#------------------------------------------------------------------------------
#$Date: 2016-03-25 13:31:46 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179849 $
#$URL: svn://www.crystallography.net/cod/cif/7/01/45/7014550.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7014550
loop_
_publ_author_name
'Ye, Hong-De'
'Ding, Guan-Yu'
'Xie, Ming-Shi'
'Li, Yi-Zhi'
'Yan, Hong'
_publ_section_title
;
 Reactivity of the 16e Cp*Co half-sandwich complex containing a
 chelating 1,2-dicarba-closo-dodecaborane-1,2-dithiolate ligand towards
 alkynes.
;
_journal_issue                   10
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              2306
_journal_page_last               2313
_journal_paper_doi               10.1039/c0dt00933d
_journal_volume                  40
_journal_year                    2011
_chemical_formula_moiety         '2(C28 H37 B10 Co S2), C H2 Cl2'
_chemical_formula_sum            'C57 H76 B20 Cl2 Co2 S4'
_chemical_formula_weight         1294.38
_chemical_name_systematic
;
?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                115.20(2)
_cell_angle_beta                 94.599(10)
_cell_angle_gamma                107.04(3)
_cell_formula_units_Z            2
_cell_length_a                   10.968(2)
_cell_length_b                   18.694(4)
_cell_length_c                   18.866(3)
_cell_measurement_temperature    291(2)
_cell_volume                     3251.1(15)
_computing_cell_refinement       SMART
_computing_data_collection       'SMART (Bruker, 2000)'
_computing_data_reduction        'SAINT (Bruker, 2000)'
_computing_molecular_graphics    SHELXTL
_computing_publication_material  SHELXTL
_computing_structure_refinement  SHELXTL
_computing_structure_solution    'SHELXL (Sheldrick, 2000)'
_diffrn_ambient_temperature      291(2)
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'Bruker CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0507
_diffrn_reflns_av_sigmaI/netI    0.0766
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       23
_diffrn_reflns_limit_k_min       -23
_diffrn_reflns_limit_l_max       23
_diffrn_reflns_limit_l_min       -23
_diffrn_reflns_number            30609
_diffrn_reflns_theta_full        26.00
_diffrn_reflns_theta_max         26.00
_diffrn_reflns_theta_min         3.03
_exptl_absorpt_coefficient_mu    0.759
_exptl_absorpt_correction_T_max  0.8388
_exptl_absorpt_correction_T_min  0.8043
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'SADABS (Bruker, 2000)'
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    1.322
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             1340
_exptl_crystal_size_max          0.30
_exptl_crystal_size_mid          0.26
_exptl_crystal_size_min          0.24
_refine_diff_density_max         0.415
_refine_diff_density_min         -0.431
_refine_diff_density_rms         0.073
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.091
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     776
_refine_ls_number_reflns         12744
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.091
_refine_ls_R_factor_all          0.0914
_refine_ls_R_factor_gt           0.0613
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0677P)²+0.5084P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1357
_refine_ls_wR_factor_ref         0.1465
_reflns_number_gt                8636
_reflns_number_total             12744
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            C0DT00933D.TXT
_cod_data_source_block           COMPLEX-8
_cod_original_cell_volume        3251.3(15)
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7014550
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
B3 B 0.0720(4) 0.8648(3) 0.6152(3) 0.0369(10) Uani 1 1 d . . .
H3 H -0.0168 0.8100 0.5797 0.044 Uiso 1 1 d R . .
B4 B 0.2089(5) 0.8719(3) 0.6789(3) 0.0422(11) Uani 1 1 d . . .
H4 H 0.1991 0.8164 0.6905 0.051 Uiso 1 1 d R . .
B5 B 0.3545(5) 0.9324(3) 0.6653(3) 0.0410(10) Uani 1 1 d . . .
H5 H 0.4427 0.9090 0.6621 0.049 Uiso 1 1 d R . .
B6 B 0.3087(4) 0.9618(3) 0.5929(2) 0.0343(9) Uani 1 1 d . . .
H6 H 0.3518 0.9556 0.5387 0.041 Uiso 1 1 d R . .
B7 B 0.2175(4) 1.0281(3) 0.6323(3) 0.0374(10) Uani 1 1 d . . .
H7 H 0.2146 1.0749 0.6131 0.045 Uiso 1 1 d R . .
B8 B 0.0728(5) 0.9695(3) 0.6450(3) 0.0390(10) Uani 1 1 d . . .
H8 H -0.0177 0.9784 0.6321 0.047 Uiso 1 1 d R . .
B9 B 0.1152(5) 0.9373(3) 0.7181(3) 0.0450(11) Uani 1 1 d . . .
H9 H 0.0462 0.9344 0.7544 0.054 Uiso 1 1 d R . .
B10 B 0.2933(5) 0.9824(3) 0.7506(3) 0.0444(11) Uani 1 1 d . . .
H10 H 0.3415 0.9998 0.8109 0.053 Uiso 1 1 d R . .
B11 B 0.3545(5) 1.0366(3) 0.6969(3) 0.0419(11) Uani 1 1 d . . .
H11 H 0.4466 1.0868 0.7240 0.050 Uiso 1 1 d R . .
B12 B 0.2073(5) 1.0409(3) 0.7281(3) 0.0465(12) Uani 1 1 d . . .
H12 H 0.2095 1.0970 0.7778 0.056 Uiso 1 1 d R . .
B13 B 0.7288(4) 0.2812(3) 0.0759(3) 0.0376(10) Uani 1 1 d . . .
H13 H 0.7549 0.2688 0.1277 0.045 Uiso 1 1 d R . .
B14 B 0.6334(4) 0.2010(3) -0.0225(3) 0.0428(11) Uani 1 1 d . . .
H14 H 0.5952 0.1343 -0.0269 0.051 Uiso 1 1 d R . .
B15 B 0.7028(4) 0.2236(3) -0.0953(3) 0.0424(11) Uani 1 1 d . . .
H15 H 0.6957 0.1674 -0.1509 0.051 Uiso 1 1 d R . .
B16 B 0.8417(4) 0.3176(3) -0.0438(3) 0.0407(10) Uani 1 1 d . . .
H16 H 0.9390 0.3305 -0.0641 0.049 Uiso 1 1 d R . .
B17 B 0.7937(5) 0.4029(3) 0.0157(3) 0.0455(11) Uani 1 1 d . . .
H17 H 0.8482 0.4699 0.0390 0.055 Uiso 1 1 d R . .
B18 B 0.7206(4) 0.3792(3) 0.0877(3) 0.0440(11) Uani 1 1 d . . .
H18 H 0.7468 0.4267 0.1476 0.053 Uiso 1 1 d R . .
B19 B 0.5810(5) 0.2842(3) 0.0356(3) 0.0479(12) Uani 1 1 d . . .
H19 H 0.5020 0.2793 0.0680 0.058 Uiso 1 1 d R . .
B20 B 0.5643(5) 0.2503(3) -0.0687(3) 0.0489(12) Uani 1 1 d . . .
H20 H 0.4596 0.2091 -0.1084 0.059 Uiso 1 1 d R . .
B21 B 0.6942(5) 0.3210(3) -0.0828(3) 0.0473(12) Uani 1 1 d . . .
H21 H 0.6924 0.3401 -0.1317 0.057 Uiso 1 1 d R . .
B22 B 0.6205(5) 0.3604(3) -0.0025(3) 0.0477(12) Uani 1 1 d . . .
H22 H 0.5555 0.3988 -0.0038 0.057 Uiso 1 1 d R . .
C1 C 0.2181(3) 0.8683(2) 0.5885(2) 0.0340(8) Uani 1 1 d . . .
C2 C 0.1360(4) 0.9220(2) 0.5659(2) 0.0338(8) Uani 1 1 d . . .
C3 C -0.0449(3) 0.6967(2) 0.3760(2) 0.0311(8) Uani 1 1 d . . .
C4 C -0.0688(4) 0.6461(2) 0.4121(2) 0.0360(8) Uani 1 1 d . . .
H4A H -0.1558 0.6102 0.3984 0.043 Uiso 1 1 calc R . .
C5 C 0.0183(3) 0.6392(2) 0.4676(2) 0.0339(8) Uani 1 1 d . . .
H5A H -0.0165 0.5911 0.4740 0.041 Uiso 1 1 calc R . .
C6 C 0.1393(4) 0.6889(2) 0.5117(2) 0.0353(8) Uani 1 1 d . . .
C7 C -0.1626(3) 0.6822(2) 0.3180(2) 0.0315(8) Uani 1 1 d . . .
C8 C -0.2009(3) 0.7485(2) 0.3173(2) 0.0334(8) Uani 1 1 d . . .
H8A H -0.1524 0.8045 0.3551 0.040 Uiso 1 1 calc R . .
C9 C -0.3068(3) 0.7308(2) 0.2625(2) 0.0357(8) Uani 1 1 d . . .
H9A H -0.3287 0.7754 0.2629 0.043 Uiso 1 1 calc R . .
C10 C -0.3840(4) 0.6486(3) 0.2055(3) 0.0447(10) Uani 1 1 d . . .
H10A H -0.4578 0.6376 0.1690 0.054 Uiso 1 1 calc R . .
C11 C -0.3481(4) 0.5837(2) 0.2045(3) 0.0427(10) Uani 1 1 d . . .
H11A H -0.3961 0.5281 0.1655 0.051 Uiso 1 1 calc R . .
C12 C -0.2424(3) 0.5999(2) 0.2605(2) 0.0335(8) Uani 1 1 d . . .
H12A H -0.2231 0.5545 0.2601 0.040 Uiso 1 1 calc R . .
C13 C 0.2161(4) 0.6705(2) 0.5672(2) 0.0353(8) Uani 1 1 d . . .
C14 C 0.3513(4) 0.6894(3) 0.5753(3) 0.0464(10) Uani 1 1 d . . .
H14A H 0.3966 0.7158 0.5482 0.056 Uiso 1 1 calc R . .
C15 C 0.4164(4) 0.6678(3) 0.6250(2) 0.0449(10) Uani 1 1 d . . .
H15A H 0.5058 0.6786 0.6299 0.054 Uiso 1 1 calc R . .
C16 C 0.3512(4) 0.6312(3) 0.6666(3) 0.0481(11) Uani 1 1 d . . .
H16A H 0.3971 0.6188 0.7007 0.058 Uiso 1 1 calc R . .
C17 C 0.2192(4) 0.6125(3) 0.6586(3) 0.0462(10) Uani 1 1 d . . .
H17A H 0.1752 0.5861 0.6861 0.055 Uiso 1 1 calc R . .
C18 C 0.1511(4) 0.6330(2) 0.6097(2) 0.0390(9) Uani 1 1 d . . .
H18A H 0.0616 0.6215 0.6053 0.047 Uiso 1 1 calc R . .
C19 C 0.1233(4) 0.7132(2) 0.2700(2) 0.0377(9) Uani 1 1 d . . .
C20 C 0.1347(4) 0.7981(2) 0.2913(2) 0.0353(8) Uani 1 1 d . . .
C21 C 0.2573(4) 0.8554(2) 0.3489(2) 0.0353(8) Uani 1 1 d . . .
C22 C 0.3201(4) 0.8056(2) 0.3645(2) 0.0371(8) Uani 1 1 d . . .
C23 C 0.2363(4) 0.7188(2) 0.3170(2) 0.0369(8) Uani 1 1 d . . .
C24 C 0.0259(4) 0.6336(3) 0.2026(2) 0.0473(10) Uani 1 1 d . . .
H24A H 0.0592 0.6191 0.1549 0.071 Uiso 1 1 calc R . .
H24B H -0.0550 0.6418 0.1928 0.071 Uiso 1 1 calc R . .
H24C H 0.0106 0.5886 0.2167 0.071 Uiso 1 1 calc R . .
C25 C 0.0489(4) 0.8274(3) 0.2533(2) 0.0446(10) Uani 1 1 d . . .
H25A H 0.0793 0.8313 0.2083 0.067 Uiso 1 1 calc R . .
H25B H 0.0519 0.8820 0.2921 0.067 Uiso 1 1 calc R . .
H25C H -0.0398 0.7875 0.2349 0.067 Uiso 1 1 calc R . .
C26 C 0.3104(4) 0.9489(3) 0.3792(3) 0.0519(11) Uani 1 1 d . . .
H26A H 0.3637 0.9764 0.4331 0.078 Uiso 1 1 calc R . .
H26B H 0.2390 0.9688 0.3794 0.078 Uiso 1 1 calc R . .
H26C H 0.3626 0.9618 0.3448 0.078 Uiso 1 1 calc R . .
C27 C 0.4548(4) 0.8367(3) 0.4141(3) 0.0422(9) Uani 1 1 d . . .
H27A H 0.5174 0.8425 0.3823 0.063 Uiso 1 1 calc R . .
H27B H 0.4618 0.7969 0.4323 0.063 Uiso 1 1 calc R . .
H27C H 0.4722 0.8908 0.4599 0.063 Uiso 1 1 calc R . .
C28 C 0.2661(5) 0.6439(3) 0.3128(3) 0.0505(11) Uani 1 1 d . . .
H28A H 0.1860 0.5996 0.3043 0.076 Uiso 1 1 calc R . .
H28B H 0.3243 0.6605 0.3625 0.076 Uiso 1 1 calc R . .
H28C H 0.3070 0.6238 0.2690 0.076 Uiso 1 1 calc R . .
C29 C 0.7987(4) 0.2494(2) -0.0043(2) 0.0325(8) Uani 1 1 d . . .
C30 C 0.8512(4) 0.3520(2) 0.0592(2) 0.0351(8) Uani 1 1 d . . .
C31 C 1.0284(3) 0.2717(2) 0.1820(2) 0.0331(8) Uani 1 1 d . . .
C32 C 0.9343(4) 0.1981(2) 0.1662(2) 0.0432(9) Uani 1 1 d . . .
H32A H 0.9157 0.1934 0.2116 0.052 Uiso 1 1 calc R . .
C33 C 0.8571(4) 0.1248(2) 0.0898(2) 0.0429(9) Uani 1 1 d . . .
H33A H 0.8149 0.0761 0.0937 0.052 Uiso 1 1 calc R . .
C34 C 0.8365(4) 0.1155(2) 0.0164(2) 0.0392(9) Uani 1 1 d . . .
C35 C 1.0938(4) 0.3313(2) 0.2676(2) 0.0347(8) Uani 1 1 d . . .
C36 C 1.1163(4) 0.4183(2) 0.3040(2) 0.0421(9) Uani 1 1 d . . .
H36A H 1.0867 0.4406 0.2734 0.050 Uiso 1 1 calc R . .
C37 C 1.1811(4) 0.4720(3) 0.3841(2) 0.0460(10) Uani 1 1 d . . .
H37A H 1.1949 0.5295 0.4062 0.055 Uiso 1 1 calc R . .
C38 C 1.2245(4) 0.4420(3) 0.4304(3) 0.0489(10) Uani 1 1 d . . .
H38A H 1.2694 0.4790 0.4839 0.059 Uiso 1 1 calc R . .
C39 C 1.2029(4) 0.3573(3) 0.3994(3) 0.0492(10) Uani 1 1 d . . .
H39A H 1.2322 0.3365 0.4316 0.059 Uiso 1 1 calc R . .
C40 C 1.1360(4) 0.3023(2) 0.3184(2) 0.0385(9) Uani 1 1 d . . .
H40A H 1.1191 0.2445 0.2980 0.046 Uiso 1 1 calc R . .
C41 C 0.7462(4) 0.0384(2) -0.0562(2) 0.0415(9) Uani 1 1 d . . .
C42 C 0.6335(4) -0.0157(2) -0.0484(3) 0.0449(10) Uani 1 1 d . . .
H42A H 0.6192 -0.0046 0.0026 0.054 Uiso 1 1 calc R . .
C43 C 0.5446(4) -0.0850(3) -0.1158(3) 0.0469(11) Uani 1 1 d . . .
H43A H 0.4716 -0.1207 -0.1099 0.056 Uiso 1 1 calc R . .
C44 C 0.5625(5) -0.1013(3) -0.1901(3) 0.0505(12) Uani 1 1 d . . .
H44A H 0.4984 -0.1459 -0.2349 0.061 Uiso 1 1 calc R . .
C45 C 0.6719(5) -0.0541(3) -0.2009(3) 0.0534(12) Uani 1 1 d . . .
H45A H 0.6858 -0.0685 -0.2524 0.064 Uiso 1 1 calc R . .
C46 C 0.7655(4) 0.0178(3) -0.1325(2) 0.0461(10) Uani 1 1 d . . .
H46A H 0.8403 0.0510 -0.1395 0.055 Uiso 1 1 calc R . .
C47 C 1.2164(4) 0.2904(3) 0.0125(2) 0.0417(9) Uani 1 1 d . . .
C48 C 1.2678(4) 0.3722(3) 0.0797(2) 0.0414(9) Uani 1 1 d . . .
C49 C 1.2951(4) 0.3647(3) 0.1504(2) 0.0413(9) Uani 1 1 d . . .
C50 C 1.2649(4) 0.2774(3) 0.1274(2) 0.0395(9) Uani 1 1 d . . .
C51 C 1.2118(4) 0.2304(3) 0.0421(2) 0.0394(9) Uani 1 1 d . . .
C52 C 1.1860(4) 0.2715(3) -0.0736(2) 0.0506(11) Uani 1 1 d . . .
H52A H 1.1441 0.3082 -0.0784 0.076 Uiso 1 1 calc R . .
H52B H 1.1283 0.2135 -0.1061 0.076 Uiso 1 1 calc R . .
H52C H 1.2659 0.2806 -0.0916 0.076 Uiso 1 1 calc R . .
C53 C 1.2956(4) 0.4542(3) 0.0757(3) 0.0468(10) Uani 1 1 d . . .
H53A H 1.3827 0.4726 0.0682 0.070 Uiso 1 1 calc R . .
H53B H 1.2887 0.4967 0.1251 0.070 Uiso 1 1 calc R . .
H53C H 1.2332 0.4455 0.0314 0.070 Uiso 1 1 calc R . .
C54 C 1.3713(4) 0.4360(3) 0.2335(3) 0.0491(10) Uani 1 1 d . . .
