#------------------------------------------------------------------------------
#$Date: 2016-03-25 13:50:30 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179866 $
#$URL: svn://www.crystallography.net/cod/cif/7/01/62/7016244.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7016244
loop_
_publ_author_name
'McLellan, R.'
'Boag, N. M.'
'Dodds, K.'
'Ellis, D.'
'Macgregor, S. A.'
'McKay, D.'
'Masters, S. L.'
'Noble-Eddy, R'
'Platt, N. P.'
'Rankin, D. W. H.'
'Robertson, H. E.'
'Rosair, G. M.'
'Welch, A. J.'
_publ_section_title
;
 New chemistry of 1,2-closo-P(2)B(10)H(10) and
 1,2-closo-As(2)B(10)H(10); in silico and gas electron diffraction
 structures, and new metalladiphospha- and metalladiarsaboranes.
;
_journal_issue                   27
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              7181
_journal_page_last               7192
_journal_paper_doi               10.1039/c1dt10540j
_journal_volume                  40
_journal_year                    2011
_chemical_formula_moiety         'C5 H14 As2 B9 Co'
_chemical_formula_sum            'C5 H14 As2 B9 Co'
_chemical_formula_weight         380.22
_chemical_name_common            x82839
_chemical_name_systematic
;

?

;
_space_group_IT_number           4
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  'P 2yb'
_symmetry_space_group_name_H-M   'P 1 21 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 113.331(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   7.2969(9)
_cell_length_b                   10.6713(13)
_cell_length_c                   8.8333(11)
_cell_measurement_reflns_used    7513
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      30.60
_cell_measurement_theta_min      2.52
_cell_volume                     631.58(14)
_computing_cell_refinement       'APEX2 (Bruker, 2009)'
_computing_data_collection       'APEX2 (Bruker, 2009)'
_computing_data_reduction        'APEX2 (Bruker, 2009)'
_computing_molecular_graphics    'SHELXTL (Sheldrick, 2008)'
_computing_publication_material  'SHELXTL (Sheldrick, 2008)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      100(2)
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 0.995
_diffrn_measurement_device_type  'Bruker APEX2'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0302
_diffrn_reflns_av_sigmaI/netI    0.0298
_diffrn_reflns_limit_h_max       10
_diffrn_reflns_limit_h_min       -10
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_k_min       -14
_diffrn_reflns_limit_l_max       12
_diffrn_reflns_limit_l_min       -12
_diffrn_reflns_number            12583
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         30.58
_diffrn_reflns_theta_min         2.51
_exptl_absorpt_coefficient_mu    6.516
_exptl_absorpt_correction_T_max  0.5619
_exptl_absorpt_correction_T_min  0.1617
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'SADABS (Bruker, 2009)'
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.999
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             364
_exptl_crystal_size_max          0.44
_exptl_crystal_size_mid          0.28
_exptl_crystal_size_min          0.10
_refine_diff_density_max         0.681
_refine_diff_density_min         -0.391
_refine_diff_density_rms         0.074
_refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881'
_refine_ls_abs_structure_Flack   0.259(11)
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.047
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     162
_refine_ls_number_reflns         3461
_refine_ls_number_restraints     6
_refine_ls_restrained_S_all      1.057
_refine_ls_R_factor_all          0.0214
_refine_ls_R_factor_gt           0.0191
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0163P)²+0.1916P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0429
_refine_ls_wR_factor_ref         0.0436
_reflns_number_gt                3290
_reflns_number_total             3461
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c1dt10540j.txt
_cod_data_source_block           x82561
_cod_original_cell_volume        631.58(13)
_cod_original_sg_symbol_H-M      P21
_cod_database_code               7016244
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Co3 Co 0.78152(4) 0.75637(3) 1.05848(3) 0.01019(6) Uani 1 1 d . . .
As1 As 0.42910(3) 0.75068(2) 0.90370(3) 0.01410(5) Uani 1 1 d D A .
As2 As 0.63940(5) 0.93105(3) 0.88066(4) 0.01194(9) Uani 0.7838(13) 1 d PD A -1
B2 B 0.6444(19) 0.8908(13) 0.878(2) 0.01194(9) Uani 0.22 1 d PD A -2
H2 H 0.6424 0.9862 0.9303 0.014 Uiso 0.2162(13) 1 calc PR A -2
As4 As 0.6373(2) 0.56602(13) 0.9145(2) 0.0131(4) Uani 0.2162(13) 1 d PD A -2
B4 B 0.6338(8) 0.6058(5) 0.8984(8) 0.0131(4) Uani 0.7838(13) 1 d PD A -1
H4 H 0.6259 0.5180 0.9650 0.016 Uiso 0.7838(13) 1 calc PR A -1
B5 B 0.4319(4) 0.6523(3) 0.6934(4) 0.0147(5) Uani 1 1 d . . .
H5 H 0.2928 0.5959 0.6309 0.018 Uiso 1 1 calc R A .
B6 B 0.4302(4) 0.8235(3) 0.6704(4) 0.0147(5) Uani 1 1 d . A .
H6 H 0.2905 0.8752 0.5941 0.018 Uiso 1 1 calc R . .
B7 B 0.8827(5) 0.8232(3) 0.8732(3) 0.0142(5) Uani 1 1 d D A .
H7 H 1.0304 0.8723 0.9235 0.017 Uiso 1 1 calc R . .
B8 B 0.8676(4) 0.6567(2) 0.8910(4) 0.0138(5) Uani 1 1 d D A .
H8 H 1.0079 0.6017 0.9554 0.017 Uiso 1 1 calc R . .
B9 B 0.6692(4) 0.5961(2) 0.7084(4) 0.0163(6) Uani 1 1 d . A .
H9 H 0.6805 0.5019 0.6570 0.020 Uiso 1 1 calc R . .
B10 B 0.5529(4) 0.7248(2) 0.5788(3) 0.0161(5) Uani 1 1 d . A .
H10 H 0.4886 0.7148 0.4414 0.019 Uiso 1 1 calc R . .
B11 B 0.6744(4) 0.8654(3) 0.6716(4) 0.0154(5) Uani 1 1 d . . .
H11 H 0.6875 0.9451 0.5939 0.019 Uiso 1 1 calc R A .
B12 B 0.8158(4) 0.7259(2) 0.6951(3) 0.0152(5) Uani 1 1 d . A .
H12 H 0.9231 0.7168 0.6336 0.018 Uiso 1 1 calc R . .
C30 C 0.9700(5) 0.6601(3) 1.2600(3) 0.0265(7) Uani 1 1 d . A .
H30 H 1.0291 0.5757 1.2591 0.032 Uiso 1 1 calc R . .
C31 C 0.7880(5) 0.6844(3) 1.2782(3) 0.0208(6) Uani 1 1 d . A .
H31 H 0.6950 0.6203 1.2908 0.025 Uiso 1 1 calc R . .
C32 C 0.7638(4) 0.8160(3) 1.2760(3) 0.0170(5) Uani 1 1 d . A .
H32 H 0.6482 0.8611 1.2845 0.020 Uiso 1 1 calc R . .
C33 C 0.9270(4) 0.8728(3) 1.2574(3) 0.0197(5) Uani 1 1 d . A .
H33 H 0.9479 0.9650 1.2516 0.024 Uiso 1 1 calc R . .
C34 C 1.0552(3) 0.7781(3) 1.2466(3) 0.0232(6) Uani 1 1 d . A .
H34 H 1.1846 0.7910 1.2347 0.028 Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
As As 0.0499 2.0058 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C34 Co3 C30 40.95(12) . . ?
C34 Co3 C33 39.98(10) . . ?
C30 Co3 C33 67.66(11) . . ?
C34 Co3 C31 68.15(12) . . ?
C30 Co3 C31 40.47(12) . . ?
C33 Co3 C31 67.25(11) . . ?
C34 Co3 C32 67.15(11) . . ?
C30 Co3 C32 67.35(11) . . ?
C33 Co3 C32 39.56(11) . . ?
C31 Co3 C32 39.91(9) . . ?
C34 Co3 B2 124.3(4) . . ?
C30 Co3 B2 165.1(4) . . ?
C33 Co3 B2 99.5(5) . . ?
C31 Co3 B2 143.0(4) . . ?
C32 Co3 B2 108.0(4) . . ?
C34 Co3 B8 99.26(10) . . ?
C30 Co3 B8 94.19(11) . . ?
C33 Co3 B8 134.68(11) . . ?
C31 Co3 B8 124.58(11) . . ?
C32 Co3 B8 161.53(11) . . ?
B2 Co3 B8 89.8(4) . . ?
C34 Co3 B4 134.44(16) . . ?
C30 Co3 B4 100.86(17) . . ?
C33 Co3 B4 166.29(17) . . ?
C31 Co3 B4 99.21(18) . . ?
C32 Co3 B4 130.17(18) . . ?
B2 Co3 B4 92.8(4) . . ?
B8 Co3 B4 50.73(16) . . ?
C34 Co3 B7 93.51(11) . . ?
C30 Co3 B7 120.70(12) . . ?
C33 Co3 B7 103.30(11) . . ?
C31 Co3 B7 160.50(12) . . ?
C32 Co3 B7 139.75(11) . . ?
B2 Co3 B7 53.1(3) . . ?
B8 Co3 B7 49.51(10) . . ?
B4 Co3 B7 88.92(18) . . ?
C34 Co3 As1 162.32(7) . . ?
C30 Co3 As1 133.37(10) . . ?
C33 Co3 As1 125.14(8) . . ?
C31 Co3 As1 98.45(9) . . ?
C32 Co3 As1 95.17(8) . . ?
B2 Co3 As1 59.8(3) . . ?
B8 Co3 As1 97.92(8) . . ?
B4 Co3 As1 56.87(14) . . ?
B7 Co3 As1 100.83(8) . . ?
C34 Co3 As2 118.38(8) . . ?
C30 Co3 As2 158.50(10) . . ?
