#------------------------------------------------------------------------------
#$Date: 2016-02-14 06:40:26 +0200 (Sun, 14 Feb 2016) $
#$Revision: 176432 $
#$URL: svn://www.crystallography.net/cod/cif/7/01/46/7014644.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7014644
loop_
_publ_author_name
'Liu, Hai-Yan'
'Wu, Hua'
'Ma, Jian-Fang'
'Liu, Ying-Ying'
'Yang, Jin'
'Ma, Ji-Cheng'
_publ_section_title
;
 Inorganic-organic hybrid compounds based on octamolybdates and
 metal-organic fragments with flexible multidentate ligand: syntheses,
 structures and characterization.
;
_journal_issue                   3
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              602
_journal_page_last               613
_journal_paper_doi               10.1039/c0dt01024c
_journal_volume                  40
_journal_year                    2011
_chemical_formula_moiety         'C36 H42 Ag4 Mo8 N18 O26'
_chemical_formula_sum            'C36 H42 Ag4 Mo8 N18 O26'
_chemical_formula_weight         2341.88
_chemical_name_systematic
;
?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                115.199(12)
_cell_angle_beta                 93.897(10)
_cell_angle_gamma                101.029(11)
_cell_formula_units_Z            1
_cell_length_a                   11.4063(14)
_cell_length_b                   11.8303(16)
_cell_length_c                   12.2270(14)
_cell_measurement_reflns_used    5139
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      67.2
_cell_measurement_theta_min      4.1
_cell_volume                     1444.4(4)
_computing_cell_refinement       CrysAlis
_computing_data_collection       'CrysAlis (Oxford Diffraction, 2006)'
_computing_data_reduction        CrysAlis
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      293(2)
_diffrn_detector_area_resol_mean 10.0
_diffrn_measured_fraction_theta_full 0.994
_diffrn_measured_fraction_theta_max 0.994
_diffrn_measurement_device_type  'Oxford Diffraction Gemini R Ultra'
_diffrn_measurement_method       'ω scan'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.54184
_diffrn_reflns_av_R_equivalents  0.0666
_diffrn_reflns_av_sigmaI/netI    0.0608
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       14
_diffrn_reflns_limit_k_min       -14
_diffrn_reflns_limit_l_max       14
_diffrn_reflns_limit_l_min       -14
_diffrn_reflns_number            16362
_diffrn_reflns_theta_full        67.21
_diffrn_reflns_theta_max         67.21
_diffrn_reflns_theta_min         4.05
_exptl_absorpt_coefficient_mu    25.192
_exptl_absorpt_correction_T_max  0.24
_exptl_absorpt_correction_T_min  0.10
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
CrysAlis (Oxford Diffraction, 2006)
;
_exptl_crystal_colour            brown
_exptl_crystal_density_diffrn    2.692
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             1116
_exptl_crystal_size_max          0.12
_exptl_crystal_size_mid          0.10
_exptl_crystal_size_min          0.06
_refine_diff_density_max         1.279
_refine_diff_density_min         -1.981
_refine_diff_density_rms         0.236
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.994
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     418
_refine_ls_number_reflns         5139
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      0.994
_refine_ls_R_factor_all          0.0774
_refine_ls_R_factor_gt           0.0519
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0951P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1287
_refine_ls_wR_factor_ref         0.1441
_reflns_number_gt                3739
_reflns_number_total             5139
_reflns_threshold_expression     >2σ(I)
_cod_data_source_file            C0DT01024C.TXT
_cod_data_source_block           6
_cod_original_cell_volume        1444.4(3)
_cod_original_sg_symbol_Hall     '-P 1 '
_cod_original_sg_symbol_H-M      'P -1 '
_cod_database_code               7014644
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
C1 C 0.3223(11) 0.0026(10) 0.4931(10) 0.045(3) Uani 1 1 d . . .
H1 H 0.2812 -0.0812 0.4384 0.054 Uiso 1 1 calc R . .
C2 C 0.3878(9) 0.1727(9) 0.6577(9) 0.037(2) Uani 1 1 d . . .
H2 H 0.4035 0.2342 0.7393 0.044 Uiso 1 1 calc R . .
C3 C 0.5173(9) 0.3061(9) 0.5751(8) 0.035(2) Uani 1 1 d . . .
H3A H 0.6006 0.3011 0.5878 0.042 Uiso 1 1 calc R . .
H3B H 0.5064 0.3806 0.6453 0.042 Uiso 1 1 calc R . .
C4 C 0.4936(8) 0.3232(8) 0.4609(9) 0.032(2) Uani 1 1 d . . .
