ?
B8A B4A B5A B6A -64.2(4) . . . . ?
B3A B4A B5A B6A -0.4(4) . . . . ?
B9A B4A B5A B6A -102.2(3) . . . . ?
B2A C1A B6A B11A 40.3(3) . . . . ?
B3A C1A B6A B11A 3.7(4) . . . . ?
B5A C1A B6A B11A -102.6(3) . . . . ?
B4A C1A B6A B11A -67.1(4) . . . . ?
B3A C1A B6A B2A -36.6(3) . . . . ?
B5A C1A B6A B2A -142.9(3) . . . . ?
B4A C1A B6A B2A -107.4(4) . . . . ?
B2A C1A B6A B5A 142.9(3) . . . . ?
B3A C1A B6A B5A 106.3(4) . . . . ?
B4A C1A B6A B5A 35.5(3) . . . . ?
B2A C1A B6A B10A 103.1(3) . . . . ?
B3A C1A B6A B10A 66.4(4) . . . . ?
B5A C1A B6A B10A -39.8(3) . . . . ?
B4A C1A B6A B10A -4.4(4) . . . . ?
B7A B2A B6A C1A 94.8(3) . . . . ?
B11A B2A B6A C1A 133.8(3) . . . . ?
B3A B2A B6A C1A 32.4(3) . . . . ?
C1A B2A B6A B11A -133.8(3) . . . . ?
B7A B2A B6A B11A -39.0(3) . . . . ?
B3A B2A B6A B11A -101.4(3) . . . . ?
C1A B2A B6A B5A -32.6(3) . . . . ?
B7A B2A B6A B5A 62.2(4) . . . . ?
B11A B2A B6A B5A 101.3(3) . . . . ?
B3A B2A B6A B5A -0.2(4) . . . . ?
C1A B2A B6A B10A -95.8(3) . . . . ?
B7A B2A B6A B10A -1.0(4) . . . . ?
B11A B2A B6A B10A 38.0(3) . . . . ?
B3A B2A B6A B10A -63.4(4) . . . . ?
B9A B5A B6A C1A -96.4(4) . . . . ?
B10A B5A B6A C1A -134.1(3) . . . . ?
B4A B5A B6A C1A -32.2(3) . . . . ?
C1A B5A B6A B11A 96.2(4) . . . . ?
B9A B5A B6A B11A -0.3(5) . . . . ?
B10A B5A B6A B11A -37.9(3) . . . . ?
B4A B5A B6A B11A 64.0(4) . . . . ?
C1A B5A B6A B2A 32.5(3) . . . . ?
B9A B5A B6A B2A -63.9(4) . . . . ?
B10A B5A B6A B2A -101.6(3) . . . . ?
B4A B5A B6A B2A 0.4(4) . . . . ?
C1A B5A B6A B10A 134.1(3) . . . . ?
B9A B5A B6A B10A 37.7(3) . . . . ?
B4A B5A B6A B10A 101.9(3) . . . . ?
C1A B3A B7A B12A -61.1(4) . . . . ?
B8A B3A B7A B12A 38.5(3) . . . . ?
B4A B3A B7A B12A -0.4(4) . . . . ?
B2A B3A B7A B12A -101.2(4) . . . . ?
C1A B3A B7A B2A 40.0(3) . . . . ?
B8A B3A B7A B2A 139.6(4) . . . . ?
B4A B3A B7A B2A 100.8(4) . . . . ?
C1A B3A B7A B11A 3.5(4) . . . . ?
B8A B3A B7A B11A 103.0(3) . . . . ?
B4A B3A B7A B11A 64.2(4) . . . . ?
B2A B3A B7A B11A -36.6(3) . . . . ?
C1A B3A B7A B8A -99.6(3) . . . . ?
B4A B3A B7A B8A -38.8(3) . . . . ?
B2A B3A B7A B8A -139.6(4) . . . . ?
C1A B3A B7A Pd -140.8(5) . . . . ?
B8A B3A B7A Pd -41.2(6) . . . . ?
B4A B3A B7A Pd -80.1(7) . . . . ?
B2A B3A B7A Pd 179.2(6) . . . . ?
C1A B2A B7A B12A 61.3(4) . . . . ?
B6A B2A B7A B12A 0.1(4) . . . . ?
B11A B2A B7A B12A -38.4(3) . . . . ?
B3A B2A B7A B12A 101.5(4) . . . . ?
C1A B2A B7A B3A -40.2(3) . . . . ?
B6A B2A B7A B3A -101.4(4) . . . . ?
B11A B2A B7A B3A -139.9(3) . . . . ?
C1A B2A B7A B11A 99.7(3) . . . . ?
B6A B2A B7A B11A 38.5(3) . . . . ?
B3A B2A B7A B11A 139.9(3) . . . . ?
C1A B2A B7A B8A -3.4(4) . . . . ?
B6A B2A B7A B8A -64.6(4) . . . . ?
B11A B2A B7A B8A -103.1(3) . . . . ?
B3A B2A B7A B8A 36.8(3) . . . . ?
C1A B2A B7A Pd 140.6(4) . . . . ?
B6A B2A B7A Pd 79.3(6) . . . . ?
B11A B2A B7A Pd 40.9(5) . . . . ?
B3A B2A B7A Pd -179.3(6) . . . . ?
P2 Pd B7A B12A 15.2(4) . . . . ?
P1 Pd B7A B12A 172.94(17) . . . . ?
P2 Pd B7A B3A 105.3(6) . . . . ?
P1 Pd B7A B3A -96.9(6) . . . . ?
B12A Pd B7A B3A 90.1(6) . . . . ?
P2 Pd B7A B2A -76.0(6) . . . . ?
P1 Pd B7A B2A 81.7(5) . . . . ?
B12A Pd B7A B2A -91.3(6) . . . . ?
P2 Pd B7A B11A -41.4(4) . . . . ?
P1 Pd B7A B11A 116.35(19) . . . . ?
B12A Pd B7A B11A -56.6(2) . . . . ?
P2 Pd B7A B8A 70.2(4) . . . . ?
P1 Pd B7A B8A -132.1(2) . . . . ?
B12A Pd B7A B8A 54.9(2) . . . . ?
C1A B4A B8A B3A 39.0(3) . . . . ?
B5A B4A B8A B3A 100.3(3) . . . . ?
B9A B4A B8A B3A 137.7(3) . . . . ?
C1A B4A B8A B12A -60.0(4) . . . . ?
B5A B4A B8A B12A 1.3(4) . . . . ?
B3A B4A B8A B12A -98.9(3) . . . . ?
B9A B4A B8A B12A 38.7(3) . . . . ?
C1A B4A B8A B7A 0.5(4) . . . . ?
B5A B4A B8A B7A 61.9(4) . . . . ?