C33 Co3 As2 91.89(8) . . ?
C31 Co3 As2 138.37(8) . . ?
C32 Co3 As2 101.48(8) . . ?
B2 Co3 As2 7.7(4) . . ?
B8 Co3 As2 95.99(8) . . ?
B4 Co3 As2 100.25(14) . . ?
B7 Co3 As2 55.68(7) . . ?
As1 Co3 As2 63.608(13) . . ?
C34 Co3 As4 127.41(9) . . ?
C30 Co3 As4 92.23(10) . . ?
C33 Co3 As4 157.78(9) . . ?
C31 Co3 As4 91.44(9) . . ?
C32 Co3 As4 125.00(8) . . ?
B2 Co3 As4 101.5(4) . . ?
B8 Co3 As4 52.63(8) . . ?
B4 Co3 As4 8.83(15) . . ?
B7 Co3 As4 95.00(9) . . ?
As1 Co3 As4 61.93(4) . . ?
As2 Co3 As4 108.99(4) . . ?
B5 As1 B4 52.18(19) . . ?
B5 As1 B6 50.00(11) . . ?
B4 As1 B6 88.49(17) . . ?
B5 As1 B2 89.5(4) . . ?
B4 As1 B2 87.5(3) . . ?
B6 As1 B2 53.8(5) . . ?
B5 As1 Co3 97.53(8) . . ?
B4 As1 Co3 55.55(16) . . ?
B6 As1 Co3 97.15(8) . . ?
B2 As1 Co3 53.3(4) . . ?
B5 As1 As4 54.86(9) . . ?
B4 As1 As4 8.07(15) . . ?
B6 As1 As4 95.02(8) . . ?
B2 As1 As4 95.2(3) . . ?
Co3 As1 As4 59.41(4) . . ?
B5 As1 As2 95.10(8) . . ?
B4 As1 As2 95.53(14) . . ?
B6 As1 As2 55.08(8) . . ?
B2 As1 As2 8.0(3) . . ?
Co3 As1 As2 58.300(14) . . ?
As4 As1 As2 103.17(4) . . ?
B11 As2 B7 52.92(11) . . ?
B11 As2 B6 50.55(11) . . ?
B7 As2 B6 90.02(11) . . ?
B11 As2 Co3 98.44(8) . . ?
B7 As2 Co3 56.76(7) . . ?
B6 As2 Co3 97.08(8) . . ?
B11 As2 As1 96.16(8) . . ?
B7 As2 As1 97.53(8) . . ?
B6 As2 As1 55.20(8) . . ?
Co3 As2 As1 58.092(14) . . ?
B7 B2 B11 58.7(4) . . ?
B7 B2 B6 103.3(7) . . ?
B11 B2 B6 55.2(5) . . ?
B7 B2 Co3 65.7(5) . . ?
B11 B2 Co3 115.1(6) . . ?
B6 B2 Co3 114.6(7) . . ?
B7 B2 As1 115.7(7) . . ?
B11 B2 As1 110.2(7) . . ?
B6 B2 As1 62.1(4) . . ?
Co3 B2 As1 66.9(4) . . ?
B7 B2 H2 121.1 . . ?
B11 B2 H2 122.6 . . ?
B6 B2 H2 124.5 . . ?
Co3 B2 H2 113.1 . . ?
As1 B2 H2 116.1 . . ?
B9 As4 B8 54.12(12) . . ?
B9 As4 B5 51.51(12) . . ?
B8 As4 B5 90.61(13) . . ?
B9 As4 Co3 99.52(10) . . ?
B8 As4 Co3 56.11(9) . . ?
B5 As4 Co3 96.92(9) . . ?
B9 As4 As1 97.56(10) . . ?
B8 As4 As1 97.93(9) . . ?
B5 As4 As1 54.80(8) . . ?
Co3 As4 As1 58.66(4) . . ?
B9 B4 B8 60.0(2) . . ?
B9 B4 B5 57.8(2) . . ?
B8 B4 B5 105.9(3) . . ?
B9 B4 Co3 116.1(3) . . ?
B8 B4 Co3 64.1(2) . . ?
B5 B4 Co3 115.8(2) . . ?
B9 B4 As1 114.6(3) . . ?
B8 B4 As1 117.0(3) . . ?
B5 B4 As1 63.31(17) . . ?
Co3 B4 As1 67.59(16) . . ?
B9 B4 H4 119.9 . . ?
B8 B4 H4 120.9 . . ?
B5 B4 H4 122.7 . . ?
Co3 B4 H4 113.6 . . ?
As1 B4 H4 114.0 . . ?
B10 B5 B9 59.93(16) . . ?
B10 B5 B6 58.93(15) . . ?
B9 B5 B6 107.8(2) . . ?
B10 B5 B4 106.7(2) . . ?
B9 B5 B4 58.5(2) . . ?
B6 B5 B4 109.6(2) . . ?
B10 B5 As1 117.54(16) . . ?
B9 B5 As1 116.24(18) . . ?
B6 B5 As1 66.83(14) . . ?
B4 B5 As1 64.5(2) . . ?
B10 B5 As4 112.52(17) . . ?
B9 B5 As4 58.70(14) . . ?
B6 B5 As4 120.0(2) . . ?
B4 B5 As4 10.50(17) . . ?
As1 B5 As4 70.34(10) . . ?
B10 B5 H5 121.0 . . ?
B9 B5 H5 121.2 . . ?
B6 B5 H5 121.0 . . ?
B4 B5 H5 122.7 . . ?
As1 B5 H5 111.9 . . ?
As4 B5 H5 112.9 . . ?
B10 B6 B11 58.80(15) . . ?
B10 B6 B5 58.45(15) . . ?
B11 B6 B5 106.1(2) . . ?
B10 B6 B2 106.1(4) . . ?
B11 B6 B2 60.4(4) . . ?
B5 B6 B2 106.6(5) . . ?
B10 B6 As2 112.83(16) . . ?
B11 B6 As2 61.35(12) . . ?
B5 B6 As2 116.91(19) . . ?
B2 B6 As2 10.6(4) . . ?
B10 B6 As1 113.98(16) . . ?
B11 B6 As1 116.35(17) . . ?
B5 B6 As1 63.17(14) . . ?
B2 B6 As1 64.1(4) . . ?
As2 B6 As1 69.73(9) . . ?
B10 B6 H6 121.5 . . ?
B11 B6 H6 122.3 . . ?
B5 B6 H6 121.4 . . ?
B2 B6 H6 124.5 . . ?
As2 B6 H6 114.4 . . ?
As1 B6 H6 113.4 . . ?
B12 B7 B8 59.69(15) . . ?
B12 B7 B11 57.89(15) . . ?
B8 B7 B11 105.4(2) . . ?
B12 B7 B2 107.9(6) . . ?
B8 B7 B2 106.6(5) . . ?
B11 B7 B2 61.8(6) . . ?
B12 B7 As2 113.55(17) . . ?
B8 B7 As2 116.76(19) . . ?
B11 B7 As2 62.02(12) . . ?
B2 B7 As2 10.2(4) . . ?
B12 B7 Co3 114.74(16) . . ?
B8 B7 Co3 63.61(14) . . ?
B11 B7 Co3 113.86(16) . . ?
B2 B7 Co3 61.2(5) . . ?
As2 B7 Co3 67.55(8) . . ?
B12 B7 H7 120.4 . . ?
B8 B7 H7 120.8 . . ?
B11 B7 H7 123.6 . . ?
B2 B7 H7 124.0 . . ?
As2 B7 H7 114.6 . . ?
Co3 B7 H7 114.6 . . ?
B12 B8 B7 59.97(16) . . ?
B12 B8 B9 59.59(16) . . ?
B7 B8 B9 109.4(2) . . ?
B12 B8 B4 108.6(3) . . ?
B7 B8 B4 113.0(2) . . ?
B9 B8 B4 59.5(2) . . ?
B12 B8 As4 115.71(17) . . ?
B7 B8 As4 124.6(2) . . ?
B9 B8 As4 60.99(13) . . ?
B4 B8 As4 11.87(16) . . ?
B12 B8 Co3 117.73(16) . . ?
B7 B8 Co3 66.87(13) . . ?
B9 B8 Co3 116.76(16) . . ?
B4 B8 Co3 65.2(2) . . ?
As4 B8 Co3 71.26(10) . . ?
B12 B8 H8 120.7 . . ?
B7 B8 H8 119.2 . . ?
B9 B8 H8 120.9 . . ?
B4 B8 H8 120.5 . . ?
As4 B8 H8 109.1 . . ?
Co3 B8 H8 112.0 . . ?
B10 B9 B12 60.13(14) . . ?
B10 B9 B5 59.38(15) . . ?
B12 B9 B5 108.89(18) . . ?
B10 B9 B4 110.4(2) . . ?
B12 B9 B4 109.2(2) . . ?
B5 B9 B4 63.7(2) . . ?
B10 B9 B8 107.98(18) . . ?
B12 B9 B8 59.43(15) . . ?
B5 B9 B8 110.9(2) . . ?
B4 B9 B8 60.5(2) . . ?
B10 B9 As4 121.78(17) . . ?
B12 B9 As4 119.10(18) . . ?
B5 B9 As4 69.80(15) . . ?
B4 B9 As4 12.83(16) . . ?
B8 B9 As4 64.89(15) . . ?
B10 B9 H9 121.8 . . ?
B12 B9 H9 121.9 . . ?
B5 B9 H9 119.8 . . ?
B4 B9 H9 119.4 . . ?
B8 B9 H9 121.4 . . ?
As4 B9 H9 106.6 . . ?
B5 B10 B11 112.24(19) . . ?
B5 B10 B6 62.63(14) . . ?
B11 B10 B6 62.31(16) . . ?
B5 B10 B9 60.68(16) . . ?
B11 B10 B9 109.49(18) . . ?
B6 B10 B9 111.4(2) . . ?
B5 B10 B12 109.98(18) . . ?
