#------------------------------------------------------------------------------
#$Date: 2016-02-16 03:10:39 +0200 (Tue, 16 Feb 2016) $
#$Revision: 176453 $
#$URL: svn://www.crystallography.net/cod/cif/7/01/45/7014592.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7014592
loop_
_publ_author_name
'Lane, Stephanie Renee'
'Sisay, Nebiat'
'Carney, Brett'
'Dannoon, Shorouk'
'Williams, Stephen'
'Engelbrecht, Hendrik Petrus'
'Barnes, Charles Leslie'
'Jurisson, Silvia Sabine'
_publ_section_title
;
 Re(V) and Re(III) complexes with sal2phen and triphenylphosphine:
 rearrangement, oxidation and reduction.
;
_journal_issue                   1
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              269
_journal_page_last               276
_journal_paper_doi               10.1039/c0dt00993h
_journal_volume                  40
_journal_year                    2011
_chemical_formula_sum            'C33.5 H26.5 Cl9.5 N2 O P Re'
_chemical_formula_weight         1027.01
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_Int_Tables_number      2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                91.8540(10)
_cell_angle_beta                 108.1690(10)
_cell_angle_gamma                115.2970(10)
_cell_formula_units_Z            2
_cell_length_a                   11.1410(8)
_cell_length_b                   11.5874(8)
_cell_length_c                   17.7337(12)
_cell_measurement_reflns_used    8342
_cell_measurement_temperature    173(2)
_cell_measurement_theta_max      27.1
_cell_measurement_theta_min      2.3
_cell_volume                     1929.7(2)
_computing_cell_refinement       'SAINT (Bruker, 1998)'
_computing_data_collection       'SMART (Bruker, 1998)'
_computing_data_reduction        'SAINT (Bruker, 1998)'
_computing_molecular_graphics    'ORTEP-III (Burnett & Johnson, 1996)'
_computing_publication_material  'CIFTAB (Sheldrick, 1997)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      173(2)
_diffrn_measured_fraction_theta_full 0.969
_diffrn_measured_fraction_theta_max 0.969
_diffrn_measurement_device_type  'Bruker SMART CCD area detector'
_diffrn_measurement_method       'omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0251
_diffrn_reflns_av_sigmaI/netI    0.0442
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_k_max       14
_diffrn_reflns_limit_k_min       -14
_diffrn_reflns_limit_l_max       19
_diffrn_reflns_limit_l_min       -22
_diffrn_reflns_number            13762
_diffrn_reflns_theta_full        27.14
_diffrn_reflns_theta_max         27.14
_diffrn_reflns_theta_min         1.98
_exptl_absorpt_coefficient_mu    3.879
_exptl_absorpt_correction_T_max  0.83
_exptl_absorpt_correction_T_min  0.28
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
Data were corrected for decay and absorption using the program SADABS
(Sheldrick, G. M. (2003). SADABS. Version 2.10. University of
Göttingen, Germany).
;
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    1.768
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       plate
_exptl_crystal_F_000             1002
_exptl_crystal_size_max          0.45
_exptl_crystal_size_mid          0.30
_exptl_crystal_size_min          0.05
_refine_diff_density_max         3.888
_refine_diff_density_min         -4.034
_refine_diff_density_rms         0.147
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.101
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     439
_refine_ls_number_reflns         8290
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.101
_refine_ls_R_factor_all          0.0630
_refine_ls_R_factor_gt           0.0515
_refine_ls_shift/su_max          0.016
_refine_ls_shift/su_mean         0.004
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0305P)²+14.0413P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1139
_refine_ls_wR_factor_ref         0.1204
_reflns_number_gt                7131
_reflns_number_total             8290
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            C0DT00993H.TXT
_cod_data_source_block           ReOPPh3t
_cod_original_sg_symbol_H-M      P-1
_cod_original_formula_sum        'C33.50 H26.50 Cl9.50 N2 O P Re'
_cod_database_code               7014592
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Re1 Re 0.13754(3) 0.20948(3) 0.350932(19) 0.03400(9) Uani 1 1 d . . .
Cl1 Cl 0.23851(16) 0.06973(14) 0.41177(11) 0.0345(3) Uani 1 1 d . . .
P1 P 0.04996(17) 0.36202(16) 0.30186(10) 0.0285(3) Uani 1 1 d . . .
O1 O 0.2434(5) 0.3288(4) 0.4506(3) 0.0377(11) Uani 1 1 d . . .
N1 N -0.0263(7) 0.1194(6) 0.4052(5) 0.0493(16) Uani 1 1 d . . .
C1 C 0.2375(7) 0.3361(6) 0.5248(4) 0.0325(14) Uani 1 1 d . . .
Cl2 Cl 0.30701(15) 0.28117(15) 0.28726(10) 0.0332(3) Uani 1 1 d . . .
N2 N -0.0124(5) 0.0826(5) 0.2744(4) 0.0344(13) Uani 1 1 d . . .
C2 C 0.3448(7) 0.4345(6) 0.5884(4) 0.0341(14) Uani 1 1 d . . .
H2 H 0.4237 0.5004 0.5794 0.041 Uiso 1 1 calc R . .
C3 C 0.3384(8) 0.4376(7) 0.6642(5) 0.0420(16) Uani 1 1 d . . .
H3 H 0.4135 0.5051 0.7074 0.050 Uiso 1 1 calc R . .
C4 C 0.2240(9) 0.3435(7) 0.6784(5) 0.0460(18) Uani 1 1 d . . .
H4 H 0.2207 0.3462 0.7313 0.055 Uiso 1 1 calc R . .
C5 C 0.1154(8) 0.2466(7) 0.6161(5) 0.0461(19) Uani 1 1 d . . .
H5 H 0.0370 0.1821 0.6262 0.055 Uiso 1 1 calc R . .
C6 C 0.1179(7) 0.2409(6) 0.5384(5) 0.0383(16) Uani 1 1 d . . .
C7 C -0.0112(9) 0.1371(8) 0.4772(6) 0.052(2) Uani 1 1 d . . .
H7 H -0.0860 0.0813 0.4937 0.063 Uiso 1 1 calc R . .
C8 C -0.1630(7) 0.0194(6) 0.3471(5) 0.0366(15) Uani 1 1 d . . .
C9 C -0.2932(8) -0.0535(8) 0.3549(6) 0.051(2) Uani 1 1 d . . .
H9 H -0.3048 -0.0436 0.4052 0.061 Uiso 1 1 calc R . .
C10 C -0.4054(8) -0.1406(9) 0.2883(7) 0.063(3) Uani 1 1 d . . .
H10 H -0.4952 -0.1905 0.2930 0.076 Uiso 1 1 calc R . .
C11 C -0.3902(8) -0.1567(8) 0.2156(7) 0.065(3) Uani 1 1 d . . .
H11 H -0.4691 -0.2181 0.1709 0.078 Uiso 1 1 calc R . .
C12 C -0.2604(8) -0.0841(8) 0.2063(5) 0.0510(19) Uani 1 1 d . . .
H12 H -0.2495 -0.0945 0.1559 0.061 Uiso 1 1 calc R . .
C13 C -0.1489(6) 0.0030(6) 0.2726(5) 0.0375(16) Uani 1 1 d . . .
C14 C -0.1126(6) 0.3279(6) 0.3209(4) 0.0293(13) Uani 1 1 d . . .
C15 C -0.1040(7) 0.3616(6) 0.3992(4) 0.0350(15) Uani 1 1 d . . .
H15 H -0.0135 0.4105 0.4408 0.042 Uiso 1 1 calc R . .
C16 C -0.2264(7) 0.3244(7) 0.4170(5) 0.0444(18) Uani 1 1 d . . .
H16 H -0.2197 0.3483 0.4705 0.053 Uiso 1 1 calc R . .
C17 C -0.3581(8) 0.2528(8) 0.3570(6) 0.053(2) Uani 1 1 d . . .
H17 H -0.4420 0.2269 0.3692 0.064 Uiso 1 1 calc R . .
C18 C -0.3680(8) 0.2191(8) 0.2798(6) 0.058(2) Uani 1 1 d . . .
H18 H -0.4591 0.1700 0.2387 0.070 Uiso 1 1 calc R . .
C19 C -0.2459(7) 0.2559(7) 0.2609(5) 0.0455(18) Uani 1 1 d . . .
H19 H -0.2537 0.2319 0.2072 0.055 Uiso 1 1 calc R . .
C20 C 0.1714(6) 0.5315(6) 0.3502(4) 0.0293(13) Uani 1 1 d . . .
C21 C 0.1232(7) 0.6224(6) 0.3556(4) 0.0340(14) Uani 1 1 d . . .
H21 H 0.0238 0.5954 0.3355 0.041 Uiso 1 1 calc R . .
C22 C 0.2175(8) 0.7524(7) 0.3898(5) 0.0421(17) Uani 1 1 d . . .
H22 H 0.1827 0.8140 0.3912 0.051 Uiso 1 1 calc R . .
C23 C 0.3622(8) 0.7917(7) 0.4218(5) 0.0475(19) Uani 1 1 d . . .
H23 H 0.4270 0.8801 0.4462 0.057 Uiso 1 1 calc R . .