H54A H 1.3600 0.4156 0.2723 0.074 Uiso 1 1 calc R . .
H54B H 1.3395 0.4817 0.2469 0.074 Uiso 1 1 calc R . .
H54C H 1.4627 0.4558 0.2339 0.074 Uiso 1 1 calc R . .
C55 C 1.2967(4) 0.2398(3) 0.1772(3) 0.0454(10) Uani 1 1 d . . .
H55A H 1.3813 0.2353 0.1738 0.068 Uiso 1 1 calc R . .
H55B H 1.2315 0.1843 0.1581 0.068 Uiso 1 1 calc R . .
H55C H 1.2982 0.2751 0.2322 0.068 Uiso 1 1 calc R . .
C56 C 1.1744(4) 0.1368(3) -0.0090(3) 0.0478(10) Uani 1 1 d . . .
H56A H 1.2482 0.1252 -0.0287 0.072 Uiso 1 1 calc R . .
H56B H 1.1027 0.1166 -0.0538 0.072 Uiso 1 1 calc R . .
H56C H 1.1483 0.1086 0.0225 0.072 Uiso 1 1 calc R . .
C57 C 0.7025(4) 0.7670(3) 0.4854(3) 0.0576(12) Uani 1 1 d . . .
H57A H 0.7902 0.7653 0.4876 0.069 Uiso 1 1 calc R . .
H57B H 0.6913 0.7961 0.4547 0.069 Uiso 1 1 calc R . .
Cl1 Cl 0.58858(11) 0.66388(7) 0.43568(7) 0.0527(3) Uani 1 1 d . . .
Cl2 Cl 0.68832(11) 0.82287(7) 0.58054(7) 0.0545(3) Uani 1 1 d . . .
Co1 Co 0.12702(5) 0.77894(3) 0.39241(3) 0.03373(13) Uani 1 1 d . . .
Co2 Co 1.09304(5) 0.29736(3) 0.09843(3) 0.03431(13) Uani 1 1 d . . .
S1 S 0.22283(9) 0.77798(6) 0.49906(5) 0.0339(2) Uani 1 1 d . . .
S2 S 0.05958(9) 0.88526(6) 0.46535(5) 0.0351(2) Uani 1 1 d . . .
S3 S 0.92095(9) 0.20183(6) -0.00036(6) 0.0350(2) Uani 1 1 d . . .
S4 S 1.01017(9) 0.40069(6) 0.12481(6) 0.0371(2) Uani 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C1 B3 C2 58.5(2) . . ?
C1 B3 B9 104.9(3) . . ?
C2 B3 B9 106.6(3) . . ?
C1 B3 B4 57.9(2) . . ?
C2 B3 B4 106.3(3) . . ?
B9 B3 B4 60.7(3) . . ?
C1 B3 B8 103.7(3) . . ?
C2 B3 B8 57.7(2) . . ?
B9 B3 B8 61.2(3) . . ?
B4 B3 B8 108.5(3) . . ?
C1 B3 H3 120.7 . . ?
C2 B3 H3 114.4 . . ?
B9 B3 H3 129.7 . . ?
B4 B3 H3 127.7 . . ?
B8 B3 H3 120.5 . . ?
C1 B4 B5 58.7(2) . . ?
C1 B4 B3 58.9(2) . . ?
B5 B4 B3 108.3(3) . . ?
C1 B4 B9 104.2(3) . . ?
B5 B4 B9 108.8(3) . . ?
B3 B4 B9 58.8(3) . . ?
C1 B4 B10 104.1(3) . . ?
B5 B4 B10 59.7(3) . . ?
B3 B4 B10 107.4(3) . . ?
B9 B4 B10 60.9(3) . . ?
C1 B4 H4 123.4 . . ?
B5 B4 H4 124.4 . . ?
B3 B4 H4 117.5 . . ?
B9 B4 H4 121.0 . . ?
B10 B4 H4 126.3 . . ?
C1 B5 B6 58.7(2) . . ?
C1 B5 B4 58.2(2) . . ?
B6 B5 B4 107.9(3) . . ?
C1 B5 B11 104.7(3) . . ?
B6 B5 B11 60.2(2) . . ?
B4 B5 B11 108.2(3) . . ?
C1 B5 B10 104.5(3) . . ?
B6 B5 B10 107.5(3) . . ?
B4 B5 B10 60.9(3) . . ?
B11 B5 B10 59.2(3) . . ?
C1 B5 H5 116.4 . . ?
B6 B5 H5 119.1 . . ?
B4 B5 H5 117.5 . . ?
B11 B5 H5 129.6 . . ?
B10 B5 H5 128.9 . . ?
C1 B6 C2 58.2(2) . . ?
C1 B6 B5 58.8(2) . . ?
C2 B6 B5 106.7(3) . . ?
C1 B6 B11 104.8(3) . . ?
C2 B6 B11 106.0(3) . . ?
B5 B6 B11 60.3(2) . . ?
C1 B6 B7 104.1(3) . . ?
C2 B6 B7 58.3(2) . . ?
B5 B6 B7 108.2(3) . . ?
B11 B6 B7 60.2(2) . . ?
C1 B6 H6 115.1 . . ?
C2 B6 H6 111.6 . . ?
B5 B6 H6 126.3 . . ?
B11 B6 H6 135.3 . . ?
B7 B6 H6 123.5 . . ?
C2 B7 B12 106.9(3) . . ?
C2 B7 B8 58.8(2) . . ?
B12 B7 B8 60.8(3) . . ?
C2 B7 B6 60.4(2) . . ?
B12 B7 B6 108.6(3) . . ?
B8 B7 B6 108.8(3) . . ?
C2 B7 B11 107.4(3) . . ?
B12 B7 B11 60.6(3) . . ?
B8 B7 B11 109.4(3) . . ?
B6 B7 B11 59.9(2) . . ?
C2 B7 H7 119.1 . . ?
B12 B7 H7 123.7 . . ?
B8 B7 H7 118.5 . . ?
B6 B7 H7 121.3 . . ?
B11 B7 H7 125.2 . . ?
C2 B8 B7 60.0(2) . . ?
C2 B8 B12 106.6(3) . . ?
B7 B8 B12 59.4(3) . . ?
C2 B8 B3 59.6(2) . . ?
B7 B8 B3 108.3(3) . . ?
B12 B8 B3 107.8(3) . . ?
C2 B8 B9 106.0(3) . . ?
B7 B8 B9 108.5(3) . . ?
B12 B8 B9 61.5(3) . . ?
B3 B8 B9 58.4(3) . . ?
C2 B8 H8 117.7 . . ?
B7 B8 H8 120.3 . . ?
B12 B8 H8 126.3 . . ?
B3 B8 H8 119.7 . . ?
B9 B8 H8 125.8 . . ?
B3 B9 B4 60.5(3) . . ?
B3 B9 B8 60.4(3) . . ?
B4 B9 B8 107.8(3) . . ?
B3 B9 B10 108.1(3) . . ?
B4 B9 B10 60.0(3) . . ?
B8 B9 B10 106.0(3) . . ?
B3 B9 B12 106.9(3) . . ?
B4 B9 B12 106.7(3) . . ?
B8 B9 B12 58.2(3) . . ?
B10 B9 B12 58.9(3) . . ?
B3 B9 H9 120.5 . . ?
B4 B9 H9 130.5 . . ?
B8 B9 H9 113.5 . . ?
B10 B9 H9 127.8 . . ?
B12 B9 H9 117.6 . . ?
B11 B10 B5 60.3(3) . . ?
B11 B10 B12 60.0(3) . . ?
B5 B10 B12 107.6(3) . . ?
B11 B10 B4 107.9(3) . . ?
B5 B10 B4 59.4(3) . . ?
B12 B10 B4 107.4(3) . . ?
B11 B10 B9 108.7(4) . . ?
B5 B10 B9 107.0(3) . . ?
B12 B10 B9 60.6(3) . . ?
B4 B10 B9 59.1(3) . . ?
B11 B10 H10 123.9 . . ?
B5 B10 H10 121.9 . . ?
B12 B10 H10 123.6 . . ?
B4 B10 H10 119.6 . . ?
B9 B10 H10 120.3 . . ?
B10 B11 B12 60.9(3) . . ?
B10 B11 B6 108.0(3) . . ?
B12 B11 B6 107.0(3) . . ?
B10 B11 B5 60.5(3) . . ?
B12 B11 B5 108.4(3) . . ?
B6 B11 B5 59.5(3) . . ?
B10 B11 B7 107.6(4) . . ?
B12 B11 B7 58.5(3) . . ?
B6 B11 B7 59.9(2) . . ?
B5 B11 B7 107.4(3) . . ?
B10 B11 H11 117.7 . . ?
B12 B11 H11 124.7 . . ?
B6 B11 H11 122.4 . . ?
B5 B11 H11 116.7 . . ?
B7 B11 H11 127.7 . . ?
B7 B12 B8 59.8(3) . . ?
B7 B12 B11 61.0(3) . . ?
B8 B12 B11 108.9(3) . . ?
B7 B12 B10 108.1(3) . . ?
B8 B12 B10 108.9(3) . . ?
B11 B12 B10 59.1(3) . . ?
B7 B12 B9 107.9(3) . . ?
B8 B12 B9 60.3(3) . . ?
B11 B12 B9 107.8(3) . . ?
B10 B12 B9 60.4(3) . . ?
B7 B12 H12 125.9 . . ?
B8 B12 H12 125.9 . . ?
B11 B12 H12 119.2 . . ?
B10 B12 H12 116.0 . . ?
B9 B12 H12 120.3 . . ?
C29 B13 C30 57.2(2) . . ?
C29 B13 B19 104.0(3) . . ?
C30 B13 B19 104.7(3) . . ?
C29 B13 B18 103.5(3) . . ?
C30 B13 B18 58.0(2) . . ?
B19 B13 B18 60.1(3) . . ?
C29 B13 B14 58.3(2) . . ?
C30 B13 B14 104.7(3) . . ?
B19 B13 B14 59.8(3) . . ?
B18 B13 B14 107.4(3) . . ?
C29 B13 H13 119.4 . . ?
C30 B13 H13 118.2 . . ?
B19 B13 H13 130.3 . . ?
B18 B13 H13 124.2 . . ?
B14 B13 H13 124.6 . . ?
C29 B14 B15 59.9(2) . . ?
C29 B14 B19 104.0(3) . . ?
B15 B14 B19 108.3(4) . . ?
C29 B14 B20 104.9(3) . . ?
B15 B14 B20 60.2(3) . . ?
B19 B14 B20 59.7(3) . . ?
C29 B14 B13 58.6(2) . . ?
B15 B14 B13 109.3(3) . . ?
B19 B14 B13 59.5(3) . . ?
B20 B14 B13 107.7(3) . . ?
C29 B14 H14 117.4 . . ?
B15 B14 H14 124.5 . . ?
B19 B14 H14 123.8 . . ?
B20 B14 H14 132.3 . . ?
B13 B14 H14 112.5 . . ?
C29 B15 B16 58.6(2) . . ?
C29 B15 B14 58.3(2) . . ?
B16 B15 B14 107.8(3) . . ?
C29 B15 B21 104.2(3) . . ?
B16 B15 B21 59.6(3) . . ?
B14 B15 B21 108.2(3) . . ?
C29 B15 B20 103.8(3) . . ?
B16 B15 B20 107.0(3) . . ?
B14 B15 B20 60.3(3) . . ?
B21 B15 B20 59.6(3) . . ?
C29 B15 H15 120.7 . . ?
B16 B15 H15 125.4 . . ?
B14 B15 H15 114.7 . . ?
B21 B15 H15 129.2 . . ?
B20 B15 H15 123.0 . . ?
C29 B16 C30 57.1(2) . . ?
C29 B16 B21 105.8(3) . . ?
C30 B16 B21 106.1(3) . . ?
C29 B16 B15 59.9(3) . . ?
C30 B16 B15 106.4(3) . . ?
B21 B16 B15 60.4(3) . . ?
C29 B16 B17 104.3(3) . . ?
C30 B16 B17 57.9(3) . . ?
B21 B16 B17 61.6(3) . . ?
B15 B16 B17 109.8(3) . . ?
C29 B16 H16 121.3 . . ?
C30 B16 H16 117.8 . . ?
B21 B16 H16 127.5 . . ?
B15 B16 H16 125.1 . . ?
B17 B16 H16 120.4 . . ?
C30 B17 B22 105.9(4) . . ?
C30 B17 B16 60.4(3) . . ?
B22 B17 B16 106.3(3) . . ?
C30 B17 B18 58.7(3) . . ?
B22 B17 B18 60.4(3) . . ?
B16 B17 B18 107.9(3) . . ?
C30 B17 B21 105.6(3) . . ?
B22 B17 B21 58.8(3) . . ?
B16 B17 B21 58.7(3) . . ?
B18 B17 B21 107.0(3) . . ?
C30 B17 H17 117.2 . . ?
B22 B17 H17 122.5 . . ?
B16 B17 H17 127.1 . . ?
B18 B17 H17 112.8 . . ?
B21 B17 H17 132.2 . . ?
C30 B18 B19 105.6(3) . . ?
C30 B18 B17 58.5(3) . . ?
B19 B18 B17 108.6(4) . . ?
C30 B18 B13 59.9(2) . . ?
B19 B18 B13 59.4(3) . . ?
B17 B18 B13 108.6(3) . . ?
C30 B18 B22 105.0(3) . . ?
B19 B18 B22 61.3(3) . . ?
B17 B18 B22 59.6(3) . . ?
B13 B18 B22 108.7(3) . . ?
C30 B18 H18 111.3 . . ?
B19 B18 H18 130.0 . . ?
B17 B18 H18 119.0 . . ?
B13 B18 H18 114.1 . . ?
B22 B18 H18 133.6 . . ?
B13 B19 B20 109.4(3) . . ?
B13 B19 B14 60.8(3) . . ?
B20 B19 B14 60.5(3) . . ?
B13 B19 B18 60.5(3) . . ?
B20 B19 B18 107.7(4) . . ?
B14 B19 B18 108.4(3) . . ?
B13 B19 B22 108.3(3) . . ?
B20 B19 B22 59.0(3) . . ?
B14 B19 B22 107.4(4) . . ?
B18 B19 B22 59.7(3) . . ?
B13 B19 H19 117.2 . . ?
B20 B19 H19 127.7 . . ?
B14 B19 H19 126.0 . . ?
B18 B19 H19 115.0 . . ?
B22 B19 H19 121.4 . . ?
B21 B20 B22 59.7(3) . . ?
B21 B20 B19 109.1(4) . . ?
B22 B20 B19 61.8(3) . . ?
B21 B20 B15 59.9(3) . . ?
B22 B20 B15 107.9(3) . . ?
B19 B20 B15 107.8(3) . . ?
B21 B20 B14 107.7(3) . . ?
B22 B20 B14 109.0(3) . . ?
B19 B20 B14 59.8(3) . . ?
B15 B20 B14 59.5(3) . . ?
B21 B20 H20 129.6 . . ?
B22 B20 H20 125.5 . . ?
B19 B20 H20 115.6 . . ?
B15 B20 H20 122.1 . . ?
B14 B20 H20 114.0 . . ?
B16 B21 B22 107.8(4) . . ?
B16 B21 B20 108.0(4) . . ?
B22 B21 B20 60.2(3) . . ?
B16 B21 B15 60.0(3) . . ?
B22 B21 B15 108.8(4) . . ?
B20 B21 B15 60.5(3) . . ?
B16 B21 B17 59.7(3) . . ?
B22 B21 B17 59.6(3) . . ?
B20 B21 B17 107.5(4) . . ?
B15 B21 B17 107.9(3) . . ?
B16 B21 H21 117.9 . . ?
B22 B21 H21 121.5 . . ?
B20 B21 H21 127.8 . . ?
B15 B21 H21 124.6 . . ?
B17 B21 H21 116.2 . . ?
B21 B22 B20 60.1(3) . . ?
B21 B22 B17 61.6(3) . . ?
B20 B22 B17 109.0(3) . . ?
B21 B22 B18 108.9(3) . . ?
B20 B22 B18 107.2(3) . . ?
B17 B22 B18 60.0(3) . . ?
B21 B22 B19 107.2(4) . . ?
B20 B22 B19 59.1(3) . . ?
B17 B22 B19 107.2(3) . . ?
B18 B22 B19 59.0(3) . . ?
B21 B22 H22 120.2 . . ?
B20 B22 H22 120.0 . . ?
B17 B22 H22 122.5 . . ?
B18 B22 H22 123.6 . . ?
B19 B22 H22 122.6 . . ?
C2 C1 B4 113.1(3) . . ?
C2 C1 B6 62.7(2) . . ?
B4 C1 B6 115.0(3) . . ?
C2 C1 B5 113.3(3) . . ?
B4 C1 B5 63.1(3) . . ?
B6 C1 B5 62.4(3) . . ?
C2 C1 B3 61.6(2) . . ?
B4 C1 B3 63.2(3) . . ?
B6 C1 B3 115.0(3) . . ?
B5 C1 B3 115.4(3) . . ?
C2 C1 S1 112.7(2) . . ?
B4 C1 S1 125.5(3) . . ?
B6 C1 S1 111.2(2) . . ?
B5 C1 S1 120.3(3) . . ?
B3 C1 S1 119.0(2) . . ?
C1 C2 B8 108.8(3) . . ?
C1 C2 B7 107.2(3) . . ?
B8 C2 B7 61.3(2) . . ?
C1 C2 B3 60.0(2) . . ?
B8 C2 B3 62.7(2) . . ?
B7 C2 B3 111.7(3) . . ?
C1 C2 S2 119.6(2) . . ?
B8 C2 S2 123.3(3) . . ?
B7 C2 S2 122.8(3) . . ?
B3 C2 S2 119.1(2) . . ?
C1 C2 B6 59.1(2) . . ?
B8 C2 B6 111.5(3) . . ?
B7 C2 B6 61.3(2) . . ?
B3 C2 B6 110.7(3) . . ?
S2 C2 B6 117.6(3) . . ?
C4 C3 C7 114.3(3) . . ?
C4 C3 Co1 124.7(3) . . ?
C7 C3 Co1 121.0(3) . . ?
