#------------------------------------------------------------------------------
#$Date: 2016-03-25 13:34:00 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179851 $
#$URL: svn://www.crystallography.net/cod/cif/7/01/47/7014781.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7014781
loop_
_publ_author_name
'Cross, Warren B.'
'Daly, Christopher G.'
'Ackerman, Rachel L.'
'George, Ian R.'
'Singh, Kuldip'
_publ_section_title
;
 N-heterocyclic carbene tethered amido complexes of palladium and
 platinum.
;
_journal_issue                   2
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              495
_journal_page_last               505
_journal_paper_doi               10.1039/c0dt01149e
_journal_volume                  40
_journal_year                    2011
_chemical_formula_moiety         'C29 H36 I2 N4 Pt'
_chemical_formula_sum            'C29 H36 I2 N4 Pt'
_chemical_formula_weight         889.51
_chemical_name_common            '[C,NH]PtI2py (11)'
_chemical_name_systematic
;
?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                95.858(4)
_cell_angle_beta                 104.069(4)
_cell_angle_gamma                114.812(4)
_cell_formula_units_Z            4
_cell_length_a                   13.412(3)
_cell_length_b                   15.242(3)
_cell_length_c                   18.357(4)
_cell_measurement_reflns_used    1016
_cell_measurement_temperature    150(2)
_cell_measurement_theta_max      21.738
_cell_measurement_theta_min      2.484
_cell_volume                     3214.1(12)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SHELXTL'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      150(2)
_diffrn_measured_fraction_theta_full 0.988
_diffrn_measured_fraction_theta_max 0.988
_diffrn_measurement_device_type  'Bruker Apex 2000 CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0920
_diffrn_reflns_av_sigmaI/netI    0.1514
_diffrn_reflns_limit_h_max       16
_diffrn_reflns_limit_h_min       -16
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       22
_diffrn_reflns_limit_l_min       -22
_diffrn_reflns_number            25327
_diffrn_reflns_theta_full        26.00
_diffrn_reflns_theta_max         26.00
_diffrn_reflns_theta_min         1.69
_exptl_absorpt_coefficient_mu    6.309
_exptl_absorpt_correction_T_max  0.831
_exptl_absorpt_correction_T_min  0.518
_exptl_absorpt_correction_type   empirical
_exptl_absorpt_process_details
;
absorption correction based on 7100 reflections(SADABS);Rint 0.1156 before
correction and 0.0454 after.
;
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.838
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       needle
_exptl_crystal_F_000             1688
_exptl_crystal_size_max          0.23
_exptl_crystal_size_mid          0.08
_exptl_crystal_size_min          0.04
_refine_diff_density_max         3.255
_refine_diff_density_min         -1.506
_refine_diff_density_rms         0.220
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.897
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     661
_refine_ls_number_reflns         12490
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      0.897
_refine_ls_R_factor_all          0.1104
_refine_ls_R_factor_gt           0.0602
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0264P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1004
_refine_ls_wR_factor_ref         0.1130
_reflns_number_gt                7475
_reflns_number_total             12490
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            C0DT01149E.TXT
_cod_data_source_block           10070
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1555 2011-01-17 13:19:09Z saulius 
;
_cod_original_cell_volume        3214.0(12)
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7014781
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Pt1 Pt 0.88150(4) 0.36141(4) 0.17011(3) 0.03228(14) Uani 1 1 d . . .
I1 I 1.10146(7) 0.48520(6) 0.21462(5) 0.0442(2) Uani 1 1 d . . .
I2 I 0.66902(7) 0.22294(7) 0.12460(5) 0.0477(3) Uani 1 1 d . . .
N1 N 0.6067(7) 0.3358(7) -0.0816(5) 0.033(2) Uani 1 1 d . . .
H1 H 0.6385 0.2975 -0.0905 0.039 Uiso 1 1 calc R . .
N2 N 0.8313(7) 0.3800(7) 0.0070(5) 0.034(3) Uani 1 1 d . . .
N3 N 0.9199(9) 0.2912(8) 0.0272(6) 0.044(3) Uani 1 1 d . . .
N4 N 0.8758(8) 0.3872(6) 0.2829(5) 0.032(2) Uani 1 1 d . . .
C1 C 0.8823(11) 0.3431(9) 0.0628(7) 0.039(3) Uani 1 1 d . . .
C2 C 0.8980(10) 0.2913(10) -0.0496(7) 0.044(3) Uani 1 1 d . . .
H2 H 0.9161 0.2576 -0.0868 0.053 Uiso 1 1 calc R . .
C3 C 0.8446(11) 0.3501(9) -0.0616(7) 0.045(4) Uani 1 1 d . . .
H3 H 0.8210 0.3671 -0.1088 0.055 Uiso 1 1 calc R . .
C4 C 0.7849(9) 0.4469(8) 0.0210(6) 0.028(3) Uani 1 1 d . . .
C5 C 0.8499(10) 0.5313(8) 0.0795(6) 0.037(3) Uani 1 1 d . . .
H5 H 0.9263 0.5465 0.1091 0.045 Uiso 1 1 calc R . .
C6 C 0.8040(10) 0.5930(9) 0.0948(6) 0.039(3) Uani 1 1 d . . .
H6 H 0.8479 0.6511 0.1355 0.046 Uiso 1 1 calc R . .
C7 C 0.6916(10) 0.5704(9) 0.0502(7) 0.040(3) Uani 1 1 d . . .
H7 H 0.6600 0.6141 0.0596 0.049 Uiso 1 1 calc R . .
C8 C 0.6290(10) 0.4870(9) -0.0056(6) 0.032(3) Uani 1 1 d . . .
H8 H 0.5523 0.4720 -0.0342 0.039 Uiso 1 1 calc R . .
C9 C 0.6709(9) 0.4221(8) -0.0233(6) 0.027(3) Uani 1 1 d . . .
C10 C 0.9756(13) 0.2320(11) 0.0637(8) 0.059(4) Uani 1 1 d . . .
H10 H 0.9879 0.2486 0.1203 0.071 Uiso 1 1 calc R . .
