#------------------------------------------------------------------------------
#$Date: 2016-03-25 13:43:39 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179860 $
#$URL: svn://www.crystallography.net/cod/cif/7/01/56/7015627.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7015627
loop_
_publ_author_name
'Zhang, Shuanming'
'Pattacini, Roberto'
'Braunstein, Pierre'
_publ_section_title
;
 Chelating or bridging Pd(ii) and Pt(ii) metalloligands from the
 functional phosphine ligand
 N-(diphenylphosphino)-1,3,4-thiadiazol-2-amine. New heterometallic
 Pd(ii)/Pt(ii) and Pt(ii)/Au(i) complexes.
;
_journal_issue                   21
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              5711
_journal_page_last               5719
_journal_paper_doi               10.1039/c0dt01782e
_journal_volume                  40
_journal_year                    2011
_chemical_formula_moiety         'C28 H22 Cl2 N6 P2 Pd Pt S2, C H2 Cl2'
_chemical_formula_sum            'C29 H24 Cl4 N6 P2 Pd Pt S2'
_chemical_formula_weight         1025.89
_chemical_name_systematic
;
?
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 120.504(2)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   10.2464(4)
_cell_length_b                   19.2382(8)
_cell_length_c                   19.7126(6)
_cell_measurement_reflns_used    53992
_cell_measurement_temperature    173(2)
_cell_measurement_theta_max      30.034
_cell_measurement_theta_min      0.998
_cell_volume                     3348.0(2)
_computing_cell_refinement       'Denzo (Nonius B.V., 1998)'
_computing_data_collection       'Collect (Nonius B.V., 1998)'
_computing_data_reduction        'Denzo (Nonius B.V., 1998)'
_computing_molecular_graphics    'PLATON 98 (Spek, 1998)'
_computing_publication_material  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      173(2)
_diffrn_detector_area_resol_mean 9
_diffrn_measured_fraction_theta_full 0.995
_diffrn_measured_fraction_theta_max 0.995
_diffrn_measurement_device_type  KappaCCD
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0576
_diffrn_reflns_av_sigmaI/netI    0.0752
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       24
_diffrn_reflns_limit_k_min       -27
_diffrn_reflns_limit_l_max       23
_diffrn_reflns_limit_l_min       -27
_diffrn_reflns_number            31573
_diffrn_reflns_theta_full        30.07
_diffrn_reflns_theta_max         30.07
_diffrn_reflns_theta_min         1.60
_exptl_absorpt_coefficient_mu    5.283
_exptl_absorpt_correction_T_max  0.564
_exptl_absorpt_correction_T_min  0.443
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'MULscanABS in PLATON (Spek, 2003)'
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    2.035
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             1976
_exptl_crystal_size_max          0.15
_exptl_crystal_size_mid          0.12
_exptl_crystal_size_min          0.10
_refine_diff_density_max         1.697
_refine_diff_density_min         -2.276
_refine_diff_density_rms         0.190
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.986
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     406
_refine_ls_number_reflns         9783
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      0.986
_refine_ls_R_factor_all          0.0746
_refine_ls_R_factor_gt           0.0392
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0333P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0711
_refine_ls_wR_factor_ref         0.0802
_reflns_number_gt                6870
_reflns_number_total             9783
_reflns_threshold_expression     I>2sigma(I)
_cod_data_source_file            c0dt01782e.txt
_cod_data_source_block           compound4a
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1555 2011-01-17 13:19:09Z saulius 
;
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               7015627
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
C1 C 0.0650(4) 0.8670(3) 0.2289(2) 0.0212(9) Uani 1 1 d . . .
C2 C 0.0420(5) 0.7493(3) 0.2652(2) 0.0294(11) Uani 1 1 d . . .
C3 C 0.2008(5) 1.0464(2) 0.2879(2) 0.0229(10) Uani 1 1 d . . .
C4 C 0.1231(6) 1.0400(3) 0.3283(3) 0.0360(12) Uani 1 1 d . . .
C5 C 0.1338(7) 1.0914(3) 0.3799(3) 0.0510(16) Uani 1 1 d . . .
C6 C 0.2211(6) 1.1491(3) 0.3919(3) 0.0405(13) Uani 1 1 d . . .