B11 B10 B12 60.00(14) . . ?
B6 B10 B12 110.86(19) . . ?
B9 B10 B12 60.18(15) . . ?
B5 B10 H10 119.4 . . ?
B11 B10 H10 120.0 . . ?
B6 B10 H10 118.7 . . ?
B9 B10 H10 121.0 . . ?
B12 B10 H10 121.3 . . ?
B10 B11 B12 60.30(15) . . ?
B10 B11 B6 58.89(14) . . ?
B12 B11 B6 108.33(18) . . ?
B10 B11 B7 107.68(18) . . ?
B12 B11 B7 58.30(14) . . ?
B6 B11 B7 111.5(2) . . ?
B10 B11 B2 109.3(4) . . ?
B12 B11 B2 106.5(4) . . ?
B6 B11 B2 64.4(4) . . ?
B7 B11 B2 59.6(4) . . ?
B10 B11 As2 118.73(16) . . ?
B12 B11 As2 116.59(17) . . ?
B6 B11 As2 68.10(14) . . ?
B7 B11 As2 65.05(12) . . ?
B2 B11 As2 11.7(4) . . ?
B10 B11 H11 120.5 . . ?
B12 B11 H11 121.4 . . ?
B6 B11 H11 120.0 . . ?
B7 B11 H11 121.9 . . ?
B2 B11 H11 122.6 . . ?
As2 B11 H11 111.0 . . ?
B8 B12 B11 110.58(19) . . ?
B8 B12 B9 60.98(16) . . ?
B11 B12 B9 108.84(17) . . ?
B8 B12 B10 108.87(17) . . ?
B11 B12 B10 59.70(14) . . ?
B9 B12 B10 59.69(15) . . ?
B8 B12 B7 60.35(14) . . ?
B11 B12 B7 63.81(16) . . ?
B9 B12 B7 110.84(19) . . ?
B10 B12 B7 111.63(18) . . ?
B8 B12 H12 121.0 . . ?
B11 B12 H12 120.1 . . ?
B9 B12 H12 121.2 . . ?
B10 B12 H12 121.3 . . ?
B7 B12 H12 118.6 . . ?
C31 C30 C34 107.8(3) . . ?
C31 C30 Co3 70.78(16) . . ?
C34 C30 Co3 69.51(15) . . ?
C31 C30 H30 126.1 . . ?
C34 C30 H30 126.1 . . ?
Co3 C30 H30 126.1 . . ?
C32 C31 C30 107.2(3) . . ?
C32 C31 Co3 70.24(18) . . ?
C30 C31 Co3 68.75(16) . . ?
C32 C31 H31 126.4 . . ?
C30 C31 H31 126.4 . . ?
Co3 C31 H31 126.4 . . ?
C33 C32 C31 108.9(3) . . ?
C33 C32 Co3 69.97(15) . . ?
C31 C32 Co3 69.85(18) . . ?
C33 C32 H32 125.5 . . ?
C31 C32 H32 125.5 . . ?
Co3 C32 H32 125.5 . . ?
C32 C33 C34 108.4(2) . . ?
C32 C33 Co3 70.48(15) . . ?
C34 C33 Co3 69.01(15) . . ?
C32 C33 H33 125.8 . . ?
C34 C33 H33 125.8 . . ?
Co3 C33 H33 125.8 . . ?
C33 C34 C30 107.7(2) . . ?
C33 C34 Co3 71.01(14) . . ?
C30 C34 Co3 69.55(15) . . ?
C33 C34 H34 126.1 . . ?
C30 C34 H34 126.1 . . ?
Co3 C34 H34 126.1 . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Co3 C34 2.043(2) . ?
Co3 C30 2.043(3) . ?
Co3 C33 2.069(3) . ?
Co3 C31 2.070(3) . ?
Co3 C32 2.076(3) . ?
Co3 B2 2.082(16) . ?
Co3 B8 2.109(3) . ?
Co3 B4 2.130(6) . ?
Co3 B7 2.166(3) . ?
Co3 As1 2.3877(4) . ?
Co3 As2 2.3931(5) . ?
Co3 As4 2.4066(16) . ?
As1 B5 2.141(3) . ?
As1 B4 2.163(5) . ?
As1 B6 2.205(3) . ?
As1 B2 2.244(13) . ?
As1 As4 2.4669(15) . ?
As1 As2 2.5196(5) . ?
As2 B11 2.083(3) . ?
As2 B7 2.139(3) . ?
As2 B6 2.202(3) . ?
B2 B7 1.899(12) . ?
B2 B11 1.941(17) . ?
B2 B6 2.014(17) . ?
B2 H2 1.1200 . ?
As4 B9 1.950(4) . ?
As4 B8 2.020(3) . ?
As4 B5 2.142(3) . ?
B4 B9 1.799(7) . ?
B4 B8 1.816(6) . ?
B4 B5 1.893(7) . ?
B4 H4 1.1200 . ?
B5 B10 1.763(4) . ?
B5 B9 1.787(4) . ?
B5 B6 1.838(4) . ?
B5 H5 1.1200 . ?
B6 B10 1.772(4) . ?
B6 B11 1.833(4) . ?
B6 H6 1.1200 . ?
B7 B12 1.784(4) . ?
B7 B8 1.791(4) . ?
B7 B11 1.882(4) . ?
B7 H7 1.1200 . ?
B8 B12 1.779(4) . ?
B8 B9 1.807(4) . ?
B8 H8 1.1200 . ?
B9 B10 1.773(4) . ?
B9 B12 1.782(4) . ?
B9 H9 1.1200 . ?
B10 B11 1.771(4) . ?
B10 B12 1.781(3) . ?
B10 H10 1.1200 . ?
B11 B12 1.776(4) . ?
B11 H11 1.1200 . ?
B12 H12 1.1200 . ?
C30 C31 1.423(4) . ?
C30 C34 1.429(4) . ?
C30 H30 1.0000 . ?
C31 C32 1.415(3) . ?
C31 H31 1.0000 . ?
C32 C33 1.402(4) . ?
C32 H32 1.0000 . ?
C33 C34 1.406(4) . ?
C33 H33 1.0000 . ?
C34 H34 1.0000 . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C34 Co3 As1 B5 -167.6(3) . . . . ?
C30 Co3 As1 B5 -104.89(14) . . . . ?
C33 Co3 As1 B5 163.64(12) . . . . ?
C31 Co3 As1 B5 -128.29(11) . . . . ?
C32 Co3 As1 B5 -168.37(11) . . . . ?
B2 Co3 As1 B5 83.8(5) . . . . ?
B8 Co3 As1 B5 -1.42(11) . . . . ?
B4 Co3 As1 B5 -32.8(2) . . . . ?
B7 Co3 As1 B5 48.73(10) . . . . ?
As2 Co3 As1 B5 91.36(8) . . . . ?
As4 Co3 As1 B5 -41.18(9) . . . . ?
C34 Co3 As1 B4 -134.9(3) . . . . ?
C30 Co3 As1 B4 -72.1(2) . . . . ?
C33 Co3 As1 B4 -163.6(2) . . . . ?
C31 Co3 As1 B4 -95.5(2) . . . . ?
C32 Co3 As1 B4 -135.6(2) . . . . ?
B2 Co3 As1 B4 116.5(5) . . . . ?
B8 Co3 As1 B4 31.3(2) . . . . ?
B7 Co3 As1 B4 81.5(2) . . . . ?
As2 Co3 As1 B4 124.13(18) . . . . ?
As4 Co3 As1 B4 -8.4(2) . . . . ?
C34 Co3 As1 B6 141.9(3) . . . . ?
C30 Co3 As1 B6 -155.33(14) . . . . ?
C33 Co3 As1 B6 113.20(12) . . . . ?
C31 Co3 As1 B6 -178.73(12) . . . . ?
C32 Co3 As1 B6 141.19(12) . . . . ?
B2 Co3 As1 B6 33.3(5) . . . . ?
B8 Co3 As1 B6 -51.86(11) . . . . ?
B4 Co3 As1 B6 -83.2(2) . . . . ?
B7 Co3 As1 B6 -1.71(10) . . . . ?
As2 Co3 As1 B6 40.93(8) . . . . ?
As4 Co3 As1 B6 -91.62(9) . . . . ?
C34 Co3 As1 B2 108.6(6) . . . . ?
C30 Co3 As1 B2 171.4(5) . . . . ?
C33 Co3 As1 B2 79.9(5) . . . . ?
C31 Co3 As1 B2 148.0(5) . . . . ?
C32 Co3 As1 B2 107.9(5) . . . . ?
B8 Co3 As1 B2 -85.2(5) . . . . ?
B4 Co3 As1 B2 -116.5(5) . . . . ?
B7 Co3 As1 B2 -35.0(5) . . . . ?
As2 Co3 As1 B2 7.6(5) . . . . ?
As4 Co3 As1 B2 -124.9(5) . . . . ?
C34 Co3 As1 As4 -126.5(3) . . . . ?
C30 Co3 As1 As4 -63.71(12) . . . . ?
C33 Co3 As1 As4 -155.18(10) . . . . ?
C31 Co3 As1 As4 -87.11(9) . . . . ?
C32 Co3 As1 As4 -127.19(8) . . . . ?
B2 Co3 As1 As4 124.9(5) . . . . ?
B8 Co3 As1 As4 39.76(9) . . . . ?
B4 Co3 As1 As4 8.4(2) . . . . ?
B7 Co3 As1 As4 89.91(9) . . . . ?
As2 Co3 As1 As4 132.55(5) . . . . ?
C34 Co3 As1 As2 101.0(3) . . . . ?
C30 Co3 As1 As2 163.75(12) . . . . ?
C33 Co3 As1 As2 72.28(10) . . . . ?
C31 Co3 As1 As2 140.35(8) . . . . ?
C32 Co3 As1 As2 100.27(8) . . . . ?
B2 Co3 As1 As2 -7.6(5) . . . . ?