C11 C 0.8959(15) 0.1215(11) 0.0346(11) 0.106(7) Uani 1 1 d . . .
H11A H 0.8299 0.1035 0.0543 0.159 Uiso 1 1 calc R . .
H11B H 0.9383 0.0849 0.0528 0.159 Uiso 1 1 calc R . .
H11C H 0.8679 0.1047 -0.0219 0.159 Uiso 1 1 calc R . .
C12 C 1.0928(12) 0.2625(12) 0.0543(9) 0.074(5) Uani 1 1 d . . .
H12A H 1.0838 0.2343 0.0012 0.111 Uiso 1 1 calc R . .
H12B H 1.1360 0.2380 0.0903 0.111 Uiso 1 1 calc R . .
H12C H 1.1352 0.3352 0.0651 0.111 Uiso 1 1 calc R . .
C13 C 0.4908(10) 0.3073(8) -0.1275(7) 0.031(3) Uani 1 1 d . . .
C14 C 0.4712(9) 0.3589(8) -0.1848(6) 0.029(3) Uani 1 1 d . . .
C15 C 0.3561(10) 0.3271(8) -0.2308(7) 0.036(3) Uani 1 1 d . . .
H15 H 0.3408 0.3635 -0.2672 0.043 Uiso 1 1 calc R . .
C16 C 0.2661(10) 0.2456(9) -0.2242(7) 0.042(3) Uani 1 1 d . . .
H16 H 0.1896 0.2226 -0.2578 0.051 Uiso 1 1 calc R . .
C17 C 0.2891(11) 0.1964(9) -0.1666(7) 0.047(4) Uani 1 1 d . . .
H17 H 0.2261 0.1406 -0.1612 0.056 Uiso 1 1 calc R . .
C18 C 0.3978(10) 0.2250(9) -0.1179(6) 0.038(3) Uani 1 1 d . . .
C19 C 0.5640(10) 0.4467(9) -0.2001(7) 0.043(3) Uani 1 1 d . . .
H19 H 0.6386 0.4637 -0.1597 0.052 Uiso 1 1 calc R . .
C20 C 0.5466(12) 0.5407(10) -0.1937(9) 0.069(5) Uani 1 1 d . . .
H20A H 0.6211 0.5995 -0.1837 0.103 Uiso 1 1 calc R . .
H20B H 0.5157 0.5460 -0.1512 0.103 Uiso 1 1 calc R . .
H20C H 0.4920 0.5363 -0.2421 0.103 Uiso 1 1 calc R . .
C21 C 0.5779(10) 0.4194(10) -0.2765(7) 0.053(4) Uani 1 1 d . . .
H21A H 0.5982 0.3647 -0.2767 0.079 Uiso 1 1 calc R . .
H21B H 0.6394 0.4771 -0.2849 0.079 Uiso 1 1 calc R . .
H21C H 0.5050 0.3985 -0.3177 0.079 Uiso 1 1 calc R . .
C22 C 0.4196(12) 0.1758(9) -0.0527(8) 0.055(4) Uani 1 1 d . . .
H22 H 0.4952 0.2237 -0.0132 0.066 Uiso 1 1 calc R . .
C23 C 0.3282(14) 0.1486(13) -0.0142(10) 0.101(7) Uani 1 1 d . . .
H23A H 0.3246 0.2086 0.0067 0.151 Uiso 1 1 calc R . .
H23B H 0.3470 0.1177 0.0278 0.151 Uiso 1 1 calc R . .
H23C H 0.2531 0.1017 -0.0520 0.151 Uiso 1 1 calc R . .
C24 C 0.4297(15) 0.0845(11) -0.0823(8) 0.090(6) Uani 1 1 d . . .
H24A H 0.4399 0.0510 -0.0404 0.136 Uiso 1 1 calc R . .
H24B H 0.4966 0.1043 -0.1011 0.136 Uiso 1 1 calc R . .
H24C H 0.3591 0.0391 -0.1246 0.136 Uiso 1 1 calc R . .
C25 C 0.9449(10) 0.3730(8) 0.3406(6) 0.032(3) Uani 1 1 d . . .
H25 H 1.0014 0.3553 0.3314 0.039 Uiso 1 1 calc R . .
C26 C 0.9355(12) 0.3839(9) 0.4148(8) 0.050(4) Uani 1 1 d . . .
H26 H 0.9841 0.3720 0.4553 0.060 Uiso 1 1 calc R . .
C27 C 0.8566(13) 0.4115(9) 0.4288(8) 0.051(4) Uani 1 1 d . . .
H27 H 0.8497 0.4191 0.4791 0.061 Uiso 1 1 calc R . .
C28 C 0.7879(11) 0.4282(9) 0.3702(9) 0.051(4) Uani 1 1 d . . .
H28 H 0.7335 0.4494 0.3786 0.061 Uiso 1 1 calc R . .
C29 C 0.7994(11) 0.4135(9) 0.2992(9) 0.047(4) Uani 1 1 d . . .
H29 H 0.7491 0.4228 0.2579 0.056 Uiso 1 1 calc R . .
Pt1A Pt 0.18314(4) 0.28397(3) 0.44412(3) 0.02569(12) Uani 1 1 d . . .
I1A I 0.12862(7) 0.29953(6) 0.57006(4) 0.0335(2) Uani 1 1 d . . .
I2A I 0.21279(7) 0.25920(6) 0.31033(4) 0.0381(2) Uani 1 1 d . . .
N1A N 0.2384(8) 0.0011(7) 0.3549(5) 0.034(2) Uani 1 1 d . . .
H1A H 0.1732 0.0004 0.3294 0.041 Uiso 1 1 calc R . .
N2A N 0.1226(7) 0.0726(6) 0.4350(5) 0.023(2) Uani 1 1 d . . .
N3A N -0.0313(8) 0.0887(7) 0.3841(5) 0.032(2) Uani 1 1 d . . .
N4A N 0.2989(7) 0.4367(6) 0.4756(5) 0.028(2) Uani 1 1 d . . .