C24 C 0.4123(8) 0.7012(7) 0.4179(5) 0.0458(18) Uani 1 1 d . . .
H24 H 0.5115 0.7277 0.4407 0.055 Uiso 1 1 calc R . .
C25 C 0.3189(7) 0.5736(6) 0.3813(4) 0.0356(15) Uani 1 1 d . . .
H25 H 0.3544 0.5133 0.3770 0.043 Uiso 1 1 calc R . .
C26 C -0.0031(8) 0.3581(8) 0.1929(4) 0.0424(17) Uani 1 1 d . . .
C27 C -0.0430(13) 0.4499(10) 0.1612(5) 0.072(3) Uani 1 1 d . . .
H27 H -0.0350 0.5181 0.1968 0.086 Uiso 1 1 calc R . .
C28 C -0.0938(16) 0.4433(13) 0.0793(6) 0.095(4) Uani 1 1 d . . .
H28 H -0.1219 0.5060 0.0583 0.114 Uiso 1 1 calc R . .
C29 C -0.1040(15) 0.3453(13) 0.0272(6) 0.096(4) Uani 1 1 d . . .
H29 H -0.1409 0.3396 -0.0296 0.115 Uiso 1 1 calc R . .
C30 C -0.0607(13) 0.2564(13) 0.0576(6) 0.086(4) Uani 1 1 d . . .
H30 H -0.0652 0.1906 0.0218 0.103 Uiso 1 1 calc R . .
C31 C -0.0104(9) 0.2621(9) 0.1405(5) 0.056(2) Uani 1 1 d . . .
H31 H 0.0190 0.2001 0.1613 0.067 Uiso 1 1 calc R . .
C32 C 0.3612(15) 0.3767(13) 0.1014(7) 0.113(5) Uani 1 1 d . . .
H32 H 0.3400 0.3199 0.1417 0.136 Uiso 1 1 calc R . .
Cl3 Cl 0.3316(6) 0.5079(4) 0.1214(3) 0.174(3) Uani 1 1 d . . .
Cl4 Cl 0.2468(4) 0.2845(4) 0.00465(19) 0.1163(13) Uani 1 1 d . . .
Cl5 Cl 0.5369(6) 0.4269(9) 0.1119(3) 0.238(4) Uani 1 1 d . . .
C33 C 0.1511(8) -0.0619(7) 0.1986(5) 0.0469(18) Uani 1 1 d . . .
H33 H 0.1835 0.0037 0.2480 0.056 Uiso 1 1 calc R . .
Cl6 Cl 0.1188(3) 0.0085(2) 0.11287(15) 0.0723(7) Uani 1 1 d . . .
Cl7 Cl 0.2845(3) -0.1075(3) 0.2061(2) 0.0891(9) Uani 1 1 d . . .
Cl8 Cl -0.0054(2) -0.1977(2) 0.19361(15) 0.0613(6) Uani 1 1 d . . .
C34 C 0.454(3) -0.021(3) -0.0279(18) 0.115(10) Uiso 0.50 1 d P . .
Cl9 Cl 0.5135(15) 0.1701(14) 0.0160(9) 0.198(5) Uiso 0.50 1 d P . .
Cl10 Cl 0.508(2) -0.051(2) 0.0730(14) 0.093(6) Uiso 0.15 1 d P . .
Cl11 Cl 0.609(2) -0.016(2) -0.0301(14) 0.183(7) Uiso 0.32 1 d P . .
Cl12 Cl 0.634(2) 0.117(2) -0.0012(13) 0.123(6) Uiso 0.20 1 d P . .
Cl13 Cl 0.4505(10) -0.0015(9) 0.0762(6) 0.083(2) Uiso 0.33 1 d P . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Re Re -1.0185 7.2310 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N2 Re1 O1 157.8(2) . . ?
N2 Re1 N1 73.5(3) . . ?
O1 Re1 N1 84.8(2) . . ?
N2 Re1 Cl2 101.99(18) . . ?
O1 Re1 Cl2 100.01(15) . . ?
N1 Re1 Cl2 173.39(17) . . ?
N2 Re1 P1 89.59(17) . . ?
O1 Re1 P1 87.03(14) . . ?
N1 Re1 P1 92.61(16) . . ?
Cl2 Re1 P1 92.14(5) . . ?
N2 Re1 Cl1 95.20(17) . . ?
O1 Re1 Cl1 87.85(14) . . ?
N1 Re1 Cl1 87.07(17) . . ?
Cl2 Re1 Cl1 88.61(5) . . ?
P1 Re1 Cl1 174.89(6) . . ?
C20 P1 C14 105.0(3) . . ?
C20 P1 C26 106.2(3) . . ?
C14 P1 C26 103.0(3) . . ?
C20 P1 Re1 114.5(2) . . ?
C14 P1 Re1 110.6(2) . . ?
C26 P1 Re1 116.3(2) . . ?
C1 O1 Re1 136.9(4) . . ?
C7 N1 C8 119.0(7) . . ?
C7 N1 Re1 127.4(6) . . ?
C8 N1 Re1 113.4(5) . . ?
O1 C1 C2 121.6(6) . . ?
O1 C1 C6 119.2(6) . . ?
C2 C1 C6 119.1(6) . . ?
C13 N2 Re1 131.2(5) . . ?
C3 C2 C1 120.5(6) . . ?
C3 C2 H2 119.7 . . ?
C1 C2 H2 119.7 . . ?
C2 C3 C4 120.7(7) . . ?
C2 C3 H3 119.6 . . ?
C4 C3 H3 119.6 . . ?
C5 C4 C3 119.7(7) . . ?
C5 C4 H4 120.1 . . ?
C3 C4 H4 120.1 . . ?
C4 C5 C6 121.1(7) . . ?
C4 C5 H5 119.4 . . ?
C6 C5 H5 119.4 . . ?
C5 C6 C1 118.7(6) . . ?
C5 C6 C7 114.5(7) . . ?
C1 C6 C7 126.7(7) . . ?
N1 C7 C6 122.7(8) . . ?
N1 C7 H7 118.7 . . ?
C6 C7 H7 118.7 . . ?
C9 C8 C13 119.4(7) . . ?
C9 C8 N1 131.7(7) . . ?
C13 C8 N1 108.9(6) . . ?
C10 C9 C8 118.7(8) . . ?
C10 C9 H9 120.6 . . ?
C8 C9 H9 120.6 . . ?
C11 C10 C9 121.4(7) . . ?
C11 C10 H10 119.3 . . ?
C9 C10 H10 119.3 . . ?
C10 C11 C12 120.8(8) . . ?
C10 C11 H11 119.6 . . ?
C12 C11 H11 119.6 . . ?
C13 C12 C11 117.7(8) . . ?
C13 C12 H12 121.2 . . ?
C11 C12 H12 121.2 . . ?
C12 C13 N2 125.5(7) . . ?
C12 C13 C8 121.9(6) . . ?
N2 C13 C8 112.6(6) . . ?
C19 C14 C15 118.9(6) . . ?
C19 C14 P1 121.3(5) . . ?
C15 C14 P1 119.4(5) . . ?
C16 C15 C14 120.5(7) . . ?
C16 C15 H15 119.7 . . ?
C14 C15 H15 119.7 . . ?
C17 C16 C15 120.0(8) . . ?
C17 C16 H16 120.0 . . ?
C15 C16 H16 120.0 . . ?
C18 C17 C16 120.1(7) . . ?
C18 C17 H17 120.0 . . ?
C16 C17 H17 120.0 . . ?
C17 C18 C19 120.6(8) . . ?
C17 C18 H18 119.7 . . ?
C19 C18 H18 119.7 . . ?
C14 C19 C18 119.8(8) . . ?
C14 C19 H19 120.1 . . ?
C18 C19 H19 120.1 . . ?
C21 C20 C25 118.2(6) . . ?
C21 C20 P1 121.9(5) . . ?
C25 C20 P1 119.8(5) . . ?
C20 C21 C22 121.2(6) . . ?
C20 C21 H21 119.4 . . ?
C22 C21 H21 119.4 . . ?
C23 C22 C21 119.8(6) . . ?
C23 C22 H22 120.1 . . ?
C21 C22 H22 120.1 . . ?
C22 C23 C24 119.7(7) . . ?
C22 C23 H23 120.2 . . ?
C24 C23 H23 120.2 . . ?
C25 C24 C23 120.3(7) . . ?
C25 C24 H24 119.9 . . ?
C23 C24 H24 119.9 . . ?
C24 C25 C20 120.7(6) . . ?
C24 C25 H25 119.6 . . ?
C20 C25 H25 119.6 . . ?
C31 C26 C27 118.9(8) . . ?
C31 C26 P1 121.5(6) . . ?
C27 C26 P1 119.5(6) . . ?
C28 C27 C26 120.8(9) . . ?
C28 C27 H27 119.6 . . ?
C26 C27 H27 119.6 . . ?
C27 C28 C29 119.9(10) . . ?
C27 C28 H28 120.1 . . ?
C29 C28 H28 120.1 . . ?
C30 C29 C28 120.0(9) . . ?
C30 C29 H29 120.0 . . ?
C28 C29 H29 120.0 . . ?