B8 Co3 As1 As2 -92.79(8) . . . . ?
B4 Co3 As1 As2 -124.13(18) . . . . ?
B7 Co3 As1 As2 -42.63(7) . . . . ?
As4 Co3 As1 As2 -132.55(5) . . . . ?
C34 Co3 As2 B11 107.78(11) . . . . ?
C30 Co3 As2 B11 121.7(2) . . . . ?
C33 Co3 As2 B11 139.17(11) . . . . ?
C31 Co3 As2 B11 -163.88(15) . . . . ?
C32 Co3 As2 B11 177.87(12) . . . . ?
B2 Co3 As2 B11 -33(2) . . . . ?
B8 Co3 As2 B11 3.86(11) . . . . ?
B4 Co3 As2 B11 -47.25(17) . . . . ?
B7 Co3 As2 B11 34.32(12) . . . . ?
As1 Co3 As2 B11 -92.03(8) . . . . ?
As4 Co3 As2 B11 -48.59(8) . . . . ?
C34 Co3 As2 B7 73.46(13) . . . . ?
C30 Co3 As2 B7 87.4(3) . . . . ?
C33 Co3 As2 B7 104.85(12) . . . . ?
C31 Co3 As2 B7 161.80(17) . . . . ?
C32 Co3 As2 B7 143.55(13) . . . . ?
B2 Co3 As2 B7 -68(2) . . . . ?
B8 Co3 As2 B7 -30.46(14) . . . . ?
B4 Co3 As2 B7 -81.57(18) . . . . ?
As1 Co3 As2 B7 -126.35(10) . . . . ?
As4 Co3 As2 B7 -82.91(11) . . . . ?
C34 Co3 As2 B6 158.82(11) . . . . ?
C30 Co3 As2 B6 172.7(2) . . . . ?
C33 Co3 As2 B6 -169.79(11) . . . . ?
C31 Co3 As2 B6 -112.84(15) . . . . ?
C32 Co3 As2 B6 -131.10(11) . . . . ?
B2 Co3 As2 B6 18(2) . . . . ?
B8 Co3 As2 B6 54.90(10) . . . . ?
B4 Co3 As2 B6 3.79(16) . . . . ?
B7 Co3 As2 B6 85.36(13) . . . . ?
As1 Co3 As2 B6 -40.99(7) . . . . ?
As4 Co3 As2 B6 2.44(8) . . . . ?
C34 Co3 As2 As1 -160.19(8) . . . . ?
C30 Co3 As2 As1 -146.3(2) . . . . ?
C33 Co3 As2 As1 -128.80(8) . . . . ?
C31 Co3 As2 As1 -71.85(13) . . . . ?
C32 Co3 As2 As1 -90.11(8) . . . . ?
B2 Co3 As2 As1 59(2) . . . . ?
B8 Co3 As2 As1 95.89(8) . . . . ?
B4 Co3 As2 As1 44.78(15) . . . . ?
B7 Co3 As2 As1 126.35(10) . . . . ?
As4 Co3 As2 As1 43.43(4) . . . . ?
B5 As1 As2 B11 0.41(11) . . . . ?
B4 As1 As2 B11 52.83(19) . . . . ?
B6 As1 As2 B11 -31.43(12) . . . . ?
B2 As1 As2 B11 47(3) . . . . ?
Co3 As1 As2 B11 96.12(8) . . . . ?
As4 As1 As2 B11 55.48(9) . . . . ?
B5 As1 As2 B7 -52.90(11) . . . . ?
B4 As1 As2 B7 -0.49(18) . . . . ?
B6 As1 As2 B7 -84.75(12) . . . . ?
B2 As1 As2 B7 -7(3) . . . . ?
Co3 As1 As2 B7 42.81(8) . . . . ?
As4 As1 As2 B7 2.17(9) . . . . ?
B5 As1 As2 B6 31.85(13) . . . . ?
B4 As1 As2 B6 84.26(19) . . . . ?
B2 As1 As2 B6 78(3) . . . . ?
Co3 As1 As2 B6 127.56(9) . . . . ?
As4 As1 As2 B6 86.92(10) . . . . ?
B5 As1 As2 Co3 -95.71(8) . . . . ?
B4 As1 As2 Co3 -43.29(17) . . . . ?
B6 As1 As2 Co3 -127.56(9) . . . . ?
B2 As1 As2 Co3 -49(3) . . . . ?
As4 As1 As2 Co3 -40.64(4) . . . . ?
C34 Co3 B2 B7 65.2(6) . . . . ?
C30 Co3 B2 B7 70.0(17) . . . . ?
C33 Co3 B2 B7 99.5(4) . . . . ?
C31 Co3 B2 B7 164.1(3) . . . . ?
C32 Co3 B2 B7 139.4(3) . . . . ?
B8 Co3 B2 B7 -35.9(4) . . . . ?
B4 Co3 B2 B7 -86.6(4) . . . . ?
As1 Co3 B2 B7 -135.2(6) . . . . ?
As2 Co3 B2 B7 107(2) . . . . ?
As4 Co3 B2 B7 -87.6(3) . . . . ?
C34 Co3 B2 B11 98.0(7) . . . . ?
C30 Co3 B2 B11 102.8(16) . . . . ?
C33 Co3 B2 B11 132.3(6) . . . . ?
C31 Co3 B2 B11 -163.1(2) . . . . ?
C32 Co3 B2 B11 172.2(5) . . . . ?
B8 Co3 B2 B11 -3.1(6) . . . . ?
B4 Co3 B2 B11 -53.8(6) . . . . ?
B7 Co3 B2 B11 32.8(4) . . . . ?
As1 Co3 B2 B11 -102.4(8) . . . . ?
As2 Co3 B2 B11 140(3) . . . . ?
As4 Co3 B2 B11 -54.8(6) . . . . ?
C34 Co3 B2 B6 159.4(3) . . . . ?
C30 Co3 B2 B6 164.2(10) . . . . ?
C33 Co3 B2 B6 -166.3(5) . . . . ?
C31 Co3 B2 B6 -101.7(8) . . . . ?
C32 Co3 B2 B6 -126.4(5) . . . . ?
B8 Co3 B2 B6 58.2(6) . . . . ?
B4 Co3 B2 B6 7.6(6) . . . . ?
B7 Co3 B2 B6 94.1(7) . . . . ?
As1 Co3 B2 B6 -41.0(4) . . . . ?
As2 Co3 B2 B6 -159(3) . . . . ?
As4 Co3 B2 B6 6.6(6) . . . . ?
C34 Co3 B2 As1 -159.62(12) . . . . ?
C30 Co3 B2 As1 -154.8(12) . . . . ?
C33 Co3 B2 As1 -125.3(2) . . . . ?
C31 Co3 B2 As1 -60.7(8) . . . . ?
C32 Co3 B2 As1 -85.4(3) . . . . ?
B8 Co3 B2 As1 99.3(3) . . . . ?
B4 Co3 B2 As1 48.6(3) . . . . ?
B7 Co3 B2 As1 135.2(6) . . . . ?
As2 Co3 B2 As1 -118(2) . . . . ?
As4 Co3 B2 As1 47.6(3) . . . . ?
B5 As1 B2 B7 -54.3(8) . . . . ?
B4 As1 B2 B7 -2.1(8) . . . . ?
B6 As1 B2 B7 -92.0(9) . . . . ?
Co3 As1 B2 B7 45.5(6) . . . . ?
As4 As1 B2 B7 0.4(9) . . . . ?
As2 As1 B2 B7 172(4) . . . . ?
B5 As1 B2 B11 9.8(6) . . . . ?
B4 As1 B2 B11 61.9(6) . . . . ?
B6 As1 B2 B11 -28.0(4) . . . . ?
Co3 As1 B2 B11 109.5(7) . . . . ?
As4 As1 B2 B11 64.4(6) . . . . ?
As2 As1 B2 B11 -124(4) . . . . ?
B5 As1 B2 B6 37.8(3) . . . . ?
B4 As1 B2 B6 89.9(3) . . . . ?
Co3 As1 B2 B6 137.5(5) . . . . ?
As4 As1 B2 B6 92.4(3) . . . . ?
As2 As1 B2 B6 -96(3) . . . . ?
B5 As1 B2 Co3 -99.8(3) . . . . ?
B4 As1 B2 Co3 -47.6(3) . . . . ?
B6 As1 B2 Co3 -137.5(5) . . . . ?
As4 As1 B2 Co3 -45.1(3) . . . . ?
As2 As1 B2 Co3 126(4) . . . . ?
C34 Co3 As4 B9 -104.81(13) . . . . ?
C30 Co3 As4 B9 -127.61(13) . . . . ?
C33 Co3 As4 B9 -152.1(2) . . . . ?
C31 Co3 As4 B9 -168.09(13) . . . . ?
C32 Co3 As4 B9 168.70(13) . . . . ?
B2 Co3 As4 B9 46.8(3) . . . . ?
B8 Co3 As4 B9 -34.04(13) . . . . ?
B4 Co3 As4 B9 40.2(11) . . . . ?
B7 Co3 As4 B9 -6.52(13) . . . . ?
As1 Co3 As4 B9 93.10(10) . . . . ?
As2 Co3 As4 B9 48.84(10) . . . . ?
C34 Co3 As4 B8 -70.77(14) . . . . ?
C30 Co3 As4 B8 -93.57(13) . . . . ?
C33 Co3 As4 B8 -118.0(2) . . . . ?
C31 Co3 As4 B8 -134.05(14) . . . . ?
C32 Co3 As4 B8 -157.25(14) . . . . ?
B2 Co3 As4 B8 80.8(4) . . . . ?
B4 Co3 As4 B8 74.2(11) . . . . ?
B7 Co3 As4 B8 27.52(14) . . . . ?
As1 Co3 As4 B8 127.14(11) . . . . ?
As2 Co3 As4 B8 82.88(10) . . . . ?