C1A C 0.0857(8) 0.1391(8) 0.4188(6) 0.026(3) Uani 1 1 d . . .
C2A C -0.0668(10) -0.0127(8) 0.3779(6) 0.031(3) Uani 1 1 d . . .
H2A H -0.1437 -0.0648 0.3559 0.037 Uiso 1 1 calc R . .
C3A C 0.0295(10) -0.0228(7) 0.4092(6) 0.030(3) Uani 1 1 d . . .
H3A H 0.0328 -0.0833 0.4129 0.036 Uiso 1 1 calc R . .
C4A C 0.2374(9) 0.0906(7) 0.4727(6) 0.024(3) Uani 1 1 d . . .
C5A C 0.2943(10) 0.1436(8) 0.5485(6) 0.028(3) Uani 1 1 d . . .
H5A H 0.2577 0.1725 0.5739 0.034 Uiso 1 1 calc R . .
C6A C 0.4009(10) 0.1559(8) 0.5879(7) 0.037(3) Uani 1 1 d . . .
H6A H 0.4393 0.1933 0.6398 0.044 Uiso 1 1 calc R . .
C7A C 0.4517(10) 0.1120(9) 0.5500(7) 0.036(3) Uani 1 1 d . . .
H7A H 0.5237 0.1154 0.5772 0.043 Uiso 1 1 calc R . .
C8A C 0.4005(10) 0.0644(8) 0.4749(7) 0.033(3) Uani 1 1 d . . .
H8A H 0.4400 0.0388 0.4497 0.039 Uiso 1 1 calc R . .
C9A C 0.2917(9) 0.0514(8) 0.4328(7) 0.029(3) Uani 1 1 d . . .
C10A C -0.1075(10) 0.1324(8) 0.3592(7) 0.035(3) Uani 1 1 d . . .
H10A H -0.0585 0.2059 0.3701 0.041 Uiso 1 1 calc R . .
C11A C -0.1674(12) 0.0952(11) 0.2725(8) 0.082(6) Uani 1 1 d . . .
H11D H -0.1094 0.1049 0.2462 0.122 Uiso 1 1 calc R . .
H11E H -0.2095 0.1323 0.2548 0.122 Uiso 1 1 calc R . .
H11F H -0.2219 0.0243 0.2606 0.122 Uiso 1 1 calc R . .
C12A C -0.1955(12) 0.1134(11) 0.4019(10) 0.077(5) Uani 1 1 d . . .
H12D H -0.2408 0.0417 0.3956 0.115 Uiso 1 1 calc R . .
H12E H -0.2473 0.1411 0.3808 0.115 Uiso 1 1 calc R . .
H12F H -0.1551 0.1452 0.4568 0.115 Uiso 1 1 calc R . .
C13A C 0.2854(10) -0.0482(9) 0.3161(6) 0.031(3) Uani 1 1 d . . .
C14A C 0.2485(10) -0.1496(9) 0.3106(6) 0.035(3) Uani 1 1 d . . .
C15A C 0.2960(11) -0.1961(9) 0.2741(7) 0.042(3) Uani 1 1 d . . .
H15A H 0.2711 -0.2651 0.2708 0.050 Uiso 1 1 calc R . .
C16A C 0.3792(11) -0.1453(10) 0.2418(7) 0.042(3) Uani 1 1 d . . .
H16A H 0.4120 -0.1789 0.2170 0.051 Uiso 1 1 calc R . .
C17A C 0.4149(11) -0.0461(11) 0.2453(7) 0.049(4) Uani 1 1 d . . .
H17A H 0.4707 -0.0121 0.2213 0.058 Uiso 1 1 calc R . .
C18A C 0.3713(11) 0.0061(9) 0.2832(7) 0.040(3) Uani 1 1 d . . .
C19A C 0.1559(9) -0.2062(8) 0.3445(6) 0.030(3) Uani 1 1 d . . .
H19A H 0.1466 -0.1569 0.3790 0.036 Uiso 1 1 calc R . .
C20A C 0.1800(11) -0.2756(10) 0.3913(7) 0.055(4) Uani 1 1 d . . .
H20D H 0.2066 -0.3146 0.3627 0.083 Uiso 1 1 calc R . .
H20E H 0.1089 -0.3205 0.4005 0.083 Uiso 1 1 calc R . .
H20F H 0.2399 -0.2366 0.4408 0.083 Uiso 1 1 calc R . .
C21A C 0.0404(10) -0.2680(9) 0.2796(7) 0.053(4) Uani 1 1 d . . .
H21D H 0.0223 -0.2244 0.2489 0.079 Uiso 1 1 calc R . .
H21E H -0.0212 -0.3001 0.3020 0.079 Uiso 1 1 calc R . .
H21F H 0.0464 -0.3188 0.2463 0.079 Uiso 1 1 calc R . .
C22A C 0.4102(10) 0.1147(10) 0.2855(7) 0.050(4) Uani 1 1 d . . .
H22A H 0.3720 0.1377 0.3181 0.060 Uiso 1 1 calc R . .
C23A C 0.5405(12) 0.1793(10) 0.3219(9) 0.073(5) Uani 1 1 d . . .
H23D H 0.5669 0.1629 0.3709 0.109 Uiso 1 1 calc R . .
H23E H 0.5581 0.2495 0.3315 0.109 Uiso 1 1 calc R . .
H23F H 0.5802 0.1670 0.2868 0.109 Uiso 1 1 calc R . .
C24A C 0.3734(14) 0.1347(12) 0.2059(9) 0.081(5) Uani 1 1 d . . .
H24D H 0.3950 0.2055 0.2113 0.122 Uiso 1 1 calc R . .
H24E H 0.2894 0.0954 0.1822 0.122 Uiso 1 1 calc R . .
H24F H 0.4124 0.1160 0.1731 0.122 Uiso 1 1 calc R . .
C25A C 0.3842(9) 0.4713(8) 0.5424(7) 0.035(3) Uani 1 1 d . . .
H25A H 0.3893 0.4262 0.5733 0.042 Uiso 1 1 calc R . .