B3A B4A B8A B7A -38.4(3) . . . . ?
B9A B4A B8A B7A 99.2(3) . . . . ?
C1A B4A B8A B9A -98.7(3) . . . . ?
B5A B4A B8A B9A -37.4(3) . . . . ?
B3A B4A B8A B9A -137.7(3) . . . . ?
C1A B3A B8A B4A -39.0(3) . . . . ?
B7A B3A B8A B4A -135.7(3) . . . . ?
B2A B3A B8A B4A -99.6(4) . . . . ?
C1A B3A B8A B12A 60.2(4) . . . . ?
B7A B3A B8A B12A -36.5(3) . . . . ?
B4A B3A B8A B12A 99.2(3) . . . . ?
B2A B3A B8A B12A -0.4(4) . . . . ?
C1A B3A B8A B7A 96.7(3) . . . . ?
B4A B3A B8A B7A 135.7(3) . . . . ?
B2A B3A B8A B7A 36.1(3) . . . . ?
C1A B3A B8A B9A -1.2(4) . . . . ?
B7A B3A B8A B9A -97.9(3) . . . . ?
B4A B3A B8A B9A 37.9(3) . . . . ?
B2A B3A B8A B9A -61.8(4) . . . . ?
B12A B7A B8A B4A -98.2(3) . . . . ?
B3A B7A B8A B4A 39.2(3) . . . . ?
B2A B7A B8A B4A 1.8(4) . . . . ?
B11A B7A B8A B4A -62.9(4) . . . . ?
Pd B7A B8A B4A -159.4(3) . . . . ?
B12A B7A B8A B3A -137.4(3) . . . . ?
B2A B7A B8A B3A -37.4(3) . . . . ?
B11A B7A B8A B3A -102.1(3) . . . . ?
Pd B7A B8A B3A 161.4(3) . . . . ?
B3A B7A B8A B12A 137.4(3) . . . . ?
B2A B7A B8A B12A 100.0(3) . . . . ?
B11A B7A B8A B12A 35.3(3) . . . . ?
Pd B7A B8A B12A -61.2(2) . . . . ?
B12A B7A B8A B9A -35.5(3) . . . . ?
B3A B7A B8A B9A 101.9(3) . . . . ?
B2A B7A B8A B9A 64.5(4) . . . . ?
B11A B7A B8A B9A -0.2(4) . . . . ?
Pd B7A B8A B9A -96.7(3) . . . . ?
C1A B5A B9A B12A -60.2(4) . . . . ?
B10A B5A B9A B12A 38.9(3) . . . . ?
B4A B5A B9A B12A -99.4(3) . . . . ?
B6A B5A B9A B12A 1.7(4) . . . . ?
C1A B5A B9A B4A 39.2(3) . . . . ?
B10A B5A B9A B4A 138.3(3) . . . . ?
B6A B5A B9A B4A 101.0(4) . . . . ?
C1A B5A B9A B8A 2.6(4) . . . . ?
B10A B5A B9A B8A 101.6(3) . . . . ?
B4A B5A B9A B8A -36.6(3) . . . . ?
B6A B5A B9A B8A 64.4(4) . . . . ?
C1A B5A B9A B10A -99.1(3) . . . . ?
B4A B5A B9A B10A -138.3(3) . . . . ?
B6A B5A B9A B10A -37.2(3) . . . . ?
C1A B4A B9A B12A 59.8(4) . . . . ?
B8A B4A B9A B12A -39.4(3) . . . . ?
B5A B4A B9A B12A 98.7(3) . . . . ?
B3A B4A B9A B12A -1.3(4) . . . . ?
C1A B4A B9A B5A -39.0(3) . . . . ?
B8A B4A B9A B5A -138.2(3) . . . . ?
B3A B4A B9A B5A -100.0(4) . . . . ?
C1A B4A B9A B8A 99.2(3) . . . . ?
B5A B4A B9A B8A 138.2(3) . . . . ?
B3A B4A B9A B8A 38.2(3) . . . . ?
C1A B4A B9A B10A -2.0(4) . . . . ?
B8A B4A B9A B10A -101.2(3) . . . . ?
B5A B4A B9A B10A 37.0(3) . . . . ?
B3A B4A B9A B10A -63.0(4) . . . . ?
B4A B8A B9A B12A 135.0(3) . . . . ?
B3A B8A B9A B12A 97.0(3) . . . . ?
B7A B8A B9A B12A 35.3(3) . . . . ?
B4A B8A B9A B5A 37.1(3) . . . . ?
B3A B8A B9A B5A -0.9(4) . . . . ?
B12A B8A B9A B5A -97.9(3) . . . . ?
B7A B8A B9A B5A -62.6(4) . . . . ?
B3A B8A B9A B4A -38.0(3) . . . . ?
B12A B8A B9A B4A -135.0(3) . . . . ?
B7A B8A B9A B4A -99.8(3) . . . . ?
B4A B8A B9A B10A 99.9(3) . . . . ?
B3A B8A B9A B10A 61.9(4) . . . . ?
B12A B8A B9A B10A -35.1(3) . . . . ?
B7A B8A B9A B10A 0.2(4) . . . . ?
C1A B5A B10A B12A 60.4(4) . . . . ?
B9A B5A B10A B12A -39.0(3) . . . . ?
B4A B5A B10A B12A -1.2(4) . . . . ?
B6A B5A B10A B12A 100.0(3) . . . . ?
C1A B5A B10A B6A -39.5(3) . . . . ?
B9A B5A B10A B6A -138.9(4) . . . . ?
B4A B5A B10A B6A -101.1(4) . . . . ?
C1A B5A B10A B11A -2.5(4) . . . . ?
B9A B5A B10A B11A -101.9(3) . . . . ?
B4A B5A B10A B11A -64.1(4) . . . . ?
B6A B5A B10A B11A 37.0(3) . . . . ?
C1A B5A B10A B9A 99.4(3) . . . . ?
B4A B5A B10A B9A 37.8(3) . . . . ?
B6A B5A B10A B9A 138.9(4) . . . . ?
C1A B6A B10A B12A -59.3(4) . . . . ?
B11A B6A B10A B12A 39.5(3) . . . . ?
B2A B6A B10A B12A 1.5(4) . . . . ?
B5A B6A B10A B12A -98.4(3) . . . . ?
C1A B6A B10A B5A 39.2(3) . . . . ?
B11A B6A B10A B5A 137.9(4) . . . . ?
B2A B6A B10A B5A 100.0(4) . . . . ?
C1A B6A B10A B11A -98.7(3) . . . . ?
B2A B6A B10A B11A -37.9(3) . . . . ?
B5A B6A B10A B11A -137.9(4) . . . . ?
C1A B6A B10A B9A 2.8(4) . . . . ?