C3 C4 C5 130.5(3) . . ?
C3 C4 H4A 114.7 . . ?
C5 C4 H4A 114.7 . . ?
C6 C5 C4 131.7(4) . . ?
C6 C5 H5A 114.1 . . ?
C4 C5 H5A 114.1 . . ?
C5 C6 C13 124.0(4) . . ?
C5 C6 S1 118.9(3) . . ?
C13 C6 S1 116.9(3) . . ?
C12 C7 C8 115.9(3) . . ?
C12 C7 C3 120.1(3) . . ?
C8 C7 C3 123.9(3) . . ?
C9 C8 C7 120.7(3) . . ?
C9 C8 H8A 119.6 . . ?
C7 C8 H8A 119.6 . . ?
C8 C9 C10 122.3(4) . . ?
C8 C9 H9A 118.8 . . ?
C10 C9 H9A 118.8 . . ?
C11 C10 C9 118.0(4) . . ?
C11 C10 H10A 121.0 . . ?
C9 C10 H10A 121.0 . . ?
C12 C11 C10 120.8(4) . . ?
C12 C11 H11A 119.6 . . ?
C10 C11 H11A 119.6 . . ?
C11 C12 C7 122.3(4) . . ?
C11 C12 H12A 118.9 . . ?
C7 C12 H12A 118.9 . . ?
C18 C13 C14 119.8(4) . . ?
C18 C13 C6 119.2(3) . . ?
C14 C13 C6 121.0(4) . . ?
C15 C14 C13 118.5(4) . . ?
C15 C14 H14A 120.8 . . ?
C13 C14 H14A 120.8 . . ?
C16 C15 C14 121.0(4) . . ?
C16 C15 H15A 119.5 . . ?
C14 C15 H15A 119.5 . . ?
C15 C16 C17 120.7(4) . . ?
C15 C16 H16A 119.7 . . ?
C17 C16 H16A 119.7 . . ?
C16 C17 C18 119.9(4) . . ?
C16 C17 H17A 120.1 . . ?
C18 C17 H17A 120.1 . . ?
C17 C18 C13 120.1(4) . . ?
C17 C18 H18A 119.9 . . ?
C13 C18 H18A 119.9 . . ?
C23 C19 C20 106.4(3) . . ?
C23 C19 C24 125.2(4) . . ?
C20 C19 C24 127.7(4) . . ?
C23 C19 Co1 70.7(2) . . ?
C20 C19 Co1 69.9(2) . . ?
C24 C19 Co1 131.8(3) . . ?
C19 C20 C21 109.1(3) . . ?
C19 C20 C25 128.0(3) . . ?
C21 C20 C25 122.3(4) . . ?
C19 C20 Co1 70.3(2) . . ?
C21 C20 Co1 73.7(2) . . ?
C25 C20 Co1 129.5(3) . . ?
C22 C21 C20 107.3(3) . . ?
C22 C21 C26 127.7(4) . . ?
C20 C21 C26 124.8(4) . . ?
C22 C21 Co1 71.5(2) . . ?
C20 C21 Co1 67.0(2) . . ?
C26 C21 Co1 130.8(3) . . ?
C21 C22 C23 107.6(3) . . ?
C21 C22 C27 126.4(3) . . ?
C23 C22 C27 125.7(4) . . ?
C21 C22 Co1 70.7(2) . . ?
C23 C22 Co1 67.3(2) . . ?
C27 C22 Co1 132.1(3) . . ?
C19 C23 C22 109.6(3) . . ?
C19 C23 C28 124.6(4) . . ?
C22 C23 C28 125.7(4) . . ?
C19 C23 Co1 69.9(2) . . ?
C22 C23 Co1 73.9(2) . . ?
C28 C23 Co1 125.6(3) . . ?
C19 C24 H24A 109.5 . . ?
C19 C24 H24B 109.5 . . ?
H24A C24 H24B 109.5 . . ?
C19 C24 H24C 109.5 . . ?
H24A C24 H24C 109.5 . . ?
H24B C24 H24C 109.5 . . ?
C20 C25 H25A 109.5 . . ?
C20 C25 H25B 109.5 . . ?
H25A C25 H25B 109.5 . . ?
C20 C25 H25C 109.5 . . ?
H25A C25 H25C 109.5 . . ?
H25B C25 H25C 109.5 . . ?
C21 C26 H26A 109.5 . . ?
C21 C26 H26B 109.5 . . ?
H26A C26 H26B 109.5 . . ?
C21 C26 H26C 109.5 . . ?
H26A C26 H26C 109.5 . . ?
H26B C26 H26C 109.5 . . ?
C22 C27 H27A 109.5 . . ?
C22 C27 H27B 109.5 . . ?
H27A C27 H27B 109.5 . . ?
C22 C27 H27C 109.5 . . ?
H27A C27 H27C 109.5 . . ?
H27B C27 H27C 109.5 . . ?
C23 C28 H28A 109.5 . . ?
C23 C28 H28B 109.5 . . ?
H28A C28 H28B 109.5 . . ?
C23 C28 H28C 109.5 . . ?
H28A C28 H28C 109.5 . . ?
H28B C28 H28C 109.5 . . ?
C30 C29 B14 112.7(3) . . ?
C30 C29 B13 62.5(2) . . ?
B14 C29 B13 63.1(2) . . ?
C30 C29 B16 62.7(2) . . ?
B14 C29 B16 113.2(3) . . ?
B13 C29 B16 115.6(3) . . ?
C30 C29 B15 112.3(3) . . ?
B14 C29 B15 61.9(3) . . ?
B13 C29 B15 114.7(3) . . ?
B16 C29 B15 61.5(3) . . ?
C30 C29 S3 113.2(2) . . ?
B14 C29 S3 125.9(3) . . ?
B13 C29 S3 118.4(3) . . ?
B16 C29 S3 112.2(2) . . ?
B15 C29 S3 121.2(2) . . ?
C29 C30 B17 109.9(3) . . ?
C29 C30 B18 109.2(3) . . ?
B17 C30 B18 62.8(3) . . ?
C29 C30 B13 60.3(2) . . ?
B17 C30 B13 113.9(3) . . ?
B18 C30 B13 62.1(3) . . ?
C29 C30 B16 60.2(2) . . ?
B17 C30 B16 61.7(3) . . ?
B18 C30 B16 112.2(3) . . ?
B13 C30 B16 111.8(3) . . ?
C29 C30 S4 118.4(2) . . ?
B17 C30 S4 121.2(3) . . ?
B18 C30 S4 123.0(3) . . ?
B13 C30 S4 118.0(3) . . ?
B16 C30 S4 117.6(3) . . ?
C32 C31 C35 116.6(3) . . ?
C32 C31 Co2 123.7(3) . . ?
C35 C31 Co2 119.4(3) . . ?
C31 C32 C33 130.6(4) . . ?
C31 C32 H32A 114.7 . . ?
C33 C32 H32A 114.7 . . ?
C34 C33 C32 131.3(4) . . ?
C34 C33 H33A 114.4 . . ?
C32 C33 H33A 114.4 . . ?
C33 C34 C41 125.9(4) . . ?
C33 C34 S3 118.8(3) . . ?
C41 C34 S3 115.3(3) . . ?
C40 C35 C36 115.5(4) . . ?
C40 C35 C31 120.5(3) . . ?
C36 C35 C31 124.0(4) . . ?
C37 C36 C35 121.9(4) . . ?
C37 C36 H36A 119.1 . . ?
C35 C36 H36A 119.1 . . ?
C38 C37 C36 120.7(4) . . ?
C38 C37 H37A 119.6 . . ?
C36 C37 H37A 119.6 . . ?
C37 C38 C39 120.5(4) . . ?
C37 C38 H38A 119.8 . . ?
C39 C38 H38A 119.8 . . ?
C38 C39 C40 119.1(4) . . ?
C38 C39 H39A 120.4 . . ?
C40 C39 H39A 120.4 . . ?
C35 C40 C39 122.2(4) . . ?
C35 C40 H40A 118.9 . . ?
C39 C40 H40A 118.9 . . ?
C46 C41 C42 117.7(4) . . ?
C46 C41 C34 122.5(4) . . ?
C42 C41 C34 119.7(4) . . ?
C43 C42 C41 120.4(4) . . ?
C43 C42 H42A 119.8 . . ?
C41 C42 H42A 119.8 . . ?
C44 C43 C42 120.7(5) . . ?
C44 C43 H43A 119.7 . . ?
C42 C43 H43A 119.7 . . ?
C43 C44 C45 121.3(4) . . ?
C43 C44 H44A 119.3 . . ?
C45 C44 H44A 119.3 . . ?
C44 C45 C46 119.2(5) . . ?
C44 C45 H45A 120.4 . . ?
C46 C45 H45A 120.4 . . ?
C41 C46 C45 120.5(5) . . ?
C41 C46 H46A 119.7 . . ?
C45 C46 H46A 119.7 . . ?
C48 C47 C51 107.3(4) . . ?
C48 C47 C52 125.5(4) . . ?
C51 C47 C52 126.9(4) . . ?
C48 C47 Co2 70.7(2) . . ?
C51 C47 Co2 67.6(2) . . ?
C52 C47 Co2 131.4(3) . . ?
C47 C48 C49 109.1(4) . . ?
C47 C48 C53 125.1(4) . . ?
C49 C48 C53 125.7(4) . . ?
C47 C48 Co2 71.4(2) . . ?
C49 C48 Co2 68.1(2) . . ?
C53 C48 Co2 129.1(3) . . ?
C48 C49 C50 108.1(4) . . ?
C48 C49 C54 126.8(4) . . ?
C50 C49 C54 123.8(4) . . ?
C48 C49 Co2 73.2(2) . . ?
C50 C49 Co2 70.1(2) . . ?
C54 C49 Co2 132.6(3) . . ?
C49 C50 C51 107.7(4) . . ?
C49 C50 C55 128.0(4) . . ?
C51 C50 C55 123.8(4) . . ?
C49 C50 Co2 70.4(2) . . ?
C51 C50 Co2 70.4(2) . . ?
C55 C50 Co2 130.9(3) . . ?
C50 C51 C47 107.7(3) . . ?
C50 C51 C56 126.4(4) . . ?
C47 C51 C56 125.5(4) . . ?
C50 C51 Co2 69.9(2) . . ?
C47 C51 Co2 73.1(2) . . ?
C56 C51 Co2 128.4(3) . . ?
C47 C52 H52A 109.5 . . ?
C47 C52 H52B 109.5 . . ?
H52A C52 H52B 109.5 . . ?
C47 C52 H52C 109.5 . . ?
H52A C52 H52C 109.5 . . ?
H52B C52 H52C 109.5 . . ?
C48 C53 H53A 109.5 . . ?
C48 C53 H53B 109.5 . . ?
H53A C53 H53B 109.5 . . ?
C48 C53 H53C 109.5 . . ?
H53A C53 H53C 109.5 . . ?
H53B C53 H53C 109.5 . . ?
C49 C54 H54A 109.5 . . ?
C49 C54 H54B 109.5 . . ?
H54A C54 H54B 109.5 . . ?
C49 C54 H54C 109.5 . . ?
H54A C54 H54C 109.5 . . ?
H54B C54 H54C 109.5 . . ?
C50 C55 H55A 109.5 . . ?
C50 C55 H55B 109.5 . . ?
H55A C55 H55B 109.5 . . ?
C50 C55 H55C 109.5 . . ?
H55A C55 H55C 109.5 . . ?
H55B C55 H55C 109.5 . . ?
C51 C56 H56A 109.5 . . ?
C51 C56 H56B 109.5 . . ?
H56A C56 H56B 109.5 . . ?
C51 C56 H56C 109.5 . . ?
H56A C56 H56C 109.5 . . ?
H56B C56 H56C 109.5 . . ?
Cl2 C57 Cl1 112.9(3) . . ?
Cl2 C57 H57A 109.0 . . ?
Cl1 C57 H57A 109.0 . . ?
Cl2 C57 H57B 109.0 . . ?
Cl1 C57 H57B 109.0 . . ?
H57A C57 H57B 107.8 . . ?
C3 Co1 C20 109.63(15) . . ?
C3 Co1 C19 90.55(15) . . ?
C20 Co1 C19 39.79(15) . . ?
C3 Co1 C23 110.43(14) . . ?
C20 Co1 C23 65.67(15) . . ?
C19 Co1 C23 39.42(15) . . ?
C3 Co1 C21 148.82(15) . . ?
C20 Co1 C21 39.31(14) . . ?
C19 Co1 C21 66.07(14) . . ?
C23 Co1 C21 64.74(14) . . ?
C3 Co1 C22 149.12(14) . . ?
C20 Co1 C22 64.90(15) . . ?
C19 Co1 C22 65.64(14) . . ?
C23 Co1 C22 38.76(14) . . ?
C21 Co1 C22 37.81(15) . . ?
C3 Co1 S1 96.24(12) . . ?
C20 Co1 S1 151.35(11) . . ?
C19 Co1 S1 131.45(12) . . ?
C23 Co1 S1 94.34(11) . . ?
C21 Co1 S1 114.60(11) . . ?
C22 Co1 S1 86.60(11) . . ?
C3 Co1 S2 89.63(10) . . ?
C20 Co1 S2 98.13(11) . . ?
C19 Co1 S2 134.16(12) . . ?
C23 Co1 S2 157.24(11) . . ?
C21 Co1 S2 92.55(11) . . ?
C22 Co1 S2 120.93(11) . . ?
S1 Co1 S2 94.02(4) . . ?
C31 Co2 C50 89.36(15) . . ?
C31 Co2 C49 102.98(16) . . ?
C50 Co2 C49 39.53(16) . . ?
C31 Co2 C51 113.95(15) . . ?
C50 Co2 C51 39.73(15) . . ?
C49 Co2 C51 66.32(15) . . ?
C31 Co2 C48 140.86(15) . . ?
C50 Co2 C48 65.06(16) . . ?
C49 Co2 C48 38.68(16) . . ?
C51 Co2 C48 64.97(16) . . ?
C31 Co2 C47 152.69(15) . . ?
C50 Co2 C47 65.59(15) . . ?
C49 Co2 C47 65.04(16) . . ?
C51 Co2 C47 39.26(16) . . ?
C48 Co2 C47 37.87(15) . . ?
C31 Co2 S3 95.70(11) . . ?
C50 Co2 S3 124.88(12) . . ?
C49 Co2 S3 154.44(12) . . ?
C51 Co2 S3 90.27(11) . . ?
C48 Co2 S3 123.02(11) . . ?
C47 Co2 S3 90.50(11) . . ?
C31 Co2 S4 93.57(11) . . ?
C50 Co2 S4 142.01(12) . . ?
C49 Co2 S4 103.43(12) . . ?
C51 Co2 S4 151.92(12) . . ?
C48 Co2 S4 90.43(12) . . ?
C47 Co2 S4 112.74(12) . . ?
S3 Co2 S4 92.52(4) . . ?
C6 S1 C1 104.02(18) . . ?
C6 S1 Co1 114.35(13) . . ?
C1 S1 Co1 107.66(13) . . ?
C2 S2 Co1 105.12(13) . . ?
C34 S3 C29 103.36(18) . . ?
C34 S3 Co2 113.03(14) . . ?
C29 S3 Co2 108.99(12) . . ?
C30 S4 Co2 106.56(13) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
B3 C1 1.710(6) . ?
B3 C2 1.737(6) . ?
B3 B9 1.752(6) . ?
B3 B4 1.782(7) . ?
B3 B8 1.789(6) . ?
B3 H3 1.0821 . ?
B4 C1 1.691(6) . ?
B4 B5 1.775(7) . ?
B4 B9 1.785(7) . ?
B4 B10 1.802(6) . ?
B4 H4 1.1257 . ?
B5 C1 1.701(5) . ?
B5 B6 1.763(7) . ?
B5 B11 1.779(6) . ?
B5 B10 1.782(7) . ?
B5 H5 1.1682 . ?
B6 C1 1.700(6) . ?
B6 C2 1.761(6) . ?
B6 B11 1.776(6) . ?
B6 B7 1.776(6) . ?
B6 H6 1.1360 . ?
B7 C2 1.722(5) . ?
B7 B12 1.737(7) . ?
B7 B8 1.745(6) . ?
B7 B11 1.781(6) . ?
B7 H7 1.0859 . ?
B8 C2 1.701(6) . ?
B8 B12 1.763(6) . ?
B8 B9 1.801(7) . ?
B8 H8 1.0796 . ?
B9 B10 1.818(7) . ?
B9 B12 1.822(7) . ?
B9 H9 1.0660 . ?
B10 B11 1.758(7) . ?
B10 B12 1.790(7) . ?
B10 H10 1.0810 . ?
B11 B12 1.774(8) . ?
B11 H11 1.0559 . ?
B12 H12 1.0607 . ?
B13 C29 1.707(5) . ?
B13 C30 1.742(6) . ?
B13 B19 1.762(7) . ?
B13 B18 1.781(7) . ?
B13 B14 1.785(6) . ?
B13 H13 1.1306 . ?
B14 C29 1.702(6) . ?
B14 B15 1.765(7) . ?
B14 B19 1.767(7) . ?
B14 B20 1.781(7) . ?
B14 H14 1.1568 . ?
B15 C29 1.731(6) . ?
B15 B16 1.759(7) . ?
B15 B21 1.767(7) . ?
B15 B20 1.779(7) . ?
B15 H15 1.1004 . ?
B16 C29 1.708(6) . ?
B16 C30 1.749(6) . ?
B16 B21 1.753(6) . ?
B16 B17 1.772(7) . ?
B16 H16 1.1562 . ?
B17 C30 1.705(6) . ?
B17 B22 1.771(7) . ?
B17 B18 1.779(7) . ?
B17 B21 1.806(7) . ?
B17 H17 1.0821 . ?
B18 C30 1.709(6) . ?
B18 B19 1.774(7) . ?
B18 B22 1.786(7) . ?
B18 H18 1.0439 . ?
B19 B20 1.766(8) . ?
B19 B22 1.815(8) . ?
B19 H19 1.1031 . ?
B20 B21 1.762(8) . ?
B20 B22 1.765(7) . ?
B20 H20 1.1507 . ?
B21 B22 1.756(7) . ?