C26A C 0.4668(9) 0.5713(8) 0.5689(7) 0.036(3) Uani 1 1 d . . .
H26A H 0.5254 0.5947 0.6176 0.043 Uiso 1 1 calc R . .
C27A C 0.4601(10) 0.6348(8) 0.5217(7) 0.036(3) Uani 1 1 d . . .
H27A H 0.5168 0.7026 0.5365 0.043 Uiso 1 1 calc R . .
C28A C 0.3708(11) 0.5997(9) 0.4530(7) 0.038(3) Uani 1 1 d . . .
H28A H 0.3634 0.6437 0.4214 0.045 Uiso 1 1 calc R . .
C29A C 0.2921(9) 0.5000(8) 0.4305(6) 0.029(3) Uani 1 1 d . . .
H29A H 0.2320 0.4755 0.3824 0.035 Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
I I -0.4742 1.8119 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C1 Pt1 N4 176.3(5) . . ?
C1 Pt1 I2 89.2(3) . . ?
N4 Pt1 I2 90.4(2) . . ?
C1 Pt1 I1 89.5(3) . . ?
N4 Pt1 I1 91.3(2) . . ?
I2 Pt1 I1 173.79(4) . . ?
C9 N1 C13 122.2(9) . . ?
C9 N1 H1 118.9 . . ?
C13 N1 H1 118.9 . . ?
C3 N2 C1 108.1(10) . . ?
C3 N2 C4 126.0(10) . . ?
C1 N2 C4 125.5(10) . . ?
C1 N3 C2 112.7(11) . . ?
C1 N3 C10 125.0(11) . . ?
C2 N3 C10 122.3(11) . . ?
C25 N4 C29 117.2(11) . . ?
C25 N4 Pt1 121.1(8) . . ?
C29 N4 Pt1 121.6(9) . . ?
N3 C1 N2 105.9(11) . . ?
N3 C1 Pt1 129.9(10) . . ?
N2 C1 Pt1 124.0(9) . . ?
C3 C2 N3 105.5(12) . . ?
C3 C2 H2 127.3 . . ?
N3 C2 H2 127.3 . . ?
C2 C3 N2 107.7(11) . . ?
C2 C3 H3 126.1 . . ?
N2 C3 H3 126.1 . . ?
C5 C4 C9 121.3(11) . . ?
C5 C4 N2 119.6(10) . . ?
C9 C4 N2 119.0(10) . . ?
C6 C5 C4 119.6(11) . . ?
C6 C5 H5 120.2 . . ?
C4 C5 H5 120.2 . . ?
C5 C6 C7 119.7(11) . . ?
C5 C6 H6 120.1 . . ?
C7 C6 H6 120.1 . . ?
C8 C7 C6 119.8(12) . . ?
C8 C7 H7 120.1 . . ?
C6 C7 H7 120.1 . . ?
C7 C8 C9 122.9(11) . . ?
C7 C8 H8 118.6 . . ?
C9 C8 H8 118.6 . . ?
C8 C9 N1 123.1(10) . . ?
C8 C9 C4 116.6(11) . . ?
N1 C9 C4 120.2(11) . . ?
C12 C10 N3 111.3(11) . . ?
C12 C10 C11 113.2(13) . . ?
N3 C10 C11 111.2(12) . . ?
C12 C10 H10 106.9 . . ?
N3 C10 H10 106.9 . . ?
C11 C10 H10 106.9 . . ?
C10 C11 H11A 109.5 . . ?
C10 C11 H11B 109.5 . . ?
H11A C11 H11B 109.5 . . ?
C10 C11 H11C 109.5 . . ?
H11A C11 H11C 109.5 . . ?
H11B C11 H11C 109.5 . . ?
C10 C12 H12A 109.5 . . ?
C10 C12 H12B 109.5 . . ?
H12A C12 H12B 109.5 . . ?
C10 C12 H12C 109.5 . . ?
H12A C12 H12C 109.5 . . ?
H12B C12 H12C 109.5 . . ?
C14 C13 C18 120.9(10) . . ?
C14 C13 N1 119.3(10) . . ?
C18 C13 N1 119.7(10) . . ?
C15 C14 C13 118.0(10) . . ?
C15 C14 C19 116.9(10) . . ?
C13 C14 C19 125.0(10) . . ?
C16 C15 C14 121.7(11) . . ?
C16 C15 H15 119.1 . . ?
C14 C15 H15 119.1 . . ?
C15 C16 C17 118.4(11) . . ?
C15 C16 H16 120.8 . . ?
C17 C16 H16 120.8 . . ?
C18 C17 C16 123.2(12) . . ?
C18 C17 H17 118.4 . . ?
C16 C17 H17 118.4 . . ?
C17 C18 C13 117.6(11) . . ?
C17 C18 C22 122.3(12) . . ?
C13 C18 C22 119.9(11) . . ?
C21 C19 C14 110.7(10) . . ?
C21 C19 C20 111.1(11) . . ?
C14 C19 C20 114.1(11) . . ?
C21 C19 H19 106.8 . . ?
C14 C19 H19 106.8 . . ?
C20 C19 H19 106.8 . . ?
C19 C20 H20A 109.5 . . ?
C19 C20 H20B 109.5 . . ?
H20A C20 H20B 109.5 . . ?
C19 C20 H20C 109.5 . . ?
H20A C20 H20C 109.5 . . ?
H20B C20 H20C 109.5 . . ?
C19 C21 H21A 109.5 . . ?
C19 C21 H21B 109.5 . . ?
H21A C21 H21B 109.5 . . ?
C19 C21 H21C 109.5 . . ?
H21A C21 H21C 109.5 . . ?
H21B C21 H21C 109.5 . . ?
C23 C22 C18 112.8(12) . . ?
C23 C22 C24 110.0(13) . . ?
C18 C22 C24 109.8(11) . . ?
C23 C22 H22 108.0 . . ?
C18 C22 H22 108.0 . . ?
C24 C22 H22 108.0 . . ?