B11A B6A B10A B9A 101.5(3) . . . . ?
B2A B6A B10A B9A 63.6(4) . . . . ?
B5A B6A B10A B9A -36.4(3) . . . . ?
B5A B9A B10A B12A 135.0(3) . . . . ?
B4A B9A B10A B12A 97.7(3) . . . . ?
B8A B9A B10A B12A 35.6(3) . . . . ?
B12A B9A B10A B5A -135.0(3) . . . . ?
B4A B9A B10A B5A -37.2(3) . . . . ?
B8A B9A B10A B5A -99.4(3) . . . . ?
B12A B9A B10A B6A -98.2(3) . . . . ?
B5A B9A B10A B6A 36.7(3) . . . . ?
B4A B9A B10A B6A -0.5(4) . . . . ?
B8A B9A B10A B6A -62.7(4) . . . . ?
B12A B9A B10A B11A -35.6(3) . . . . ?
B5A B9A B10A B11A 99.3(3) . . . . ?
B4A B9A B10A B11A 62.1(4) . . . . ?
B8A B9A B10A B11A -0.1(4) . . . . ?
C1A B6A B11A B2A -39.3(3) . . . . ?
B5A B6A B11A B2A -100.3(4) . . . . ?
B10A B6A B11A B2A -137.8(3) . . . . ?
C1A B6A B11A B12A 59.7(4) . . . . ?
B2A B6A B11A B12A 99.0(3) . . . . ?
B5A B6A B11A B12A -1.3(4) . . . . ?
B10A B6A B11A B12A -38.8(3) . . . . ?
C1A B6A B11A B7A -1.2(4) . . . . ?
B2A B6A B11A B7A 38.1(3) . . . . ?
B5A B6A B11A B7A -62.2(4) . . . . ?
B10A B6A B11A B7A -99.7(3) . . . . ?
C1A B6A B11A B10A 98.6(3) . . . . ?
B2A B6A B11A B10A 137.8(3) . . . . ?
B5A B6A B11A B10A 37.6(3) . . . . ?
C1A B2A B11A B6A 39.7(3) . . . . ?
B7A B2A B11A B6A 136.4(3) . . . . ?
B3A B2A B11A B6A 100.7(4) . . . . ?
C1A B2A B11A B12A -59.9(4) . . . . ?
B7A B2A B11A B12A 36.7(3) . . . . ?
B6A B2A B11A B12A -99.7(3) . . . . ?
B3A B2A B11A B12A 1.0(4) . . . . ?
C1A B2A B11A B7A -96.7(3) . . . . ?
B6A B2A B11A B7A -136.4(3) . . . . ?
B3A B2A B11A B7A -35.7(3) . . . . ?
C1A B2A B11A B10A 1.9(4) . . . . ?
B7A B2A B11A B10A 98.5(3) . . . . ?
B6A B2A B11A B10A -37.9(3) . . . . ?
B3A B2A B11A B10A 62.8(4) . . . . ?
B12A B7A B11A B6A 98.7(3) . . . . ?
B3A B7A B11A B6A -1.5(4) . . . . ?
B2A B7A B11A B6A -38.6(3) . . . . ?
B8A B7A B11A B6A 63.3(4) . . . . ?
Pd B7A B11A B6A 162.2(3) . . . . ?
B12A B7A B11A B2A 137.3(3) . . . . ?
B3A B7A B11A B2A 37.2(3) . . . . ?
B8A B7A B11A B2A 102.0(3) . . . . ?
Pd B7A B11A B2A -159.2(3) . . . . ?
B3A B7A B11A B12A -100.2(3) . . . . ?
B2A B7A B11A B12A -137.3(3) . . . . ?
B8A B7A B11A B12A -35.4(3) . . . . ?
Pd B7A B11A B12A 63.5(2) . . . . ?
B12A B7A B11A B10A 35.5(3) . . . . ?
B3A B7A B11A B10A -64.7(4) . . . . ?
B2A B7A B11A B10A -101.8(3) . . . . ?
B8A B7A B11A B10A 0.1(4) . . . . ?
Pd B7A B11A B10A 99.0(3) . . . . ?
B12A B10A B11A B6A -135.2(3) . . . . ?
B5A B10A B11A B6A -37.4(3) . . . . ?
B9A B10A B11A B6A -100.0(3) . . . . ?
B12A B10A B11A B2A -97.4(3) . . . . ?
B5A B10A B11A B2A 0.4(4) . . . . ?
B6A B10A B11A B2A 37.8(3) . . . . ?
B9A B10A B11A B2A -62.2(4) . . . . ?
B5A B10A B11A B12A 97.8(3) . . . . ?
B6A B10A B11A B12A 135.2(3) . . . . ?
B9A B10A B11A B12A 35.2(3) . . . . ?
B12A B10A B11A B7A -35.2(3) . . . . ?
B5A B10A B11A B7A 62.6(4) . . . . ?
B6A B10A B11A B7A 100.0(3) . . . . ?
B9A B10A B11A B7A 0.0(4) . . . . ?
B3A B7A B12A B10A 66.1(4) . . . . ?
B2A B7A B12A B10A 0.9(4) . . . . ?
B11A B7A B12A B10A -37.3(3) . . . . ?
B8A B7A B12A B10A 104.4(3) . . . . ?
Pd B7A B12A B10A -144.3(3) . . . . ?
B3A B7A B12A B9A -0.4(4) . . . . ?
B2A B7A B12A B9A -65.6(4) . . . . ?
B11A B7A B12A B9A -103.9(3) . . . . ?
B8A B7A B12A B9A 37.8(3) . . . . ?
Pd B7A B12A B9A 149.1(3) . . . . ?
B3A B7A B12A B11A 103.4(3) . . . . ?
B2A B7A B12A B11A 38.2(3) . . . . ?
B8A B7A B12A B11A 141.7(3) . . . . ?
Pd B7A B12A B11A -107.0(2) . . . . ?
B3A B7A B12A B8A -38.2(3) . . . . ?
B2A B7A B12A B8A -103.4(3) . . . . ?
B11A B7A B12A B8A -141.7(3) . . . . ?
Pd B7A B12A B8A 111.3(2) . . . . ?
B3A B7A B12A Pd -149.6(3) . . . . ?
B2A B7A B12A Pd 145.2(3) . . . . ?
B11A B7A B12A Pd 107.0(2) . . . . ?
B8A B7A B12A Pd -111.3(2) . . . . ?
B5A B10A B12A B7A -64.1(4) . . . . ?
B6A B10A B12A B7A -1.5(4) . . . . ?
B11A B10A B12A B7A 37.4(3) . . . . ?
B9A B10A B12A B7A -103.1(3) . . . . ?
B5A B10A B12A B9A 39.0(3) . . . . ?