B21 H21 1.1231 . ?
B22 H22 1.1562 . ?
C1 C2 1.684(5) . ?
C1 S1 1.828(4) . ?
C2 S2 1.752(4) . ?
C3 C4 1.363(5) . ?
C3 C7 1.501(5) . ?
C3 Co1 1.954(4) . ?
C4 C5 1.433(5) . ?
C4 H4A 0.9300 . ?
C5 C6 1.326(5) . ?
C5 H5A 0.9300 . ?
C6 C13 1.502(5) . ?
C6 S1 1.775(4) . ?
C7 C12 1.395(5) . ?
C7 C8 1.425(5) . ?
C8 C9 1.349(5) . ?
C8 H8A 0.9300 . ?
C9 C10 1.385(5) . ?
C9 H9A 0.9300 . ?
C10 C11 1.374(6) . ?
C10 H10A 0.9300 . ?
C11 C12 1.369(5) . ?
C11 H11A 0.9300 . ?
C12 H12A 0.9300 . ?
C13 C18 1.386(6) . ?
C13 C14 1.399(5) . ?
C14 C15 1.391(6) . ?
C14 H14A 0.9300 . ?
C15 C16 1.361(6) . ?
C15 H15A 0.9300 . ?
C16 C17 1.366(6) . ?
C16 H16A 0.9300 . ?
C17 C18 1.384(6) . ?
C17 H17A 0.9300 . ?
C18 H18A 0.9300 . ?
C19 C23 1.415(6) . ?
C19 C20 1.423(5) . ?
C19 C24 1.487(5) . ?
C19 Co1 2.093(4) . ?
C20 C21 1.438(5) . ?
C20 C25 1.494(5) . ?
C20 Co1 2.088(4) . ?
C21 C22 1.415(6) . ?
C21 C26 1.491(5) . ?
C21 Co1 2.178(4) . ?
C22 C23 1.427(5) . ?
C22 C27 1.486(5) . ?
C22 Co1 2.190(4) . ?
C23 C28 1.500(6) . ?
C23 Co1 2.103(4) . ?
C24 H24A 0.9600 . ?
C24 H24B 0.9600 . ?
C24 H24C 0.9600 . ?
C25 H25A 0.9600 . ?
C25 H25B 0.9600 . ?
C25 H25C 0.9600 . ?
C26 H26A 0.9600 . ?
C26 H26B 0.9600 . ?
C26 H26C 0.9600 . ?
C27 H27A 0.9600 . ?
C27 H27B 0.9600 . ?
C27 H27C 0.9600 . ?
C28 H28A 0.9600 . ?
C28 H28B 0.9600 . ?
C28 H28C 0.9600 . ?
C29 C30 1.652(5) . ?
C29 S3 1.826(4) . ?
C30 S4 1.780(4) . ?
C31 C32 1.348(5) . ?
C31 C35 1.476(5) . ?
C31 Co2 1.959(4) . ?
C32 C33 1.454(5) . ?
C32 H32A 0.9300 . ?
C33 C34 1.311(6) . ?
C33 H33A 0.9300 . ?
C34 C41 1.483(5) . ?
C34 S3 1.780(4) . ?
C35 C40 1.396(6) . ?
C35 C36 1.402(5) . ?
C36 C37 1.384(6) . ?
C36 H36A 0.9300 . ?
C37 C38 1.347(6) . ?
C37 H37A 0.9300 . ?
C38 C39 1.369(6) . ?
C38 H38A 0.9300 . ?
C39 C40 1.404(5) . ?
C39 H39A 0.9300 . ?
C40 H40A 0.9300 . ?
C41 C46 1.373(6) . ?
C41 C42 1.413(6) . ?
C42 C43 1.380(5) . ?
C42 H42A 0.9300 . ?
C43 C44 1.345(7) . ?
C43 H43A 0.9300 . ?
C44 C45 1.352(7) . ?
C44 H44A 0.9300 . ?
C45 C46 1.424(5) . ?
C45 H45A 0.9300 . ?
C46 H46A 0.9300 . ?
C47 C48 1.412(6) . ?
C47 C51 1.441(6) . ?
C47 C52 1.493(6) . ?
C47 Co2 2.180(4) . ?
C48 C49 1.417(6) . ?
C48 C53 1.510(6) . ?
C48 Co2 2.171(4) . ?
C49 C50 1.422(6) . ?
C49 C54 1.512(5) . ?
C49 Co2 2.103(4) . ?
C50 C51 1.430(6) . ?
C50 C55 1.467(6) . ?
C50 Co2 2.100(4) . ?
C51 C56 1.496(5) . ?
C51 Co2 2.107(4) . ?
C52 H52A 0.9600 . ?
C52 H52B 0.9600 . ?
C52 H52C 0.9600 . ?
C53 H53A 0.9600 . ?
C53 H53B 0.9600 . ?
C53 H53C 0.9600 . ?
C54 H54A 0.9600 . ?
C54 H54B 0.9600 . ?
C54 H54C 0.9600 . ?
C55 H55A 0.9600 . ?
C55 H55B 0.9600 . ?
C55 H55C 0.9600 . ?
C56 H56A 0.9600 . ?
C56 H56B 0.9600 . ?
C56 H56C 0.9600 . ?
C57 Cl2 1.698(5) . ?
C57 Cl1 1.738(5) . ?
C57 H57A 0.9700 . ?
C57 H57B 0.9700 . ?
Co1 S1 2.2037(11) . ?
Co1 S2 2.2555(12) . ?
Co2 S3 2.2027(14) . ?
Co2 S4 2.2557(12) . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C2 B3 B4 C1 -34.2(3) . . . . ?
B9 B3 B4 C1 -134.4(3) . . . . ?
B8 B3 B4 C1 -94.9(3) . . . . ?
C1 B3 B4 B5 33.1(3) . . . . ?
C2 B3 B4 B5 -1.1(4) . . . . ?
B9 B3 B4 B5 -101.3(3) . . . . ?
B8 B3 B4 B5 -61.8(4) . . . . ?
C1 B3 B4 B9 134.4(3) . . . . ?
C2 B3 B4 B9 100.2(3) . . . . ?
B8 B3 B4 B9 39.5(3) . . . . ?
C1 B3 B4 B10 96.2(3) . . . . ?
C2 B3 B4 B10 62.0(4) . . . . ?
B9 B3 B4 B10 -38.2(3) . . . . ?
B8 B3 B4 B10 1.3(4) . . . . ?
B3 B4 B5 C1 -33.2(3) . . . . ?
B9 B4 B5 C1 -95.6(3) . . . . ?
B10 B4 B5 C1 -133.1(3) . . . . ?
C1 B4 B5 B6 32.6(3) . . . . ?
B3 B4 B5 B6 -0.6(4) . . . . ?
B9 B4 B5 B6 -62.9(4) . . . . ?
B10 B4 B5 B6 -100.5(3) . . . . ?
C1 B4 B5 B11 96.3(3) . . . . ?
B3 B4 B5 B11 63.1(4) . . . . ?
B9 B4 B5 B11 0.7(4) . . . . ?
B10 B4 B5 B11 -36.8(3) . . . . ?
C1 B4 B5 B10 133.1(3) . . . . ?
B3 B4 B5 B10 99.9(3) . . . . ?
B9 B4 B5 B10 37.5(3) . . . . ?
B4 B5 B6 C1 -32.4(3) . . . . ?
B11 B5 B6 C1 -133.6(3) . . . . ?
B10 B5 B6 C1 -96.7(3) . . . . ?
C1 B5 B6 C2 34.4(3) . . . . ?
B4 B5 B6 C2 2.0(4) . . . . ?
B11 B5 B6 C2 -99.2(3) . . . . ?
B10 B5 B6 C2 -62.3(4) . . . . ?
C1 B5 B6 B11 133.6(3) . . . . ?
B4 B5 B6 B11 101.2(4) . . . . ?
B10 B5 B6 B11 36.9(3) . . . . ?
C1 B5 B6 B7 95.7(3) . . . . ?
B4 B5 B6 B7 63.3(4) . . . . ?
B11 B5 B6 B7 -37.8(3) . . . . ?
B10 B5 B6 B7 -0.9(4) . . . . ?
C1 B6 B7 C2 -37.4(3) . . . . ?
B5 B6 B7 C2 -98.8(3) . . . . ?
B11 B6 B7 C2 -136.7(3) . . . . ?
C1 B6 B7 B12 61.8(4) . . . . ?
C2 B6 B7 B12 99.3(3) . . . . ?
B5 B6 B7 B12 0.5(4) . . . . ?
B11 B6 B7 B12 -37.4(3) . . . . ?
C1 B6 B7 B8 -2.8(4) . . . . ?
C2 B6 B7 B8 34.7(3) . . . . ?
B5 B6 B7 B8 -64.1(4) . . . . ?
B11 B6 B7 B8 -102.0(4) . . . . ?
C1 B6 B7 B11 99.2(3) . . . . ?
C2 B6 B7 B11 136.7(3) . . . . ?
B5 B6 B7 B11 37.9(3) . . . . ?
B12 B7 B8 C2 -136.6(3) . . . . ?
B6 B7 B8 C2 -35.3(3) . . . . ?
B11 B7 B8 C2 -99.1(3) . . . . ?
C2 B7 B8 B12 136.6(3) . . . . ?
B6 B7 B8 B12 101.3(4) . . . . ?
B11 B7 B8 B12 37.5(3) . . . . ?
C2 B7 B8 B3 36.3(3) . . . . ?
B12 B7 B8 B3 -100.3(4) . . . . ?
B6 B7 B8 B3 1.0(4) . . . . ?
B11 B7 B8 B3 -62.8(4) . . . . ?
C2 B7 B8 B9 98.2(3) . . . . ?
B12 B7 B8 B9 -38.5(3) . . . . ?
B6 B7 B8 B9 62.8(4) . . . . ?
B11 B7 B8 B9 -0.9(4) . . . . ?
C1 B3 B8 C2 37.7(3) . . . . ?
B9 B3 B8 C2 137.3(3) . . . . ?
B4 B3 B8 C2 98.0(3) . . . . ?
C1 B3 B8 B7 1.2(4) . . . . ?
C2 B3 B8 B7 -36.4(3) . . . . ?
B9 B3 B8 B7 100.8(4) . . . . ?
B4 B3 B8 B7 61.6(4) . . . . ?
C1 B3 B8 B12 -61.5(4) . . . . ?
C2 B3 B8 B12 -99.2(3) . . . . ?
B9 B3 B8 B12 38.1(3) . . . . ?
B4 B3 B8 B12 -1.2(4) . . . . ?
C1 B3 B8 B9 -99.6(3) . . . . ?
C2 B3 B8 B9 -137.3(3) . . . . ?
B4 B3 B8 B9 -39.3(3) . . . . ?
C1 B3 B9 B4 -38.7(3) . . . . ?
C2 B3 B9 B4 -99.7(3) . . . . ?
B8 B3 B9 B4 -136.5(3) . . . . ?
C1 B3 B9 B8 97.7(3) . . . . ?
C2 B3 B9 B8 36.8(3) . . . . ?
B4 B3 B9 B8 136.5(3) . . . . ?
C1 B3 B9 B10 -0.8(4) . . . . ?
C2 B3 B9 B10 -61.7(4) . . . . ?
B4 B3 B9 B10 38.0(3) . . . . ?
B8 B3 B9 B10 -98.5(4) . . . . ?
C1 B3 B9 B12 61.3(4) . . . . ?
C2 B3 B9 B12 0.3(4) . . . . ?
B4 B3 B9 B12 100.0(4) . . . . ?
B8 B3 B9 B12 -36.4(3) . . . . ?
C1 B4 B9 B3 39.1(3) . . . . ?
B5 B4 B9 B3 100.5(3) . . . . ?
B10 B4 B9 B3 137.5(3) . . . . ?
C1 B4 B9 B8 0.1(4) . . . . ?
B5 B4 B9 B8 61.5(4) . . . . ?
B3 B4 B9 B8 -39.0(3) . . . . ?
B10 B4 B9 B8 98.5(4) . . . . ?
C1 B4 B9 B10 -98.4(3) . . . . ?
B5 B4 B9 B10 -37.0(3) . . . . ?
B3 B4 B9 B10 -137.5(3) . . . . ?
C1 B4 B9 B12 -61.1(4) . . . . ?
B5 B4 B9 B12 0.2(4) . . . . ?
B3 B4 B9 B12 -100.3(3) . . . . ?
B10 B4 B9 B12 37.3(3) . . . . ?
C2 B8 B9 B3 -37.5(3) . . . . ?
B7 B8 B9 B3 -100.5(3) . . . . ?
B12 B8 B9 B3 -138.1(4) . . . . ?
C2 B8 B9 B4 1.5(4) . . . . ?
B7 B8 B9 B4 -61.5(4) . . . . ?
B12 B8 B9 B4 -99.0(4) . . . . ?
B3 B8 B9 B4 39.0(3) . . . . ?
C2 B8 B9 B10 64.5(4) . . . . ?
B7 B8 B9 B10 1.5(4) . . . . ?
B12 B8 B9 B10 -36.0(3) . . . . ?
B3 B8 B9 B10 102.1(4) . . . . ?
C2 B8 B9 B12 100.6(3) . . . . ?
B7 B8 B9 B12 37.5(3) . . . . ?
B3 B8 B9 B12 138.1(4) . . . . ?
C1 B5 B10 B11 -98.6(3) . . . . ?
B6 B5 B10 B11 -37.3(3) . . . . ?
B4 B5 B10 B11 -138.5(3) . . . . ?
C1 B5 B10 B12 -60.3(4) . . . . ?
B6 B5 B10 B12 1.0(4) . . . . ?
B4 B5 B10 B12 -100.1(4) . . . . ?
B11 B5 B10 B12 38.3(3) . . . . ?
C1 B5 B10 B4 39.9(3) . . . . ?
B6 B5 B10 B4 101.2(3) . . . . ?
B11 B5 B10 B4 138.5(3) . . . . ?
C1 B5 B10 B9 3.6(4) . . . . ?
B6 B5 B10 B9 64.9(4) . . . . ?
B4 B5 B10 B9 -36.3(3) . . . . ?
B11 B5 B10 B9 102.2(4) . . . . ?
C1 B4 B10 B11 -2.8(4) . . . . ?
B5 B4 B10 B11 37.2(3) . . . . ?
B3 B4 B10 B11 -64.2(4) . . . . ?
B9 B4 B10 B11 -101.5(4) . . . . ?
C1 B4 B10 B5 -40.1(3) . . . . ?
B3 B4 B10 B5 -101.4(3) . . . . ?
B9 B4 B10 B5 -138.7(4) . . . . ?
C1 B4 B10 B12 60.5(4) . . . . ?
B5 B4 B10 B12 100.5(4) . . . . ?
B3 B4 B10 B12 -0.9(4) . . . . ?
B9 B4 B10 B12 -38.2(3) . . . . ?
C1 B4 B10 B9 98.6(4) . . . . ?
B5 B4 B10 B9 138.7(4) . . . . ?
B3 B4 B10 B9 37.3(3) . . . . ?
B3 B9 B10 B11 61.9(4) . . . . ?
B4 B9 B10 B11 100.1(4) . . . . ?
B8 B9 B10 B11 -1.6(4) . . . . ?
B12 B9 B10 B11 -37.3(3) . . . . ?
B3 B9 B10 B5 -1.8(5) . . . . ?
B4 B9 B10 B5 36.4(3) . . . . ?
B8 B9 B10 B5 -65.3(4) . . . . ?
B12 B9 B10 B5 -101.0(4) . . . . ?
B3 B9 B10 B12 99.2(4) . . . . ?
B4 B9 B10 B12 137.4(3) . . . . ?
B8 B9 B10 B12 35.7(3) . . . . ?
B3 B9 B10 B4 -38.2(3) . . . . ?
B8 B9 B10 B4 -101.7(3) . . . . ?
B12 B9 B10 B4 -137.4(3) . . . . ?
B5 B10 B11 B12 136.9(3) . . . . ?
B4 B10 B11 B12 100.1(4) . . . . ?
B9 B10 B11 B12 37.6(3) . . . . ?
B5 B10 B11 B6 37.1(3) . . . . ?
B12 B10 B11 B6 -99.8(3) . . . . ?
B4 B10 B11 B6 0.3(5) . . . . ?
B9 B10 B11 B6 -62.2(4) . . . . ?
B12 B10 B11 B5 -136.9(3) . . . . ?
B4 B10 B11 B5 -36.8(3) . . . . ?
B9 B10 B11 B5 -99.4(3) . . . . ?
B5 B10 B11 B7 100.4(3) . . . . ?
B12 B10 B11 B7 -36.5(3) . . . . ?
B4 B10 B11 B7 63.6(4) . . . . ?
B9 B10 B11 B7 1.0(4) . . . . ?
C1 B6 B11 B10 2.3(4) . . . . ?
C2 B6 B11 B10 62.9(4) . . . . ?
B5 B6 B11 B10 -37.6(3) . . . . ?
B7 B6 B11 B10 100.3(4) . . . . ?
C1 B6 B11 B12 -61.9(4) . . . . ?
C2 B6 B11 B12 -1.3(4) . . . . ?
B5 B6 B11 B12 -101.8(4) . . . . ?
B7 B6 B11 B12 36.1(3) . . . . ?
C1 B6 B11 B5 39.9(3) . . . . ?
C2 B6 B11 B5 100.5(3) . . . . ?
B7 B6 B11 B5 137.8(3) . . . . ?
C1 B6 B11 B7 -98.0(3) . . . . ?
C2 B6 B11 B7 -37.4(3) . . . . ?
B5 B6 B11 B7 -137.8(3) . . . . ?
C1 B5 B11 B10 98.4(4) . . . . ?
B6 B5 B11 B10 138.2(3) . . . . ?
B4 B5 B11 B10 37.6(3) . . . . ?
C1 B5 B11 B12 59.4(4) . . . . ?
B6 B5 B11 B12 99.3(3) . . . . ?
B4 B5 B11 B12 -1.4(4) . . . . ?
B10 B5 B11 B12 -39.0(3) . . . . ?
C1 B5 B11 B6 -39.8(3) . . . . ?