C5 C 0.3804(8) 0.3400(8) 0.4300(9) 0.032(2) Uani 1 1 d . . .
C6 C 0.3534(8) 0.3466(8) 0.3187(8) 0.0275(18) Uani 1 1 d . . .
C7 C 0.4417(8) 0.3450(9) 0.2432(9) 0.0297(19) Uani 1 1 d . . .
C8 C 0.5569(7) 0.3324(8) 0.2792(8) 0.0246(17) Uani 1 1 d . . .
C9 C 0.5808(7) 0.3183(8) 0.3859(8) 0.0267(18) Uani 1 1 d . . .
C10 C 0.7028(9) 0.2986(12) 0.4222(9) 0.043(2) Uani 1 1 d . . .
H10A H 0.7274 0.3462 0.5095 0.065 Uiso 1 1 calc R . .
H10B H 0.7621 0.3286 0.3823 0.065 Uiso 1 1 calc R . .
H10C H 0.6959 0.2087 0.3978 0.065 Uiso 1 1 calc R . .
C11 C 0.4134(10) 0.3554(11) 0.1258(10) 0.043(2) Uani 1 1 d . . .
H11A H 0.3439 0.2880 0.0745 0.064 Uiso 1 1 calc R . .
H11B H 0.4817 0.3470 0.0837 0.064 Uiso 1 1 calc R . .
H11C H 0.3967 0.4376 0.1446 0.064 Uiso 1 1 calc R . .
C12 C 0.2259(9) 0.3476(11) 0.2782(12) 0.047(3) Uani 1 1 d . . .
H12A H 0.2042 0.4215 0.3398 0.057 Uiso 1 1 calc R . .
H12B H 0.2216 0.3553 0.2022 0.057 Uiso 1 1 calc R . .
C13 C 0.2869(9) 0.3480(9) 0.5126(10) 0.037(2) Uani 1 1 d . . .
H13A H 0.2353 0.2638 0.4869 0.056 Uiso 1 1 calc R . .
H13B H 0.2391 0.4049 0.5079 0.056 Uiso 1 1 calc R . .
H13C H 0.3267 0.3805 0.5955 0.056 Uiso 1 1 calc R . .
C14 C 0.6537(9) 0.3315(10) 0.2009(9) 0.037(2) Uani 1 1 d . . .
H14A H 0.6451 0.3883 0.1640 0.044 Uiso 1 1 calc R . .
H14B H 0.7325 0.3654 0.2529 0.044 Uiso 1 1 calc R . .
C15 C 0.0252(9) 0.2162(10) 0.2807(9) 0.037(2) Uani 1 1 d . . .
H15 H -0.0145 0.2824 0.3089 0.045 Uiso 1 1 calc R . .
C16 C 0.0715(11) 0.0358(11) 0.2258(14) 0.064(4) Uani 1 1 d . . .
H16 H 0.0672 -0.0489 0.2110 0.076 Uiso 1 1 calc R . .
C17 C 0.6843(14) 0.0204(12) 0.0191(13) 0.063(3) Uani 1 1 d . . .
H17 H 0.7108 -0.0533 0.0061 0.075 Uiso 1 1 calc R . .
C18 C 0.6058(10) 0.1529(11) -0.0120(10) 0.045(2) Uani 1 1 d . . .
H18 H 0.5666 0.1925 -0.0495 0.055 Uiso 1 1 calc R . .
N1 N 0.4354(7) 0.1885(7) 0.5668(7) 0.0286(16) Uani 1 1 d . . .
N2 N 0.3939(8) 0.0824(8) 0.4621(7) 0.0395(19) Uani 1 1 d . . .
N3 N 0.3162(8) 0.0581(9) 0.6144(8) 0.045(2) Uani 1 1 d . . .
N4 N 0.6489(7) 0.2041(8) 0.1042(7) 0.0359(18) Uani 1 1 d . . .
N5 N 0.7012(11) 0.1217(11) 0.1293(9) 0.059(3) Uani 1 1 d . . .
N6 N 0.6256(10) 0.0354(9) -0.0705(9) 0.050(2) Uani 1 1 d . . .
N7 N 0.1392(7) 0.2284(7) 0.2597(7) 0.0324(17) Uani 1 1 d . . .
N8 N 0.1693(8) 0.1145(9) 0.2212(10) 0.056(3) Uani 1 1 d . . .
N9 N -0.0221(8) 0.0947(8) 0.2550(9) 0.043(2) Uani 1 1 d . . .
O1 O 0.0130(5) -0.3933(5) 0.1118(5) 0.0253(12) Uani 1 1 d . . .