C22 C23 H23A 109.5 . . ?
C22 C23 H23B 109.5 . . ?
H23A C23 H23B 109.5 . . ?
C22 C23 H23C 109.5 . . ?
H23A C23 H23C 109.5 . . ?
H23B C23 H23C 109.5 . . ?
C22 C24 H24A 109.5 . . ?
C22 C24 H24B 109.5 . . ?
H24A C24 H24B 109.5 . . ?
C22 C24 H24C 109.5 . . ?
H24A C24 H24C 109.5 . . ?
H24B C24 H24C 109.5 . . ?
N4 C25 C26 120.9(12) . . ?
N4 C25 H25 119.6 . . ?
C26 C25 H25 119.6 . . ?
C27 C26 C25 119.9(12) . . ?
C27 C26 H26 120.1 . . ?
C25 C26 H26 120.1 . . ?
C28 C27 C26 119.2(13) . . ?
C28 C27 H27 120.4 . . ?
C26 C27 H27 120.4 . . ?
C29 C28 C27 117.8(14) . . ?
C29 C28 H28 121.1 . . ?
C27 C28 H28 121.1 . . ?
N4 C29 C28 125.0(13) . . ?
N4 C29 H29 117.5 . . ?
C28 C29 H29 117.5 . . ?
C1A Pt1A N4A 175.2(4) . . ?
C1A Pt1A I2A 86.5(3) . . ?
N4A Pt1A I2A 93.6(2) . . ?
C1A Pt1A I1A 90.1(3) . . ?
N4A Pt1A I1A 90.2(2) . . ?
I2A Pt1A I1A 173.58(3) . . ?
C9A N1A C13A 122.2(9) . . ?
C9A N1A H1A 118.9 . . ?
C13A N1A H1A 118.9 . . ?
C1A N2A C3A 109.8(9) . . ?
C1A N2A C4A 127.7(9) . . ?
C3A N2A C4A 122.4(9) . . ?
C1A N3A C2A 108.7(9) . . ?
C1A N3A C10A 126.2(9) . . ?
C2A N3A C10A 125.2(9) . . ?
C25A N4A C29A 119.0(9) . . ?
C25A N4A Pt1A 117.8(7) . . ?
C29A N4A Pt1A 123.2(7) . . ?
N2A C1A N3A 107.5(9) . . ?
N2A C1A Pt1A 125.6(7) . . ?
N3A C1A Pt1A 126.8(8) . . ?
C3A C2A N3A 107.0(10) . . ?
C3A C2A H2A 126.5 . . ?
N3A C2A H2A 126.5 . . ?
C2A C3A N2A 107.0(9) . . ?
C2A C3A H3A 126.5 . . ?
N2A C3A H3A 126.5 . . ?
C5A C4A C9A 120.0(10) . . ?
C5A C4A N2A 120.8(10) . . ?
C9A C4A N2A 119.2(10) . . ?
C6A C5A C4A 122.1(11) . . ?
C6A C5A H5A 118.9 . . ?
C4A C5A H5A 118.9 . . ?
C5A C6A C7A 117.9(11) . . ?
C5A C6A H6A 121.1 . . ?
C7A C6A H6A 121.1 . . ?
C8A C7A C6A 120.9(11) . . ?
C8A C7A H7A 119.6 . . ?
C6A C7A H7A 119.6 . . ?
C7A C8A C9A 122.4(12) . . ?
C7A C8A H8A 118.8 . . ?
C9A C8A H8A 118.8 . . ?
C8A C9A C4A 116.4(11) . . ?
C8A C9A N1A 122.2(11) . . ?
C4A C9A N1A 121.3(10) . . ?
N3A C10A C12A 112.9(10) . . ?
N3A C10A C11A 109.9(10) . . ?
C12A C10A C11A 110.8(11) . . ?
N3A C10A H10A 107.7 . . ?
C12A C10A H10A 107.7 . . ?
C11A C10A H10A 107.7 . . ?
C10A C11A H11D 109.5 . . ?
C10A C11A H11E 109.5 . . ?
H11D C11A H11E 109.5 . . ?
C10A C11A H11F 109.5 . . ?
H11D C11A H11F 109.5 . . ?
H11E C11A H11F 109.5 . . ?
C10A C12A H12D 109.5 . . ?
C10A C12A H12E 109.5 . . ?
H12D C12A H12E 109.5 . . ?
C10A C12A H12F 109.5 . . ?
H12D C12A H12F 109.5 . . ?
H12E C12A H12F 109.5 . . ?
C14A C13A N1A 120.1(11) . . ?
C14A C13A C18A 120.3(11) . . ?
N1A C13A C18A 119.6(11) . . ?
C15A C14A C13A 119.5(12) . . ?
C15A C14A C19A 120.9(11) . . ?
C13A C14A C19A 119.6(11) . . ?
C14A C15A C16A 121.2(12) . . ?
C14A C15A H15A 119.4 . . ?
C16A C15A H15A 119.4 . . ?
C17A C16A C15A 120.0(13) . . ?
C17A C16A H16A 120.0 . . ?
C15A C16A H16A 120.0 . . ?
C16A C17A C18A 121.4(13) . . ?
C16A C17A H17A 119.3 . . ?
C18A C17A H17A 119.3 . . ?
C17A C18A C13A 117.4(12) . . ?
C17A C18A C22A 120.7(12) . . ?
C13A C18A C22A 121.8(12) . . ?
C14A C19A C20A 115.1(10) . . ?
C14A C19A C21A 109.6(9) . . ?
C20A C19A C21A 107.9(10) . . ?
C14A C19A H19A 108.0 . . ?
C20A C19A H19A 108.0 . . ?
C21A C19A H19A 108.0 . . ?
C19A C20A H20D 109.5 . . ?
C19A C20A H20E 109.5 . . ?
H20D C20A H20E 109.5 . . ?
C19A C20A H20F 109.5 . . ?
H20D C20A H20F 109.5 . . ?
H20E C20A H20F 109.5 . . ?
C19A C21A H21D 109.5 . . ?