C7 C 0.2955(5) 1.1570(3) 0.3512(3) 0.0344(12) Uani 1 1 d . . .
C8 C 0.2874(5) 1.1057(3) 0.2997(3) 0.0286(11) Uani 1 1 d . . .
C9 C 0.2140(4) 1.0027(2) 0.1492(2) 0.0215(10) Uani 1 1 d . . .
C10 C 0.1268(4) 1.0597(3) 0.1076(2) 0.0257(10) Uani 1 1 d . . .
C11 C 0.1125(5) 1.0761(3) 0.0353(2) 0.0287(11) Uani 1 1 d . . .
C12 C 0.1848(5) 1.0377(3) 0.0061(2) 0.0347(13) Uani 1 1 d . . .
C13 C 0.2734(5) 0.9807(3) 0.0473(2) 0.0347(12) Uani 1 1 d . . .
C14 C 0.2866(5) 0.9624(3) 0.1190(2) 0.0292(11) Uani 1 1 d . . .
C15 C 0.6837(4) 0.8253(3) 0.3914(2) 0.0217(10) Uani 1 1 d . . .
C16 C 0.6305(5) 0.7096(3) 0.4204(3) 0.0313(11) Uani 1 1 d . . .
C17 C 0.6362(4) 0.9843(3) 0.2682(2) 0.0233(10) Uani 1 1 d . . .
C18 C 0.6308(5) 1.0557(3) 0.2575(3) 0.0322(11) Uani 1 1 d . . .
C19 C 0.6570(6) 1.0833(3) 0.2005(3) 0.0410(13) Uani 1 1 d . . .
C20 C 0.6859(6) 1.0403(3) 0.1536(3) 0.0415(14) Uani 1 1 d . . .
C21 C 0.6879(5) 0.9698(3) 0.1626(3) 0.0361(13) Uani 1 1 d . . .
C22 C 0.6641(5) 0.9408(3) 0.2205(3) 0.0304(11) Uani 1 1 d . . .
C23 C 0.6760(4) 1.0115(2) 0.4198(2) 0.0211(9) Uani 1 1 d . . .
C24 C 0.5907(5) 1.0357(3) 0.4507(2) 0.0277(11) Uani 1 1 d . . .
C25 C 0.6499(5) 1.0853(3) 0.5103(3) 0.0327(12) Uani 1 1 d . . .
C26 C 0.7943(5) 1.1100(3) 0.5394(3) 0.0331(12) Uani 1 1 d . . .
C27 C 0.8812(5) 1.0861(3) 0.5097(3) 0.0351(12) Uani 1 1 d . . .
C28 C 0.8237(5) 1.0372(3) 0.4502(2) 0.0294(11) Uani 1 1 d . . .
C29 C 0.3090(6) 0.7415(4) 0.1182(3) 0.064(2) Uani 1 1 d . . .
Cl1 Cl 0.14250(12) 0.69533(7) 0.43026(6) 0.0354(3) Uani 1 1 d . . .
Cl2 Cl 0.50222(12) 0.67948(7) 0.53075(6) 0.0347(3) Uani 1 1 d . . .
Cl3 Cl 0.47012(17) 0.74545(10) 0.21244(8) 0.0643(5) Uani 1 1 d . . .
Cl4 Cl 0.14370(19) 0.73705(14) 0.12024(10) 0.0937(8) Uani 1 1 d . . .
N1 N 0.0487(4) 0.9291(2) 0.19997(19) 0.0246(9) Uani 1 1 d . . .
N2 N 0.1962(3) 0.8390(2) 0.28698(18) 0.0208(8) Uani 1 1 d . . .
N3 N 0.1792(4) 0.7720(2) 0.30686(19) 0.0228(8) Uani 1 1 d . . .
N4 N 0.7368(4) 0.8817(2) 0.3790(2) 0.0235(8) Uani 1 1 d . . .
N5 N 0.5416(3) 0.81670(19) 0.38078(18) 0.0181(7) Uani 1 1 d . . .
N6 N 0.5166(4) 0.7512(2) 0.39922(18) 0.0214(8) Uani 1 1 d . . .
P1 P 0.21280(11) 0.97174(6) 0.23548(6) 0.0207(2) Uani 1 1 d . . .