C29 C30 C31 120.2(9) . . ?
C29 C30 H30 119.9 . . ?
C31 C30 H30 119.9 . . ?
C26 C31 C30 120.1(9) . . ?
C26 C31 H31 120.0 . . ?
C30 C31 H31 120.0 . . ?
Cl5 C32 Cl3 111.4(8) . . ?
Cl5 C32 Cl4 110.6(9) . . ?
Cl3 C32 Cl4 110.7(8) . . ?
Cl5 C32 H32 108.0 . . ?
Cl3 C32 H32 108.0 . . ?
Cl4 C32 H32 108.0 . . ?
Cl7 C33 Cl8 110.0(4) . . ?
Cl7 C33 Cl6 110.5(4) . . ?
Cl8 C33 Cl6 110.2(4) . . ?
Cl7 C33 H33 108.7 . . ?
Cl8 C33 H33 108.7 . . ?
Cl6 C33 H33 108.7 . . ?
C34 C34 Cl10 103(5) 2_655 2_655 ?
C34 C34 Cl12 97(4) 2_655 2_655 ?
Cl10 C34 Cl12 160(3) 2_655 2_655 ?
C34 C34 Cl13 90(4) 2_655 2_655 ?
Cl10 C34 Cl13 43.4(16) 2_655 2_655 ?
Cl12 C34 Cl13 142(3) 2_655 2_655 ?
C34 C34 Cl11 79(4) 2_655 2_655 ?
Cl10 C34 Cl11 119(3) 2_655 2_655 ?
Cl12 C34 Cl11 60.9(19) 2_655 2_655 ?
Cl13 C34 Cl11 157(3) 2_655 2_655 ?
C34 C34 Cl11 63(3) 2_655 . ?
Cl10 C34 Cl11 73(2) 2_655 . ?
Cl12 C34 Cl11 121(3) 2_655 . ?
Cl13 C34 Cl11 34.1(11) 2_655 . ?
Cl11 C34 Cl11 141.6(19) 2_655 . ?
C34 C34 Cl10 41(3) 2_655 . ?
Cl10 C34 Cl10 144(2) 2_655 . ?
Cl12 C34 Cl10 56.1(18) 2_655 . ?
Cl13 C34 Cl10 119.6(19) 2_655 . ?
Cl11 C34 Cl10 63.9(16) 2_655 . ?
Cl11 C34 Cl10 85.5(15) . . ?
C34 C34 Cl12 47(3) 2_655 . ?
Cl10 C34 Cl12 55.6(19) 2_655 . ?
Cl12 C34 Cl12 144(2) 2_655 . ?
Cl13 C34 Cl12 54.7(14) 2_655 . ?
Cl11 C34 Cl12 104.3(19) 2_655 . ?
Cl11 C34 Cl12 49.1(12) . . ?
Cl10 C34 Cl12 88.3(14) . . ?
C34 C34 Cl13 54(3) 2_655 . ?
Cl10 C34 Cl13 136(3) 2_655 . ?
Cl12 C34 Cl13 55.7(16) 2_655 . ?
Cl13 C34 Cl13 144.4(18) 2_655 . ?
Cl11 C34 Cl13 31.2(10) 2_655 . ?
Cl11 C34 Cl13 113.8(16) . . ?
Cl10 C34 Cl13 33.1(9) . . ?
Cl12 C34 Cl13 94.1(14) . . ?
C34 C34 Cl9 82(4) 2_655 2_655 ?
Cl10 C34 Cl9 123(3) 2_655 2_655 ?
Cl12 C34 Cl9 63.7(18) 2_655 2_655 ?
Cl13 C34 Cl9 80.6(17) 2_655 2_655 ?
Cl11 C34 Cl9 118(2) 2_655 2_655 ?
Cl11 C34 Cl9 59.5(14) . 2_655 ?
Cl10 C34 Cl9 63.1(14) . 2_655 ?
Cl12 C34 Cl9 104.3(17) . 2_655 ?
Cl13 C34 Cl9 93.1(16) . 2_655 ?
C34 C34 Cl9 66(3) 2_655 . ?
Cl10 C34 Cl9 67(2) 2_655 . ?
Cl12 C34 Cl9 118(2) 2_655 . ?
Cl13 C34 Cl9 98.9(19) 2_655 . ?
Cl11 C34 Cl9 57.8(14) 2_655 . ?
Cl11 C34 Cl9 103.2(17) . . ?
Cl10 C34 Cl9 91.4(15) . . ?
Cl12 C34 Cl9 54.1(12) . . ?
Cl13 C34 Cl9 69.0(12) . . ?
Cl9 C34 Cl9 148.6(15) 2_655 . ?
Cl12 Cl9 Cl11 96.9(12) . 2_655 ?
Cl12 Cl9 C34 43.1(12) . 2_655 ?
Cl11 Cl9 C34 54.9(13) 2_655 2_655 ?
Cl12 Cl9 Cl10 48.3(10) . 2_655 ?
Cl11 Cl9 Cl10 78.9(11) 2_655 2_655 ?
C34 Cl9 Cl10 55.5(13) 2_655 2_655 ?
Cl12 Cl9 C34 56.8(13) . . ?
Cl11 Cl9 C34 46.7(12) 2_655 . ?
C34 Cl9 C34 31.4(15) 2_655 . ?
Cl10 Cl9 C34 35.1(11) 2_655 . ?
Cl12 Cl9 Cl13 84.2(10) . . ?
Cl11 Cl9 Cl13 25.0(7) 2_655 . ?
C34 Cl9 Cl13 41.8(11) 2_655 . ?
Cl10 Cl9 Cl13 86.2(9) 2_655 . ?
C34 Cl9 Cl13 51.2(11) . . ?
Cl13 Cl10 C34 84(2) . 2_655 ?
Cl13 Cl10 Cl12 72.3(17) . 2_655 ?
C34 Cl10 Cl12 84(2) 2_655 2_655 ?
Cl13 Cl10 Cl11 26.4(11) . 2_655 ?
C34 Cl10 Cl11 67(2) 2_655 2_655 ?
Cl12 Cl10 Cl11 52.6(12) 2_655 2_655 ?
Cl13 Cl10 C34 77.1(18) . . ?
C34 Cl10 C34 36(2) 2_655 . ?
Cl12 Cl10 C34 47.6(13) 2_655 . ?
Cl11 Cl10 C34 51.4(13) 2_655 . ?
Cl13 Cl10 Cl9 130.9(19) . 2_655 ?
C34 Cl10 Cl9 78(2) 2_655 2_655 ?
Cl12 Cl10 Cl9 60.7(12) 2_655 2_655 ?
Cl11 Cl10 Cl9 105.7(14) 2_655 2_655 ?
C34 Cl10 Cl9 61.4(13) . 2_655 ?
Cl13 Cl10 Cl11 116.5(18) . . ?
C34 Cl10 Cl11 34.9(19) 2_655 . ?
Cl12 Cl10 Cl11 83.8(14) 2_655 . ?
Cl11 Cl10 Cl11 94.4(13) 2_655 . ?
C34 Cl10 Cl11 45.8(13) . . ?
Cl9 Cl10 Cl11 48.0(8) 2_655 . ?
Cl13 Cl11 Cl12 76.4(18) 2_655 . ?
Cl13 Cl11 C34 93(2) 2_655 2_655 ?
Cl12 Cl11 C34 53.4(16) . 2_655 ?
Cl13 Cl11 C34 61.2(17) 2_655 . ?
Cl12 Cl11 C34 70.1(18) . . ?
C34 Cl11 C34 38.4(19) 2_655 . ?
Cl13 Cl11 Cl10 28.7(13) 2_655 2_655 ?
Cl12 Cl11 Cl10 55.0(13) . 2_655 ?
C34 Cl11 Cl10 64.7(17) 2_655 2_655 ?
C34 Cl11 Cl10 40.5(13) . 2_655 ?
Cl13 Cl11 Cl9 103.0(18) 2_655 2_655 ?
Cl12 Cl11 Cl9 128.5(17) . 2_655 ?
C34 Cl11 Cl9 75.5(17) 2_655 2_655 ?
C34 Cl11 Cl9 65.7(15) . 2_655 ?
Cl10 Cl11 Cl9 100.9(14) 2_655 2_655 ?
Cl13 Cl11 Cl10 109.8(18) 2_655 . ?
Cl12 Cl11 Cl10 78.2(14) . . ?
C34 Cl11 Cl10 26.6(15) 2_655 . ?
C34 Cl11 Cl10 48.6(14) . . ?
Cl10 Cl11 Cl10 85.6(13) 2_655 . ?
Cl9 Cl11 Cl10 53.0(9) 2_655 . ?
C34 Cl12 Cl11 65.8(19) 2_655 . ?
C34 Cl12 Cl10 76.2(19) 2_655 2_655 ?
Cl11 Cl12 Cl10 72.4(16) . 2_655 ?
C34 Cl12 Cl13 78.4(18) 2_655 2_655 ?
Cl11 Cl12 Cl13 36.7(10) . 2_655 ?
Cl10 Cl12 Cl13 39.3(10) 2_655 2_655 ?
C34 Cl12 Cl9 73.1(19) 2_655 . ?