C19A C21A H21E 109.5 . . ?
H21D C21A H21E 109.5 . . ?
C19A C21A H21F 109.5 . . ?
H21D C21A H21F 109.5 . . ?
H21E C21A H21F 109.5 . . ?
C18A C22A C23A 113.6(11) . . ?
C18A C22A C24A 113.0(11) . . ?
C23A C22A C24A 108.3(12) . . ?
C18A C22A H22A 107.2 . . ?
C23A C22A H22A 107.2 . . ?
C24A C22A H22A 107.2 . . ?
C22A C23A H23D 109.5 . . ?
C22A C23A H23E 109.5 . . ?
H23D C23A H23E 109.5 . . ?
C22A C23A H23F 109.5 . . ?
H23D C23A H23F 109.5 . . ?
H23E C23A H23F 109.5 . . ?
C22A C24A H24D 109.5 . . ?
C22A C24A H24E 109.5 . . ?
H24D C24A H24E 109.5 . . ?
C22A C24A H24F 109.5 . . ?
H24D C24A H24F 109.5 . . ?
H24E C24A H24F 109.5 . . ?
N4A C25A C26A 122.8(11) . . ?
N4A C25A H25A 118.6 . . ?
C26A C25A H25A 118.6 . . ?
C27A C26A C25A 117.5(10) . . ?
C27A C26A H26A 121.2 . . ?
C25A C26A H26A 121.2 . . ?
C26A C27A C28A 119.9(11) . . ?
C26A C27A H27A 120.1 . . ?
C28A C27A H27A 120.1 . . ?
C27A C28A C29A 119.4(11) . . ?
C27A C28A H28A 120.3 . . ?
C29A C28A H28A 120.3 . . ?
N4A C29A C28A 121.3(10) . . ?
N4A C29A H29A 119.3 . . ?
C28A C29A H29A 119.3 . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pt1 C1 1.965(13) . ?
Pt1 N4 2.094(10) . ?
Pt1 I2 2.5901(10) . ?
Pt1 I1 2.6024(10) . ?
N1 C9 1.389(12) . ?
N1 C13 1.426(13) . ?
N1 H1 0.8800 . ?
N2 C3 1.374(14) . ?
N2 C1 1.391(14) . ?
N2 C4 1.430(14) . ?
N3 C1 1.301(14) . ?
N3 C2 1.370(14) . ?
N3 C10 1.505(14) . ?
N4 C25 1.328(13) . ?
N4 C29 1.330(14) . ?
C2 C3 1.365(16) . ?
C2 H2 0.9500 . ?
C3 H3 0.9500 . ?
C4 C5 1.375(14) . ?
C4 C9 1.411(14) . ?
C5 C6 1.363(15) . ?
C5 H5 0.9500 . ?
C6 C7 1.402(15) . ?
C6 H6 0.9500 . ?
C7 C8 1.338(14) . ?
C7 H7 0.9500 . ?
C8 C9 1.375(15) . ?
C8 H8 0.9500 . ?
C10 C12 1.501(17) . ?
C10 C11 1.514(19) . ?
C10 H10 1.0000 . ?
C11 H11A 0.9800 . ?
C11 H11B 0.9800 . ?
C11 H11C 0.9800 . ?
C12 H12A 0.9800 . ?
C12 H12B 0.9800 . ?
C12 H12C 0.9800 . ?
C13 C14 1.415(14) . ?
C13 C18 1.415(15) . ?
C14 C15 1.409(14) . ?
C14 C19 1.507(15) . ?
C15 C16 1.363(15) . ?
C15 H15 0.9500 . ?
C16 C17 1.405(16) . ?
C16 H16 0.9500 . ?
C17 C18 1.366(15) . ?
C17 H17 0.9500 . ?
C18 C22 1.509(15) . ?
C19 C21 1.497(16) . ?
C19 C20 1.543(17) . ?
C19 H19 1.0000 . ?
C20 H20A 0.9800 . ?
C20 H20B 0.9800 . ?
C20 H20C 0.9800 . ?
C21 H21A 0.9800 . ?
C21 H21B 0.9800 . ?
C21 H21C 0.9800 . ?
C22 C23 1.492(18) . ?
C22 C24 1.513(18) . ?
C22 H22 1.0000 . ?
C23 H23A 0.9800 . ?
C23 H23B 0.9800 . ?
C23 H23C 0.9800 . ?
C24 H24A 0.9800 . ?
C24 H24B 0.9800 . ?
C24 H24C 0.9800 . ?
C25 C26 1.396(16) . ?
C25 H25 0.9500 . ?
C26 C27 1.359(17) . ?
C26 H26 0.9500 . ?
C27 C28 1.358(17) . ?
C27 H27 0.9500 . ?
C28 C29 1.357(17) . ?
C28 H28 0.9500 . ?
C29 H29 0.9500 . ?
Pt1A C1A 1.968(11) . ?
Pt1A N4A 2.102(8) . ?
Pt1A I2A 2.5969(11) . ?
Pt1A I1A 2.6060(10) . ?
N1A C9A 1.401(13) . ?
N1A C13A 1.406(13) . ?
N1A H1A 0.8800 . ?
N2A C1A 1.331(13) . ?
N2A C3A 1.394(12) . ?
N2A C4A 1.419(13) . ?
N3A C1A 1.365(12) . ?
N3A C2A 1.396(13) . ?
N3A C10A 1.451(13) . ?
N4A C25A 1.331(13) . ?
N4A C29A 1.350(12) . ?
C2A C3A 1.359(14) . ?
C2A H2A 0.9500 . ?
C3A H3A 0.9500 . ?
C4A C5A 1.382(14) . ?
C4A C9A 1.400(15) . ?
C5A C6A 1.360(14) . ?
C5A H5A 0.9500 . ?
C6A C7A 1.383(15) . ?
C6A H6A 0.9500 . ?
C7A C8A 1.348(15) . ?
C7A H7A 0.9500 . ?
C8A C9A 1.393(14) . ?
C8A H8A 0.9500 . ?
C10A C12A 1.516(16) . ?