P2 P 0.60878(11) 0.94598(6) 0.34384(6) 0.0202(2) Uani 1 1 d . . .
Pd1 Pd 0.33610(3) 0.727364(19) 0.411854(17) 0.02123(8) Uani 1 1 d . . .
Pt1 Pt 0.389666(16) 0.894302(9) 0.314650(8) 0.01790(5) Uani 1 1 d . . .
S1 S -0.08371(12) 0.80730(7) 0.19690(7) 0.0320(3) Uani 1 1 d . . .
S2 S 0.78438(12) 0.74687(7) 0.42234(7) 0.0308(3) Uani 1 1 d . . .
H2 H 0.0623 1.0001 0.3204 0.043 Uiso 1 1 calc R . .
H3 H 0.0802 1.0866 0.4073 0.061 Uiso 1 1 calc R . .
H4 H 0.2298 1.1836 0.4284 0.049 Uiso 1 1 calc R . .
H5 H 0.3532 1.1979 0.3583 0.041 Uiso 1 1 calc R . .
H6 H 0.341 1.1112 0.2724 0.034 Uiso 1 1 calc R . .
H8 H 0.0776 1.0871 0.1281 0.031 Uiso 1 1 calc R . .
H9 H 0.0516 1.1145 0.006 0.034 Uiso 1 1 calc R . .
H10 H 0.1746 1.05 -0.043 0.042 Uiso 1 1 calc R . .
H11 H 0.3242 0.9545 0.0268 0.042 Uiso 1 1 calc R . .
H12 H 0.3445 0.923 0.1472 0.035 Uiso 1 1 calc R . .
H14 H 0.0128 0.7041 0.2717 0.035 Uiso 1 1 calc R . .
H16 H 0.6093 1.0855 0.289 0.039 Uiso 1 1 calc R . .
H17 H 0.655 1.1323 0.1937 0.049 Uiso 1 1 calc R . .
H18 H 0.7045 1.0598 0.115 0.05 Uiso 1 1 calc R . .
H19 H 0.7055 0.9403 0.1293 0.043 Uiso 1 1 calc R . .
H20 H 0.667 0.8918 0.2272 0.036 Uiso 1 1 calc R . .
H22 H 0.4911 1.0184 0.4314 0.033 Uiso 1 1 calc R . .
H23 H 0.5899 1.1022 0.5309 0.039 Uiso 1 1 calc R . .
H24 H 0.834 1.1437 0.5802 0.04 Uiso 1 1 calc R . .
H25 H 0.9812 1.1033 0.5301 0.042 Uiso 1 1 calc R . .
H26 H 0.8844 1.0208 0.4298 0.035 Uiso 1 1 calc R . .
H28 H 0.6288 0.6623 0.4338 0.038 Uiso 1 1 calc R . .
H29A H 0.3062 0.7832 0.0881 0.076 Uiso 1 1 calc R . .
H29B H 0.3164 0.7002 0.0904 0.076 Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pd Pd -0.9988 1.0072 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N6 Pd1 N3 94.43(13) . . ?
N6 Pd1 Cl1 176.67(11) . . ?
N3 Pd1 Cl1 88.52(10) . . ?
N6 Pd1 Cl2 88.07(10) . . ?
N3 Pd1 Cl2 177.04(10) . . ?
Cl1 Pd1 Cl2 89.03(4) . . ?
N2 Pt1 N5 96.27(14) . . ?
N2 Pt1 P2 175.14(11) . . ?
N5 Pt1 P2 79.84(10) . . ?
N2 Pt1 P1 80.25(10) . . ?
N5 Pt1 P1 175.23(10) . . ?
P2 Pt1 P1 103.46(4) . . ?
C1 N1 P1 113.0(3) . . ?
C1 N2 N3 113.3(3) . . ?
C1 N2 Pt1 115.1(3) . . ?
N3 N2 Pt1 130.3(2) . . ?
C2 N3 N2 112.8(4) . . ?
C2 N3 Pd1 122.8(3) . . ?
N2 N3 Pd1 121.9(2) . . ?
C15 N4 P2 112.4(3) . . ?
N6 N5 C15 113.4(3) . . ?