Cl11 Cl12 Cl9 129.8(17) . . ?
Cl10 Cl12 Cl9 71.0(14) 2_655 . ?
Cl13 Cl12 Cl9 109.0(14) 2_655 . ?
C34 Cl12 C34 36(2) 2_655 . ?
Cl11 Cl12 C34 60.7(16) . . ?
Cl10 Cl12 C34 40.7(12) 2_655 . ?
Cl13 Cl12 C34 51.6(12) 2_655 . ?
Cl9 Cl12 C34 69.1(14) . . ?
Cl11 Cl13 Cl10 125(2) 2_655 . ?
Cl11 Cl13 C34 84.6(19) 2_655 2_655 ?
Cl10 Cl13 C34 53.0(17) . 2_655 ?
Cl11 Cl13 Cl12 66.8(16) 2_655 2_655 ?
Cl10 Cl13 Cl12 68.4(16) . 2_655 ?
C34 Cl13 Cl12 73.7(15) 2_655 2_655 ?
Cl11 Cl13 C34 56.3(17) 2_655 . ?
Cl10 Cl13 C34 69.8(18) . . ?
C34 Cl13 C34 35.6(18) 2_655 . ?
Cl12 Cl13 C34 45.9(12) 2_655 . ?
Cl11 Cl13 Cl9 52.0(15) 2_655 . ?
Cl10 Cl13 Cl9 109.9(15) . . ?
C34 Cl13 Cl9 57.6(15) 2_655 . ?
Cl12 Cl13 Cl9 101.2(10) 2_655 . ?
C34 Cl13 Cl9 59.8(12) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Re1 N2 1.775(6) . ?
Re1 O1 1.891(5) . ?
Re1 N1 2.208(7) . ?
Re1 Cl2 2.3621(15) . ?
Re1 P1 2.4244(16) . ?
Re1 Cl1 2.4422(15) . ?
P1 C20 1.822(7) . ?
P1 C14 1.825(6) . ?
P1 C26 1.829(7) . ?
O1 C1 1.340(8) . ?
N1 C7 1.233(11) . ?
N1 C8 1.469(10) . ?
C1 C2 1.383(10) . ?
C1 C6 1.419(10) . ?
N2 C13 1.391(8) . ?
C2 C3 1.367(10) . ?
C2 H2 0.9500 . ?
C3 C4 1.381(10) . ?
C3 H3 0.9500 . ?
C4 C5 1.368(11) . ?
C4 H4 0.9500 . ?
C5 C6 1.385(11) . ?
C5 H5 0.9500 . ?
C6 C7 1.469(11) . ?
C7 H7 0.9500 . ?
C8 C9 1.386(10) . ?
C8 C13 1.394(10) . ?
C9 C10 1.378(13) . ?
C9 H9 0.9500 . ?
C10 C11 1.369(14) . ?
C10 H10 0.9500 . ?
C11 C12 1.394(12) . ?
C11 H11 0.9500 . ?
C12 C13 1.372(10) . ?
C12 H12 0.9500 . ?
C14 C19 1.389(10) . ?
C14 C15 1.394(9) . ?
C15 C16 1.385(9) . ?
C15 H15 0.9500 . ?
C16 C17 1.379(11) . ?
C16 H16 0.9500 . ?
C17 C18 1.368(13) . ?
C17 H17 0.9500 . ?
C18 C19 1.394(11) . ?
C18 H18 0.9500 . ?
C19 H19 0.9500 . ?
C20 C21 1.384(8) . ?
C20 C25 1.405(9) . ?
C21 C22 1.390(9) . ?
C21 H21 0.9500 . ?
C22 C23 1.383(10) . ?
C22 H22 0.9500 . ?
C23 C24 1.392(10) . ?
C23 H23 0.9500 . ?
C24 C25 1.376(10) . ?
C24 H24 0.9500 . ?
C25 H25 0.9500 . ?
C26 C31 1.384(10) . ?
C26 C27 1.390(11) . ?
C27 C28 1.371(13) . ?
C27 H27 0.9500 . ?
C28 C29 1.382(15) . ?
C28 H28 0.9500 . ?
C29 C30 1.373(15) . ?
C29 H29 0.9500 . ?
C30 C31 1.388(13) . ?
C30 H30 0.9500 . ?
C31 H31 0.9500 . ?
C32 Cl5 1.731(16) . ?
C32 Cl3 1.736(17) . ?
C32 Cl4 1.751(12) . ?
C32 H32 1.0000 . ?
C33 Cl7 1.748(8) . ?
C33 Cl8 1.753(8) . ?
C33 Cl6 1.761(8) . ?
C33 H33 1.0000 . ?
C34 C34 1.09(5) 2_655 ?
C34 Cl10 1.22(4) 2_655 ?
C34 Cl12 1.37(4) 2_655 ?
C34 Cl13 1.51(4) 2_655 ?
C34 Cl11 1.55(4) 2_655 ?
C34 Cl11 1.72(4) . ?
C34 Cl10 1.80(4) . ?
C34 Cl12 1.85(4) . ?
C34 Cl13 1.87(4) . ?
C34 Cl9 1.91(4) 2_655 ?
C34 Cl9 2.07(4) . ?
Cl9 Cl12 1.79(3) . ?
Cl9 Cl11 1.81(2) 2_655 ?
Cl9 C34 1.91(4) 2_655 ?
Cl9 Cl10 1.94(3) 2_655 ?
Cl9 Cl13 2.236(18) . ?
Cl10 Cl13 1.05(2) . ?
Cl10 C34 1.22(4) 2_655 ?
Cl10 Cl12 1.54(3) 2_655 ?
Cl10 Cl11 1.79(3) 2_655 ?
Cl10 Cl9 1.94(3) 2_655 ?
Cl10 Cl11 2.39(3) . ?
Cl11 Cl13 0.97(2) 2_655 ?
Cl11 Cl12 1.49(3) . ?
Cl11 C34 1.55(4) 2_655 ?
Cl11 Cl10 1.79(3) 2_655 ?
Cl11 Cl9 1.81(2) 2_655 ?
Cl12 C34 1.37(4) 2_655 ?
Cl12 Cl10 1.54(3) 2_655 ?
Cl12 Cl13 1.57(2) 2_655 ?
Cl13 Cl11 0.97(2) 2_655 ?
Cl13 C34 1.51(4) 2_655 ?
Cl13 Cl12 1.57(2) 2_655 ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
N2 Re1 P1 C20 -173.5(3) . . . . ?
O1 Re1 P1 C20 28.4(3) . . . . ?
N1 Re1 P1 C20 113.1(3) . . . . ?
Cl2 Re1 P1 C20 -71.5(2) . . . . ?
Cl1 Re1 P1 C20 26.8(7) . . . . ?
N2 Re1 P1 C14 68.1(3) . . . . ?
O1 Re1 P1 C14 -90.0(3) . . . . ?
N1 Re1 P1 C14 -5.3(3) . . . . ?
Cl2 Re1 P1 C14 170.1(2) . . . . ?
Cl1 Re1 P1 C14 -91.5(6) . . . . ?
N2 Re1 P1 C26 -48.9(3) . . . . ?
O1 Re1 P1 C26 153.0(3) . . . . ?
N1 Re1 P1 C26 -122.4(3) . . . . ?
Cl2 Re1 P1 C26 53.0(3) . . . . ?
Cl1 Re1 P1 C26 151.4(6) . . . . ?
N2 Re1 O1 C1 25.7(9) . . . . ?
N1 Re1 O1 C1 14.4(6) . . . . ?
Cl2 Re1 O1 C1 -161.0(5) . . . . ?
P1 Re1 O1 C1 107.3(6) . . . . ?
Cl1 Re1 O1 C1 -72.8(6) . . . . ?
N2 Re1 N1 C7 168.9(7) . . . . ?
O1 Re1 N1 C7 -15.5(6) . . . . ?
Cl2 Re1 N1 C7 121.7(16) . . . . ?
P1 Re1 N1 C7 -102.3(6) . . . . ?
Cl1 Re1 N1 C7 72.6(6) . . . . ?
N2 Re1 N1 C8 -5.2(4) . . . . ?
O1 Re1 N1 C8 170.4(4) . . . . ?
Cl2 Re1 N1 C8 -52.4(19) . . . . ?
P1 Re1 N1 C8 83.6(4) . . . . ?
Cl1 Re1 N1 C8 -101.5(4) . . . . ?
Re1 O1 C1 C2 172.6(5) . . . . ?
Re1 O1 C1 C6 -7.7(9) . . . . ?
O1 Re1 N2 C13 -4.7(10) . . . . ?
N1 Re1 N2 C13 7.0(6) . . . . ?
Cl2 Re1 N2 C13 -178.0(5) . . . . ?
P1 Re1 N2 C13 -85.8(6) . . . . ?
Cl1 Re1 N2 C13 92.4(6) . . . . ?
O1 C1 C2 C3 -178.0(6) . . . . ?
C6 C1 C2 C3 2.3(9) . . . . ?
C1 C2 C3 C4 -0.8(10) . . . . ?
C2 C3 C4 C5 -0.4(11) . . . . ?
C3 C4 C5 C6 -0.1(11) . . . . ?