C34 Co3 As4 B5 -156.83(12) . . . . ?
C30 Co3 As4 B5 -179.63(12) . . . . ?
C33 Co3 As4 B5 155.9(2) . . . . ?
C31 Co3 As4 B5 139.89(12) . . . . ?
C32 Co3 As4 B5 116.68(14) . . . . ?
B2 Co3 As4 B5 -5.2(3) . . . . ?
B8 Co3 As4 B5 -86.06(14) . . . . ?
B4 Co3 As4 B5 -11.8(11) . . . . ?
B7 Co3 As4 B5 -58.54(12) . . . . ?
As1 Co3 As4 B5 41.08(8) . . . . ?
As2 Co3 As4 B5 -3.18(10) . . . . ?
C34 Co3 As4 As1 162.09(9) . . . . ?
C30 Co3 As4 As1 139.29(9) . . . . ?
C33 Co3 As4 As1 114.8(2) . . . . ?
C31 Co3 As4 As1 98.81(9) . . . . ?
C32 Co3 As4 As1 75.60(11) . . . . ?
B2 Co3 As4 As1 -46.3(3) . . . . ?
B8 Co3 As4 As1 -127.14(11) . . . . ?
B4 Co3 As4 As1 -52.9(11) . . . . ?
B7 Co3 As4 As1 -99.62(8) . . . . ?
As2 Co3 As4 As1 -44.26(3) . . . . ?
B5 As1 As4 B9 30.46(13) . . . . ?
B4 As1 As4 B9 -37.4(14) . . . . ?
B6 As1 As4 B9 -1.23(13) . . . . ?
B2 As1 As4 B9 -55.3(5) . . . . ?
Co3 As1 As4 B9 -96.58(10) . . . . ?
As2 As1 As4 B9 -56.50(10) . . . . ?
B5 As1 As4 B8 85.11(14) . . . . ?
B4 As1 As4 B8 17.3(14) . . . . ?
B6 As1 As4 B8 53.43(12) . . . . ?
B2 As1 As4 B8 -0.6(5) . . . . ?
Co3 As1 As4 B8 -41.92(9) . . . . ?
As2 As1 As4 B8 -1.85(10) . . . . ?
B4 As1 As4 B5 -67.8(14) . . . . ?
B6 As1 As4 B5 -31.69(14) . . . . ?
B2 As1 As4 B5 -85.7(5) . . . . ?
Co3 As1 As4 B5 -127.03(10) . . . . ?
As2 As1 As4 B5 -86.96(10) . . . . ?
B5 As1 As4 Co3 127.03(10) . . . . ?
B4 As1 As4 Co3 59.2(14) . . . . ?
B6 As1 As4 Co3 95.35(8) . . . . ?
B2 As1 As4 Co3 41.3(5) . . . . ?
As2 As1 As4 Co3 40.07(3) . . . . ?
C34 Co3 B4 B9 -90.1(3) . . . . ?
C30 Co3 B4 B9 -117.4(3) . . . . ?
C33 Co3 B4 B9 -149.6(5) . . . . ?
C31 Co3 B4 B9 -158.4(3) . . . . ?
C32 Co3 B4 B9 173.2(2) . . . . ?
B2 Co3 B4 B9 56.7(4) . . . . ?
B8 Co3 B4 B9 -30.8(2) . . . . ?
B7 Co3 B4 B9 3.7(3) . . . . ?
As1 Co3 B4 B9 107.4(3) . . . . ?
As2 Co3 B4 B9 58.5(3) . . . . ?
As4 Co3 B4 B9 -129.8(13) . . . . ?
C34 Co3 B4 B8 -59.3(3) . . . . ?
C30 Co3 B4 B8 -86.51(18) . . . . ?
C33 Co3 B4 B8 -118.7(6) . . . . ?
C31 Co3 B4 B8 -127.60(17) . . . . ?
C32 Co3 B4 B8 -155.95(15) . . . . ?
B2 Co3 B4 B8 87.5(4) . . . . ?
B7 Co3 B4 B8 34.58(18) . . . . ?
As1 Co3 B4 B8 138.3(2) . . . . ?
As2 Co3 B4 B8 89.38(15) . . . . ?
As4 Co3 B4 B8 -98.9(11) . . . . ?
C34 Co3 B4 B5 -155.17(19) . . . . ?
C30 Co3 B4 B5 177.6(3) . . . . ?
C33 Co3 B4 B5 145.4(5) . . . . ?
C31 Co3 B4 B5 136.5(3) . . . . ?
C32 Co3 B4 B5 108.2(3) . . . . ?
B2 Co3 B4 B5 -8.4(4) . . . . ?
B8 Co3 B4 B5 -95.9(3) . . . . ?
B7 Co3 B4 B5 -61.3(3) . . . . ?
As1 Co3 B4 B5 42.4(2) . . . . ?
As2 Co3 B4 B5 -6.5(3) . . . . ?
As4 Co3 B4 B5 165.2(14) . . . . ?
C34 Co3 B4 As1 162.46(12) . . . . ?
C30 Co3 B4 As1 135.21(13) . . . . ?
C33 Co3 B4 As1 103.0(6) . . . . ?
C31 Co3 B4 As1 94.12(14) . . . . ?
C32 Co3 B4 As1 65.8(2) . . . . ?
B2 Co3 B4 As1 -50.7(3) . . . . ?
B8 Co3 B4 As1 -138.3(2) . . . . ?
B7 Co3 B4 As1 -103.70(12) . . . . ?
As2 Co3 B4 As1 -48.89(12) . . . . ?
As4 Co3 B4 As1 122.8(12) . . . . ?
B5 As1 B4 B9 27.6(2) . . . . ?
B6 As1 B4 B9 -9.9(3) . . . . ?
B2 As1 B4 B9 -63.7(5) . . . . ?
Co3 As1 B4 B9 -109.6(3) . . . . ?
As4 As1 B4 B9 134.2(16) . . . . ?
As2 As1 B4 B9 -64.6(3) . . . . ?
B5 As1 B4 B8 95.0(4) . . . . ?
B6 As1 B4 B8 57.5(3) . . . . ?
B2 As1 B4 B8 3.7(5) . . . . ?
Co3 As1 B4 B8 -42.2(3) . . . . ?
As4 As1 B4 B8 -158.4(17) . . . . ?
As2 As1 B4 B8 2.8(3) . . . . ?
B6 As1 B4 B5 -37.48(17) . . . . ?
B2 As1 B4 B5 -91.3(5) . . . . ?
Co3 As1 B4 B5 -137.2(2) . . . . ?
As4 As1 B4 B5 106.5(14) . . . . ?
As2 As1 B4 B5 -92.17(15) . . . . ?
B5 As1 B4 Co3 137.2(2) . . . . ?
B6 As1 B4 Co3 99.73(13) . . . . ?
B2 As1 B4 Co3 45.9(5) . . . . ?
As4 As1 B4 Co3 -116.3(15) . . . . ?
As2 As1 B4 Co3 45.03(12) . . . . ?
B9 B4 B5 B10 -37.1(2) . . . . ?
B8 B4 B5 B10 0.4(3) . . . . ?
Co3 B4 B5 B10 68.8(3) . . . . ?
As1 B4 B5 B10 113.06(18) . . . . ?
B8 B4 B5 B9 37.5(2) . . . . ?
Co3 B4 B5 B9 105.9(3) . . . . ?
As1 B4 B5 B9 150.1(2) . . . . ?
B9 B4 B5 B6 -99.4(2) . . . . ?
B8 B4 B5 B6 -61.8(3) . . . . ?
Co3 B4 B5 B6 6.6(4) . . . . ?
As1 B4 B5 B6 50.8(2) . . . . ?
B9 B4 B5 As1 -150.1(2) . . . . ?
B8 B4 B5 As1 -112.6(3) . . . . ?
Co3 B4 B5 As1 -44.2(2) . . . . ?
B9 B4 B5 As4 88.1(11) . . . . ?
B8 B4 B5 As4 125.6(12) . . . . ?
Co3 B4 B5 As4 -166.0(13) . . . . ?
As1 B4 B5 As4 -121.8(11) . . . . ?
B4 As1 B5 B10 -96.3(3) . . . . ?
B6 As1 B5 B10 31.10(15) . . . . ?
B2 As1 B5 B10 -9.1(4) . . . . ?
Co3 As1 B5 B10 -61.93(18) . . . . ?
As4 As1 B5 B10 -105.8(2) . . . . ?
As2 As1 B5 B10 -3.28(18) . . . . ?
B4 As1 B5 B9 -28.2(2) . . . . ?
B6 As1 B5 B9 99.2(2) . . . . ?
B2 As1 B5 B9 59.0(4) . . . . ?
Co3 As1 B5 B9 6.18(18) . . . . ?
As4 As1 B5 B9 -37.70(15) . . . . ?
As2 As1 B5 B9 64.82(17) . . . . ?
B4 As1 B5 B6 -127.4(2) . . . . ?
B2 As1 B5 B6 -40.2(4) . . . . ?
Co3 As1 B5 B6 -93.03(13) . . . . ?
As4 As1 B5 B6 -136.91(17) . . . . ?
As2 As1 B5 B6 -34.39(14) . . . . ?
B6 As1 B5 B4 127.4(2) . . . . ?
B2 As1 B5 B4 87.3(4) . . . . ?
Co3 As1 B5 B4 34.40(19) . . . . ?
As4 As1 B5 B4 -9.47(19) . . . . ?
As2 As1 B5 B4 93.05(18) . . . . ?
B4 As1 B5 As4 9.47(18) . . . . ?
B6 As1 B5 As4 136.91(17) . . . . ?
B2 As1 B5 As4 96.7(4) . . . . ?
Co3 As1 B5 As4 43.88(8) . . . . ?
As2 As1 B5 As4 102.52(7) . . . . ?
B9 As4 B5 B10 -27.52(16) . . . . ?
B8 As4 B5 B10 13.25(19) . . . . ?