C10A C11A 1.519(16) . ?
C10A H10A 1.0000 . ?
C11A H11D 0.9800 . ?
C11A H11E 0.9800 . ?
C11A H11F 0.9800 . ?
C12A H12D 0.9800 . ?
C12A H12E 0.9800 . ?
C12A H12F 0.9800 . ?
C13A C14A 1.396(15) . ?
C13A C18A 1.419(16) . ?
C14A C15A 1.359(15) . ?
C14A C19A 1.502(15) . ?
C15A C16A 1.374(16) . ?
C15A H15A 0.9500 . ?
C16A C17A 1.370(17) . ?
C16A H16A 0.9500 . ?
C17A C18A 1.391(16) . ?
C17A H17A 0.9500 . ?
C18A C22A 1.505(17) . ?
C19A C20A 1.516(15) . ?
C19A C21A 1.535(14) . ?
C19A H19A 1.0000 . ?
C20A H20D 0.9800 . ?
C20A H20E 0.9800 . ?
C20A H20F 0.9800 . ?
C21A H21D 0.9800 . ?
C21A H21E 0.9800 . ?
C21A H21F 0.9800 . ?
C22A C23A 1.524(16) . ?
C22A C24A 1.529(17) . ?
C22A H22A 1.0000 . ?
C23A H23D 0.9800 . ?
C23A H23E 0.9800 . ?
C23A H23F 0.9800 . ?
C24A H24D 0.9800 . ?
C24A H24E 0.9800 . ?
C24A H24F 0.9800 . ?
C25A C26A 1.399(14) . ?
C25A H25A 0.9500 . ?
C26A C27A 1.378(15) . ?
C26A H26A 0.9500 . ?
C27A C28A 1.379(15) . ?
C27A H27A 0.9500 . ?
C28A C29A 1.382(14) . ?
C28A H28A 0.9500 . ?
C29A H29A 0.9500 . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C1 Pt1 N4 C25 -158(6) . . . . ?
I2 Pt1 N4 C25 117.6(8) . . . . ?
I1 Pt1 N4 C25 -56.5(8) . . . . ?
C1 Pt1 N4 C29 25(7) . . . . ?
I2 Pt1 N4 C29 -59.1(9) . . . . ?
I1 Pt1 N4 C29 126.9(9) . . . . ?
C2 N3 C1 N2 0.4(14) . . . . ?
C10 N3 C1 N2 -176.3(11) . . . . ?
C2 N3 C1 Pt1 175.7(9) . . . . ?
C10 N3 C1 Pt1 -1.0(19) . . . . ?
C3 N2 C1 N3 -2.1(13) . . . . ?
C4 N2 C1 N3 -175.6(10) . . . . ?
C3 N2 C1 Pt1 -177.7(8) . . . . ?
C4 N2 C1 Pt1 8.7(15) . . . . ?
N4 Pt1 C1 N3 179(59) . . . . ?
I2 Pt1 C1 N3 -96.8(12) . . . . ?
I1 Pt1 C1 N3 77.1(12) . . . . ?
N4 Pt1 C1 N2 -7(7) . . . . ?
I2 Pt1 C1 N2 77.7(9) . . . . ?
I1 Pt1 C1 N2 -108.4(9) . . . . ?
C1 N3 C2 C3 1.3(15) . . . . ?
C10 N3 C2 C3 178.2(11) . . . . ?
N3 C2 C3 N2 -2.6(14) . . . . ?
C1 N2 C3 C2 2.9(13) . . . . ?
C4 N2 C3 C2 176.4(10) . . . . ?
C3 N2 C4 C5 -123.3(12) . . . . ?
C1 N2 C4 C5 49.1(15) . . . . ?
C3 N2 C4 C9 59.7(15) . . . . ?
C1 N2 C4 C9 -127.9(11) . . . . ?
C9 C4 C5 C6 -0.5(17) . . . . ?
N2 C4 C5 C6 -177.5(10) . . . . ?
C4 C5 C6 C7 -0.8(18) . . . . ?
C5 C6 C7 C8 1.9(18) . . . . ?
C6 C7 C8 C9 -1.8(18) . . . . ?
C7 C8 C9 N1 -179.5(11) . . . . ?
C7 C8 C9 C4 0.5(17) . . . . ?
C13 N1 C9 C8 -0.6(16) . . . . ?
C13 N1 C9 C4 179.5(10) . . . . ?
C5 C4 C9 C8 0.7(16) . . . . ?
N2 C4 C9 C8 177.6(9) . . . . ?
C5 C4 C9 N1 -179.4(10) . . . . ?
N2 C4 C9 N1 -2.4(15) . . . . ?
C1 N3 C10 C12 -124.4(14) . . . . ?
C2 N3 C10 C12 59.1(17) . . . . ?
C1 N3 C10 C11 108.4(15) . . . . ?
C2 N3 C10 C11 -68.1(17) . . . . ?
C9 N1 C13 C14 74.1(14) . . . . ?
C9 N1 C13 C18 -109.2(13) . . . . ?
C18 C13 C14 C15 1.4(17) . . . . ?
N1 C13 C14 C15 178.2(10) . . . . ?
C18 C13 C14 C19 -179.5(11) . . . . ?
N1 C13 C14 C19 -2.8(17) . . . . ?
C13 C14 C15 C16 -4.0(17) . . . . ?
C19 C14 C15 C16 176.8(11) . . . . ?
C14 C15 C16 C17 4.1(18) . . . . ?
C15 C16 C17 C18 -1.6(19) . . . . ?
C16 C17 C18 C13 -0.9(19) . . . . ?
C16 C17 C18 C22 175.5(12) . . . . ?
C14 C13 C18 C17 0.9(18) . . . . ?
N1 C13 C18 C17 -175.8(11) . . . . ?
C14 C13 C18 C22 -175.5(11) . . . . ?
N1 C13 C18 C22 7.7(17) . . . . ?
C15 C14 C19 C21 -69.7(14) . . . . ?
C13 C14 C19 C21 111.2(13) . . . . ?