C4 C5 C6 C1 1.6(10) . . . . ?
C4 C5 C6 C7 -175.6(6) . . . . ?
O1 C1 C6 C5 177.6(6) . . . . ?
C2 C1 C6 C5 -2.7(9) . . . . ?
O1 C1 C6 C7 -5.6(9) . . . . ?
C2 C1 C6 C7 174.1(6) . . . . ?
C8 N1 C7 C6 -175.6(6) . . . . ?
Re1 N1 C7 C6 10.6(10) . . . . ?
C5 C6 C7 N1 179.5(7) . . . . ?
C1 C6 C7 N1 2.6(11) . . . . ?
C7 N1 C8 C9 9.7(11) . . . . ?
Re1 N1 C8 C9 -175.7(7) . . . . ?
C7 N1 C8 C13 -171.1(6) . . . . ?
Re1 N1 C8 C13 3.5(6) . . . . ?
C13 C8 C9 C10 0.0(11) . . . . ?
N1 C8 C9 C10 179.1(7) . . . . ?
C8 C9 C10 C11 0.4(13) . . . . ?
C9 C10 C11 C12 -0.7(15) . . . . ?
C10 C11 C12 C13 0.4(13) . . . . ?
C11 C12 C13 N2 179.6(7) . . . . ?
C11 C12 C13 C8 0.1(12) . . . . ?
Re1 N2 C13 C12 173.3(6) . . . . ?
Re1 N2 C13 C8 -7.0(9) . . . . ?
C9 C8 C13 C12 -0.3(11) . . . . ?
N1 C8 C13 C12 -179.6(6) . . . . ?
C9 C8 C13 N2 -179.9(6) . . . . ?
N1 C8 C13 N2 0.8(8) . . . . ?
C20 P1 C14 C19 138.1(6) . . . . ?
C26 P1 C14 C19 27.1(6) . . . . ?
Re1 P1 C14 C19 -97.9(6) . . . . ?
C20 P1 C14 C15 -49.3(6) . . . . ?
C26 P1 C14 C15 -160.2(5) . . . . ?
Re1 P1 C14 C15 74.8(5) . . . . ?
C19 C14 C15 C16 -0.2(10) . . . . ?
P1 C14 C15 C16 -173.0(5) . . . . ?
C14 C15 C16 C17 0.4(11) . . . . ?
C15 C16 C17 C18 -0.4(12) . . . . ?
C16 C17 C18 C19 0.3(13) . . . . ?
C15 C14 C19 C18 0.1(10) . . . . ?
P1 C14 C19 C18 172.8(6) . . . . ?
C17 C18 C19 C14 -0.1(12) . . . . ?
C14 P1 C20 C21 -31.9(6) . . . . ?
C26 P1 C20 C21 76.8(6) . . . . ?
Re1 P1 C20 C21 -153.5(5) . . . . ?
C14 P1 C20 C25 149.9(5) . . . . ?
C26 P1 C20 C25 -101.4(6) . . . . ?
Re1 P1 C20 C25 28.4(6) . . . . ?
C25 C20 C21 C22 0.8(10) . . . . ?
P1 C20 C21 C22 -177.4(6) . . . . ?
C20 C21 C22 C23 -2.3(11) . . . . ?
C21 C22 C23 C24 1.3(12) . . . . ?
C22 C23 C24 C25 1.1(12) . . . . ?
C23 C24 C25 C20 -2.6(12) . . . . ?
C21 C20 C25 C24 1.7(10) . . . . ?
P1 C20 C25 C24 179.9(6) . . . . ?
C20 P1 C26 C31 137.0(7) . . . . ?
C14 P1 C26 C31 -113.0(7) . . . . ?
Re1 P1 C26 C31 8.2(8) . . . . ?
C20 P1 C26 C27 -45.9(8) . . . . ?
C14 P1 C26 C27 64.2(8) . . . . ?
Re1 P1 C26 C27 -174.6(7) . . . . ?
C31 C26 C27 C28 2.3(16) . . . . ?
P1 C26 C27 C28 -174.9(10) . . . . ?
C26 C27 C28 C29 -1(2) . . . . ?
C27 C28 C29 C30 -1(2) . . . . ?
C28 C29 C30 C31 2(2) . . . . ?
C27 C26 C31 C30 -1.8(14) . . . . ?
P1 C26 C31 C30 175.4(8) . . . . ?
C29 C30 C31 C26 -0.3(18) . . . . ?
C34 C34 Cl9 Cl12 53(3) 2_655 . . . ?
Cl10 C34 Cl9 Cl12 -63(2) 2_655 . . . ?
Cl12 C34 Cl9 Cl12 139(2) 2_655 . . . ?
Cl13 C34 Cl9 Cl12 -33.3(13) 2_655 . . . ?
Cl11 C34 Cl9 Cl12 144.6(19) 2_655 . . . ?
Cl11 C34 Cl9 Cl12 1.2(15) . . . . ?
Cl10 C34 Cl9 Cl12 86.9(15) . . . . ?
Cl13 C34 Cl9 Cl12 111.9(14) . . . . ?
Cl9 C34 Cl9 Cl12 53(3) 2_655 . . . ?
C34 C34 Cl9 Cl11 -92(4) 2_655 . . 2_655 ?
Cl10 C34 Cl9 Cl11 152(3) 2_655 . . 2_655 ?
Cl12 C34 Cl9 Cl11 -6.1(19) 2_655 . . 2_655 ?
Cl13 C34 Cl9 Cl11 -178(2) 2_655 . . 2_655 ?
Cl11 C34 Cl9 Cl11 -143(2) . . . 2_655 ?
Cl10 C34 Cl9 Cl11 -57.7(16) . . . 2_655 ?
Cl12 C34 Cl9 Cl11 -144.6(19) . . . 2_655 ?
Cl13 C34 Cl9 Cl11 -32.8(11) . . . 2_655 ?
Cl9 C34 Cl9 Cl11 -92(4) 2_655 . . 2_655 ?
Cl10 C34 Cl9 C34 -116(5) 2_655 . . 2_655 ?
Cl12 C34 Cl9 C34 85(4) 2_655 . . 2_655 ?
Cl13 C34 Cl9 C34 -86(4) 2_655 . . 2_655 ?
Cl11 C34 Cl9 C34 92(4) 2_655 . . 2_655 ?
Cl11 C34 Cl9 C34 -52(3) . . . 2_655 ?
Cl10 C34 Cl9 C34 34(3) . . . 2_655 ?
Cl12 C34 Cl9 C34 -53(3) . . . 2_655 ?
Cl13 C34 Cl9 C34 59(3) . . . 2_655 ?
Cl9 C34 Cl9 C34 0.000(8) 2_655 . . 2_655 ?
C34 C34 Cl9 Cl10 116(5) 2_655 . . 2_655 ?
Cl12 C34 Cl9 Cl10 -158(3) 2_655 . . 2_655 ?
Cl13 C34 Cl9 Cl10 29.9(15) 2_655 . . 2_655 ?
Cl11 C34 Cl9 Cl10 -152(3) 2_655 . . 2_655 ?
Cl11 C34 Cl9 Cl10 64(2) . . . 2_655 ?
Cl10 C34 Cl9 Cl10 150(2) . . . 2_655 ?
Cl12 C34 Cl9 Cl10 63(2) . . . 2_655 ?
Cl13 C34 Cl9 Cl10 175(2) . . . 2_655 ?
Cl9 C34 Cl9 Cl10 116(5) 2_655 . . 2_655 ?
C34 C34 Cl9 Cl13 -59(3) 2_655 . . . ?
Cl10 C34 Cl9 Cl13 -175(2) 2_655 . . . ?
Cl12 C34 Cl9 Cl13 26.7(18) 2_655 . . . ?
Cl13 C34 Cl9 Cl13 -145.2(18) 2_655 . . . ?
Cl11 C34 Cl9 Cl13 32.8(11) 2_655 . . . ?
Cl11 C34 Cl9 Cl13 -110.7(17) . . . . ?
Cl10 C34 Cl9 Cl13 -25.0(10) . . . . ?
Cl12 C34 Cl9 Cl13 -111.9(14) . . . . ?
Cl9 C34 Cl9 Cl13 -59(3) 2_655 . . . ?
C34 C34 Cl10 Cl13 97(5) 2_655 . . . ?
Cl10 C34 Cl10 Cl13 97(5) 2_655 . . . ?
Cl12 C34 Cl10 Cl13 -78(2) 2_655 . . . ?
Cl13 C34 Cl10 Cl13 147(2) 2_655 . . . ?
Cl11 C34 Cl10 Cl13 -6.6(16) 2_655 . . . ?
Cl11 C34 Cl10 Cl13 149(2) . . . . ?
Cl12 C34 Cl10 Cl13 100.2(18) . . . . ?
Cl9 C34 Cl10 Cl13 -152.8(18) 2_655 . . . ?
Cl9 C34 Cl10 Cl13 46.2(16) . . . . ?
Cl10 C34 Cl10 C34 0.004(7) 2_655 . . 2_655 ?
Cl12 C34 Cl10 C34 -175(6) 2_655 . . 2_655 ?
Cl13 C34 Cl10 C34 50(4) 2_655 . . 2_655 ?