O2 O 0.1795(5) -0.3954(5) -0.0235(5) 0.0268(12) Uani 1 1 d . . .
O3 O 0.2299(7) -0.1786(7) 0.2020(7) 0.0471(18) Uani 1 1 d . . .
O4 O 0.3694(6) -0.3469(8) 0.1637(6) 0.0461(18) Uani 1 1 d . . .
O5 O 0.1824(6) -0.3523(8) 0.2974(6) 0.0430(17) Uani 1 1 d . . .
O6 O 0.0191(7) -0.3603(13) 0.4628(7) 0.079(3) Uani 1 1 d . . .
O7 O 0.0454(8) -0.1770(10) 0.3833(11) 0.087(4) Uani 1 1 d . . .
O8 O -0.1457(6) -0.3891(7) 0.2631(6) 0.0358(15) Uani 1 1 d . . .
O9 O -0.3405(6) -0.4374(7) 0.0912(7) 0.0419(16) Uani 1 1 d . . .
O10 O -0.1632(7) -0.2256(7) 0.1533(7) 0.0498(19) Uani 1 1 d . . .
O11 O -0.1594(5) -0.4394(6) -0.0609(6) 0.0294(13) Uani 1 1 d . . .
O12 O 0.0071(6) -0.4461(7) -0.2182(6) 0.0354(14) Uani 1 1 d . . .
O13 O 0.0319(6) -0.2260(6) -0.0121(7) 0.0403(16) Uani 1 1 d . . .
Mo1 Mo 0.02144(7) -0.33839(9) 0.33418(7) 0.0455(3) Uani 1 1 d . . .
Mo2 Mo -0.18765(6) -0.38464(7) 0.11162(6) 0.02754(19) Uani 1 1 d . . .
Mo3 Mo 0.01482(6) -0.38491(6) -0.05961(6) 0.02485(19) Uani 1 1 d . . .
Mo4 Mo 0.22252(6) -0.33725(7) 0.15626(6) 0.0291(2) Uani 1 1 d . . .
Ag1 Ag 0.17519(8) -0.01196(8) 0.69283(9) 0.0585(3) Uani 1 1 d . . .
Ag2 Ag 0.36767(8) 0.05671(8) 0.26648(7) 0.0517(2) Uani 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mo Mo -0.0483 2.7339 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag 0.1306 4.2820 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N2 C1 N3 111.7(9) . . ?
N3 C2 N1 109.5(8) . . ?
N1 C3 C4 111.9(7) . . ?
C9 C4 C5 120.7(9) . . ?
C9 C4 C3 121.0(8) . . ?
C5 C4 C3 118.3(9) . . ?
C4 C5 C6 119.1(8) . . ?
C4 C5 C13 120.7(9) . . ?
C6 C5 C13 120.3(9) . . ?
C7 C6 C5 120.9(8) . . ?
C7 C6 C12 120.3(9) . . ?
C5 C6 C12 118.7(8) . . ?
C6 C7 C8 118.6(8) . . ?
C6 C7 C11 120.7(8) . . ?
C8 C7 C11 120.7(8) . . ?
C9 C8 C7 120.3(8) . . ?
C9 C8 C14 119.9(8) . . ?
C7 C8 C14 119.8(8) . . ?
C4 C9 C8 120.4(8) . . ?
C4 C9 C10 119.0(9) . . ?
C8 C9 C10 120.6(8) . . ?
N7 C12 C6 110.9(8) . . ?
N4 C14 C8 113.4(8) . . ?
N9 C15 N7 109.1(9) . . ?
N8 C16 N9 111.8(10) . . ?
N5 C17 N6 113.5(11) . . ?
N4 C18 N6 110.7(10) . . ?
N2 N1 C2 109.7(8) . . ?
N2 N1 C3 123.0(7) . . ?
C2 N1 C3 127.2(8) . . ?
C1 N2 N1 104.3(8) . . ?
C1 N2 Ag2 120.2(7) . . ?
N1 N2 Ag2 130.1(6) . . ?
C2 N3 C1 104.7(9) . . ?
C2 N3 Ag1 128.9(7) . . ?
C1 N3 Ag1 123.6(7) . . ?
C18 N4 N5 110.0(9) . . ?
C18 N4 C14 129.8(9) . . ?
N5 N4 C14 120.1(8) . . ?
C17 N5 N4 102.6(10) . . ?
C18 N6 C17 103.2(10) . . ?
C18 N6 Ag2 123.3(8) . 2_655 ?
C17 N6 Ag2 128.2(8) . 2_655 ?
C15 N7 N8 110.4(8) . . ?