Co3 As4 B5 B10 69.16(17) . . . . ?
As1 As4 B5 B10 112.54(18) . . . . ?
B8 As4 B5 B9 40.77(14) . . . . ?
Co3 As4 B5 B9 96.68(13) . . . . ?
As1 As4 B5 B9 140.06(15) . . . . ?
B9 As4 B5 B6 -93.6(2) . . . . ?
B8 As4 B5 B6 -52.8(2) . . . . ?
Co3 As4 B5 B6 3.1(2) . . . . ?
As1 As4 B5 B6 46.48(18) . . . . ?
B9 As4 B5 B4 -85.5(11) . . . . ?
B8 As4 B5 B4 -44.7(11) . . . . ?
Co3 As4 B5 B4 11.2(11) . . . . ?
As1 As4 B5 B4 54.6(11) . . . . ?
B9 As4 B5 As1 -140.06(15) . . . . ?
B8 As4 B5 As1 -99.29(10) . . . . ?
Co3 As4 B5 As1 -43.38(7) . . . . ?
B9 B5 B6 B10 36.1(2) . . . . ?
B4 B5 B6 B10 98.1(3) . . . . ?
As1 B5 B6 B10 147.67(15) . . . . ?
As4 B5 B6 B10 99.7(2) . . . . ?
B10 B5 B6 B11 -35.86(19) . . . . ?
B9 B5 B6 B11 0.2(3) . . . . ?
B4 B5 B6 B11 62.3(3) . . . . ?
As1 B5 B6 B11 111.81(18) . . . . ?
As4 B5 B6 B11 63.8(3) . . . . ?
B10 B5 B6 B2 -99.1(4) . . . . ?
B9 B5 B6 B2 -63.0(4) . . . . ?
B4 B5 B6 B2 -0.9(5) . . . . ?
As1 B5 B6 B2 48.6(4) . . . . ?
As4 B5 B6 B2 0.6(5) . . . . ?
B10 B5 B6 As2 -101.47(19) . . . . ?
B9 B5 B6 As2 -65.4(3) . . . . ?
B4 B5 B6 As2 -3.3(3) . . . . ?
As1 B5 B6 As2 46.20(15) . . . . ?
As4 B5 B6 As2 -1.8(3) . . . . ?
B10 B5 B6 As1 -147.67(15) . . . . ?
B9 B5 B6 As1 -111.57(19) . . . . ?
B4 B5 B6 As1 -49.5(2) . . . . ?
As4 B5 B6 As1 -47.97(16) . . . . ?
B7 B2 B6 B10 3.0(7) . . . . ?
B11 B2 B6 B10 38.3(4) . . . . ?
Co3 B2 B6 B10 -66.2(6) . . . . ?
As1 B2 B6 B10 -109.3(2) . . . . ?
B7 B2 B6 B11 -35.3(4) . . . . ?
Co3 B2 B6 B11 -104.5(6) . . . . ?
As1 B2 B6 B11 -147.6(4) . . . . ?
B7 B2 B6 B5 64.1(7) . . . . ?
B11 B2 B6 B5 99.5(3) . . . . ?
Co3 B2 B6 B5 -5.0(7) . . . . ?
As1 B2 B6 B5 -48.1(3) . . . . ?
B7 B2 B6 As2 -128(2) . . . . ?
B11 B2 B6 As2 -92(2) . . . . ?
Co3 B2 B6 As2 163(3) . . . . ?
As1 B2 B6 As2 120(2) . . . . ?
B7 B2 B6 As1 112.2(7) . . . . ?
B11 B2 B6 As1 147.6(4) . . . . ?
Co3 B2 B6 As1 43.1(5) . . . . ?
B11 As2 B6 B10 29.49(16) . . . . ?
B7 As2 B6 B10 -9.16(18) . . . . ?
Co3 As2 B6 B10 -65.63(16) . . . . ?
As1 As2 B6 B10 -108.33(18) . . . . ?
B7 As2 B6 B11 -38.65(13) . . . . ?
Co3 As2 B6 B11 -95.12(11) . . . . ?
As1 As2 B6 B11 -137.82(14) . . . . ?
B11 As2 B6 B5 94.5(2) . . . . ?
B7 As2 B6 B5 55.8(2) . . . . ?
Co3 As2 B6 B5 -0.7(2) . . . . ?
As1 As2 B6 B5 -43.36(17) . . . . ?
B11 As2 B6 B2 82(2) . . . . ?
B7 As2 B6 B2 43(2) . . . . ?
Co3 As2 B6 B2 -13(2) . . . . ?
As1 As2 B6 B2 -56(2) . . . . ?
B11 As2 B6 As1 137.82(14) . . . . ?
B7 As2 B6 As1 99.17(9) . . . . ?
Co3 As2 B6 As1 42.70(6) . . . . ?
B5 As1 B6 B10 -29.92(15) . . . . ?
B4 As1 B6 B10 8.9(2) . . . . ?
B2 As1 B6 B10 97.0(4) . . . . ?
Co3 As1 B6 B10 63.94(17) . . . . ?
As4 As1 B6 B10 4.19(17) . . . . ?
As2 As1 B6 B10 106.76(18) . . . . ?
B5 As1 B6 B11 -95.6(2) . . . . ?
B4 As1 B6 B11 -56.7(2) . . . . ?
B2 As1 B6 B11 31.4(4) . . . . ?
Co3 As1 B6 B11 -1.71(17) . . . . ?
As4 As1 B6 B11 -61.46(17) . . . . ?
As2 As1 B6 B11 41.11(14) . . . . ?
B4 As1 B6 B5 38.9(2) . . . . ?
B2 As1 B6 B5 126.9(4) . . . . ?
Co3 As1 B6 B5 93.85(14) . . . . ?
As4 As1 B6 B5 34.11(15) . . . . ?
As2 As1 B6 B5 136.68(17) . . . . ?
B5 As1 B6 B2 -126.9(4) . . . . ?
B4 As1 B6 B2 -88.1(4) . . . . ?
Co3 As1 B6 B2 -33.1(4) . . . . ?
As4 As1 B6 B2 -92.8(4) . . . . ?
As2 As1 B6 B2 9.8(4) . . . . ?
B5 As1 B6 As2 -136.68(17) . . . . ?
B4 As1 B6 As2 -97.82(16) . . . . ?
B2 As1 B6 As2 -9.8(4) . . . . ?
Co3 As1 B6 As2 -42.83(6) . . . . ?
As4 As1 B6 As2 -102.57(6) . . . . ?
B11 B2 B7 B12 -36.1(4) . . . . ?
B6 B2 B7 B12 -2.3(7) . . . . ?
Co3 B2 B7 B12 108.9(3) . . . . ?
As1 B2 B7 B12 62.9(9) . . . . ?
B11 B2 B7 B8 -98.9(3) . . . . ?
B6 B2 B7 B8 -65.1(7) . . . . ?
Co3 B2 B7 B8 46.1(4) . . . . ?
As1 B2 B7 B8 0.1(10) . . . . ?
B6 B2 B7 B11 33.8(4) . . . . ?
Co3 B2 B7 B11 145.0(5) . . . . ?
As1 B2 B7 B11 99.0(9) . . . . ?
B11 B2 B7 As2 89(3) . . . . ?
B6 B2 B7 As2 122(3) . . . . ?
Co3 B2 B7 As2 -126(3) . . . . ?
As1 B2 B7 As2 -172(4) . . . . ?
B11 B2 B7 Co3 -145.0(5) . . . . ?
B6 B2 B7 Co3 -111.2(6) . . . . ?
As1 B2 B7 Co3 -46.0(6) . . . . ?
B11 As2 B7 B12 -27.35(15) . . . . ?
B6 As2 B7 B12 9.84(17) . . . . ?
Co3 As2 B7 B12 108.30(18) . . . . ?
As1 As2 B7 B12 64.69(16) . . . . ?
B11 As2 B7 B8 -94.0(2) . . . . ?
B6 As2 B7 B8 -56.8(2) . . . . ?
Co3 As2 B7 B8 41.68(17) . . . . ?
As1 As2 B7 B8 -1.9(2) . . . . ?
B6 As2 B7 B11 37.19(13) . . . . ?
Co3 As2 B7 B11 135.65(14) . . . . ?
As1 As2 B7 B11 92.04(11) . . . . ?
B11 As2 B7 B2 -86(3) . . . . ?
B6 As2 B7 B2 -49(3) . . . . ?
Co3 As2 B7 B2 50(3) . . . . ?
As1 As2 B7 B2 6(3) . . . . ?
B11 As2 B7 Co3 -135.65(14) . . . . ?
B6 As2 B7 Co3 -98.46(9) . . . . ?
As1 As2 B7 Co3 -43.61(6) . . . . ?
C34 Co3 B7 B12 131.07(18) . . . . ?
C30 Co3 B7 B12 98.6(2) . . . . ?
C33 Co3 B7 B12 170.32(17) . . . . ?
C31 Co3 B7 B12 111.8(3) . . . . ?
C32 Co3 B7 B12 -170.92(16) . . . . ?
B2 Co3 B7 B12 -97.7(6) . . . . ?
B8 Co3 B7 B12 31.89(15) . . . . ?
B4 Co3 B7 B12 -3.4(2) . . . . ?
As1 Co3 B7 B12 -59.33(17) . . . . ?
As2 Co3 B7 B12 -106.60(19) . . . . ?
As4 Co3 B7 B12 3.02(17) . . . . ?
C34 Co3 B7 B8 99.18(16) . . . . ?
C30 Co3 B7 B8 66.72(19) . . . . ?
C33 Co3 B7 B8 138.43(16) . . . . ?
C31 Co3 B7 B8 79.9(4) . . . . ?
C32 Co3 B7 B8 157.19(17) . . . . ?
B2 Co3 B7 B8 -129.6(6) . . . . ?
B4 Co3 B7 B8 -35.3(2) . . . . ?
As1 Co3 B7 B8 -91.21(14) . . . . ?