B4 B5 B11 B6 -100.6(3) . . . . ?
B10 B5 B11 B6 -138.2(3) . . . . ?
C1 B5 B11 B7 -2.3(4) . . . . ?
B6 B5 B11 B7 37.5(3) . . . . ?
B4 B5 B11 B7 -63.2(4) . . . . ?
B10 B5 B11 B7 -100.7(4) . . . . ?
C2 B7 B11 B10 -62.3(4) . . . . ?
B12 B7 B11 B10 37.6(3) . . . . ?
B8 B7 B11 B10 -0.1(4) . . . . ?
B6 B7 B11 B10 -101.0(3) . . . . ?
C2 B7 B11 B12 -99.9(3) . . . . ?
B8 B7 B11 B12 -37.7(3) . . . . ?
B6 B7 B11 B12 -138.6(3) . . . . ?
C2 B7 B11 B6 38.7(3) . . . . ?
B12 B7 B11 B6 138.6(3) . . . . ?
B8 B7 B11 B6 101.0(3) . . . . ?
C2 B7 B11 B5 1.4(4) . . . . ?
B12 B7 B11 B5 101.4(4) . . . . ?
B8 B7 B11 B5 63.7(4) . . . . ?
B6 B7 B11 B5 -37.3(3) . . . . ?
C2 B7 B12 B8 -37.9(3) . . . . ?
B6 B7 B12 B8 -101.6(3) . . . . ?
B11 B7 B12 B8 -138.7(3) . . . . ?
C2 B7 B12 B11 100.8(3) . . . . ?
B8 B7 B12 B11 138.7(3) . . . . ?
B6 B7 B12 B11 37.1(3) . . . . ?
C2 B7 B12 B10 63.9(4) . . . . ?
B8 B7 B12 B10 101.7(3) . . . . ?
B6 B7 B12 B10 0.1(4) . . . . ?
B11 B7 B12 B10 -36.9(3) . . . . ?
C2 B7 B12 B9 0.0(5) . . . . ?
B8 B7 B12 B9 37.8(3) . . . . ?
B6 B7 B12 B9 -63.8(4) . . . . ?
B11 B7 B12 B9 -100.9(4) . . . . ?
C2 B8 B12 B7 38.3(3) . . . . ?
B3 B8 B12 B7 101.1(3) . . . . ?
B9 B8 B12 B7 137.8(3) . . . . ?
C2 B8 B12 B11 0.8(4) . . . . ?
B7 B8 B12 B11 -37.6(3) . . . . ?
B3 B8 B12 B11 63.5(4) . . . . ?
B9 B8 B12 B11 100.2(4) . . . . ?
C2 B8 B12 B10 -62.1(4) . . . . ?
B7 B8 B12 B10 -100.4(4) . . . . ?
B3 B8 B12 B10 0.6(4) . . . . ?
B9 B8 B12 B10 37.4(3) . . . . ?
C2 B8 B12 B9 -99.4(3) . . . . ?
B7 B8 B12 B9 -137.8(3) . . . . ?
B3 B8 B12 B9 -36.7(3) . . . . ?
B10 B11 B12 B7 -138.3(3) . . . . ?
B6 B11 B12 B7 -36.7(3) . . . . ?
B5 B11 B12 B7 -99.5(3) . . . . ?
B10 B11 B12 B8 -101.2(4) . . . . ?
B6 B11 B12 B8 0.4(4) . . . . ?
B5 B11 B12 B8 -62.4(4) . . . . ?
B7 B11 B12 B8 37.1(3) . . . . ?
B6 B11 B12 B10 101.5(3) . . . . ?
B5 B11 B12 B10 38.8(3) . . . . ?
B7 B11 B12 B10 138.3(3) . . . . ?
B10 B11 B12 B9 -37.3(3) . . . . ?
B6 B11 B12 B9 64.3(4) . . . . ?
B5 B11 B12 B9 1.5(4) . . . . ?
B7 B11 B12 B9 101.0(3) . . . . ?
B11 B10 B12 B7 37.8(3) . . . . ?
B5 B10 B12 B7 -0.7(4) . . . . ?
B4 B10 B12 B7 -63.3(4) . . . . ?
B9 B10 B12 B7 -100.7(3) . . . . ?
B11 B10 B12 B8 101.2(4) . . . . ?
B5 B10 B12 B8 62.7(4) . . . . ?
B4 B10 B12 B8 0.2(5) . . . . ?
B9 B10 B12 B8 -37.3(3) . . . . ?
B5 B10 B12 B11 -38.5(3) . . . . ?
B4 B10 B12 B11 -101.0(4) . . . . ?
B9 B10 B12 B11 -138.5(3) . . . . ?
B11 B10 B12 B9 138.5(3) . . . . ?
B5 B10 B12 B9 100.0(3) . . . . ?
B4 B10 B12 B9 37.5(3) . . . . ?
B3 B9 B12 B7 -0.2(5) . . . . ?
B4 B9 B12 B7 63.3(4) . . . . ?
B8 B9 B12 B7 -37.6(3) . . . . ?
B10 B9 B12 B7 101.1(4) . . . . ?
B3 B9 B12 B8 37.4(3) . . . . ?
B4 B9 B12 B8 100.9(3) . . . . ?
B10 B9 B12 B8 138.7(3) . . . . ?
B3 B9 B12 B11 -64.6(4) . . . . ?
B4 B9 B12 B11 -1.1(4) . . . . ?
B8 B9 B12 B11 -102.0(3) . . . . ?
B10 B9 B12 B11 36.7(3) . . . . ?
B3 B9 B12 B10 -101.3(4) . . . . ?
B4 B9 B12 B10 -37.8(3) . . . . ?
B8 B9 B12 B10 -138.7(3) . . . . ?
C30 B13 B14 C29 34.9(3) . . . . ?
B19 B13 B14 C29 133.6(4) . . . . ?
B18 B13 B14 C29 95.5(3) . . . . ?
C29 B13 B14 B15 -33.2(3) . . . . ?
C30 B13 B14 B15 1.7(4) . . . . ?
B19 B13 B14 B15 100.4(4) . . . . ?
B18 B13 B14 B15 62.3(4) . . . . ?
C29 B13 B14 B19 -133.6(4) . . . . ?
C30 B13 B14 B19 -98.7(4) . . . . ?
B18 B13 B14 B19 -38.1(3) . . . . ?
C29 B13 B14 B20 -97.0(4) . . . . ?
C30 B13 B14 B20 -62.1(4) . . . . ?
B19 B13 B14 B20 36.6(3) . . . . ?
B18 B13 B14 B20 -1.6(4) . . . . ?
B19 B14 B15 C29 95.8(3) . . . . ?
B20 B14 B15 C29 132.5(3) . . . . ?
B13 B14 B15 C29 32.7(3) . . . . ?
C29 B14 B15 B16 -32.7(3) . . . . ?
B19 B14 B15 B16 63.1(4) . . . . ?
B20 B14 B15 B16 99.8(4) . . . . ?
B13 B14 B15 B16 0.0(4) . . . . ?
C29 B14 B15 B21 -95.7(3) . . . . ?
B19 B14 B15 B21 0.1(4) . . . . ?
B20 B14 B15 B21 36.8(3) . . . . ?
B13 B14 B15 B21 -63.1(4) . . . . ?
C29 B14 B15 B20 -132.5(3) . . . . ?
B19 B14 B15 B20 -36.7(3) . . . . ?
B13 B14 B15 B20 -99.8(4) . . . . ?
B14 B15 B16 C29 32.6(3) . . . . ?
B21 B15 B16 C29 133.7(3) . . . . ?
B20 B15 B16 C29 96.1(3) . . . . ?
C29 B15 B16 C30 -34.3(3) . . . . ?
B14 B15 B16 C30 -1.7(4) . . . . ?
B21 B15 B16 C30 99.5(4) . . . . ?
B20 B15 B16 C30 61.9(4) . . . . ?
C29 B15 B16 B21 -133.7(3) . . . . ?
B14 B15 B16 B21 -101.1(4) . . . . ?
B20 B15 B16 B21 -37.6(3) . . . . ?
C29 B15 B16 B17 -95.4(3) . . . . ?
B14 B15 B16 B17 -62.8(4) . . . . ?
B21 B15 B16 B17 38.3(3) . . . . ?
B20 B15 B16 B17 0.7(5) . . . . ?
C29 B16 B17 C30 34.7(3) . . . . ?
B21 B16 B17 C30 135.2(4) . . . . ?
B15 B16 B17 C30 97.4(4) . . . . ?
C29 B16 B17 B22 -64.5(4) . . . . ?
C30 B16 B17 B22 -99.3(4) . . . . ?
B21 B16 B17 B22 35.9(4) . . . . ?
B15 B16 B17 B22 -1.9(5) . . . . ?
C29 B16 B17 B18 -1.0(4) . . . . ?
C30 B16 B17 B18 -35.8(3) . . . . ?
B21 B16 B17 B18 99.4(4) . . . . ?
B15 B16 B17 B18 61.6(4) . . . . ?
C29 B16 B17 B21 -100.4(4) . . . . ?
C30 B16 B17 B21 -135.2(4) . . . . ?
B15 B16 B17 B21 -37.8(3) . . . . ?
B22 B17 B18 C30 135.5(3) . . . . ?
B16 B17 B18 C30 36.5(3) . . . . ?
B21 B17 B18 C30 98.3(3) . . . . ?
C30 B17 B18 B19 -97.2(3) . . . . ?
B22 B17 B18 B19 38.2(3) . . . . ?
B16 B17 B18 B19 -60.8(4) . . . . ?
B21 B17 B18 B19 1.0(4) . . . . ?
C30 B17 B18 B13 -34.2(3) . . . . ?
B22 B17 B18 B13 101.3(4) . . . . ?
B16 B17 B18 B13 2.3(4) . . . . ?
B21 B17 B18 B13 64.1(4) . . . . ?
C30 B17 B18 B22 -135.5(3) . . . . ?
B16 B17 B18 B22 -99.0(4) . . . . ?
B21 B17 B18 B22 -37.2(3) . . . . ?
C29 B13 B18 C30 -36.2(3) . . . . ?
B19 B13 B18 C30 -134.8(3) . . . . ?
B14 B13 B18 C30 -96.8(3) . . . . ?
C29 B13 B18 B19 98.6(3) . . . . ?
C30 B13 B18 B19 134.8(3) . . . . ?
B14 B13 B18 B19 38.0(3) . . . . ?
C29 B13 B18 B17 -2.6(4) . . . . ?
C30 B13 B18 B17 33.6(3) . . . . ?
B19 B13 B18 B17 -101.1(4) . . . . ?
B14 B13 B18 B17 -63.1(4) . . . . ?
C29 B13 B18 B22 60.7(4) . . . . ?
C30 B13 B18 B22 96.9(4) . . . . ?
B19 B13 B18 B22 -37.9(3) . . . . ?
B14 B13 B18 B22 0.1(4) . . . . ?
C29 B13 B19 B20 2.1(4) . . . . ?
C30 B13 B19 B20 61.3(4) . . . . ?
B18 B13 B19 B20 99.8(4) . . . . ?
B14 B13 B19 B20 -37.4(3) . . . . ?
C29 B13 B19 B14 39.4(3) . . . . ?
C30 B13 B19 B14 98.7(3) . . . . ?
B18 B13 B19 B14 137.2(4) . . . . ?
C29 B13 B19 B18 -97.7(3) . . . . ?
C30 B13 B19 B18 -38.5(3) . . . . ?
B14 B13 B19 B18 -137.2(4) . . . . ?
C29 B13 B19 B22 -60.7(4) . . . . ?
C30 B13 B19 B22 -1.4(4) . . . . ?
B18 B13 B19 B22 37.1(3) . . . . ?
B14 B13 B19 B22 -100.1(4) . . . . ?
C29 B14 B19 B13 -39.6(3) . . . . ?
B15 B14 B19 B13 -102.0(3) . . . . ?
B20 B14 B19 B13 -138.9(4) . . . . ?
C29 B14 B19 B20 99.3(4) . . . . ?
B15 B14 B19 B20 36.9(3) . . . . ?
B13 B14 B19 B20 138.9(4) . . . . ?
C29 B14 B19 B18 -1.0(5) . . . . ?
B15 B14 B19 B18 -63.4(4) . . . . ?
B20 B14 B19 B18 -100.3(4) . . . . ?
B13 B14 B19 B18 38.6(3) . . . . ?
C29 B14 B19 B22 62.1(4) . . . . ?
B15 B14 B19 B22 -0.4(4) . . . . ?
B20 B14 B19 B22 -37.3(3) . . . . ?
B13 B14 B19 B22 101.6(4) . . . . ?
C30 B18 B19 B13 39.6(3) . . . . ?
B17 B18 B19 B13 101.0(3) . . . . ?
B22 B18 B19 B13 138.5(3) . . . . ?
C30 B18 B19 B20 -63.1(4) . . . . ?
B17 B18 B19 B20 -1.7(4) . . . . ?
B13 B18 B19 B20 -102.7(4) . . . . ?
B22 B18 B19 B20 35.7(3) . . . . ?
C30 B18 B19 B14 0.9(5) . . . . ?
B17 B18 B19 B14 62.3(4) . . . . ?
B13 B18 B19 B14 -38.7(3) . . . . ?
B22 B18 B19 B14 99.8(4) . . . . ?
C30 B18 B19 B22 -98.9(4) . . . . ?
B17 B18 B19 B22 -37.4(3) . . . . ?
B13 B18 B19 B22 -138.5(3) . . . . ?
B13 B19 B20 B21 -62.4(5) . . . . ?
B14 B19 B20 B21 -99.9(4) . . . . ?
B18 B19 B20 B21 1.7(5) . . . . ?
B22 B19 B20 B21 37.8(3) . . . . ?
B13 B19 B20 B22 -100.2(4) . . . . ?
B14 B19 B20 B22 -137.6(3) . . . . ?
B18 B19 B20 B22 -36.0(3) . . . . ?
B13 B19 B20 B15 1.0(5) . . . . ?
B14 B19 B20 B15 -36.4(3) . . . . ?
B18 B19 B20 B15 65.2(4) . . . . ?
B22 B19 B20 B15 101.2(4) . . . . ?
B13 B19 B20 B14 37.5(3) . . . . ?
B18 B19 B20 B14 101.6(4) . . . . ?
B22 B19 B20 B14 137.6(3) . . . . ?
C29 B15 B20 B21 98.5(3) . . . . ?
B16 B15 B20 B21 37.6(3) . . . . ?
B14 B15 B20 B21 138.7(3) . . . . ?
C29 B15 B20 B22 61.7(4) . . . . ?
B16 B15 B20 B22 0.8(5) . . . . ?
B14 B15 B20 B22 101.9(4) . . . . ?
B21 B15 B20 B22 -36.8(3) . . . . ?
C29 B15 B20 B19 -3.6(5) . . . . ?
B16 B15 B20 B19 -64.6(4) . . . . ?
B14 B15 B20 B19 36.6(3) . . . . ?
B21 B15 B20 B19 -102.2(4) . . . . ?
C29 B15 B20 B14 -40.2(3) . . . . ?
B16 B15 B20 B14 -101.1(3) . . . . ?
B21 B15 B20 B14 -138.7(3) . . . . ?
C29 B14 B20 B21 4.5(4) . . . . ?
B15 B14 B20 B21 -36.8(3) . . . . ?
B19 B14 B20 B21 102.2(4) . . . . ?
B13 B14 B20 B21 65.7(4) . . . . ?
C29 B14 B20 B22 -58.8(4) . . . . ?
B15 B14 B20 B22 -100.0(4) . . . . ?
B19 B14 B20 B22 38.9(3) . . . . ?
B13 B14 B20 B22 2.5(4) . . . . ?
C29 B14 B20 B19 -97.7(3) . . . . ?
B15 B14 B20 B19 -139.0(3) . . . . ?
B13 B14 B20 B19 -36.5(3) . . . . ?
C29 B14 B20 B15 41.3(3) . . . . ?
B19 B14 B20 B15 139.0(3) . . . . ?
B13 B14 B20 B15 102.5(3) . . . . ?
C29 B16 B21 B22 61.4(4) . . . . ?
C30 B16 B21 B22 1.9(5) . . . . ?
B15 B16 B21 B22 101.9(4) . . . . ?
B17 B16 B21 B22 -36.6(3) . . . . ?
C29 B16 B21 B20 -2.2(4) . . . . ?
C30 B16 B21 B20 -61.8(4) . . . . ?
B15 B16 B21 B20 38.3(3) . . . . ?
B17 B16 B21 B20 -100.2(4) . . . . ?
C29 B16 B21 B15 -40.5(3) . . . . ?
C30 B16 B21 B15 -100.0(3) . . . . ?
B17 B16 B21 B15 -138.5(4) . . . . ?
C29 B16 B21 B17 98.0(3) . . . . ?
C30 B16 B21 B17 38.4(3) . . . . ?
B15 B16 B21 B17 138.5(4) . . . . ?
B22 B20 B21 B16 100.6(4) . . . . ?
B19 B20 B21 B16 61.9(4) . . . . ?
B15 B20 B21 B16 -38.0(3) . . . . ?
B14 B20 B21 B16 -1.4(5) . . . . ?
B19 B20 B21 B22 -38.7(3) . . . . ?
B15 B20 B21 B22 -138.6(3) . . . . ?
B14 B20 B21 B22 -102.0(4) . . . . ?
B22 B20 B21 B15 138.6(3) . . . . ?
B19 B20 B21 B15 99.9(4) . . . . ?
B14 B20 B21 B15 36.6(3) . . . . ?
B22 B20 B21 B17 37.6(3) . . . . ?
B19 B20 B21 B17 -1.1(5) . . . . ?
B15 B20 B21 B17 -101.0(4) . . . . ?
B14 B20 B21 B17 -64.4(4) . . . . ?
C29 B15 B21 B16 39.5(3) . . . . ?
B14 B15 B21 B16 100.3(3) . . . . ?
B20 B15 B21 B16 137.4(4) . . . . ?
C29 B15 B21 B22 -60.6(4) . . . . ?
B16 B15 B21 B22 -100.1(4) . . . . ?
B14 B15 B21 B22 0.2(4) . . . . ?