Cl11 C34 Cl10 C34 -104(5) 2_655 . . 2_655 ?
Cl11 C34 Cl10 C34 52(4) . . . 2_655 ?
Cl12 C34 Cl10 C34 3(4) . . . 2_655 ?
Cl13 C34 Cl10 C34 -97(5) . . . 2_655 ?
Cl9 C34 Cl10 C34 110(5) 2_655 . . 2_655 ?
Cl9 C34 Cl10 C34 -51(4) . . . 2_655 ?
C34 C34 Cl10 Cl12 175(6) 2_655 . . 2_655 ?
Cl10 C34 Cl10 Cl12 175(6) 2_655 . . 2_655 ?
Cl13 C34 Cl10 Cl12 -135(3) 2_655 . . 2_655 ?
Cl11 C34 Cl10 Cl12 71.1(19) 2_655 . . 2_655 ?
Cl11 C34 Cl10 Cl12 -133(2) . . . 2_655 ?
Cl12 C34 Cl10 Cl12 178(2) . . . 2_655 ?
Cl13 C34 Cl10 Cl12 78(2) . . . 2_655 ?
Cl9 C34 Cl10 Cl12 -75.1(17) 2_655 . . 2_655 ?
Cl9 C34 Cl10 Cl12 124(2) . . . 2_655 ?
C34 C34 Cl10 Cl11 104(5) 2_655 . . 2_655 ?
Cl10 C34 Cl10 Cl11 104(5) 2_655 . . 2_655 ?
Cl12 C34 Cl10 Cl11 -71.1(19) 2_655 . . 2_655 ?
Cl13 C34 Cl10 Cl11 154(3) 2_655 . . 2_655 ?
Cl11 C34 Cl10 Cl11 156.0(19) . . . 2_655 ?
Cl12 C34 Cl10 Cl11 106.8(19) . . . 2_655 ?
Cl13 C34 Cl10 Cl11 6.6(16) . . . 2_655 ?
Cl9 C34 Cl10 Cl11 -146.2(18) 2_655 . . 2_655 ?
Cl9 C34 Cl10 Cl11 52.8(13) . . . 2_655 ?
C34 C34 Cl10 Cl9 -110(5) 2_655 . . 2_655 ?
Cl10 C34 Cl10 Cl9 -110(5) 2_655 . . 2_655 ?
Cl12 C34 Cl10 Cl9 75.1(17) 2_655 . . 2_655 ?
Cl13 C34 Cl10 Cl9 -60(2) 2_655 . . 2_655 ?
Cl11 C34 Cl10 Cl9 146.2(18) 2_655 . . 2_655 ?
Cl11 C34 Cl10 Cl9 -57.9(13) . . . 2_655 ?
Cl12 C34 Cl10 Cl9 -107.0(16) . . . 2_655 ?
Cl13 C34 Cl10 Cl9 152.8(18) . . . 2_655 ?
Cl9 C34 Cl10 Cl9 -161.0(15) . . . 2_655 ?
C34 C34 Cl10 Cl11 -52(4) 2_655 . . . ?
Cl10 C34 Cl10 Cl11 -52(4) 2_655 . . . ?
Cl12 C34 Cl10 Cl11 133(2) 2_655 . . . ?
Cl13 C34 Cl10 Cl11 -2.1(15) 2_655 . . . ?
Cl11 C34 Cl10 Cl11 -156.0(19) 2_655 . . . ?
Cl12 C34 Cl10 Cl11 -49.1(12) . . . . ?
Cl13 C34 Cl10 Cl11 -149(2) . . . . ?
Cl9 C34 Cl10 Cl11 57.9(13) 2_655 . . . ?
Cl9 C34 Cl10 Cl11 -103.1(17) . . . . ?
C34 C34 Cl11 Cl13 -141(5) 2_655 . . 2_655 ?
Cl10 C34 Cl11 Cl13 -26.0(19) 2_655 . . 2_655 ?
Cl12 C34 Cl11 Cl13 138(3) 2_655 . . 2_655 ?
Cl11 C34 Cl11 Cl13 -141(5) 2_655 . . 2_655 ?
Cl10 C34 Cl11 Cl13 -177(2) . . . 2_655 ?
Cl12 C34 Cl11 Cl13 -85(2) . . . 2_655 ?
Cl13 C34 Cl11 Cl13 -159(3) . . . 2_655 ?
Cl9 C34 Cl11 Cl13 122.0(19) 2_655 . . 2_655 ?
Cl9 C34 Cl11 Cl13 -86(2) . . . 2_655 ?
C34 C34 Cl11 Cl12 -56(4) 2_655 . . . ?
Cl10 C34 Cl11 Cl12 59(2) 2_655 . . . ?
Cl12 C34 Cl11 Cl12 -137(2) 2_655 . . . ?
Cl13 C34 Cl11 Cl12 85(2) 2_655 . . . ?
Cl11 C34 Cl11 Cl12 -56(4) 2_655 . . . ?
Cl10 C34 Cl11 Cl12 -91.6(16) . . . . ?
Cl13 C34 Cl11 Cl12 -73.9(19) . . . . ?
Cl9 C34 Cl11 Cl12 -152.9(17) 2_655 . . . ?
Cl9 C34 Cl11 Cl12 -1.3(16) . . . . ?
Cl10 C34 Cl11 C34 115(5) 2_655 . . 2_655 ?
Cl12 C34 Cl11 C34 -81(4) 2_655 . . 2_655 ?
Cl13 C34 Cl11 C34 141(5) 2_655 . . 2_655 ?
Cl11 C34 Cl11 C34 -0.003(4) 2_655 . . 2_655 ?
Cl10 C34 Cl11 C34 -36(3) . . . 2_655 ?
Cl12 C34 Cl11 C34 56(4) . . . 2_655 ?
Cl13 C34 Cl11 C34 -18(2) . . . 2_655 ?
Cl9 C34 Cl11 C34 -97(4) 2_655 . . 2_655 ?
Cl9 C34 Cl11 C34 54(3) . . . 2_655 ?
C34 C34 Cl11 Cl10 -115(5) 2_655 . . 2_655 ?
Cl12 C34 Cl11 Cl10 164(4) 2_655 . . 2_655 ?
Cl13 C34 Cl11 Cl10 26.0(19) 2_655 . . 2_655 ?
Cl11 C34 Cl11 Cl10 -115(5) 2_655 . . 2_655 ?
Cl10 C34 Cl11 Cl10 -151(2) . . . 2_655 ?
Cl12 C34 Cl11 Cl10 -59(2) . . . 2_655 ?
Cl13 C34 Cl11 Cl10 -133(3) . . . 2_655 ?
Cl9 C34 Cl11 Cl10 148(2) 2_655 . . 2_655 ?
Cl9 C34 Cl11 Cl10 -60.3(19) . . . 2_655 ?
C34 C34 Cl11 Cl9 97(4) 2_655 . . 2_655 ?
Cl10 C34 Cl11 Cl9 -148(2) 2_655 . . 2_655 ?
Cl12 C34 Cl11 Cl9 16(2) 2_655 . . 2_655 ?
Cl13 C34 Cl11 Cl9 -122.0(19) 2_655 . . 2_655 ?
Cl11 C34 Cl11 Cl9 97(4) 2_655 . . 2_655 ?
Cl10 C34 Cl11 Cl9 61.2(14) . . . 2_655 ?
Cl12 C34 Cl11 Cl9 152.9(17) . . . 2_655 ?
Cl13 C34 Cl11 Cl9 79.0(19) . . . 2_655 ?
Cl9 C34 Cl11 Cl9 151.6(16) . . . 2_655 ?
C34 C34 Cl11 Cl10 36(3) 2_655 . . . ?
Cl10 C34 Cl11 Cl10 151(2) 2_655 . . . ?
Cl12 C34 Cl11 Cl10 -45(2) 2_655 . . . ?
Cl13 C34 Cl11 Cl10 177(2) 2_655 . . . ?
Cl11 C34 Cl11 Cl10 36(3) 2_655 . . . ?
Cl12 C34 Cl11 Cl10 91.6(16) . . . . ?
Cl13 C34 Cl11 Cl10 17.7(12) . . . . ?
Cl9 C34 Cl11 Cl10 -61.2(14) 2_655 . . . ?
Cl9 C34 Cl11 Cl10 90.4(16) . . . . ?
Cl13 Cl10 Cl11 Cl13 -31(3) . . . 2_655 ?
C34 Cl10 Cl11 Cl13 -52(3) 2_655 . . 2_655 ?
Cl12 Cl10 Cl11 Cl13 36(2) 2_655 . . 2_655 ?
Cl11 Cl10 Cl11 Cl13 -15.6(16) 2_655 . . 2_655 ?
C34 Cl10 Cl11 Cl13 3(2) . . . 2_655 ?
Cl9 Cl10 Cl11 Cl13 92(2) 2_655 . . 2_655 ?
Cl13 Cl10 Cl11 Cl12 40(2) . . . . ?
C34 Cl10 Cl11 Cl12 19(3) 2_655 . . . ?
Cl12 Cl10 Cl11 Cl12 106.8(16) 2_655 . . . ?