As2 Co3 B7 B8 -138.49(18) . . . . ?
As4 Co3 B7 B8 -28.87(15) . . . . ?
C34 Co3 B7 B11 -164.79(16) . . . . ?
C30 Co3 B7 B11 162.74(16) . . . . ?
C33 Co3 B7 B11 -125.54(16) . . . . ?
C31 Co3 B7 B11 176.0(3) . . . . ?
C32 Co3 B7 B11 -106.8(2) . . . . ?
B2 Co3 B7 B11 -33.5(6) . . . . ?
B8 Co3 B7 B11 96.0(2) . . . . ?
B4 Co3 B7 B11 60.7(2) . . . . ?
As1 Co3 B7 B11 4.81(16) . . . . ?
As2 Co3 B7 B11 -42.46(13) . . . . ?
As4 Co3 B7 B11 67.16(15) . . . . ?
C34 Co3 B7 B2 -131.2(6) . . . . ?
C30 Co3 B7 B2 -163.7(6) . . . . ?
C33 Co3 B7 B2 -92.0(6) . . . . ?
C31 Co3 B7 B2 -150.5(6) . . . . ?
C32 Co3 B7 B2 -73.2(6) . . . . ?
B8 Co3 B7 B2 129.6(6) . . . . ?
B4 Co3 B7 B2 94.3(6) . . . . ?
As1 Co3 B7 B2 38.4(6) . . . . ?
As2 Co3 B7 B2 -8.9(5) . . . . ?
As4 Co3 B7 B2 100.7(6) . . . . ?
C34 Co3 B7 As2 -122.33(9) . . . . ?
C30 Co3 B7 As2 -154.80(11) . . . . ?
C33 Co3 B7 As2 -83.08(10) . . . . ?
C31 Co3 B7 As2 -141.6(3) . . . . ?
C32 Co3 B7 As2 -64.32(19) . . . . ?
B2 Co3 B7 As2 8.9(5) . . . . ?
B8 Co3 B7 As2 138.49(18) . . . . ?
B4 Co3 B7 As2 103.20(15) . . . . ?
As1 Co3 B7 As2 47.27(7) . . . . ?
As4 Co3 B7 As2 109.62(6) . . . . ?
B11 B7 B8 B12 36.87(17) . . . . ?
B2 B7 B8 B12 101.4(6) . . . . ?
As2 B7 B8 B12 102.9(2) . . . . ?
Co3 B7 B8 B12 146.24(15) . . . . ?
B12 B7 B8 B9 -34.59(18) . . . . ?
B11 B7 B8 B9 2.3(3) . . . . ?
B2 B7 B8 B9 66.8(6) . . . . ?
As2 B7 B8 B9 68.3(2) . . . . ?
Co3 B7 B8 B9 111.64(18) . . . . ?
B12 B7 B8 B4 -98.8(3) . . . . ?
B11 B7 B8 B4 -62.0(3) . . . . ?
B2 B7 B8 B4 2.6(7) . . . . ?
As2 B7 B8 B4 4.1(4) . . . . ?
Co3 B7 B8 B4 47.4(3) . . . . ?
B12 B7 B8 As4 -102.1(2) . . . . ?
B11 B7 B8 As4 -65.3(3) . . . . ?
B2 B7 B8 As4 -0.7(6) . . . . ?
As2 B7 B8 As4 0.8(3) . . . . ?
Co3 B7 B8 As4 44.10(19) . . . . ?
B12 B7 B8 Co3 -146.24(14) . . . . ?
B11 B7 B8 Co3 -109.37(16) . . . . ?
B2 B7 B8 Co3 -44.8(6) . . . . ?
As2 B7 B8 Co3 -43.32(15) . . . . ?
B9 B4 B8 B12 35.2(2) . . . . ?
B5 B4 B8 B12 -1.3(3) . . . . ?
Co3 B4 B8 B12 -112.68(19) . . . . ?
As1 B4 B8 B12 -69.0(4) . . . . ?
B9 B4 B8 B7 99.7(3) . . . . ?
B5 B4 B8 B7 63.2(4) . . . . ?
Co3 B4 B8 B7 -48.2(2) . . . . ?
As1 B4 B8 B7 -4.5(5) . . . . ?
B5 B4 B8 B9 -36.5(2) . . . . ?
Co3 B4 B8 B9 -147.9(2) . . . . ?
As1 B4 B8 B9 -104.2(3) . . . . ?
B9 B4 B8 As4 -93.6(11) . . . . ?
B5 B4 B8 As4 -130.1(13) . . . . ?
Co3 B4 B8 As4 118.5(12) . . . . ?
As1 B4 B8 As4 162.2(14) . . . . ?
B9 B4 B8 Co3 147.9(2) . . . . ?
B5 B4 B8 Co3 111.4(3) . . . . ?
As1 B4 B8 Co3 43.7(3) . . . . ?
B9 As4 B8 B12 24.59(17) . . . . ?
B5 As4 B8 B12 -14.52(19) . . . . ?
Co3 As4 B8 B12 -112.46(18) . . . . ?
As1 As4 B8 B12 -69.03(17) . . . . ?
B9 As4 B8 B7 94.5(3) . . . . ?
B5 As4 B8 B7 55.4(2) . . . . ?
Co3 As4 B8 B7 -42.5(2) . . . . ?
As1 As4 B8 B7 0.9(2) . . . . ?
B5 As4 B8 B9 -39.11(14) . . . . ?
Co3 As4 B8 B9 -137.04(14) . . . . ?
As1 As4 B8 B9 -93.62(12) . . . . ?
B9 As4 B8 B4 79.6(11) . . . . ?
B5 As4 B8 B4 40.5(11) . . . . ?
Co3 As4 B8 B4 -57.4(11) . . . . ?
As1 As4 B8 B4 -14.0(11) . . . . ?
B9 As4 B8 Co3 137.04(14) . . . . ?
B5 As4 B8 Co3 97.94(10) . . . . ?
As1 As4 B8 Co3 43.42(7) . . . . ?
C34 Co3 B8 B12 -119.62(18) . . . . ?
C30 Co3 B8 B12 -160.56(19) . . . . ?
C33 Co3 B8 B12 -98.2(2) . . . . ?
C31 Co3 B8 B12 170.61(17) . . . . ?
C32 Co3 B8 B12 -160.7(3) . . . . ?
B2 Co3 B8 B12 5.1(4) . . . . ?
B4 Co3 B8 B12 98.8(3) . . . . ?
B7 Co3 B8 B12 -32.93(16) . . . . ?
As1 Co3 B8 B12 64.58(17) . . . . ?
As2 Co3 B8 B12 0.47(18) . . . . ?
As4 Co3 B8 B12 109.8(2) . . . . ?
C34 Co3 B8 B7 -86.69(17) . . . . ?
C30 Co3 B8 B7 -127.64(17) . . . . ?
C33 Co3 B8 B7 -65.2(2) . . . . ?
C31 Co3 B8 B7 -156.47(16) . . . . ?
C32 Co3 B8 B7 -127.7(3) . . . . ?
B2 Co3 B8 B7 38.0(4) . . . . ?
B4 Co3 B8 B7 131.8(3) . . . . ?
As1 Co3 B8 B7 97.51(14) . . . . ?
As2 Co3 B8 B7 33.40(15) . . . . ?
As4 Co3 B8 B7 142.76(19) . . . . ?
C34 Co3 B8 B9 172.42(18) . . . . ?
C30 Co3 B8 B9 131.48(19) . . . . ?
C33 Co3 B8 B9 -166.13(16) . . . . ?
C31 Co3 B8 B9 102.6(2) . . . . ?
C32 Co3 B8 B9 131.4(3) . . . . ?
B2 Co3 B8 B9 -62.8(4) . . . . ?
B4 Co3 B8 B9 30.9(2) . . . . ?
B7 Co3 B8 B9 -100.9(2) . . . . ?
As1 Co3 B8 B9 -3.38(17) . . . . ?
As2 Co3 B8 B9 -67.49(17) . . . . ?
As4 Co3 B8 B9 41.87(15) . . . . ?
C34 Co3 B8 B4 141.6(2) . . . . ?
C30 Co3 B8 B4 100.6(2) . . . . ?
C33 Co3 B8 B4 163.0(2) . . . . ?
C31 Co3 B8 B4 71.8(2) . . . . ?
C32 Co3 B8 B4 100.5(4) . . . . ?
B2 Co3 B8 B4 -93.7(4) . . . . ?
B7 Co3 B8 B4 -131.8(3) . . . . ?
As1 Co3 B8 B4 -34.2(2) . . . . ?
As2 Co3 B8 B4 -98.4(2) . . . . ?
As4 Co3 B8 B4 11.0(2) . . . . ?
C34 Co3 B8 As4 130.55(11) . . . . ?
C30 Co3 B8 As4 89.61(12) . . . . ?
C33 Co3 B8 As4 152.00(13) . . . . ?
C31 Co3 B8 As4 60.78(15) . . . . ?
C32 Co3 B8 As4 89.5(3) . . . . ?
B2 Co3 B8 As4 -104.7(4) . . . . ?
B4 Co3 B8 As4 -11.0(2) . . . . ?
B7 Co3 B8 As4 -142.76(19) . . . . ?
As1 Co3 B8 As4 -45.25(8) . . . . ?
As2 Co3 B8 As4 -109.36(7) . . . . ?
B6 B5 B9 B10 -35.7(2) . . . . ?
B4 B5 B9 B10 -138.1(2) . . . . ?
As1 B5 B9 B10 -108.08(19) . . . . ?
As4 B5 B9 B10 -150.46(17) . . . . ?
B10 B5 B9 B12 35.51(18) . . . . ?
B6 B5 B9 B12 -0.2(3) . . . . ?
B4 B5 B9 B12 -102.6(3) . . . . ?
As1 B5 B9 B12 -72.6(2) . . . . ?