B6A B10A B12A B9A 101.5(3) . . . . ?
B11A B10A B12A B9A 140.5(3) . . . . ?
B5A B10A B12A B11A -101.5(3) . . . . ?
B6A B10A B12A B11A -38.9(3) . . . . ?
B9A B10A B12A B11A -140.5(3) . . . . ?
B5A B10A B12A B8A 2.1(4) . . . . ?
B6A B10A B12A B8A 64.6(4) . . . . ?
B11A B10A B12A B8A 103.5(3) . . . . ?
B9A B10A B12A B8A -37.0(3) . . . . ?
B5A B10A B12A Pd -145.9(4) . . . . ?
B6A B10A B12A Pd -83.4(5) . . . . ?
B11A B10A B12A Pd -44.4(5) . . . . ?
B9A B10A B12A Pd 175.1(5) . . . . ?
B5A B9A B12A B7A 63.5(4) . . . . ?
B4A B9A B12A B7A 1.1(4) . . . . ?
B8A B9A B12A B7A -37.8(3) . . . . ?
B10A B9A B12A B7A 102.7(3) . . . . ?
B5A B9A B12A B10A -39.2(3) . . . . ?
B4A B9A B12A B10A -101.6(3) . . . . ?
B8A B9A B12A B10A -140.4(3) . . . . ?
B5A B9A B12A B11A -2.5(4) . . . . ?
B4A B9A B12A B11A -64.9(4) . . . . ?
B8A B9A B12A B11A -103.8(3) . . . . ?
B10A B9A B12A B11A 36.6(3) . . . . ?
B5A B9A B12A B8A 101.3(3) . . . . ?
B4A B9A B12A B8A 38.8(3) . . . . ?
B10A B9A B12A B8A 140.4(3) . . . . ?
B5A B9A B12A Pd 146.5(5) . . . . ?
B4A B9A B12A Pd 84.0(6) . . . . ?
B8A B9A B12A Pd 45.2(5) . . . . ?
B10A B9A B12A Pd -174.4(6) . . . . ?
B6A B11A B12A B7A -99.9(3) . . . . ?
B2A B11A B12A B7A -37.1(3) . . . . ?
B10A B11A B12A B7A -139.4(3) . . . . ?
B6A B11A B12A B10A 39.5(3) . . . . ?
B2A B11A B12A B10A 102.3(3) . . . . ?
B7A B11A B12A B10A 139.4(3) . . . . ?
B6A B11A B12A B9A 2.4(4) . . . . ?
B2A B11A B12A B9A 65.2(4) . . . . ?
B7A B11A B12A B9A 102.3(3) . . . . ?
B10A B11A B12A B9A -37.1(3) . . . . ?
B6A B11A B12A B8A -64.1(4) . . . . ?
B2A B11A B12A B8A -1.3(4) . . . . ?
B7A B11A B12A B8A 35.8(3) . . . . ?
B10A B11A B12A B8A -103.6(3) . . . . ?
B6A B11A B12A Pd -163.2(3) . . . . ?
B2A B11A B12A Pd -100.4(3) . . . . ?
B7A B11A B12A Pd -63.3(2) . . . . ?
B10A B11A B12A Pd 157.3(3) . . . . ?
B4A B8A B12A B7A 99.7(3) . . . . ?
B3A B8A B12A B7A 36.9(3) . . . . ?
B9A B8A B12A B7A 139.1(3) . . . . ?
B4A B8A B12A B10A -2.1(4) . . . . ?
B3A B8A B12A B10A -65.0(4) . . . . ?
B7A B8A B12A B10A -101.9(3) . . . . ?
B9A B8A B12A B10A 37.2(3) . . . . ?
B4A B8A B12A B9A -39.4(3) . . . . ?
B3A B8A B12A B9A -102.3(3) . . . . ?
B7A B8A B12A B9A -139.1(3) . . . . ?
B4A B8A B12A B11A 63.9(4) . . . . ?
B3A B8A B12A B11A 1.1(4) . . . . ?
B7A B8A B12A B11A -35.8(3) . . . . ?
B9A B8A B12A B11A 103.3(3) . . . . ?
B4A B8A B12A Pd 160.8(2) . . . . ?
B3A B8A B12A Pd 97.9(3) . . . . ?
B7A B8A B12A Pd 61.0(2) . . . . ?
B9A B8A B12A Pd -159.9(3) . . . . ?
P2 Pd B12A B7A -173.17(18) . . . . ?
P1 Pd B12A B7A -15.4(4) . . . . ?
P2 Pd B12A B10A -78.3(5) . . . . ?
P1 Pd B12A B10A 79.5(5) . . . . ?
B7A Pd B12A B10A 94.9(5) . . . . ?
P2 Pd B12A B9A 92.6(5) . . . . ?
P1 Pd B12A B9A -109.6(5) . . . . ?
B7A Pd B12A B9A -94.2(6) . . . . ?
P2 Pd B12A B11A -116.09(19) . . . . ?
P1 Pd B12A B11A 41.7(4) . . . . ?
B7A Pd B12A B11A 57.1(2) . . . . ?
P2 Pd B12A B8A 131.47(19) . . . . ?
P1 Pd B12A B8A -70.8(3) . . . . ?
B7A Pd B12A B8A -55.4(2) . . . . ?
B4B C1B B2B B3B -36.9(4) . . . . ?
B5B C1B B2B B3B -103.3(5) . . . . ?
B6B C1B B2B B3B -140.2(4) . . . . ?
B3B C1B B2B B7B 39.1(4) . . . . ?
B4B C1B B2B B7B 2.3(5) . . . . ?
B5B C1B B2B B7B -64.2(5) . . . . ?
B6B C1B B2B B7B -101.1(4) . . . . ?
B3B C1B B2B B11B 101.7(4) . . . . ?
B4B C1B B2B B11B 64.8(5) . . . . ?
B5B C1B B2B B11B -1.6(6) . . . . ?
B6B C1B B2B B11B -38.5(3) . . . . ?
B3B C1B B2B B6B 140.2(4) . . . . ?
B4B C1B B2B B6B 103.3(4) . . . . ?
B5B C1B B2B B6B 36.9(4) . . . . ?
B5B C1B B3B B4B -36.1(4) . . . . ?
B6B C1B B3B B4B -103.4(5) . . . . ?
B2B C1B B3B B4B -140.8(4) . . . . ?
B4B C1B B3B B2B 140.8(4) . . . . ?
B5B C1B B3B B2B 104.7(5) . . . . ?
B6B C1B B3B B2B 37.4(4) . . . . ?
B4B C1B B3B B8B 39.0(4) . . . . ?
B5B C1B B3B B8B 2.9(6) . . . . ?
B6B C1B B3B B8B -64.4(5) . . . . ?