N6 N5 Pt1 130.3(2) . . ?
C15 N5 Pt1 114.2(3) . . ?
C16 N6 N5 113.2(4) . . ?
C16 N6 Pd1 123.0(3) . . ?
N5 N6 Pd1 122.8(3) . . ?
N1 P1 C9 104.67(18) . . ?
N1 P1 C3 106.4(2) . . ?
C9 P1 C3 108.1(2) . . ?
N1 P1 Pt1 104.50(14) . . ?
C9 P1 Pt1 118.88(14) . . ?
C3 P1 Pt1 113.17(13) . . ?
N4 P2 C23 106.49(18) . . ?
N4 P2 C17 103.0(2) . . ?
C23 P2 C17 104.2(2) . . ?
N4 P2 Pt1 104.47(14) . . ?
C23 P2 Pt1 115.62(14) . . ?
C17 P2 Pt1 121.49(13) . . ?
C2 S1 C1 88.6(2) . . ?
C16 S2 C15 88.9(2) . . ?
C4 C3 C8 118.7(5) . . ?
C4 C3 P1 118.8(4) . . ?
C8 C3 P1 121.6(3) . . ?
C5 C4 C3 120.3(5) . . ?
C5 C4 H2 119.9 . . ?
C3 C4 H2 119.9 . . ?
C6 C5 C4 120.5(5) . . ?
C6 C5 H3 119.7 . . ?
C4 C5 H3 119.7 . . ?
C7 C6 C5 120.0(5) . . ?
C7 C6 H4 120.0 . . ?
C5 C6 H4 120.0 . . ?
C6 C7 C8 120.3(5) . . ?
C6 C7 H5 119.8 . . ?
C8 C7 H5 119.8 . . ?
C7 C8 C3 120.1(5) . . ?
C7 C8 H6 119.9 . . ?
C3 C8 H6 119.9 . . ?
C10 C9 C14 120.5(4) . . ?
C10 C9 P1 120.5(3) . . ?
C14 C9 P1 118.4(3) . . ?
C9 C10 C11 119.0(4) . . ?
C9 C10 H8 120.5 . . ?
C11 C10 H8 120.5 . . ?
C12 C11 C10 120.8(5) . . ?
C12 C11 H9 119.6 . . ?
C10 C11 H9 119.6 . . ?
C11 C12 C13 120.9(4) . . ?
C11 C12 H10 119.5 . . ?
C13 C12 H10 119.5 . . ?
C12 C13 C14 119.2(5) . . ?
C12 C13 H11 120.4 . . ?
C14 C13 H11 120.4 . . ?
C13 C14 C9 119.5(4) . . ?
C13 C14 H12 120.3 . . ?
C9 C14 H12 120.3 . . ?
N1 C1 N2 126.0(4) . . ?
N1 C1 S1 123.5(3) . . ?
N2 C1 S1 110.5(3) . . ?
N3 C2 S1 114.8(4) . . ?
N3 C2 H14 122.6 . . ?
S1 C2 H14 122.6 . . ?
C18 C17 C22 119.9(4) . . ?
C18 C17 P2 121.2(4) . . ?
C22 C17 P2 118.8(4) . . ?
C19 C18 C17 119.6(5) . . ?
C19 C18 H16 120.2 . . ?
C17 C18 H16 120.2 . . ?
C20 C19 C18 120.6(5) . . ?
C20 C19 H17 119.7 . . ?
C18 C19 H17 119.7 . . ?
C19 C20 C21 120.2(5) . . ?
C19 C20 H18 119.9 . . ?
C21 C20 H18 119.9 . . ?
C20 C21 C22 120.3(5) . . ?
C20 C21 H19 119.9 . . ?
C20 C21 H19 119.9 . . ?
C17 C22 C21 119.5(5) . . ?
C17 C22 H20 120.3 . . ?
C21 C22 H20 120.3 . . ?
C24 C23 C28 118.7(4) . . ?
C24 C23 P2 122.9(3) . . ?
C28 C23 P2 118.4(3) . . ?
C23 C24 C25 120.2(4) . . ?
C23 C24 H22 119.9 . . ?
C25 C24 H22 119.9 . . ?
C26 C25 C24 120.5(5) . . ?