Cl11 Cl10 Cl11 Cl12 55.2(13) 2_655 . . . ?
C34 Cl10 Cl11 Cl12 74(2) . . . . ?
Cl9 Cl10 Cl11 Cl12 162.4(17) 2_655 . . . ?
Cl13 Cl10 Cl11 C34 21(3) . . . 2_655 ?
Cl12 Cl10 Cl11 C34 88(3) 2_655 . . 2_655 ?
Cl11 Cl10 Cl11 C34 36(2) 2_655 . . 2_655 ?
C34 Cl10 Cl11 C34 55(4) . . . 2_655 ?
Cl9 Cl10 Cl11 C34 144(3) 2_655 . . 2_655 ?
Cl13 Cl10 Cl11 C34 -34(2) . . . . ?
C34 Cl10 Cl11 C34 -55(4) 2_655 . . . ?
Cl12 Cl10 Cl11 C34 33.0(18) 2_655 . . . ?
Cl11 Cl10 Cl11 C34 -18.6(16) 2_655 . . . ?
Cl9 Cl10 Cl11 C34 88.6(18) 2_655 . . . ?
Cl13 Cl10 Cl11 Cl10 -15.1(15) . . . 2_655 ?
C34 Cl10 Cl11 Cl10 -36(2) 2_655 . . 2_655 ?
Cl12 Cl10 Cl11 Cl10 51.6(12) 2_655 . . 2_655 ?
Cl11 Cl10 Cl11 Cl10 0.001(1) 2_655 . . 2_655 ?
C34 Cl10 Cl11 Cl10 18.6(16) . . . 2_655 ?
Cl9 Cl10 Cl11 Cl10 107.2(14) 2_655 . . 2_655 ?
Cl13 Cl10 Cl11 Cl9 -122(2) . . . 2_655 ?
C34 Cl10 Cl11 Cl9 -144(3) 2_655 . . 2_655 ?
Cl12 Cl10 Cl11 Cl9 -55.6(13) 2_655 . . 2_655 ?
Cl11 Cl10 Cl11 Cl9 -107.2(14) 2_655 . . 2_655 ?
C34 Cl10 Cl11 Cl9 -88.6(18) . . . 2_655 ?
Cl13 Cl11 Cl12 C34 104(2) 2_655 . . 2_655 ?
C34 Cl11 Cl12 C34 40(2) . . . 2_655 ?
Cl10 Cl11 Cl12 C34 82(2) 2_655 . . 2_655 ?
Cl9 Cl11 Cl12 C34 8(2) 2_655 . . 2_655 ?
Cl10 Cl11 Cl12 C34 -10.4(15) . . . 2_655 ?
Cl13 Cl11 Cl12 Cl10 21.1(15) 2_655 . . 2_655 ?
C34 Cl11 Cl12 Cl10 -82(2) 2_655 . . 2_655 ?
C34 Cl11 Cl12 Cl10 -42.8(14) . . . 2_655 ?
Cl9 Cl11 Cl12 Cl10 -75(2) 2_655 . . 2_655 ?
Cl10 Cl11 Cl12 Cl10 -92.9(13) . . . 2_655 ?
C34 Cl11 Cl12 Cl13 -104(2) 2_655 . . 2_655 ?
C34 Cl11 Cl12 Cl13 -64.0(16) . . . 2_655 ?
Cl10 Cl11 Cl12 Cl13 -21.1(15) 2_655 . . 2_655 ?
Cl9 Cl11 Cl12 Cl13 -96(2) 2_655 . . 2_655 ?
Cl10 Cl11 Cl12 Cl13 -114.0(16) . . . 2_655 ?
Cl13 Cl11 Cl12 Cl9 66(2) 2_655 . . . ?
C34 Cl11 Cl12 Cl9 -38(2) 2_655 . . . ?
C34 Cl11 Cl12 Cl9 2(2) . . . . ?
Cl10 Cl11 Cl12 Cl9 45(2) 2_655 . . . ?
Cl9 Cl11 Cl12 Cl9 -30(4) 2_655 . . . ?
Cl10 Cl11 Cl12 Cl9 -48(2) . . . . ?
Cl13 Cl11 Cl12 C34 64.0(16) 2_655 . . . ?
C34 Cl11 Cl12 C34 -40(2) 2_655 . . . ?
Cl10 Cl11 Cl12 C34 42.8(14) 2_655 . . . ?
Cl9 Cl11 Cl12 C34 -32(2) 2_655 . . . ?
Cl10 Cl11 Cl12 C34 -50.0(14) . . . . ?
Cl11 Cl9 Cl12 C34 -12.4(17) 2_655 . . 2_655 ?
Cl10 Cl9 Cl12 C34 -80.9(19) 2_655 . . 2_655 ?
C34 Cl9 Cl12 C34 -37(2) . . . 2_655 ?
Cl13 Cl9 Cl12 C34 9.2(14) . . . 2_655 ?
Cl11 Cl9 Cl12 Cl11 23(3) 2_655 . . . ?
C34 Cl9 Cl12 Cl11 36(2) 2_655 . . . ?
Cl10 Cl9 Cl12 Cl11 -45(2) 2_655 . . . ?
C34 Cl9 Cl12 Cl11 -2(2) . . . . ?
Cl13 Cl9 Cl12 Cl11 45(2) . . . . ?
Cl11 Cl9 Cl12 Cl10 68.5(15) 2_655 . . 2_655 ?
C34 Cl9 Cl12 Cl10 80.9(19) 2_655 . . 2_655 ?
C34 Cl9 Cl12 Cl10 43.4(13) . . . 2_655 ?
Cl13 Cl9 Cl12 Cl10 90.0(13) . . . 2_655 ?
Cl11 Cl9 Cl12 Cl13 58.6(17) 2_655 . . 2_655 ?
C34 Cl9 Cl12 Cl13 71.0(18) 2_655 . . 2_655 ?
Cl10 Cl9 Cl12 Cl13 -9.9(12) 2_655 . . 2_655 ?
C34 Cl9 Cl12 Cl13 33.5(13) . . . 2_655 ?
Cl13 Cl9 Cl12 Cl13 80.1(13) . . . 2_655 ?
Cl11 Cl9 Cl12 C34 25.1(15) 2_655 . . . ?
C34 Cl9 Cl12 C34 37(2) 2_655 . . . ?
Cl10 Cl9 Cl12 C34 -43.4(13) 2_655 . . . ?
Cl13 Cl9 Cl12 C34 46.6(12) . . . . ?
Cl10 C34 Cl12 C34 175(6) 2_655 . . 2_655 ?
Cl12 C34 Cl12 C34 -0.003(7) 2_655 . . 2_655 ?
Cl13 C34 Cl12 C34 -132(5) 2_655 . . 2_655 ?
Cl11 C34 Cl12 C34 60(4) 2_655 . . 2_655 ?
Cl11 C34 Cl12 C34 -89(4) . . . 2_655 ?
Cl10 C34 Cl12 C34 -3(3) . . . 2_655 ?
Cl13 C34 Cl12 C34 30(3) . . . 2_655 ?
Cl9 C34 Cl12 C34 -65(4) 2_655 . . 2_655 ?
Cl9 C34 Cl12 C34 90(4) . . . 2_655 ?
C34 C34 Cl12 Cl11 89(4) 2_655 . . . ?
Cl10 C34 Cl12 Cl11 -97(2) 2_655 . . . ?
Cl12 C34 Cl12 Cl11 89(4) 2_655 . . . ?
Cl13 C34 Cl12 Cl11 -43.3(13) 2_655 . . . ?
Cl11 C34 Cl12 Cl11 148(2) 2_655 . . . ?
Cl10 C34 Cl12 Cl11 85.5(17) . . . . ?
Cl13 C34 Cl12 Cl11 118.1(18) . . . . ?
Cl9 C34 Cl12 Cl11 23.9(15) 2_655 . . . ?
Cl9 C34 Cl12 Cl11 178.5(19) . . . . ?
C34 C34 Cl12 Cl10 -175(6) 2_655 . . 2_655 ?
Cl12 C34 Cl12 Cl10 -175(6) 2_655 . . 2_655 ?
Cl13 C34 Cl12 Cl10 53.6(17) 2_655 . . 2_655 ?
Cl11 C34 Cl12 Cl10 -115(3) 2_655 . . 2_655 ?
Cl11 C34 Cl12 Cl10 97(2) . . . 2_655 ?
Cl10 C34 Cl12 Cl10 -178(3) . . . 2_655 ?
Cl13 C34 Cl12 Cl10 -145(3) . . . 2_655 ?
Cl9 C34 Cl12 Cl10 121(3) 2_655 . . 2_655 ?
Cl9 C34 Cl12 Cl10 -85(2) . . . 2_655 ?
C34 C34 Cl12 Cl13 132(5) 2_655 . . 2_655 ?
Cl10 C34 Cl12 Cl13 -53.6(17) 2_655 . . 2_655 ?
Cl12 C34 Cl12 Cl13 132(5) 2_655 . . 2_655 ?
Cl11 C34 Cl12 Cl13 -169(3) 2_655 . . 2_655 ?
Cl11 C34 Cl12 Cl13 43.3(13) . . . 2_655 ?