B2B C1B B3B B8B -101.8(5) . . . . ?
B4B C1B B3B B7B 101.6(5) . . . . ?
B5B C1B B3B B7B 65.5(5) . . . . ?
B6B C1B B3B B7B -1.8(6) . . . . ?
B2B C1B B3B B7B -39.2(4) . . . . ?
B7B B2B B3B C1B -135.7(4) . . . . ?
B11B B2B B3B C1B -97.9(4) . . . . ?
B6B B2B B3B C1B -35.0(4) . . . . ?
C1B B2B B3B B4B 35.2(4) . . . . ?
B7B B2B B3B B4B -100.5(5) . . . . ?
B11B B2B B3B B4B -62.7(5) . . . . ?
B6B B2B B3B B4B 0.2(6) . . . . ?
C1B B2B B3B B8B 99.3(5) . . . . ?
B7B B2B B3B B8B -36.4(4) . . . . ?
B11B B2B B3B B8B 1.4(6) . . . . ?
B6B B2B B3B B8B 64.3(5) . . . . ?
C1B B2B B3B B7B 135.7(4) . . . . ?
B11B B2B B3B B7B 37.8(4) . . . . ?
B6B B2B B3B B7B 100.7(4) . . . . ?
B3B C1B B4B B5B -141.2(4) . . . . ?
B6B C1B B4B B5B -37.3(4) . . . . ?
B2B C1B B4B B5B -104.3(5) . . . . ?
B5B C1B B4B B3B 141.2(4) . . . . ?
B6B C1B B4B B3B 103.9(5) . . . . ?
B2B C1B B4B B3B 36.9(4) . . . . ?
B3B C1B B4B B9B -101.4(5) . . . . ?
B5B C1B B4B B9B 39.8(4) . . . . ?
B6B C1B B4B B9B 2.5(6) . . . . ?
B2B C1B B4B B9B -64.5(5) . . . . ?
B3B C1B B4B B8B -38.7(4) . . . . ?
B5B C1B B4B B8B 102.6(5) . . . . ?
B6B C1B B4B B8B 65.3(5) . . . . ?
B2B C1B B4B B8B -1.8(6) . . . . ?
B2B B3B B4B C1B -35.4(4) . . . . ?
B8B B3B B4B C1B -136.2(4) . . . . ?
B7B B3B B4B C1B -99.1(4) . . . . ?
C1B B3B B4B B5B 34.6(4) . . . . ?
B2B B3B B4B B5B -0.8(6) . . . . ?
B8B B3B B4B B5B -101.6(5) . . . . ?
B7B B3B B4B B5B -64.5(5) . . . . ?
C1B B3B B4B B9B 99.4(5) . . . . ?
B2B B3B B4B B9B 64.0(6) . . . . ?
B8B B3B B4B B9B -36.8(4) . . . . ?
B7B B3B B4B B9B 0.3(6) . . . . ?
C1B B3B B4B B8B 136.2(4) . . . . ?
B2B B3B B4B B8B 100.8(5) . . . . ?
B7B B3B B4B B8B 37.1(4) . . . . ?
B3B C1B B5B B4B 36.4(4) . . . . ?
B6B C1B B5B B4B 140.3(4) . . . . ?
B2B C1B B5B B4B 103.5(5) . . . . ?
B3B C1B B5B B6B -103.9(5) . . . . ?
B4B C1B B5B B6B -140.3(4) . . . . ?
B2B C1B B5B B6B -36.8(4) . . . . ?
B3B C1B B5B B9B -2.5(6) . . . . ?
B4B C1B B5B B9B -38.9(4) . . . . ?
B6B C1B B5B B9B 101.4(4) . . . . ?
B2B C1B B5B B9B 64.6(5) . . . . ?
B3B C1B B5B B10B -65.6(6) . . . . ?
B4B C1B B5B B10B -102.0(5) . . . . ?
B6B C1B B5B B10B 38.3(4) . . . . ?
B2B C1B B5B B10B 1.5(6) . . . . ?
B3B B4B B5B C1B -34.3(4) . . . . ?
B9B B4B B5B C1B -135.7(4) . . . . ?
B8B B4B B5B C1B -98.1(4) . . . . ?
C1B B4B B5B B6B 35.4(4) . . . . ?
B3B B4B B5B B6B 1.1(6) . . . . ?
B9B B4B B5B B6B -100.4(4) . . . . ?
B8B B4B B5B B6B -62.7(5) . . . . ?
C1B B4B B5B B9B 135.7(4) . . . . ?
B3B B4B B5B B9B 101.4(5) . . . . ?
B8B B4B B5B B9B 37.7(4) . . . . ?
C1B B4B B5B B10B 98.3(5) . . . . ?
B3B B4B B5B B10B 64.0(6) . . . . ?
B9B B4B B5B B10B -37.4(4) . . . . ?
B8B B4B B5B B10B 0.3(6) . . . . ?
B3B C1B B6B B10B 65.0(5) . . . . ?
B4B C1B B6B B10B -1.9(5) . . . . ?
B5B C1B B6B B10B -38.8(4) . . . . ?
B2B C1B B6B B10B 102.3(4) . . . . ?
B3B C1B B6B B11B 1.3(5) . . . . ?
B4B C1B B6B B11B -65.6(5) . . . . ?
B5B C1B B6B B11B -102.5(4) . . . . ?
B2B C1B B6B B11B 38.6(4) . . . . ?
B3B C1B B6B B5B 103.8(5) . . . . ?
B4B C1B B6B B5B 36.9(4) . . . . ?
B2B C1B B6B B5B 141.1(4) . . . . ?
B3B C1B B6B B2B -37.3(4) . . . . ?
B4B C1B B6B B2B -104.2(5) . . . . ?
B5B C1B B6B B2B -141.1(4) . . . . ?
B4B B5B B6B C1B -35.4(4) . . . . ?
B9B B5B B6B C1B -98.7(5) . . . . ?
B10B B5B B6B C1B -136.2(4) . . . . ?
C1B B5B B6B B10B 136.2(4) . . . . ?
B4B B5B B6B B10B 100.8(5) . . . . ?
B9B B5B B6B B10B 37.6(4) . . . . ?
C1B B5B B6B B11B 97.9(4) . . . . ?
B4B B5B B6B B11B 62.5(5) . . . . ?
B9B B5B B6B B11B -0.8(6) . . . . ?
B10B B5B B6B B11B -38.4(4) . . . . ?
C1B B5B B6B B2B 34.5(4) . . . . ?
B4B B5B B6B B2B -1.0(6) . . . . ?
B9B B5B B6B B2B -64.2(5) . . . . ?
B10B B5B B6B B2B -101.8(4) . . . . ?
B3B B2B B6B C1B 34.7(4) . . . . ?