B20 B15 B21 B22 37.3(3) . . . . ?
C29 B15 B21 B20 -97.9(3) . . . . ?
B16 B15 B21 B20 -137.4(4) . . . . ?
B14 B15 B21 B20 -37.1(3) . . . . ?
C29 B15 B21 B17 2.6(4) . . . . ?
B16 B15 B21 B17 -37.0(3) . . . . ?
B14 B15 B21 B17 63.3(4) . . . . ?
B20 B15 B21 B17 100.5(4) . . . . ?
C30 B17 B21 B16 -39.5(3) . . . . ?
B22 B17 B21 B16 -138.9(4) . . . . ?
B18 B17 B21 B16 -100.9(4) . . . . ?
C30 B17 B21 B22 99.3(4) . . . . ?
B16 B17 B21 B22 138.9(4) . . . . ?
B18 B17 B21 B22 37.9(3) . . . . ?
C30 B17 B21 B20 61.5(4) . . . . ?
B22 B17 B21 B20 -37.9(3) . . . . ?
B16 B17 B21 B20 101.0(4) . . . . ?
B18 B17 B21 B20 0.0(4) . . . . ?
C30 B17 B21 B15 -2.4(4) . . . . ?
B22 B17 B21 B15 -101.8(4) . . . . ?
B16 B17 B21 B15 37.1(3) . . . . ?
B18 B17 B21 B15 -63.8(4) . . . . ?
B16 B21 B22 B20 -101.0(4) . . . . ?
B15 B21 B22 B20 -37.4(3) . . . . ?
B17 B21 B22 B20 -137.6(4) . . . . ?
B16 B21 B22 B17 36.6(3) . . . . ?
B20 B21 B22 B17 137.6(4) . . . . ?
B15 B21 B22 B17 100.2(4) . . . . ?
B16 B21 B22 B18 -1.6(5) . . . . ?
B20 B21 B22 B18 99.4(4) . . . . ?
B15 B21 B22 B18 61.9(4) . . . . ?
B17 B21 B22 B18 -38.2(3) . . . . ?
B16 B21 B22 B19 -64.0(4) . . . . ?
B20 B21 B22 B19 37.0(3) . . . . ?
B15 B21 B22 B19 -0.4(4) . . . . ?
B17 B21 B22 B19 -100.6(4) . . . . ?
B19 B20 B22 B21 137.9(4) . . . . ?
B15 B20 B22 B21 36.9(3) . . . . ?
B14 B20 B22 B21 99.9(4) . . . . ?
B21 B20 B22 B17 -38.9(4) . . . . ?
B19 B20 B22 B17 99.1(4) . . . . ?
B15 B20 B22 B17 -1.9(5) . . . . ?
B14 B20 B22 B17 61.1(5) . . . . ?
B21 B20 B22 B18 -102.3(4) . . . . ?
B19 B20 B22 B18 35.6(3) . . . . ?
B15 B20 B22 B18 -65.4(4) . . . . ?
B14 B20 B22 B18 -2.4(5) . . . . ?
B21 B20 B22 B19 -137.9(4) . . . . ?
B15 B20 B22 B19 -101.0(4) . . . . ?
B14 B20 B22 B19 -38.0(3) . . . . ?
C30 B17 B22 B21 -99.0(4) . . . . ?
B16 B17 B22 B21 -35.8(3) . . . . ?
B18 B17 B22 B21 -137.5(4) . . . . ?
C30 B17 B22 B20 -60.8(5) . . . . ?
B16 B17 B22 B20 2.3(5) . . . . ?
B18 B17 B22 B20 -99.3(4) . . . . ?
B21 B17 B22 B20 38.2(4) . . . . ?
C30 B17 B22 B18 38.5(3) . . . . ?
B16 B17 B22 B18 101.7(4) . . . . ?
B21 B17 B22 B18 137.5(4) . . . . ?
C30 B17 B22 B19 1.7(4) . . . . ?
B16 B17 B22 B19 64.8(4) . . . . ?
B18 B17 B22 B19 -36.8(3) . . . . ?
B21 B17 B22 B19 100.7(4) . . . . ?
C30 B18 B22 B21 0.7(5) . . . . ?
B19 B18 B22 B21 -99.2(4) . . . . ?
B17 B18 B22 B21 38.9(3) . . . . ?
B13 B18 B22 B21 -62.1(4) . . . . ?
C30 B18 B22 B20 64.1(4) . . . . ?
B19 B18 B22 B20 -35.7(3) . . . . ?
B17 B18 B22 B20 102.4(4) . . . . ?
B13 B18 B22 B20 1.4(5) . . . . ?
C30 B18 B22 B17 -38.3(3) . . . . ?
B19 B18 B22 B17 -138.1(3) . . . . ?
B13 B18 B22 B17 -101.0(4) . . . . ?
C30 B18 B22 B19 99.8(3) . . . . ?
B17 B18 B22 B19 138.1(3) . . . . ?
B13 B18 B22 B19 37.1(3) . . . . ?
B13 B19 B22 B21 64.7(4) . . . . ?
B20 B19 B22 B21 -37.4(3) . . . . ?
B14 B19 B22 B21 0.5(4) . . . . ?
B18 B19 B22 B21 102.1(3) . . . . ?
B13 B19 B22 B20 102.1(4) . . . . ?
B14 B19 B22 B20 37.9(3) . . . . ?
B18 B19 B22 B20 139.5(3) . . . . ?
B13 B19 B22 B17 -0.1(5) . . . . ?
B20 B19 B22 B17 -102.3(4) . . . . ?
B14 B19 B22 B17 -64.3(4) . . . . ?
B18 B19 B22 B17 37.3(3) . . . . ?
B13 B19 B22 B18 -37.4(3) . . . . ?
B20 B19 B22 B18 -139.5(3) . . . . ?
B14 B19 B22 B18 -101.6(3) . . . . ?
B5 B4 C1 C2 -105.4(3) . . . . ?
B3 B4 C1 C2 37.2(3) . . . . ?
B9 B4 C1 C2 -1.8(4) . . . . ?
B10 B4 C1 C2 -64.8(4) . . . . ?
B5 B4 C1 B6 -36.0(3) . . . . ?
B3 B4 C1 B6 106.7(3) . . . . ?
B9 B4 C1 B6 67.6(4) . . . . ?
B10 B4 C1 B6 4.6(4) . . . . ?
B3 B4 C1 B5 142.6(3) . . . . ?
B9 B4 C1 B5 103.6(3) . . . . ?
B10 B4 C1 B5 40.6(3) . . . . ?
B5 B4 C1 B3 -142.6(3) . . . . ?
B9 B4 C1 B3 -39.1(3) . . . . ?
B10 B4 C1 B3 -102.1(3) . . . . ?
B5 B4 C1 S1 109.4(3) . . . . ?
B3 B4 C1 S1 -107.9(3) . . . . ?
B9 B4 C1 S1 -147.0(3) . . . . ?
B10 B4 C1 S1 150.0(3) . . . . ?
B5 B6 C1 C2 140.5(3) . . . . ?
B11 B6 C1 C2 99.8(3) . . . . ?
B7 B6 C1 C2 37.5(3) . . . . ?
C2 B6 C1 B4 -104.3(3) . . . . ?
B5 B6 C1 B4 36.2(3) . . . . ?
B11 B6 C1 B4 -4.5(4) . . . . ?
B7 B6 C1 B4 -66.8(4) . . . . ?
C2 B6 C1 B5 -140.5(3) . . . . ?
B11 B6 C1 B5 -40.6(3) . . . . ?
B7 B6 C1 B5 -103.0(3) . . . . ?
C2 B6 C1 B3 -33.6(3) . . . . ?
B5 B6 C1 B3 106.8(3) . . . . ?
B11 B6 C1 B3 66.2(4) . . . . ?
B7 B6 C1 B3 3.8(4) . . . . ?
C2 B6 C1 S1 105.4(3) . . . . ?
B5 B6 C1 S1 -114.1(3) . . . . ?
B11 B6 C1 S1 -154.7(3) . . . . ?
B7 B6 C1 S1 142.9(2) . . . . ?
B6 B5 C1 C2 -38.0(3) . . . . ?
B4 B5 C1 C2 105.1(3) . . . . ?
B11 B5 C1 C2 2.5(4) . . . . ?
B10 B5 C1 C2 63.9(4) . . . . ?
B6 B5 C1 B4 -143.1(3) . . . . ?
B11 B5 C1 B4 -102.6(4) . . . . ?
B10 B5 C1 B4 -41.2(3) . . . . ?
B4 B5 C1 B6 143.1(3) . . . . ?
B11 B5 C1 B6 40.5(3) . . . . ?
B10 B5 C1 B6 101.9(3) . . . . ?
B6 B5 C1 B3 -106.3(4) . . . . ?
B4 B5 C1 B3 36.8(3) . . . . ?
B11 B5 C1 B3 -65.8(4) . . . . ?
B10 B5 C1 B3 -4.4(4) . . . . ?
B6 B5 C1 S1 99.7(3) . . . . ?
B4 B5 C1 S1 -117.2(3) . . . . ?
B11 B5 C1 S1 140.2(3) . . . . ?
B10 B5 C1 S1 -158.4(3) . . . . ?
B9 B3 C1 C2 -100.6(3) . . . . ?
B4 B3 C1 C2 -140.7(3) . . . . ?
B8 B3 C1 C2 -37.3(3) . . . . ?
C2 B3 C1 B4 140.7(3) . . . . ?
B9 B3 C1 B4 40.1(3) . . . . ?
B8 B3 C1 B4 103.4(3) . . . . ?
C2 B3 C1 B6 34.1(3) . . . . ?
B9 B3 C1 B6 -66.6(4) . . . . ?
B4 B3 C1 B6 -106.7(3) . . . . ?
B8 B3 C1 B6 -3.2(4) . . . . ?
C2 B3 C1 B5 104.0(3) . . . . ?
B9 B3 C1 B5 3.3(4) . . . . ?
B4 B3 C1 B5 -36.8(3) . . . . ?
B8 B3 C1 B5 66.7(4) . . . . ?
C2 B3 C1 S1 -101.7(3) . . . . ?
B9 B3 C1 S1 157.7(3) . . . . ?
B4 B3 C1 S1 117.6(3) . . . . ?
B8 B3 C1 S1 -139.0(3) . . . . ?
B4 C1 C2 B8 2.9(4) . . . . ?
B6 C1 C2 B8 -104.4(3) . . . . ?
B5 C1 C2 B8 -66.5(4) . . . . ?
B3 C1 C2 B8 40.8(3) . . . . ?
S1 C1 C2 B8 152.6(3) . . . . ?
B4 C1 C2 B7 67.7(4) . . . . ?
B6 C1 C2 B7 -39.6(3) . . . . ?
B5 C1 C2 B7 -1.7(4) . . . . ?
B3 C1 C2 B7 105.6(3) . . . . ?
S1 C1 C2 B7 -142.6(3) . . . . ?
B4 C1 C2 B3 -37.9(3) . . . . ?
B6 C1 C2 B3 -145.2(3) . . . . ?
B5 C1 C2 B3 -107.3(3) . . . . ?
S1 C1 C2 B3 111.8(3) . . . . ?
B4 C1 C2 S2 -146.4(3) . . . . ?
B6 C1 C2 S2 106.3(3) . . . . ?
B5 C1 C2 S2 144.2(3) . . . . ?
B3 C1 C2 S2 -108.5(3) . . . . ?
S1 C1 C2 S2 3.3(4) . . . . ?
B4 C1 C2 B6 107.3(3) . . . . ?
B5 C1 C2 B6 37.9(3) . . . . ?
B3 C1 C2 B6 145.2(3) . . . . ?
S1 C1 C2 B6 -103.0(3) . . . . ?
B7 B8 C2 C1 99.8(3) . . . . ?
B12 B8 C2 C1 61.7(4) . . . . ?
B3 B8 C2 C1 -39.6(3) . . . . ?
B9 B8 C2 C1 -2.6(4) . . . . ?
B12 B8 C2 B7 -38.1(3) . . . . ?
B3 B8 C2 B7 -139.3(3) . . . . ?
B9 B8 C2 B7 -102.4(4) . . . . ?
B7 B8 C2 B3 139.3(3) . . . . ?
B12 B8 C2 B3 101.3(4) . . . . ?
B9 B8 C2 B3 36.9(3) . . . . ?
B7 B8 C2 S2 -112.2(3) . . . . ?
B12 B8 C2 S2 -150.3(3) . . . . ?
B3 B8 C2 S2 108.4(3) . . . . ?
B9 B8 C2 S2 145.4(3) . . . . ?
B7 B8 C2 B6 36.4(3) . . . . ?
B12 B8 C2 B6 -1.6(4) . . . . ?
B3 B8 C2 B6 -102.9(3) . . . . ?
B9 B8 C2 B6 -66.0(4) . . . . ?
B12 B7 C2 C1 -63.6(4) . . . . ?
B8 B7 C2 C1 -102.4(3) . . . . ?
B6 B7 C2 C1 38.6(3) . . . . ?
B11 B7 C2 C1 0.1(4) . . . . ?
B12 B7 C2 B8 38.8(3) . . . . ?
B6 B7 C2 B8 141.0(3) . . . . ?
B11 B7 C2 B8 102.5(4) . . . . ?
B12 B7 C2 B3 0.3(4) . . . . ?
B8 B7 C2 B3 -38.5(3) . . . . ?
B6 B7 C2 B3 102.4(3) . . . . ?
B11 B7 C2 B3 63.9(4) . . . . ?
B12 B7 C2 S2 151.8(3) . . . . ?
B8 B7 C2 S2 113.0(3) . . . . ?
B6 B7 C2 S2 -106.0(3) . . . . ?
B11 B7 C2 S2 -144.5(3) . . . . ?
B12 B7 C2 B6 -102.2(4) . . . . ?
B8 B7 C2 B6 -141.0(3) . . . . ?
B11 B7 C2 B6 -38.5(3) . . . . ?
B9 B3 C2 C1 97.5(3) . . . . ?
B4 B3 C2 C1 34.0(3) . . . . ?
B8 B3 C2 C1 135.8(3) . . . . ?
C1 B3 C2 B8 -135.8(3) . . . . ?
B9 B3 C2 B8 -38.3(3) . . . . ?
B4 B3 C2 B8 -101.9(3) . . . . ?
C1 B3 C2 B7 -97.9(3) . . . . ?
B9 B3 C2 B7 -0.4(4) . . . . ?
B4 B3 C2 B7 -63.9(4) . . . . ?
B8 B3 C2 B7 38.0(3) . . . . ?
C1 B3 C2 S2 109.4(3) . . . . ?
B9 B3 C2 S2 -153.1(3) . . . . ?
B4 B3 C2 S2 143.3(3) . . . . ?
B8 B3 C2 S2 -114.8(3) . . . . ?
C1 B3 C2 B6 -31.6(3) . . . . ?
B9 B3 C2 B6 65.9(4) . . . . ?
B4 B3 C2 B6 2.4(4) . . . . ?
B8 B3 C2 B6 104.3(3) . . . . ?
B5 B6 C2 C1 -34.6(3) . . . . ?
B11 B6 C2 C1 -97.8(3) . . . . ?
B7 B6 C2 C1 -136.1(3) . . . . ?
C1 B6 C2 B8 99.7(3) . . . . ?
B5 B6 C2 B8 65.0(4) . . . . ?
B11 B6 C2 B8 1.9(4) . . . . ?
B7 B6 C2 B8 -36.4(3) . . . . ?
C1 B6 C2 B7 136.1(3) . . . . ?
B5 B6 C2 B7 101.4(3) . . . . ?
B11 B6 C2 B7 38.3(3) . . . . ?
C1 B6 C2 B3 31.9(3) . . . . ?
B5 B6 C2 B3 -2.7(4) . . . . ?
B11 B6 C2 B3 -65.9(4) . . . . ?
B7 B6 C2 B3 -104.2(3) . . . . ?
C1 B6 C2 S2 -109.7(3) . . . . ?
B5 B6 C2 S2 -144.4(3) . . . . ?
B11 B6 C2 S2 152.5(3) . . . . ?
B7 B6 C2 S2 114.2(3) . . . . ?
C7 C3 C4 C5 177.4(4) . . . . ?
Co1 C3 C4 C5 -0.2(6) . . . . ?
C3 C4 C5 C6 14.5(7) . . . . ?
C4 C5 C6 C13 -179.8(4) . . . . ?
C4 C5 C6 S1 -5.4(6) . . . . ?
C4 C3 C7 C12 -47.6(5) . . . . ?
Co1 C3 C7 C12 130.2(3) . . . . ?
C4 C3 C7 C8 132.2(4) . . . . ?
Co1 C3 C7 C8 -50.1(5) . . . . ?
C12 C7 C8 C9 -1.4(5) . . . . ?
C3 C7 C8 C9 178.8(3) . . . . ?
C7 C8 C9 C10 1.0(6) . . . . ?
C8 C9 C10 C11 -1.6(6) . . . . ?
C9 C10 C11 C12 2.7(7) . . . . ?
C10 C11 C12 C7 -3.3(6) . . . . ?
C8 C7 C12 C11 2.6(6) . . . . ?
C3 C7 C12 C11 -177.7(4) . . . . ?
C5 C6 C13 C18 -36.2(6) . . . . ?
S1 C6 C13 C18 149.3(3) . . . . ?
C5 C6 C13 C14 142.7(4) . . . . ?
S1 C6 C13 C14 -31.8(5) . . . . ?
C18 C13 C14 C15 1.5(6) . . . . ?
C6 C13 C14 C15 -177.4(4) . . . . ?
C13 C14 C15 C16 -1.7(6) . . . . ?
C14 C15 C16 C17 1.9(7) . . . . ?
C15 C16 C17 C18 -1.8(7) . . . . ?
C16 C17 C18 C13 1.6(6) . . . . ?
C14 C13 C18 C17 -1.5(6) . . . . ?
C6 C13 C18 C17 177.5(4) . . . . ?
C23 C19 C20 C21 2.3(4) . . . . ?
C24 C19 C20 C21 -168.1(4) . . . . ?
Co1 C19 C20 C21 64.0(3) . . . . ?
C23 C19 C20 C25 173.0(4) . . . . ?