Cl10 C34 Cl12 Cl13 129(2) . . . 2_655 ?
Cl13 C34 Cl12 Cl13 161(2) . . . 2_655 ?
Cl9 C34 Cl12 Cl13 67.2(16) 2_655 . . 2_655 ?
Cl9 C34 Cl12 Cl13 -138.3(16) . . . 2_655 ?
C34 C34 Cl12 Cl9 -90(4) 2_655 . . . ?
Cl10 C34 Cl12 Cl9 85(2) 2_655 . . . ?
Cl12 C34 Cl12 Cl9 -90(4) 2_655 . . . ?
Cl13 C34 Cl12 Cl9 138.3(16) 2_655 . . . ?
Cl11 C34 Cl12 Cl9 -30.4(18) 2_655 . . . ?
Cl11 C34 Cl12 Cl9 -178.5(19) . . . . ?
Cl10 C34 Cl12 Cl9 -92.9(15) . . . . ?
Cl13 C34 Cl12 Cl9 -60.3(13) . . . . ?
Cl9 C34 Cl12 Cl9 -154.6(17) 2_655 . . . ?
C34 Cl10 Cl13 Cl11 48(3) 2_655 . . 2_655 ?
Cl12 Cl10 Cl13 Cl11 -38(3) 2_655 . . 2_655 ?
C34 Cl10 Cl13 Cl11 12(3) . . . 2_655 ?
Cl9 Cl10 Cl13 Cl11 -20(4) 2_655 . . 2_655 ?
Cl11 Cl10 Cl13 Cl11 36(3) . . . 2_655 ?
Cl12 Cl10 Cl13 C34 -85(2) 2_655 . . 2_655 ?
Cl11 Cl10 Cl13 C34 -48(3) 2_655 . . 2_655 ?
C34 Cl10 Cl13 C34 -36(2) . . . 2_655 ?
Cl9 Cl10 Cl13 C34 -68(3) 2_655 . . 2_655 ?
Cl11 Cl10 Cl13 C34 -12.0(16) . . . 2_655 ?
C34 Cl10 Cl13 Cl12 85(2) 2_655 . . 2_655 ?
Cl11 Cl10 Cl13 Cl12 38(3) 2_655 . . 2_655 ?
C34 Cl10 Cl13 Cl12 49.3(13) . . . 2_655 ?
Cl9 Cl10 Cl13 Cl12 17(2) 2_655 . . 2_655 ?
Cl11 Cl10 Cl13 Cl12 73.4(17) . . . 2_655 ?
C34 Cl10 Cl13 C34 36(2) 2_655 . . . ?
Cl12 Cl10 Cl13 C34 -49.3(13) 2_655 . . . ?
Cl11 Cl10 Cl13 C34 -12(3) 2_655 . . . ?
Cl9 Cl10 Cl13 C34 -32(2) 2_655 . . . ?
Cl11 Cl10 Cl13 C34 24.1(16) . . . . ?
C34 Cl10 Cl13 Cl9 -9(2) 2_655 . . . ?
Cl12 Cl10 Cl13 Cl9 -94.5(13) 2_655 . . . ?
Cl11 Cl10 Cl13 Cl9 -57(2) 2_655 . . . ?
C34 Cl10 Cl13 Cl9 -45.2(15) . . . . ?
Cl9 Cl10 Cl13 Cl9 -77(2) 2_655 . . . ?
Cl11 Cl10 Cl13 Cl9 -21(2) . . . . ?
C34 C34 Cl13 Cl11 138(5) 2_655 . . 2_655 ?
Cl10 C34 Cl13 Cl11 69(4) 2_655 . . 2_655 ?
Cl12 C34 Cl13 Cl11 -89(2) 2_655 . . 2_655 ?
Cl13 C34 Cl13 Cl11 138(5) 2_655 . . 2_655 ?
Cl11 C34 Cl13 Cl11 158(3) . . . 2_655 ?
Cl10 C34 Cl13 Cl11 -168(3) . . . 2_655 ?
Cl12 C34 Cl13 Cl11 111(2) . . . 2_655 ?
Cl9 C34 Cl13 Cl11 -144(2) 2_655 . . 2_655 ?
Cl9 C34 Cl13 Cl11 62.1(19) . . . 2_655 ?
C34 C34 Cl13 Cl10 -54(4) 2_655 . . . ?
Cl10 C34 Cl13 Cl10 -123(4) 2_655 . . . ?
Cl12 C34 Cl13 Cl10 79(2) 2_655 . . . ?
Cl13 C34 Cl13 Cl10 -54(4) 2_655 . . . ?
Cl11 C34 Cl13 Cl10 168(3) 2_655 . . . ?
Cl11 C34 Cl13 Cl10 -34(2) . . . . ?
Cl12 C34 Cl13 Cl10 -80.5(19) . . . . ?
Cl9 C34 Cl13 Cl10 24.1(16) 2_655 . . . ?
Cl9 C34 Cl13 Cl10 -129.4(18) . . . . ?
Cl10 C34 Cl13 C34 -69(4) 2_655 . . 2_655 ?
Cl12 C34 Cl13 C34 133(5) 2_655 . . 2_655 ?
Cl13 C34 Cl13 C34 0.003(3) 2_655 . . 2_655 ?
Cl11 C34 Cl13 C34 -138(5) 2_655 . . 2_655 ?
Cl11 C34 Cl13 C34 20(2) . . . 2_655 ?
Cl10 C34 Cl13 C34 54(4) . . . 2_655 ?
Cl12 C34 Cl13 C34 -27(3) . . . 2_655 ?
Cl9 C34 Cl13 C34 78(4) 2_655 . . 2_655 ?
Cl9 C34 Cl13 C34 -75(4) . . . 2_655 ?
C34 C34 Cl13 Cl12 -133(5) 2_655 . . 2_655 ?
Cl10 C34 Cl13 Cl12 158(5) 2_655 . . 2_655 ?
Cl13 C34 Cl13 Cl12 -133(5) 2_655 . . 2_655 ?
Cl11 C34 Cl13 Cl12 89(2) 2_655 . . 2_655 ?
Cl11 C34 Cl13 Cl12 -113(3) . . . 2_655 ?
Cl10 C34 Cl13 Cl12 -79(2) . . . 2_655 ?
Cl12 C34 Cl13 Cl12 -160(2) . . . 2_655 ?
Cl9 C34 Cl13 Cl12 -55.0(16) 2_655 . . 2_655 ?
Cl9 C34 Cl13 Cl12 151(2) . . . 2_655 ?
C34 C34 Cl13 Cl9 75(4) 2_655 . . . ?
Cl10 C34 Cl13 Cl9 6(3) 2_655 . . . ?
Cl12 C34 Cl13 Cl9 -151(2) 2_655 . . . ?
Cl13 C34 Cl13 Cl9 75(4) 2_655 . . . ?
Cl11 C34 Cl13 Cl9 -62.1(19) 2_655 . . . ?
Cl11 C34 Cl13 Cl9 96(2) . . . . ?
Cl10 C34 Cl13 Cl9 129.4(18) . . . . ?
Cl12 C34 Cl13 Cl9 48.9(12) . . . . ?
Cl9 C34 Cl13 Cl9 153.5(15) 2_655 . . . ?
Cl12 Cl9 Cl13 Cl11 -120(2) . . . 2_655 ?
C34 Cl9 Cl13 Cl11 -111(2) 2_655 . . 2_655 ?
Cl10 Cl9 Cl13 Cl11 -71.7(19) 2_655 . . 2_655 ?
C34 Cl9 Cl13 Cl11 -69(2) . . . 2_655 ?
Cl12 Cl9 Cl13 Cl10 -0.8(18) . . . . ?
Cl11 Cl9 Cl13 Cl10 119(3) 2_655 . . . ?
C34 Cl9 Cl13 Cl10 9(2) 2_655 . . . ?
Cl10 Cl9 Cl13 Cl10 48(2) 2_655 . . . ?
C34 Cl9 Cl13 Cl10 50.5(18) . . . . ?
Cl12 Cl9 Cl13 C34 -9.4(15) . . . 2_655 ?
Cl11 Cl9 Cl13 C34 111(2) 2_655 . . 2_655 ?
Cl10 Cl9 Cl13 C34 39.1(14) 2_655 . . 2_655 ?
C34 Cl9 Cl13 C34 42(2) . . . 2_655 ?
Cl12 Cl9 Cl13 Cl12 -71.7(14) . . . 2_655 ?
Cl11 Cl9 Cl13 Cl12 48.5(19) 2_655 . . 2_655 ?
C34 Cl9 Cl13 Cl12 -62.3(15) 2_655 . . 2_655 ?
Cl10 Cl9 Cl13 Cl12 -23.2(12) 2_655 . . 2_655 ?
C34 Cl9 Cl13 Cl12 -20.4(14) . . . 2_655 ?
Cl12 Cl9 Cl13 C34 -51.3(13) . . . . ?
Cl11 Cl9 Cl13 C34 69(2) 2_655 . . . ?
C34 Cl9 Cl13 C34 -42(2) 2_655 . . . ?
Cl10 Cl9 Cl13 C34 -2.8(13) 2_655 . . . ?