B7B B2B B6B C1B 98.3(4) . . . . ?
B11B B2B B6B C1B 136.1(4) . . . . ?
C1B B2B B6B B10B -98.2(5) . . . . ?
B3B B2B B6B B10B -63.5(5) . . . . ?
B7B B2B B6B B10B 0.1(5) . . . . ?
B11B B2B B6B B10B 37.9(4) . . . . ?
C1B B2B B6B B11B -136.1(4) . . . . ?
B3B B2B B6B B11B -101.4(4) . . . . ?
B7B B2B B6B B11B -37.8(4) . . . . ?
C1B B2B B6B B5B -34.2(4) . . . . ?
B3B B2B B6B B5B 0.5(5) . . . . ?
B7B B2B B6B B5B 64.0(5) . . . . ?
B11B B2B B6B B5B 101.9(4) . . . . ?
C1B B2B B7B B8B -1.8(5) . . . . ?
B3B B2B B7B B8B 36.3(4) . . . . ?
B11B B2B B7B B8B -101.4(5) . . . . ?
B6B B2B B7B B8B -63.7(5) . . . . ?
C1B B2B B7B B11B 99.6(4) . . . . ?
B3B B2B B7B B11B 137.7(4) . . . . ?
B6B B2B B7B B11B 37.7(4) . . . . ?
C1B B2B B7B B12B 62.0(5) . . . . ?
B3B B2B B7B B12B 100.2(4) . . . . ?
B11B B2B B7B B12B -37.6(4) . . . . ?
B6B B2B B7B B12B 0.2(5) . . . . ?
C1B B2B B7B B3B -38.1(4) . . . . ?
B11B B2B B7B B3B -137.7(4) . . . . ?
B6B B2B B7B B3B -100.0(4) . . . . ?
C1B B3B B7B B8B -100.1(4) . . . . ?
B4B B3B B7B B8B -37.4(4) . . . . ?
B2B B3B B7B B8B -139.3(4) . . . . ?
C1B B3B B7B B11B 1.5(5) . . . . ?
B4B B3B B7B B11B 64.3(5) . . . . ?
B2B B3B B7B B11B -37.6(4) . . . . ?
B8B B3B B7B B11B 101.7(5) . . . . ?
C1B B3B B7B B12B -62.6(5) . . . . ?
B4B B3B B7B B12B 0.2(5) . . . . ?
B2B B3B B7B B12B -101.7(4) . . . . ?
B8B B3B B7B B12B 37.6(4) . . . . ?
C1B B3B B7B B2B 39.2(4) . . . . ?
B4B B3B B7B B2B 101.9(5) . . . . ?
B8B B3B B7B B2B 139.3(4) . . . . ?
B11B B7B B8B B9B 0.6(6) . . . . ?
B12B B7B B8B B9B -37.7(4) . . . . ?
B2B B7B B8B B9B 64.2(6) . . . . ?
B3B B7B B8B B9B 100.4(5) . . . . ?
B11B B7B B8B B3B -99.8(4) . . . . ?
B12B B7B B8B B3B -138.0(4) . . . . ?
B2B B7B B8B B3B -36.2(4) . . . . ?
B11B B7B B8B B4B -62.8(5) . . . . ?
B12B B7B B8B B4B -101.0(5) . . . . ?
B2B B7B B8B B4B 0.8(6) . . . . ?
B3B B7B B8B B4B 37.0(4) . . . . ?
B11B B7B B8B B12B 38.2(4) . . . . ?
B2B B7B B8B B12B 101.8(4) . . . . ?
B3B B7B B8B B12B 138.0(4) . . . . ?
C1B B3B B8B B9B -2.0(6) . . . . ?
B4B B3B B8B B9B 36.6(4) . . . . ?
B2B B3B B8B B9B -65.3(5) . . . . ?
B7B B3B B8B B9B -101.8(4) . . . . ?
C1B B3B B8B B7B 99.8(4) . . . . ?
B4B B3B B8B B7B 138.4(4) . . . . ?
B2B B3B B8B B7B 36.5(4) . . . . ?
C1B B3B B8B B4B -38.6(4) . . . . ?
B2B B3B B8B B4B -101.9(5) . . . . ?
B7B B3B B8B B4B -138.4(4) . . . . ?
C1B B3B B8B B12B 62.2(6) . . . . ?
B4B B3B B8B B12B 100.8(5) . . . . ?
B2B B3B B8B B12B -1.1(6) . . . . ?
B7B B3B B8B B12B -37.6(4) . . . . ?
C1B B4B B8B B9B -100.9(4) . . . . ?
B5B B4B B8B B9B -38.3(4) . . . . ?
B3B B4B B8B B9B -138.9(4) . . . . ?
C1B B4B B8B B7B 0.6(6) . . . . ?
B5B B4B B8B B7B 63.2(6) . . . . ?
B3B B4B B8B B7B -37.5(4) . . . . ?
B9B B4B B8B B7B 101.5(5) . . . . ?
C1B B4B B8B B3B 38.0(4) . . . . ?
B5B B4B B8B B3B 100.7(5) . . . . ?
B9B B4B B8B B3B 138.9(4) . . . . ?
C1B B4B B8B B12B -63.0(5) . . . . ?
B5B B4B B8B B12B -0.3(6) . . . . ?
B3B B4B B8B B12B -101.0(4) . . . . ?
B9B B4B B8B B12B 38.0(4) . . . . ?
C1B B4B B9B B8B 98.9(4) . . . . ?
B5B B4B B9B B8B 138.0(4) . . . . ?
B3B B4B B9B B8B 36.9(4) . . . . ?
C1B B4B B9B B5B -39.1(4) . . . . ?
B3B B4B B9B B5B -101.1(5) . . . . ?
B8B B4B B9B B5B -138.0(4) . . . . ?
C1B B4B B9B B12B 61.3(5) . . . . ?
B5B B4B B9B B12B 100.3(4) . . . . ?
B3B B4B B9B B12B -0.7(6) . . . . ?
B8B B4B B9B B12B -37.6(4) . . . . ?
C1B B4B B9B B10B -2.1(6) . . . . ?
B5B B4B B9B B10B 37.0(4) . . . . ?
B3B B4B B9B B10B -64.1(5) . . . . ?
B8B B4B B9B B10B -101.0(4) . . . . ?
B7B B8B B9B B4B -100.6(5) . . . . ?
B3B B8B B9B B4B -36.5(4) . . . . ?
B12B B8B B9B B4B -138.0(4) . . . . ?
B7B B8B B9B B5B -63.6(5) . . . . ?
B3B B8B B9B B5B 0.5(6) . . . . ?
B4B B8B B9B B5B 37.0(4) . . . . ?
B12B B8B B9B B5B -101.0(4) . . . . ?