C15 N7 C12 127.2(8) . . ?
N8 N7 C12 122.4(8) . . ?
C16 N8 N7 103.8(9) . . ?
C16 N8 Ag2 112.8(9) . . ?
N7 N8 Ag2 131.6(6) . . ?
C15 N9 C16 104.6(9) . . ?
C15 N9 Ag1 130.6(7) . 2_556 ?
C16 N9 Ag1 121.1(8) . 2_556 ?
Mo3 O1 Mo2 92.6(2) . . ?
Mo3 O1 Mo4 91.9(2) . . ?
Mo2 O1 Mo4 162.4(3) . . ?
Mo3 O1 Mo3 104.5(2) . 2_545 ?
Mo2 O1 Mo3 98.0(2) . 2_545 ?
Mo4 O1 Mo3 97.3(2) . 2_545 ?
Mo3 O1 Mo1 164.5(3) . . ?
Mo2 O1 Mo1 85.75(18) . . ?
Mo4 O1 Mo1 85.36(19) . . ?
Mo3 O1 Mo1 91.0(2) 2_545 . ?
Mo3 O2 Mo4 109.1(3) . . ?
Mo3 O2 Mo2 109.3(2) . 2_545 ?
Mo4 O2 Mo2 103.5(2) . 2_545 ?
Mo4 O5 Mo1 117.3(4) . . ?
Mo2 O8 Mo1 118.5(3) . . ?
Mo3 O11 Mo2 108.8(3) . . ?
Mo3 O11 Mo4 110.0(3) . 2_545 ?
Mo2 O11 Mo4 105.6(3) . 2_545 ?
Mo3 O12 Mo1 119.3(3) . 2_545 ?
O7 Mo1 O6 105.6(6) . . ?
O7 Mo1 O8 99.0(4) . . ?
O6 Mo1 O8 103.4(3) . . ?
O7 Mo1 O5 97.1(4) . . ?
O6 Mo1 O5 103.3(4) . . ?
O8 Mo1 O5 143.7(3) . . ?
O7 Mo1 O12 164.3(5) . 2_545 ?
O6 Mo1 O12 90.1(5) . 2_545 ?
O8 Mo1 O12 77.9(3) . 2_545 ?
O5 Mo1 O12 77.9(3) . 2_545 ?
O7 Mo1 O1 95.4(5) . . ?
O6 Mo1 O1 159.0(5) . . ?
O8 Mo1 O1 73.0(2) . . ?
O5 Mo1 O1 73.3(2) . . ?
O12 Mo1 O1 68.9(2) 2_545 . ?
O10 Mo2 O9 104.7(4) . . ?
O10 Mo2 O8 102.8(4) . . ?
O9 Mo2 O8 99.1(3) . . ?
O10 Mo2 O11 97.3(3) . . ?
O9 Mo2 O11 101.6(3) . . ?
O8 Mo2 O11 146.3(3) . . ?
O10 Mo2 O1 96.3(3) . . ?
O9 Mo2 O1 158.8(3) . . ?
O8 Mo2 O1 77.8(2) . . ?
O11 Mo2 O1 73.3(2) . . ?
O10 Mo2 O2 164.8(3) . 2_545 ?
O9 Mo2 O2 87.4(3) . 2_545 ?
O8 Mo2 O2 84.0(2) . 2_545 ?
O11 Mo2 O2 70.8(2) . 2_545 ?
O1 Mo2 O2 71.5(2) . 2_545 ?
O13 Mo3 O12 103.5(3) . . ?
O13 Mo3 O2 102.1(3) . . ?
O12 Mo3 O2 96.6(3) . . ?
O13 Mo3 O11 100.8(3) . . ?
O12 Mo3 O11 96.9(3) . . ?
O2 Mo3 O11 149.8(2) . . ?
O13 Mo3 O1 100.3(3) . . ?
O12 Mo3 O1 156.2(3) . . ?
O2 Mo3 O1 79.0(2) . . ?
O11 Mo3 O1 77.8(2) . . ?
O13 Mo3 O1 175.6(3) . 2_545 ?
O12 Mo3 O1 80.7(3) . 2_545 ?
O2 Mo3 O1 78.3(2) . 2_545 ?
O11 Mo3 O1 77.4(2) . 2_545 ?
O1 Mo3 O1 75.5(2) . 2_545 ?
O13 Mo3 Mo4 92.1(3) . . ?
O12 Mo3 Mo4 132.6(2) . . ?
O2 Mo3 Mo4 36.06(17) . . ?
O11 Mo3 Mo4 123.96(18) . . ?