C26 C25 H23 119.8 . . ?
C24 C25 H23 119.8 . . ?
C27 C26 C25 120.1(5) . . ?
C27 C26 H24 119.9 . . ?
C25 C26 H24 119.9 . . ?
C26 C27 C28 120.1(4) . . ?
C26 C27 H25 120.0 . . ?
C28 C27 H25 120.0 . . ?
C27 C28 C23 120.4(4) . . ?
C27 C28 H26 119.8 . . ?
C23 C28 H26 119.8 . . ?
N4 C15 N5 126.2(4) . . ?
N4 C15 S2 123.9(3) . . ?
N5 C15 S2 109.9(3) . . ?
N6 C16 S2 114.5(4) . . ?
N6 C16 H28 122.7 . . ?
S2 C16 H28 122.7 . . ?
Cl4 C29 Cl3 112.8(3) . . ?
Cl4 C29 H29A 109.0 . . ?
Cl3 C29 H29A 109.0 . . ?
Cl4 C29 H29B 109.0 . . ?
Cl3 C29 H29B 109.0 . . ?
H29A C29 H29B 107.8 . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Cl1 Pd1 2.2754(11) . ?
Cl2 Pd1 2.2779(11) . ?
N1 P1 1.671(4) . ?
N2 N3 1.383(5) . ?
N2 Pt1 2.065(3) . ?
N3 Pd1 2.056(3) . ?
N4 P2 1.676(4) . ?
N5 N6 1.371(5) . ?
N5 Pt1 2.072(3) . ?
N6 Pd1 2.040(3) . ?
P1 Pt1 2.2512(11) . ?
P2 Pt1 2.2469(11) . ?
C1 N1 1.297(6) . ?
C1 N2 1.359(5) . ?
C1 S1 1.751(4) . ?
C2 N3 1.292(5) . ?
C2 S1 1.719(5) . ?
C2 H14 0.9500 . ?
C3 C4 1.387(6) . ?
C3 C8 1.392(6) . ?
C3 P1 1.810(5) . ?
C4 C5 1.382(7) . ?
C4 H2 0.9500 . ?
C5 C6 1.369(8) . ?
C5 H3 0.9500 . ?
C6 C7 1.367(7) . ?
C6 H4 0.9500 . ?
C7 C8 1.389(6) . ?
C7 H5 0.9500 . ?
C8 H6 0.9500 . ?
C9 C10 1.389(6) . ?
C9 C14 1.399(6) . ?
C9 P1 1.808(4) . ?
C10 C11 1.391(6) . ?
C10 H8 0.9500 . ?
C11 C12 1.364(7) . ?
C11 H9 0.9500 . ?
C12 C13 1.392(7) . ?
C12 H10 0.9500 . ?
C13 C14 1.395(6) . ?
C13 H11 0.9500 . ?
C14 H12 0.9500 . ?
C15 N4 1.291(5) . ?
C15 N5 1.371(5) . ?
C15 S2 1.754(5) . ?
C16 N6 1.298(6) . ?
C16 S2 1.715(5) . ?
C16 H28 0.9500 . ?
C17 C18 1.387(7) . ?
C17 C22 1.394(6) . ?
C17 P2 1.808(4) . ?
C18 C19 1.387(6) . ?
C18 H16 0.9500 . ?
C19 C20 1.380(7) . ?
C19 H17 0.9500 . ?
C20 C21 1.368(7) . ?
C20 H18 0.9500 . ?
C21 C22 1.399(6) . ?
C21 H19 0.9500 . ?
C22 H20 0.9500 . ?
C23 C24 1.376(6) . ?
C23 C28 1.405(6) . ?
C23 P2 1.804(4) . ?
C24 C25 1.391(6) . ?
C24 H22 0.9500 . ?
C25 C26 1.372(7) . ?
C25 H23 0.9500 . ?
C26 C27 1.370(7) . ?
C26 H24 0.9500 . ?
C27 C28 1.381(6) . ?
C27 H25 0.9500 . ?
C28 H26 0.9500 . ?
C29 Cl4 1.716(6) . ?
C29 Cl3 1.751(5) . ?
C29 H29A 0.9900 . ?
C29 H29B 0.9900 . ?