B7B B8B B9B B12B 37.4(4) . . . . ?
B3B B8B B9B B12B 101.5(4) . . . . ?
B4B B8B B9B B12B 138.0(4) . . . . ?
B7B B8B B9B B10B -0.5(6) . . . . ?
B3B B8B B9B B10B 63.6(5) . . . . ?
B4B B8B B9B B10B 100.0(5) . . . . ?
B12B B8B B9B B10B -37.9(4) . . . . ?
C1B B5B B9B B4B 38.8(4) . . . . ?
B6B B5B B9B B4B 101.2(4) . . . . ?
B10B B5B B9B B4B 138.3(4) . . . . ?
C1B B5B B9B B8B 1.2(5) . . . . ?
B4B B5B B9B B8B -37.6(4) . . . . ?
B6B B5B B9B B8B 63.6(5) . . . . ?
B10B B5B B9B B8B 100.8(4) . . . . ?
C1B B5B B9B B12B -62.1(5) . . . . ?
B4B B5B B9B B12B -100.9(5) . . . . ?
B6B B5B B9B B12B 0.3(6) . . . . ?
B10B B5B B9B B12B 37.5(4) . . . . ?
C1B B5B B9B B10B -99.6(4) . . . . ?
B4B B5B B9B B10B -138.3(4) . . . . ?
B6B B5B B9B B10B -37.2(4) . . . . ?
C1B B6B B10B O 160.0(7) . . . . ?
B11B B6B B10B O -100.2(8) . . . . ?
B5B B6B B10B O 122.1(8) . . . . ?
B2B B6B B10B O -137.7(7) . . . . ?
C1B B6B B10B B5B 38.0(4) . . . . ?
B11B B6B B10B B5B 137.7(4) . . . . ?
B2B B6B B10B B5B 100.2(5) . . . . ?
C1B B6B B10B B12B -62.6(5) . . . . ?
B11B B6B B10B B12B 37.2(3) . . . . ?
B5B B6B B10B B12B -100.6(4) . . . . ?
B2B B6B B10B B12B -0.3(5) . . . . ?
C1B B6B B10B B11B -99.8(4) . . . . ?
B5B B6B B10B B11B -137.7(4) . . . . ?
B2B B6B B10B B11B -37.5(4) . . . . ?
C1B B6B B10B B9B 0.5(5) . . . . ?
B11B B6B B10B B9B 100.3(4) . . . . ?
B5B B6B B10B B9B -37.4(4) . . . . ?
B2B B6B B10B B9B 62.8(5) . . . . ?
C1B B5B B10B O 180.0(5) . . . . ?
B4B B5B B10B O 117.4(6) . . . . ?
B6B B5B B10B O -141.8(7) . . . . ?
B9B B5B B10B O 80.2(6) . . . . ?
C1B B5B B10B B6B -38.3(4) . . . . ?
B4B B5B B10B B6B -100.8(5) . . . . ?
B9B B5B B10B B6B -138.0(4) . . . . ?
C1B B5B B10B B12B 62.4(5) . . . . ?
B4B B5B B10B B12B -0.1(6) . . . . ?
B6B B5B B10B B12B 100.7(4) . . . . ?
B9B B5B B10B B12B -37.3(4) . . . . ?
C1B B5B B10B B11B -0.8(6) . . . . ?
B4B B5B B10B B11B -63.3(5) . . . . ?
B6B B5B B10B B11B 37.5(4) . . . . ?
B9B B5B B10B B11B -100.6(4) . . . . ?
C1B B5B B10B B9B 99.7(5) . . . . ?
B4B B5B B10B B9B 37.2(4) . . . . ?
B6B B5B B10B B9B 138.0(4) . . . . ?
B4B B9B B10B O -167.8(4) . . . . ?
B8B B9B B10B O 128.6(4) . . . . ?
B5B B9B B10B O -131.2(4) . . . . ?
B12B B9B B10B O 90.7(4) . . . . ?
B4B B9B B10B B6B 0.9(5) . . . . ?
B8B B9B B10B B6B -62.6(5) . . . . ?
B5B B9B B10B B6B 37.5(4) . . . . ?
B12B B9B B10B B6B -100.5(4) . . . . ?
B4B B9B B10B B5B -36.6(4) . . . . ?
B8B B9B B10B B5B -100.2(5) . . . . ?
B12B B9B B10B B5B -138.1(4) . . . . ?
B4B B9B B10B B12B 101.5(5) . . . . ?
B8B B9B B10B B12B 37.9(4) . . . . ?
B5B B9B B10B B12B 138.1(4) . . . . ?
B4B B9B B10B B11B 63.9(5) . . . . ?
B8B B9B B10B B11B 0.3(5) . . . . ?
B5B B9B B10B B11B 100.5(4) . . . . ?
B12B B9B B10B B11B -37.6(4) . . . . ?
C1B B6B B11B B7B -0.3(5) . . . . ?
B10B B6B B11B B7B -100.1(4) . . . . ?
B5B B6B B11B B7B -62.0(5) . . . . ?
B2B B6B B11B B7B 38.0(4) . . . . ?
C1B B6B B11B B2B -38.3(4) . . . . ?
B10B B6B B11B B2B -138.2(4) . . . . ?
B5B B6B B11B B2B -100.0(4) . . . . ?
C1B B6B B11B B12B 62.7(5) . . . . ?
B10B B6B B11B B12B -37.2(4) . . . . ?
B5B B6B B11B B12B 1.0(5) . . . . ?
B2B B6B B11B B12B 101.0(4) . . . . ?
C1B B6B B11B B10B 99.9(4) . . . . ?
B5B B6B B11B B10B 38.2(4) . . . . ?
B2B B6B B11B B10B 138.2(4) . . . . ?
B8B B7B B11B B6B 62.4(5) . . . . ?
B12B B7B B11B B6B 100.4(4) . . . . ?
B2B B7B B11B B6B -38.2(4) . . . . ?
B3B B7B B11B B6B -0.8(5) . . . . ?
B8B B7B B11B B2B 100.6(4) . . . . ?
B12B B7B B11B B2B 138.6(4) . . . . ?
B3B B7B B11B B2B 37.4(4) . . . . ?
B8B B7B B11B B12B -38.0(4) . . . . ?
B2B B7B B11B B12B -138.6(4) . . . . ?
B3B B7B B11B B12B -101.2(4) . . . . ?
B8B B7B B11B B10B -0.4(5) . . . . ?
B12B B7B B11B B10B 37.6(3) . . . . ?
B2B B7B B11B B10B -101.0(4) . . . . ?
B3B B7B B11B B10B -63.5(5) . . . . ?
C1B B2B B11B B6B 38.2(4) . . . . ?