O1 Mo3 Mo4 46.21(14) . . ?
O1 Mo3 Mo4 85.69(14) 2_545 . ?
O3 Mo4 O4 104.7(4) . . ?
O3 Mo4 O5 100.2(4) . . ?
O4 Mo4 O5 101.6(3) . . ?
O3 Mo4 O2 97.2(3) . . ?
O4 Mo4 O2 99.5(3) . . ?
O5 Mo4 O2 148.1(3) . . ?
O3 Mo4 O1 92.8(3) . . ?
O4 Mo4 O1 162.0(3) . . ?
O5 Mo4 O1 78.9(2) . . ?
O2 Mo4 O1 73.7(2) . . ?
O3 Mo4 O11 163.3(3) . 2_545 ?
O4 Mo4 O11 89.9(3) . 2_545 ?
O5 Mo4 O11 84.3(3) . 2_545 ?
O2 Mo4 O11 72.0(2) . 2_545 ?
O1 Mo4 O11 72.1(2) . 2_545 ?
O3 Mo4 Mo3 85.0(3) . . ?
O4 Mo4 Mo3 134.4(2) . . ?
O5 Mo4 Mo3 120.8(2) . . ?
O2 Mo4 Mo3 34.88(16) . . ?
O1 Mo4 Mo3 41.89(14) . . ?
O11 Mo4 Mo3 78.90(15) 2_545 . ?
N9 Ag1 N3 171.9(4) 2_556 . ?
N6 Ag2 N2 155.9(4) 2_655 . ?
N6 Ag2 N8 90.0(4) 2_655 . ?
N2 Ag2 N8 109.4(4) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
C1 N2 1.324(14) . ?
C1 N3 1.356(14) . ?
C2 N3 1.301(13) . ?
C2 N1 1.335(13) . ?
C3 N1 1.480(11) . ?
C3 C4 1.508(14) . ?
C4 C9 1.391(13) . ?
C4 C5 1.394(14) . ?
C5 C6 1.413(14) . ?
C5 C13 1.506(13) . ?
C6 C7 1.409(13) . ?
C6 C12 1.508(14) . ?
C7 C8 1.412(13) . ?
C7 C11 1.511(13) . ?
C8 C9 1.399(13) . ?
C8 C14 1.508(12) . ?
C9 C10 1.522(13) . ?
C12 N7 1.477(13) . ?
C14 N4 1.454(13) . ?
C15 N9 1.323(14) . ?
C15 N7 1.335(12) . ?
C16 N8 1.330(16) . ?
C16 N9 1.372(15) . ?
C17 N5 1.338(17) . ?
C17 N6 1.338(17) . ?
C18 N4 1.299(14) . ?
C18 N6 1.338(15) . ?
N1 N2 1.327(11) . ?
N2 Ag2 2.270(8) . ?
N3 Ag1 2.137(9) . ?
N4 N5 1.361(14) . ?
N6 Ag2 2.184(9) 2_655 ?
N7 N8 1.347(13) . ?
N8 Ag2 2.577(10) . ?
N9 Ag1 2.107(9) 2_556 ?
O1 Mo3 2.141(6) . ?
O1 Mo2 2.310(5) . ?
O1 Mo4 2.315(5) . ?
O1 Mo3 2.371(6) 2_545 ?
O1 Mo1 2.503(6) . ?
O2 Mo3 1.939(6) . ?
O2 Mo4 1.996(6) . ?
O2 Mo2 2.380(6) 2_545 ?
O3 Mo4 1.698(8) . ?
O4 Mo4 1.700(7) . ?
O5 Mo4 1.886(7) . ?
O5 Mo1 1.940(7) . ?
O6 Mo1 1.701(9) . ?
O7 Mo1 1.698(11) . ?
O8 Mo2 1.906(7) . ?
O8 Mo1 1.908(6) . ?
O9 Mo2 1.698(7) . ?
O10 Mo2 1.685(7) . ?
O11 Mo3 1.965(6) . ?
O11 Mo2 1.995(6) . ?
O11 Mo4 2.322(6) 2_545 ?
O12 Mo3 1.746(7) . ?
O12 Mo1 2.272(7) 2_545 ?
O13 Mo3 1.680(7) . ?
Mo1 O12 2.272(7) 2_545 ?
Mo2 O2 2.380(6) 2_545 ?
Mo3 O1 2.371(6) 2_545 ?
Mo3 Mo4 3.2045(11) . ?
Mo4 O11 2.322(6) 2_545 ?
Ag1 N9 2.107(9) 2_556 ?
Ag2 N6 2.184(9) 2_655 ?