C24 C19 C20 C25 2.6(7) . . . . ?
Co1 C19 C20 C25 -125.3(4) . . . . ?
C23 C19 C20 Co1 -61.6(3) . . . . ?
C24 C19 C20 Co1 127.9(4) . . . . ?
C19 C20 C21 C22 -1.3(4) . . . . ?
C25 C20 C21 C22 -172.6(4) . . . . ?
Co1 C20 C21 C22 60.5(3) . . . . ?
C19 C20 C21 C26 173.6(4) . . . . ?
C25 C20 C21 C26 2.2(6) . . . . ?
Co1 C20 C21 C26 -124.7(4) . . . . ?
C19 C20 C21 Co1 -61.8(3) . . . . ?
C25 C20 C21 Co1 126.9(4) . . . . ?
C20 C21 C22 C23 -0.3(4) . . . . ?
C26 C21 C22 C23 -174.9(4) . . . . ?
Co1 C21 C22 C23 57.3(3) . . . . ?
C20 C21 C22 C27 173.8(4) . . . . ?
C26 C21 C22 C27 -0.9(7) . . . . ?
Co1 C21 C22 C27 -128.6(4) . . . . ?
C20 C21 C22 Co1 -57.6(3) . . . . ?
C26 C21 C22 Co1 127.7(4) . . . . ?
C20 C19 C23 C22 -2.5(4) . . . . ?
C24 C19 C23 C22 168.3(4) . . . . ?
Co1 C19 C23 C22 -63.7(3) . . . . ?
C20 C19 C23 C28 -178.8(4) . . . . ?
C24 C19 C23 C28 -8.0(6) . . . . ?
Co1 C19 C23 C28 120.1(4) . . . . ?
C20 C19 C23 Co1 61.1(3) . . . . ?
C24 C19 C23 Co1 -128.1(4) . . . . ?
C21 C22 C23 C19 1.7(4) . . . . ?
C27 C22 C23 C19 -172.3(4) . . . . ?
Co1 C22 C23 C19 61.2(3) . . . . ?
C21 C22 C23 C28 178.0(4) . . . . ?
C27 C22 C23 C28 3.9(6) . . . . ?
Co1 C22 C23 C28 -122.6(4) . . . . ?
C21 C22 C23 Co1 -59.4(3) . . . . ?
C27 C22 C23 Co1 126.5(4) . . . . ?
B15 B14 C29 C30 104.1(3) . . . . ?
B19 B14 C29 C30 0.7(5) . . . . ?
B20 B14 C29 C30 62.6(4) . . . . ?
B13 B14 C29 C30 -39.3(3) . . . . ?
B15 B14 C29 B13 143.3(3) . . . . ?
B19 B14 C29 B13 40.0(3) . . . . ?
B20 B14 C29 B13 101.9(3) . . . . ?
B15 B14 C29 B16 35.2(3) . . . . ?
B19 B14 C29 B16 -68.1(4) . . . . ?
B20 B14 C29 B16 -6.2(4) . . . . ?
B13 B14 C29 B16 -108.1(4) . . . . ?
B19 B14 C29 B15 -103.3(4) . . . . ?
B20 B14 C29 B15 -41.5(3) . . . . ?
B13 B14 C29 B15 -143.3(3) . . . . ?
B15 B14 C29 S3 -109.8(3) . . . . ?
B19 B14 C29 S3 146.9(3) . . . . ?
B20 B14 C29 S3 -151.2(3) . . . . ?
B13 B14 C29 S3 106.9(3) . . . . ?
B19 B13 C29 C30 98.6(3) . . . . ?
B18 B13 C29 C30 36.6(3) . . . . ?
B14 B13 C29 C30 138.8(3) . . . . ?
C30 B13 C29 B14 -138.8(3) . . . . ?
B19 B13 C29 B14 -40.2(3) . . . . ?
B18 B13 C29 B14 -102.2(3) . . . . ?
C30 B13 C29 B16 -34.5(3) . . . . ?
B19 B13 C29 B16 64.1(4) . . . . ?
B18 B13 C29 B16 2.1(4) . . . . ?
B14 B13 C29 B16 104.3(4) . . . . ?
C30 B13 C29 B15 -103.4(3) . . . . ?
B19 B13 C29 B15 -4.7(4) . . . . ?
B18 B13 C29 B15 -66.8(4) . . . . ?
B14 B13 C29 B15 35.4(3) . . . . ?
C30 B13 C29 S3 102.9(3) . . . . ?
B19 B13 C29 S3 -158.5(3) . . . . ?
B18 B13 C29 S3 139.5(3) . . . . ?
B14 B13 C29 S3 -118.3(3) . . . . ?
B21 B16 C29 C30 -99.2(3) . . . . ?
B15 B16 C29 C30 -139.9(3) . . . . ?
B17 B16 C29 C30 -35.1(3) . . . . ?
C30 B16 C29 B14 104.6(3) . . . . ?
B21 B16 C29 B14 5.4(4) . . . . ?
B15 B16 C29 B14 -35.4(3) . . . . ?
B17 B16 C29 B14 69.5(4) . . . . ?
C30 B16 C29 B13 34.4(3) . . . . ?
B21 B16 C29 B13 -64.7(4) . . . . ?
B15 B16 C29 B13 -105.5(3) . . . . ?
B17 B16 C29 B13 -0.7(4) . . . . ?
C30 B16 C29 B15 139.9(3) . . . . ?
B21 B16 C29 B15 40.8(3) . . . . ?
B17 B16 C29 B15 104.8(3) . . . . ?
C30 B16 C29 S3 -105.5(3) . . . . ?
B21 B16 C29 S3 155.3(3) . . . . ?
B15 B16 C29 S3 114.5(3) . . . . ?
B17 B16 C29 S3 -140.7(3) . . . . ?
B16 B15 C29 C30 38.2(3) . . . . ?
B14 B15 C29 C30 -104.7(3) . . . . ?
B21 B15 C29 C30 -1.8(4) . . . . ?
B20 B15 C29 C30 -63.5(4) . . . . ?
B16 B15 C29 B14 142.9(3) . . . . ?
B21 B15 C29 B14 102.9(4) . . . . ?
B20 B15 C29 B14 41.3(3) . . . . ?
B16 B15 C29 B13 107.0(4) . . . . ?
B14 B15 C29 B13 -35.9(3) . . . . ?
B21 B15 C29 B13 67.0(4) . . . . ?
B20 B15 C29 B13 5.4(4) . . . . ?
B14 B15 C29 B16 -142.9(3) . . . . ?
B21 B15 C29 B16 -40.0(3) . . . . ?
B20 B15 C29 B16 -101.7(4) . . . . ?
B16 B15 C29 S3 -100.1(3) . . . . ?
B14 B15 C29 S3 117.0(3) . . . . ?
B21 B15 C29 S3 -140.1(3) . . . . ?
B20 B15 C29 S3 158.3(3) . . . . ?
B14 C29 C30 B17 -67.3(4) . . . . ?
B13 C29 C30 B17 -106.9(3) . . . . ?
B16 C29 C30 B17 38.0(3) . . . . ?
B15 C29 C30 B17 0.3(4) . . . . ?
S3 C29 C30 B17 142.0(3) . . . . ?
B14 C29 C30 B18 -0.2(4) . . . . ?
B13 C29 C30 B18 -39.8(3) . . . . ?
B16 C29 C30 B18 105.1(3) . . . . ?
B15 C29 C30 B18 67.4(4) . . . . ?
S3 C29 C30 B18 -150.8(3) . . . . ?
B14 C29 C30 B13 39.6(3) . . . . ?
B16 C29 C30 B13 144.9(3) . . . . ?
B15 C29 C30 B13 107.2(3) . . . . ?
S3 C29 C30 B13 -111.1(3) . . . . ?
B14 C29 C30 B16 -105.3(4) . . . . ?
B13 C29 C30 B16 -144.9(3) . . . . ?
B15 C29 C30 B16 -37.7(3) . . . . ?
S3 C29 C30 B16 104.0(3) . . . . ?
B14 C29 C30 S4 147.4(3) . . . . ?
B13 C29 C30 S4 107.8(3) . . . . ?
B16 C29 C30 S4 -107.3(3) . . . . ?
B15 C29 C30 S4 -145.0(3) . . . . ?
S3 C29 C30 S4 -3.3(4) . . . . ?
B22 B17 C30 C29 62.7(4) . . . . ?
B16 B17 C30 C29 -37.4(3) . . . . ?
B18 B17 C30 C29 102.0(3) . . . . ?
B21 B17 C30 C29 1.3(4) . . . . ?
B22 B17 C30 B18 -39.4(3) . . . . ?
B16 B17 C30 B18 -139.4(3) . . . . ?
B21 B17 C30 B18 -100.7(4) . . . . ?
B22 B17 C30 B13 -2.8(4) . . . . ?
B16 B17 C30 B13 -102.8(3) . . . . ?
B18 B17 C30 B13 36.6(3) . . . . ?
B21 B17 C30 B13 -64.1(4) . . . . ?
B22 B17 C30 B16 100.0(4) . . . . ?
B18 B17 C30 B16 139.4(3) . . . . ?
B21 B17 C30 B16 38.7(3) . . . . ?
B22 B17 C30 S4 -153.2(3) . . . . ?
B16 B17 C30 S4 106.8(3) . . . . ?
B18 B17 C30 S4 -113.8(3) . . . . ?
B21 B17 C30 S4 145.5(3) . . . . ?
B19 B18 C30 C29 -0.4(4) . . . . ?
B17 B18 C30 C29 -103.0(3) . . . . ?
B13 B18 C30 C29 39.0(3) . . . . ?
B22 B18 C30 C29 -64.3(4) . . . . ?
B19 B18 C30 B17 102.6(4) . . . . ?
B13 B18 C30 B17 142.0(3) . . . . ?
B22 B18 C30 B17 38.8(3) . . . . ?
B19 B18 C30 B13 -39.4(3) . . . . ?
B17 B18 C30 B13 -142.0(3) . . . . ?
B22 B18 C30 B13 -103.2(3) . . . . ?
B19 B18 C30 B16 64.4(4) . . . . ?
B17 B18 C30 B16 -38.2(3) . . . . ?
B13 B18 C30 B16 103.8(3) . . . . ?
B22 B18 C30 B16 0.6(4) . . . . ?
B19 B18 C30 S4 -146.3(3) . . . . ?
B17 B18 C30 S4 111.1(3) . . . . ?
B13 B18 C30 S4 -106.9(3) . . . . ?
B22 B18 C30 S4 149.9(3) . . . . ?
B19 B13 C30 C29 -97.4(3) . . . . ?
B18 B13 C30 C29 -136.9(3) . . . . ?
B14 B13 C30 C29 -35.4(3) . . . . ?
C29 B13 C30 B17 100.1(3) . . . . ?
B19 B13 C30 B17 2.7(4) . . . . ?
B18 B13 C30 B17 -36.8(3) . . . . ?
B14 B13 C30 B17 64.7(4) . . . . ?
C29 B13 C30 B18 136.9(3) . . . . ?
B19 B13 C30 B18 39.5(3) . . . . ?
B14 B13 C30 B18 101.5(3) . . . . ?
C29 B13 C30 B16 32.5(3) . . . . ?
B19 B13 C30 B16 -64.9(4) . . . . ?
B18 B13 C30 B16 -104.4(3) . . . . ?
B14 B13 C30 B16 -2.9(4) . . . . ?
C29 B13 C30 S4 -108.5(3) . . . . ?
B19 B13 C30 S4 154.1(3) . . . . ?
B18 B13 C30 S4 114.6(3) . . . . ?
B14 B13 C30 S4 -143.9(3) . . . . ?
B21 B16 C30 C29 98.6(4) . . . . ?
B15 B16 C30 C29 35.5(3) . . . . ?
B17 B16 C30 C29 138.9(3) . . . . ?
C29 B16 C30 B17 -138.9(3) . . . . ?
B21 B16 C30 B17 -40.2(3) . . . . ?
B15 B16 C30 B17 -103.4(3) . . . . ?
C29 B16 C30 B18 -100.2(3) . . . . ?
B21 B16 C30 B18 -1.5(4) . . . . ?
B15 B16 C30 B18 -64.7(4) . . . . ?
B17 B16 C30 B18 38.7(3) . . . . ?
C29 B16 C30 B13 -32.6(3) . . . . ?
B21 B16 C30 B13 66.1(4) . . . . ?
B15 B16 C30 B13 2.9(4) . . . . ?
B17 B16 C30 B13 106.3(3) . . . . ?
C29 B16 C30 S4 108.7(3) . . . . ?
B21 B16 C30 S4 -152.7(3) . . . . ?
B15 B16 C30 S4 144.1(3) . . . . ?
B17 B16 C30 S4 -112.5(3) . . . . ?
C35 C31 C32 C33 -176.2(4) . . . . ?
Co2 C31 C32 C33 -2.7(6) . . . . ?
C31 C32 C33 C34 -16.1(8) . . . . ?
C32 C33 C34 C41 -174.8(4) . . . . ?
C32 C33 C34 S3 4.4(7) . . . . ?
C32 C31 C35 C40 45.5(5) . . . . ?
Co2 C31 C35 C40 -128.3(3) . . . . ?
C32 C31 C35 C36 -133.4(4) . . . . ?
Co2 C31 C35 C36 52.8(5) . . . . ?
C40 C35 C36 C37 2.8(6) . . . . ?
C31 C35 C36 C37 -178.3(4) . . . . ?
C35 C36 C37 C38 -0.5(7) . . . . ?
C36 C37 C38 C39 -1.2(7) . . . . ?
C37 C38 C39 C40 0.6(7) . . . . ?
C36 C35 C40 C39 -3.5(6) . . . . ?
C31 C35 C40 C39 177.6(4) . . . . ?
C38 C39 C40 C35 1.9(6) . . . . ?
C33 C34 C41 C46 -152.6(4) . . . . ?
S3 C34 C41 C46 28.2(5) . . . . ?
C33 C34 C41 C42 29.1(6) . . . . ?
S3 C34 C41 C42 -150.2(3) . . . . ?
C46 C41 C42 C43 -2.2(6) . . . . ?
C34 C41 C42 C43 176.2(4) . . . . ?
C41 C42 C43 C44 -1.1(6) . . . . ?
C42 C43 C44 C45 4.5(6) . . . . ?
C43 C44 C45 C46 -4.5(6) . . . . ?
C42 C41 C46 C45 2.2(6) . . . . ?
C34 C41 C46 C45 -176.2(4) . . . . ?
C44 C45 C46 C41 1.0(6) . . . . ?
C51 C47 C48 C49 -0.1(4) . . . . ?
C52 C47 C48 C49 -174.5(4) . . . . ?
Co2 C47 C48 C49 57.8(3) . . . . ?
C51 C47 C48 C53 176.8(4) . . . . ?
C52 C47 C48 C53 2.5(7) . . . . ?
Co2 C47 C48 C53 -125.2(4) . . . . ?
C51 C47 C48 Co2 -57.9(3) . . . . ?
C52 C47 C48 Co2 127.7(4) . . . . ?
C47 C48 C49 C50 2.0(4) . . . . ?
C53 C48 C49 C50 -174.9(4) . . . . ?
Co2 C48 C49 C50 61.8(3) . . . . ?
C47 C48 C49 C54 169.1(4) . . . . ?
C53 C48 C49 C54 -7.8(7) . . . . ?
Co2 C48 C49 C54 -131.1(4) . . . . ?
C47 C48 C49 Co2 -59.8(3) . . . . ?
C53 C48 C49 Co2 123.2(4) . . . . ?
C48 C49 C50 C51 -3.1(4) . . . . ?
C54 C49 C50 C51 -170.7(4) . . . . ?
Co2 C49 C50 C51 60.8(3) . . . . ?
C48 C49 C50 C55 169.1(4) . . . . ?
C54 C49 C50 C55 1.5(6) . . . . ?
Co2 C49 C50 C55 -127.0(4) . . . . ?
C48 C49 C50 Co2 -63.8(3) . . . . ?
C54 C49 C50 Co2 128.6(4) . . . . ?
C49 C50 C51 C47 3.0(4) . . . . ?
C55 C50 C51 C47 -169.6(4) . . . . ?
Co2 C50 C51 C47 63.8(3) . . . . ?
C49 C50 C51 C56 175.8(4) . . . . ?
C55 C50 C51 C56 3.2(6) . . . . ?
Co2 C50 C51 C56 -123.5(4) . . . . ?
C49 C50 C51 Co2 -60.7(3) . . . . ?
C55 C50 C51 Co2 126.7(4) . . . . ?
C48 C47 C51 C50 -1.8(4) . . . . ?
C52 C47 C51 C50 172.5(4) . . . . ?
Co2 C47 C51 C50 -61.7(3) . . . . ?
C48 C47 C51 C56 -174.6(4) . . . . ?
C52 C47 C51 C56 -0.4(7) . . . . ?
Co2 C47 C51 C56 125.5(4) . . . . ?
C48 C47 C51 Co2 59.9(3) . . . . ?
C52 C47 C51 Co2 -125.9(4) . . . . ?
C4 C3 Co1 C20 153.9(3) . . . . ?
C7 C3 Co1 C20 -23.6(3) . . . . ?
C4 C3 Co1 C19 118.2(3) . . . . ?
C7 C3 Co1 C19 -59.2(3) . . . . ?
C4 C3 Co1 C23 83.4(3) . . . . ?
C7 C3 Co1 C23 -94.1(3) . . . . ?
C4 C3 Co1 C21 158.1(3) . . . . ?
C7 C3 Co1 C21 -19.4(4) . . . . ?
C4 C3 Co1 C22 80.2(4) . . . . ?
C7 C3 Co1 C22 -97.3(4) . . . . ?
C4 C3 Co1 S1 -13.6(3) . . . . ?
C7 C3 Co1 S1 168.9(3) . . . . ?
C4 C3 Co1 S2 -107.6(3) . . . . ?
C7 C3 Co1 S2 74.9(3) . . . . ?
C19 C20 Co1 C3 -65.6(2) . . . . ?
C21 C20 Co1 C3 176.6(2) . . . . ?
C25 C20 Co1 C3 57.8(4) . . . . ?