B3B B2B B11B B6B 99.4(4) . . . . ?
B7B B2B B11B B6B 137.4(4) . . . . ?
C1B B2B B11B B7B -99.2(4) . . . . ?
B3B B2B B11B B7B -38.0(4) . . . . ?
B6B B2B B11B B7B -137.4(4) . . . . ?
C1B B2B B11B B12B -62.4(5) . . . . ?
B3B B2B B11B B12B -1.1(5) . . . . ?
B7B B2B B11B B12B 36.9(4) . . . . ?
B6B B2B B11B B12B -100.6(4) . . . . ?
C1B B2B B11B B10B 1.1(5) . . . . ?
B3B B2B B11B B10B 62.3(5) . . . . ?
B7B B2B B11B B10B 100.3(4) . . . . ?
B6B B2B B11B B10B -37.1(4) . . . . ?
O B10B B11B B6B 141.6(6) . . . . ?
B5B B10B B11B B6B -37.7(4) . . . . ?
B12B B10B B11B B6B -138.3(4) . . . . ?
B9B B10B B11B B6B -100.8(4) . . . . ?
O B10B B11B B7B -117.5(5) . . . . ?
B6B B10B B11B B7B 100.9(4) . . . . ?
B5B B10B B11B B7B 63.2(5) . . . . ?
B12B B10B B11B B7B -37.5(4) . . . . ?
B9B B10B B11B B7B 0.1(5) . . . . ?
O B10B B11B B2B 179.2(4) . . . . ?
B6B B10B B11B B2B 37.5(4) . . . . ?
B5B B10B B11B B2B -0.2(5) . . . . ?
B12B B10B B11B B2B -100.8(4) . . . . ?
B9B B10B B11B B2B -63.3(5) . . . . ?
O B10B B11B B12B -80.0(5) . . . . ?
B6B B10B B11B B12B 138.3(4) . . . . ?
B5B B10B B11B B12B 100.6(5) . . . . ?
B9B B10B B11B B12B 37.5(4) . . . . ?
B11B B7B B12B B8B -137.7(4) . . . . ?
B2B B7B B12B B8B -100.4(5) . . . . ?
B3B B7B B12B B8B -37.4(4) . . . . ?
B8B B7B B12B B9B 36.7(4) . . . . ?
B11B B7B B12B B9B -101.0(4) . . . . ?
B2B B7B B12B B9B -63.7(5) . . . . ?
B3B B7B B12B B9B -0.7(5) . . . . ?
B8B B7B B12B B11B 137.7(4) . . . . ?
B2B B7B B12B B11B 37.3(4) . . . . ?
B3B B7B B12B B11B 100.3(4) . . . . ?
B8B B7B B12B B10B 100.1(4) . . . . ?
B11B B7B B12B B10B -37.6(3) . . . . ?
B2B B7B B12B B10B -0.4(5) . . . . ?
B3B B7B B12B B10B 62.7(5) . . . . ?
B9B B8B B12B B7B 138.4(4) . . . . ?
B3B B8B B12B B7B 37.8(4) . . . . ?
B4B B8B B12B B7B 100.9(5) . . . . ?
B7B B8B B12B B9B -138.4(4) . . . . ?
B3B B8B B12B B9B -100.6(5) . . . . ?
B4B B8B B12B B9B -37.6(4) . . . . ?
B9B B8B B12B B11B 101.0(4) . . . . ?
B7B B8B B12B B11B -37.4(4) . . . . ?
B3B B8B B12B B11B 0.4(6) . . . . ?
B4B B8B B12B B11B 63.4(5) . . . . ?
B9B B8B B12B B10B 37.8(4) . . . . ?
B7B B8B B12B B10B -100.6(4) . . . . ?
B3B B8B B12B B10B -62.8(5) . . . . ?
B4B B8B B12B B10B 0.3(5) . . . . ?
B4B B9B B12B B7B 0.9(5) . . . . ?
B8B B9B B12B B7B -36.9(4) . . . . ?
B5B B9B B12B B7B 63.2(5) . . . . ?
B10B B9B B12B B7B 100.6(4) . . . . ?
B4B B9B B12B B8B 37.8(4) . . . . ?
B5B B9B B12B B8B 100.1(5) . . . . ?
B10B B9B B12B B8B 137.5(4) . . . . ?
B4B B9B B12B B11B -62.0(5) . . . . ?
B8B B9B B12B B11B -99.8(5) . . . . ?
B5B B9B B12B B11B 0.3(6) . . . . ?
B10B B9B B12B B11B 37.7(4) . . . . ?
B4B B9B B12B B10B -99.7(5) . . . . ?
B8B B9B B12B B10B -137.5(4) . . . . ?
B5B B9B B12B B10B -37.4(4) . . . . ?
B6B B11B B12B B7B -100.8(4) . . . . ?
B2B B11B B12B B7B -37.0(4) . . . . ?
B10B B11B B12B B7B -137.7(4) . . . . ?
B6B B11B B12B B8B -63.3(5) . . . . ?
B7B B11B B12B B8B 37.5(4) . . . . ?
B2B B11B B12B B8B 0.5(5) . . . . ?
B10B B11B B12B B8B -100.3(4) . . . . ?
B6B B11B B12B B9B -0.8(5) . . . . ?
B7B B11B B12B B9B 100.0(5) . . . . ?
B2B B11B B12B B9B 63.0(5) . . . . ?
B10B B11B B12B B9B -37.7(4) . . . . ?
B6B B11B B12B B10B 37.0(4) . . . . ?
B7B B11B B12B B10B 137.7(4) . . . . ?
B2B B11B B12B B10B 100.7(4) . . . . ?
O B10B B12B B7B 158.7(4) . . . . ?
B6B B10B B12B B7B 0.4(5) . . . . ?
B5B B10B B12B B7B -63.0(5) . . . . ?
B11B B10B B12B B7B 37.5(4) . . . . ?
B9B B10B B12B B7B -100.3(4) . . . . ?
O B10B B12B B8B -138.4(4) . . . . ?
B6B B10B B12B B8B 63.3(5) . . . . ?
B5B B10B B12B B8B -0.1(5) . . . . ?
B11B B10B B12B B8B 100.4(4) . . . . ?
B9B B10B B12B B8B -37.4(4) . . . . ?
O B10B B12B B9B -101.0(4) . . . . ?
B6B B10B B12B B9B 100.8(4) . . . . ?
B5B B10B B12B B9B 37.3(4) . . . . ?
B11B B10B B12B B9B 137.8(4) . . . . ?
O B10B B12B B11B 121.2(4) . . . . ?
B6B B10B B12B B11B -37.0(4) . . . . ?
B5B B10B B12B B11B -100.5(4) . . . . ?
B9B B10B B12B B11B -137.8(4) . . . . ?