C15 C14 C19 C20 56.5(15) . . . . ?
C13 C14 C19 C20 -122.6(13) . . . . ?
C17 C18 C22 C23 -37.6(18) . . . . ?
C13 C18 C22 C23 138.7(13) . . . . ?
C17 C18 C22 C24 85.5(16) . . . . ?
C13 C18 C22 C24 -98.1(14) . . . . ?
C29 N4 C25 C26 1.1(16) . . . . ?
Pt1 N4 C25 C26 -175.7(8) . . . . ?
N4 C25 C26 C27 -1.6(19) . . . . ?
C25 C26 C27 C28 0(2) . . . . ?
C26 C27 C28 C29 2(2) . . . . ?
C25 N4 C29 C28 0.8(18) . . . . ?
Pt1 N4 C29 C28 177.6(10) . . . . ?
C27 C28 C29 N4 -2(2) . . . . ?
C1A Pt1A N4A C25A -35(5) . . . . ?
I2A Pt1A N4A C25A -126.5(8) . . . . ?
I1A Pt1A N4A C25A 58.6(8) . . . . ?
C1A Pt1A N4A C29A 144(4) . . . . ?
I2A Pt1A N4A C29A 51.8(9) . . . . ?
I1A Pt1A N4A C29A -123.0(8) . . . . ?
C3A N2A C1A N3A 1.2(12) . . . . ?
C4A N2A C1A N3A -178.5(10) . . . . ?
C3A N2A C1A Pt1A 179.4(7) . . . . ?
C4A N2A C1A Pt1A -0.3(16) . . . . ?
C2A N3A C1A N2A -0.9(12) . . . . ?
C10A N3A C1A N2A 177.9(10) . . . . ?
C2A N3A C1A Pt1A -179.0(8) . . . . ?
C10A N3A C1A Pt1A -0.3(16) . . . . ?
N4A Pt1A C1A N2A -2(5) . . . . ?
I2A Pt1A C1A N2A 89.9(9) . . . . ?
I1A Pt1A C1A N2A -95.5(9) . . . . ?
N4A Pt1A C1A N3A 176(4) . . . . ?
I2A Pt1A C1A N3A -92.2(9) . . . . ?
I1A Pt1A C1A N3A 82.3(9) . . . . ?
C1A N3A C2A C3A 0.2(12) . . . . ?
C10A N3A C2A C3A -178.6(10) . . . . ?
N3A C2A C3A N2A 0.5(12) . . . . ?
C1A N2A C3A C2A -1.1(13) . . . . ?
C4A N2A C3A C2A 178.6(9) . . . . ?
C1A N2A C4A C5A 63.7(15) . . . . ?
C3A N2A C4A C5A -116.0(11) . . . . ?
C1A N2A C4A C9A -118.1(12) . . . . ?
C3A N2A C4A C9A 62.2(14) . . . . ?
C9A C4A C5A C6A -3.1(16) . . . . ?
N2A C4A C5A C6A 175.1(10) . . . . ?
C4A C5A C6A C7A -0.8(16) . . . . ?
C5A C6A C7A C8A 4.4(17) . . . . ?
C6A C7A C8A C9A -4.0(18) . . . . ?
C7A C8A C9A C4A 0.0(16) . . . . ?
C7A C8A C9A N1A -179.5(11) . . . . ?
C5A C4A C9A C8A 3.5(15) . . . . ?
N2A C4A C9A C8A -174.8(9) . . . . ?
C5A C4A C9A N1A -177.1(10) . . . . ?
N2A C4A C9A N1A 4.7(15) . . . . ?
C13A N1A C9A C8A 6.6(16) . . . . ?
C13A N1A C9A C4A -172.9(10) . . . . ?
C1A N3A C10A C12A -116.6(13) . . . . ?
C2A N3A C10A C12A 62.0(15) . . . . ?
C1A N3A C10A C11A 119.2(12) . . . . ?
C2A N3A C10A C11A -62.2(15) . . . . ?
C9A N1A C13A C14A 94.5(13) . . . . ?
C9A N1A C13A C18A -84.8(14) . . . . ?
N1A C13A C14A C15A -178.9(10) . . . . ?
C18A C13A C14A C15A 0.4(17) . . . . ?
N1A C13A C14A C19A 1.7(16) . . . . ?
C18A C13A C14A C19A -178.9(10) . . . . ?
C13A C14A C15A C16A -0.5(18) . . . . ?
C19A C14A C15A C16A 178.9(10) . . . . ?
C14A C15A C16A C17A -0.7(19) . . . . ?
C15A C16A C17A C18A 2.0(19) . . . . ?
C16A C17A C18A C13A -2.0(18) . . . . ?
C16A C17A C18A C22A -179.1(11) . . . . ?
C14A C13A C18A C17A 0.8(17) . . . . ?
N1A C13A C18A C17A -179.9(10) . . . . ?
C14A C13A C18A C22A 177.8(10) . . . . ?
N1A C13A C18A C22A -2.9(17) . . . . ?
C15A C14A C19A C20A 45.9(15) . . . . ?
C13A C14A C19A C20A -134.8(11) . . . . ?
C15A C14A C19A C21A -75.9(14) . . . . ?
C13A C14A C19A C21A 103.4(12) . . . . ?
C17A C18A C22A C23A -58.4(17) . . . . ?
C13A C18A C22A C23A 124.7(13) . . . . ?
C17A C18A C22A C24A 65.5(16) . . . . ?
C13A C18A C22A C24A -111.5(14) . . . . ?
C29A N4A C25A C26A 1.1(17) . . . . ?
Pt1A N4A C25A C26A 179.5(9) . . . . ?
N4A C25A C26A C27A -2.2(18) . . . . ?
C25A C26A C27A C28A 3.1(17) . . . . ?
C26A C27A C28A C29A -3.1(18) . . . . ?
C25A N4A C29A C28A -0.9(17) . . . . ?
Pt1A N4A C29A C28A -179.3(8) . . . . ?
C27A C28A C29A N4A 2.0(18) . . . . ?