C21 C20 Co1 C19 -117.8(3) . . . . ?
C25 C20 Co1 C19 123.5(4) . . . . ?
C19 C20 Co1 C23 38.6(2) . . . . ?
C21 C20 Co1 C23 -79.2(2) . . . . ?
C25 C20 Co1 C23 162.1(4) . . . . ?
C19 C20 Co1 C21 117.8(3) . . . . ?
C25 C20 Co1 C21 -118.7(4) . . . . ?
C19 C20 Co1 C22 81.4(2) . . . . ?
C21 C20 Co1 C22 -36.4(2) . . . . ?
C25 C20 Co1 C22 -155.1(4) . . . . ?
C19 C20 Co1 S1 87.7(3) . . . . ?
C21 C20 Co1 S1 -30.1(4) . . . . ?
C25 C20 Co1 S1 -148.8(3) . . . . ?
C19 C20 Co1 S2 -158.2(2) . . . . ?
C21 C20 Co1 S2 84.1(2) . . . . ?
C25 C20 Co1 S2 -34.7(4) . . . . ?
C23 C19 Co1 C3 -122.6(2) . . . . ?
C20 C19 Co1 C3 120.9(2) . . . . ?
C24 C19 Co1 C3 -2.2(4) . . . . ?
C23 C19 Co1 C20 116.5(3) . . . . ?
C24 C19 Co1 C20 -123.1(5) . . . . ?
C20 C19 Co1 C23 -116.5(3) . . . . ?
C24 C19 Co1 C23 120.3(5) . . . . ?
C23 C19 Co1 C21 78.7(2) . . . . ?
C20 C19 Co1 C21 -37.8(2) . . . . ?
C24 C19 Co1 C21 -160.9(5) . . . . ?
C23 C19 Co1 C22 37.1(2) . . . . ?
C20 C19 Co1 C22 -79.4(2) . . . . ?
C24 C19 Co1 C22 157.5(5) . . . . ?
C23 C19 Co1 S1 -23.7(3) . . . . ?
C20 C19 Co1 S1 -140.27(19) . . . . ?
C24 C19 Co1 S1 96.6(4) . . . . ?
C23 C19 Co1 S2 147.43(19) . . . . ?
C20 C19 Co1 S2 30.9(3) . . . . ?
C24 C19 Co1 S2 -92.2(4) . . . . ?
C19 C23 Co1 C3 64.1(3) . . . . ?
C22 C23 Co1 C3 -177.4(2) . . . . ?
C28 C23 Co1 C3 -54.7(4) . . . . ?
C19 C23 Co1 C20 -38.9(2) . . . . ?
C22 C23 Co1 C20 79.6(2) . . . . ?
C28 C23 Co1 C20 -157.7(4) . . . . ?
C22 C23 Co1 C19 118.5(3) . . . . ?
C28 C23 Co1 C19 -118.8(4) . . . . ?
C19 C23 Co1 C21 -82.4(2) . . . . ?
C22 C23 Co1 C21 36.1(2) . . . . ?
C28 C23 Co1 C21 158.8(4) . . . . ?
C19 C23 Co1 C22 -118.5(3) . . . . ?
C28 C23 Co1 C22 122.7(5) . . . . ?
C19 C23 Co1 S1 162.4(2) . . . . ?
C22 C23 Co1 S1 -79.1(2) . . . . ?
C28 C23 Co1 S1 43.6(4) . . . . ?
C19 C23 Co1 S2 -86.3(4) . . . . ?
C22 C23 Co1 S2 32.2(4) . . . . ?
C28 C23 Co1 S2 154.9(3) . . . . ?
C22 C21 Co1 C3 -125.1(3) . . . . ?
C20 C21 Co1 C3 -6.2(4) . . . . ?
C26 C21 Co1 C3 110.6(4) . . . . ?
C22 C21 Co1 C20 -118.8(3) . . . . ?
C26 C21 Co1 C20 116.9(5) . . . . ?
C22 C21 Co1 C19 -80.5(2) . . . . ?
C20 C21 Co1 C19 38.3(2) . . . . ?
C26 C21 Co1 C19 155.1(4) . . . . ?
C22 C21 Co1 C23 -37.0(2) . . . . ?
C20 C21 Co1 C23 81.8(2) . . . . ?
C26 C21 Co1 C23 -161.3(4) . . . . ?
C20 C21 Co1 C22 118.8(3) . . . . ?
C26 C21 Co1 C22 -124.3(5) . . . . ?
C22 C21 Co1 S1 45.9(2) . . . . ?
C20 C21 Co1 S1 164.66(19) . . . . ?
C26 C21 Co1 S1 -78.5(4) . . . . ?
C22 C21 Co1 S2 141.5(2) . . . . ?
C20 C21 Co1 S2 -99.7(2) . . . . ?
C26 C21 Co1 S2 17.1(4) . . . . ?
C21 C22 Co1 C3 124.3(3) . . . . ?
C23 C22 Co1 C3 4.8(4) . . . . ?
C27 C22 Co1 C3 -113.6(4) . . . . ?
C21 C22 Co1 C20 37.8(2) . . . . ?
C23 C22 Co1 C20 -81.8(2) . . . . ?
C27 C22 Co1 C20 159.8(4) . . . . ?
C21 C22 Co1 C19 81.8(2) . . . . ?
C23 C22 Co1 C19 -37.8(2) . . . . ?
C27 C22 Co1 C19 -156.2(4) . . . . ?
C21 C22 Co1 C23 119.6(3) . . . . ?
C27 C22 Co1 C23 -118.4(5) . . . . ?
C23 C22 Co1 C21 -119.6(3) . . . . ?
C27 C22 Co1 C21 122.0(5) . . . . ?
C21 C22 Co1 S1 -139.2(2) . . . . ?
C23 C22 Co1 S1 101.3(2) . . . . ?
C27 C22 Co1 S1 -17.2(4) . . . . ?
C21 C22 Co1 S2 -46.5(2) . . . . ?
C23 C22 Co1 S2 -166.10(19) . . . . ?
C27 C22 Co1 S2 75.5(4) . . . . ?
C32 C31 Co2 C50 -104.8(3) . . . . ?
C35 C31 Co2 C50 68.5(3) . . . . ?
C32 C31 Co2 C49 -142.2(3) . . . . ?
C35 C31 Co2 C49 31.1(3) . . . . ?
C32 C31 Co2 C51 -72.6(4) . . . . ?
C35 C31 Co2 C51 100.7(3) . . . . ?
C32 C31 Co2 C48 -151.8(3) . . . . ?
C35 C31 Co2 C48 21.5(4) . . . . ?
C32 C31 Co2 C47 -82.1(5) . . . . ?
C35 C31 Co2 C47 91.3(4) . . . . ?
C32 C31 Co2 S3 20.2(3) . . . . ?
C35 C31 Co2 S3 -166.5(3) . . . . ?
C32 C31 Co2 S4 113.1(3) . . . . ?
C35 C31 Co2 S4 -73.6(3) . . . . ?
C49 C50 Co2 C31 -111.5(3) . . . . ?
C51 C50 Co2 C31 130.4(2) . . . . ?
C55 C50 Co2 C31 12.2(4) . . . . ?
C51 C50 Co2 C49 -118.1(3) . . . . ?
C55 C50 Co2 C49 123.7(5) . . . . ?
C49 C50 Co2 C51 118.1(3) . . . . ?
C55 C50 Co2 C51 -118.2(5) . . . . ?
C49 C50 Co2 C48 37.9(2) . . . . ?
C51 C50 Co2 C48 -80.2(2) . . . . ?
C55 C50 Co2 C48 161.6(4) . . . . ?
C49 C50 Co2 C47 79.7(3) . . . . ?
C51 C50 Co2 C47 -38.3(2) . . . . ?
C55 C50 Co2 C47 -156.5(4) . . . . ?
C49 C50 Co2 S3 152.0(2) . . . . ?
C51 C50 Co2 S3 33.9(3) . . . . ?
C55 C50 Co2 S3 -84.3(4) . . . . ?
C49 C50 Co2 S4 -16.5(3) . . . . ?
C51 C50 Co2 S4 -134.6(2) . . . . ?
C55 C50 Co2 S4 107.2(4) . . . . ?
C48 C49 Co2 C31 -170.3(2) . . . . ?
C50 C49 Co2 C31 72.7(3) . . . . ?
C54 C49 Co2 C31 -45.4(4) . . . . ?
C48 C49 Co2 C50 117.0(3) . . . . ?
C54 C49 Co2 C50 -118.1(5) . . . . ?
C48 C49 Co2 C51 79.0(3) . . . . ?
C50 C49 Co2 C51 -38.0(2) . . . . ?
C54 C49 Co2 C51 -156.1(5) . . . . ?
C50 C49 Co2 C48 -117.0(3) . . . . ?
C54 C49 Co2 C48 124.9(5) . . . . ?
C48 C49 Co2 C47 35.7(2) . . . . ?
C50 C49 Co2 C47 -81.3(3) . . . . ?
C54 C49 Co2 C47 160.6(5) . . . . ?
C48 C49 Co2 S3 53.8(4) . . . . ?
C50 C49 Co2 S3 -63.2(4) . . . . ?
C54 C49 Co2 S3 178.7(3) . . . . ?
C48 C49 Co2 S4 -73.4(2) . . . . ?
C50 C49 Co2 S4 169.6(2) . . . . ?
C54 C49 Co2 S4 51.5(4) . . . . ?
C50 C51 Co2 C31 -56.4(3) . . . . ?
C47 C51 Co2 C31 -173.2(2) . . . . ?
C56 C51 Co2 C31 64.6(4) . . . . ?
C47 C51 Co2 C50 -116.8(3) . . . . ?
C56 C51 Co2 C50 121.0(5) . . . . ?
C50 C51 Co2 C49 37.8(2) . . . . ?
C47 C51 Co2 C49 -79.0(2) . . . . ?
C56 C51 Co2 C49 158.8(4) . . . . ?
C50 C51 Co2 C48 80.4(2) . . . . ?
C47 C51 Co2 C48 -36.4(2) . . . . ?
C56 C51 Co2 C48 -158.6(4) . . . . ?
C50 C51 Co2 C47 116.8(3) . . . . ?
C56 C51 Co2 C47 -122.2(5) . . . . ?
C50 C51 Co2 S3 -152.8(2) . . . . ?
C47 C51 Co2 S3 90.5(2) . . . . ?
C56 C51 Co2 S3 -31.7(4) . . . . ?
C50 C51 Co2 S4 111.4(3) . . . . ?
C47 C51 Co2 S4 -5.4(4) . . . . ?
C56 C51 Co2 S4 -127.6(3) . . . . ?
C47 C48 Co2 C31 135.5(3) . . . . ?
C49 C48 Co2 C31 15.1(4) . . . . ?
C53 C48 Co2 C31 -103.9(4) . . . . ?
C47 C48 Co2 C50 81.7(3) . . . . ?
C49 C48 Co2 C50 -38.7(2) . . . . ?
C53 C48 Co2 C50 -157.7(4) . . . . ?
C47 C48 Co2 C49 120.4(3) . . . . ?
C53 C48 Co2 C49 -119.0(5) . . . . ?
C47 C48 Co2 C51 37.7(2) . . . . ?
C49 C48 Co2 C51 -82.8(3) . . . . ?
C53 C48 Co2 C51 158.2(4) . . . . ?
C49 C48 Co2 C47 -120.4(3) . . . . ?
C53 C48 Co2 C47 120.6(5) . . . . ?
C47 C48 Co2 S3 -35.0(3) . . . . ?
C49 C48 Co2 S3 -155.5(2) . . . . ?
C53 C48 Co2 S3 85.5(4) . . . . ?
C47 C48 Co2 S4 -128.3(2) . . . . ?
C49 C48 Co2 S4 111.3(2) . . . . ?
C53 C48 Co2 S4 -7.7(4) . . . . ?
C48 C47 Co2 C31 -105.3(4) . . . . ?
C51 C47 Co2 C31 13.7(4) . . . . ?
C52 C47 Co2 C31 133.9(4) . . . . ?
C48 C47 Co2 C50 -80.2(3) . . . . ?
C51 C47 Co2 C50 38.8(2) . . . . ?
C52 C47 Co2 C50 159.1(4) . . . . ?
C48 C47 Co2 C49 -36.5(2) . . . . ?
C51 C47 Co2 C49 82.5(2) . . . . ?
C52 C47 Co2 C49 -157.2(5) . . . . ?
C48 C47 Co2 C51 -119.0(3) . . . . ?
C52 C47 Co2 C51 120.3(5) . . . . ?
C51 C47 Co2 C48 119.0(3) . . . . ?
C52 C47 Co2 C48 -120.8(5) . . . . ?
C48 C47 Co2 S3 151.2(2) . . . . ?
C51 C47 Co2 S3 -89.8(2) . . . . ?
C52 C47 Co2 S3 30.4(4) . . . . ?
C48 C47 Co2 S4 58.3(2) . . . . ?
C51 C47 Co2 S4 177.25(19) . . . . ?
C52 C47 Co2 S4 -62.5(4) . . . . ?
C5 C6 S1 C1 105.1(3) . . . . ?
C13 C6 S1 C1 -80.1(3) . . . . ?
C5 C6 S1 Co1 -12.1(3) . . . . ?
C13 C6 S1 Co1 162.7(2) . . . . ?
C2 C1 S1 C6 -118.1(3) . . . . ?
B4 C1 S1 C6 27.2(4) . . . . ?
B6 C1 S1 C6 173.7(2) . . . . ?
B5 C1 S1 C6 104.1(3) . . . . ?
B3 C1 S1 C6 -49.0(3) . . . . ?
C2 C1 S1 Co1 3.6(3) . . . . ?
B4 C1 S1 Co1 148.9(3) . . . . ?
B6 C1 S1 Co1 -64.6(3) . . . . ?
B5 C1 S1 Co1 -134.2(3) . . . . ?
B3 C1 S1 Co1 72.7(3) . . . . ?
C3 Co1 S1 C6 17.99(17) . . . . ?
C20 Co1 S1 C6 -136.8(3) . . . . ?
C19 Co1 S1 C6 -78.3(2) . . . . ?
C23 Co1 S1 C6 -93.14(17) . . . . ?
C21 Co1 S1 C6 -157.29(17) . . . . ?
C22 Co1 S1 C6 -131.14(17) . . . . ?
S2 Co1 S1 C6 108.06(14) . . . . ?
C3 Co1 S1 C1 -97.05(16) . . . . ?
C20 Co1 S1 C1 108.1(3) . . . . ?
C19 Co1 S1 C1 166.68(18) . . . . ?
C23 Co1 S1 C1 151.83(16) . . . . ?
C21 Co1 S1 C1 87.67(17) . . . . ?
C22 Co1 S1 C1 113.82(17) . . . . ?
S2 Co1 S1 C1 -6.98(13) . . . . ?
C1 C2 S2 Co1 -8.2(3) . . . . ?
B8 C2 S2 Co1 -153.0(3) . . . . ?
B7 C2 S2 Co1 132.2(3) . . . . ?
B3 C2 S2 Co1 -78.2(3) . . . . ?
B6 C2 S2 Co1 60.1(3) . . . . ?
C3 Co1 S2 C2 104.60(17) . . . . ?
C20 Co1 S2 C2 -145.61(17) . . . . ?
C19 Co1 S2 C2 -165.00(19) . . . . ?
C23 Co1 S2 C2 -102.9(3) . . . . ?
C21 Co1 S2 C2 -106.51(17) . . . . ?
C22 Co1 S2 C2 -80.06(18) . . . . ?
S1 Co1 S2 C2 8.38(13) . . . . ?
C33 C34 S3 C29 -99.6(4) . . . . ?
C41 C34 S3 C29 79.7(3) . . . . ?
C33 C34 S3 Co2 18.0(4) . . . . ?
C41 C34 S3 Co2 -162.6(3) . . . . ?
C30 C29 S3 C34 126.2(3) . . . . ?
B14 C29 S3 C34 -19.9(4) . . . . ?
B13 C29 S3 C34 56.1(3) . . . . ?
B16 C29 S3 C34 -165.2(3) . . . . ?
B15 C29 S3 C34 -95.9(3) . . . . ?
C30 C29 S3 Co2 5.7(3) . . . . ?
B14 C29 S3 Co2 -140.4(3) . . . . ?
B13 C29 S3 Co2 -64.4(3) . . . . ?
B16 C29 S3 Co2 74.4(3) . . . . ?
B15 C29 S3 Co2 143.6(3) . . . . ?
C31 Co2 S3 C34 -25.57(18) . . . . ?
C50 Co2 S3 C34 67.6(2) . . . . ?
C49 Co2 S3 C34 111.5(3) . . . . ?
C51 Co2 S3 C34 88.54(19) . . . . ?
C48 Co2 S3 C34 148.4(2) . . . . ?
C47 Co2 S3 C34 127.79(18) . . . . ?
S4 Co2 S3 C34 -119.42(15) . . . . ?
C31 Co2 S3 C29 88.75(16) . . . . ?
C50 Co2 S3 C29 -178.05(18) . . . . ?
C49 Co2 S3 C29 -134.2(3) . . . . ?
C51 Co2 S3 C29 -157.15(17) . . . . ?
C48 Co2 S3 C29 -97.25(19) . . . . ?
C47 Co2 S3 C29 -117.89(17) . . . . ?
S4 Co2 S3 C29 -5.10(13) . . . . ?
C29 C30 S4 Co2 -0.7(3) . . . . ?
B17 C30 S4 Co2 -142.0(3) . . . . ?
B18 C30 S4 Co2 142.2(3) . . . . ?
B13 C30 S4 Co2 68.8(3) . . . . ?
B16 C30 S4 Co2 -70.0(3) . . . . ?
C31 Co2 S4 C30 -92.45(18) . . . . ?
C50 Co2 S4 C30 174.0(2) . . . . ?
C49 Co2 S4 C30 163.29(18) . . . . ?
C51 Co2 S4 C30 98.7(3) . . . . ?
C48 Co2 S4 C30 126.51(17) . . . . ?
C47 Co2 S4 C30 95.03(18) . . . . ?
S3 Co2 S4 C30 3.42(14) . . . . ?