As4 B5 B9 B12 -114.9(2) . . . . ?
B10 B5 B9 B4 138.1(2) . . . . ?
B6 B5 B9 B4 102.5(3) . . . . ?
As1 B5 B9 B4 30.1(2) . . . . ?
As4 B5 B9 B4 -12.31(19) . . . . ?
B10 B5 B9 B8 99.1(2) . . . . ?
B6 B5 B9 B8 63.4(3) . . . . ?
B4 B5 B9 B8 -39.0(2) . . . . ?
As1 B5 B9 B8 -9.0(3) . . . . ?
As4 B5 B9 B8 -51.36(17) . . . . ?
B10 B5 B9 As4 150.46(17) . . . . ?
B6 B5 B9 As4 114.8(2) . . . . ?
B4 B5 B9 As4 12.31(19) . . . . ?
As1 B5 B9 As4 42.38(15) . . . . ?
B8 B4 B9 B10 -99.6(2) . . . . ?
B5 B4 B9 B10 37.8(2) . . . . ?
Co3 B4 B9 B10 -67.5(3) . . . . ?
As1 B4 B9 B10 8.5(4) . . . . ?
B8 B4 B9 B12 -35.3(2) . . . . ?
B5 B4 B9 B12 102.1(2) . . . . ?
Co3 B4 B9 B12 -3.1(4) . . . . ?
As1 B4 B9 B12 72.8(3) . . . . ?
B8 B4 B9 B5 -137.4(2) . . . . ?
Co3 B4 B9 B5 -105.3(3) . . . . ?
As1 B4 B9 B5 -29.3(2) . . . . ?
B5 B4 B9 B8 137.4(2) . . . . ?
Co3 B4 B9 B8 32.2(2) . . . . ?
As1 B4 B9 B8 108.1(3) . . . . ?
B8 B4 B9 As4 106.9(10) . . . . ?
B5 B4 B9 As4 -115.7(10) . . . . ?
Co3 B4 B9 As4 139.0(11) . . . . ?
As1 B4 B9 As4 -145.0(12) . . . . ?
B12 B8 B9 B10 -36.89(17) . . . . ?
B7 B8 B9 B10 -2.1(3) . . . . ?
B4 B8 B9 B10 103.8(3) . . . . ?
As4 B8 B9 B10 117.35(19) . . . . ?
Co3 B8 B9 B10 71.1(2) . . . . ?
B7 B8 B9 B12 34.74(18) . . . . ?
B4 B8 B9 B12 140.7(2) . . . . ?
As4 B8 B9 B12 154.24(17) . . . . ?
Co3 B8 B9 B12 107.95(19) . . . . ?
B12 B8 B9 B5 -100.2(2) . . . . ?
B7 B8 B9 B5 -65.4(3) . . . . ?
B4 B8 B9 B5 40.5(2) . . . . ?
As4 B8 B9 B5 54.05(17) . . . . ?
Co3 B8 B9 B5 7.8(3) . . . . ?
B12 B8 B9 B4 -140.7(2) . . . . ?
B7 B8 B9 B4 -105.9(3) . . . . ?
As4 B8 B9 B4 13.57(18) . . . . ?
Co3 B8 B9 B4 -32.7(2) . . . . ?
B12 B8 B9 As4 -154.24(17) . . . . ?
B7 B8 B9 As4 -119.5(2) . . . . ?
B4 B8 B9 As4 -13.57(18) . . . . ?
Co3 B8 B9 As4 -46.28(14) . . . . ?
B8 As4 B9 B10 -96.4(2) . . . . ?
B5 As4 B9 B10 29.95(18) . . . . ?
Co3 As4 B9 B10 -61.4(2) . . . . ?
As1 As4 B9 B10 -2.0(2) . . . . ?
B8 As4 B9 B12 -25.36(17) . . . . ?
B5 As4 B9 B12 100.9(2) . . . . ?
Co3 As4 B9 B12 9.6(2) . . . . ?
As1 As4 B9 B12 68.99(19) . . . . ?
B8 As4 B9 B5 -126.30(18) . . . . ?
Co3 As4 B9 B5 -91.31(13) . . . . ?
As1 As4 B9 B5 -31.95(12) . . . . ?
B8 As4 B9 B4 -66.9(10) . . . . ?
B5 As4 B9 B4 59.4(10) . . . . ?
Co3 As4 B9 B4 -31.9(9) . . . . ?
As1 As4 B9 B4 27.5(9) . . . . ?
B5 As4 B9 B8 126.30(18) . . . . ?
Co3 As4 B9 B8 35.00(12) . . . . ?
As1 As4 B9 B8 94.35(12) . . . . ?
B9 B5 B10 B11 -100.6(2) . . . . ?
B6 B5 B10 B11 39.0(2) . . . . ?
B4 B5 B10 B11 -64.2(3) . . . . ?
As1 B5 B10 B11 5.3(3) . . . . ?
As4 B5 B10 B11 -73.5(2) . . . . ?
B9 B5 B10 B6 -139.6(2) . . . . ?
B4 B5 B10 B6 -103.2(3) . . . . ?
As1 B5 B10 B6 -33.68(16) . . . . ?
As4 B5 B10 B6 -112.5(2) . . . . ?
B6 B5 B10 B9 139.6(2) . . . . ?
B4 B5 B10 B9 36.4(2) . . . . ?
As1 B5 B10 B9 105.9(2) . . . . ?
As4 B5 B10 B9 27.14(16) . . . . ?
B9 B5 B10 B12 -35.80(18) . . . . ?
B6 B5 B10 B12 103.8(2) . . . . ?
B4 B5 B10 B12 0.6(3) . . . . ?
As1 B5 B10 B12 70.1(2) . . . . ?
As4 B5 B10 B12 -8.7(2) . . . . ?
B11 B6 B10 B5 138.9(2) . . . . ?
B2 B6 B10 B5 99.8(5) . . . . ?
As2 B6 B10 B5 108.5(2) . . . . ?
As1 B6 B10 B5 31.49(15) . . . . ?
B5 B6 B10 B11 -138.9(2) . . . . ?
B2 B6 B10 B11 -39.1(5) . . . . ?
As2 B6 B10 B11 -30.33(16) . . . . ?
As1 B6 B10 B11 -107.38(19) . . . . ?
B11 B6 B10 B9 101.5(2) . . . . ?
B5 B6 B10 B9 -37.4(2) . . . . ?
B2 B6 B10 B9 62.4(5) . . . . ?
As2 B6 B10 B9 71.2(2) . . . . ?
As1 B6 B10 B9 -5.9(2) . . . . ?
B11 B6 B10 B12 36.47(18) . . . . ?
B5 B6 B10 B12 -102.4(2) . . . . ?
B2 B6 B10 B12 -2.6(5) . . . . ?
As2 B6 B10 B12 6.1(2) . . . . ?
As1 B6 B10 B12 -70.9(2) . . . . ?
B12 B9 B10 B5 -140.68(19) . . . . ?
B4 B9 B10 B5 -39.7(2) . . . . ?
B8 B9 B10 B5 -104.1(2) . . . . ?
As4 B9 B10 B5 -32.98(19) . . . . ?
B12 B9 B10 B11 -35.50(18) . . . . ?
B5 B9 B10 B11 105.2(2) . . . . ?
B4 B9 B10 B11 65.5(3) . . . . ?
B8 B9 B10 B11 1.1(2) . . . . ?
As4 B9 B10 B11 72.2(2) . . . . ?
B12 B9 B10 B6 -102.5(2) . . . . ?
B5 B9 B10 B6 38.2(2) . . . . ?
B4 B9 B10 B6 -1.5(3) . . . . ?
B8 B9 B10 B6 -65.9(2) . . . . ?
As4 B9 B10 B6 5.2(3) . . . . ?
B5 B9 B10 B12 140.68(19) . . . . ?
B4 B9 B10 B12 101.0(3) . . . . ?
B8 B9 B10 B12 36.58(17) . . . . ?
As4 B9 B10 B12 107.7(2) . . . . ?
B5 B10 B11 B12 101.0(2) . . . . ?
B6 B10 B11 B12 140.1(2) . . . . ?
B9 B10 B11 B12 35.57(18) . . . . ?
B5 B10 B11 B6 -39.1(2) . . . . ?
B9 B10 B11 B6 -104.5(2) . . . . ?
B12 B10 B11 B6 -140.1(2) . . . . ?
B5 B10 B11 B7 65.7(2) . . . . ?
B6 B10 B11 B7 104.9(2) . . . . ?
B9 B10 B11 B7 0.3(2) . . . . ?
B12 B10 B11 B7 -35.24(16) . . . . ?
B5 B10 B11 B2 2.6(5) . . . . ?
B6 B10 B11 B2 41.7(5) . . . . ?
B9 B10 B11 B2 -62.8(5) . . . . ?
B12 B10 B11 B2 -98.4(5) . . . . ?
B5 B10 B11 As2 -5.0(3) . . . . ?
B6 B10 B11 As2 34.14(17) . . . . ?
B9 B10 B11 As2 -70.4(2) . . . . ?
B12 B10 B11 As2 -105.96(19) . . . . ?
B5 B6 B11 B10 35.70(19) . . . . ?
B2 B6 B11 B10 135.9(5) . . . . ?
As2 B6 B11 B10 147.97(16) . . . . ?
As1 B6 B11 B10 103.31(19) . . . . ?
B10 B6 B11 B12 -35.94(18) . . . . ?
B5 B6 B11 B12 -0.2(3) . . . . ?
B2 B6 B11 B12 99.9(5) . . . . ?
As2 B6 B11 B12 112.03(18) . . . . ?
As1 B6 B11 B12 67.4(2) . . . . ?
B10 B6 B11 B7 -98.3(2) . . . . ?
B5 B6 B11 B7 -62.6(3) . . . . ?
B2 B6 B11 B7 37.6(5) . . . . ?
As2 B6 B11 B7 49.71(15) . . . . ?
As1 B6 B11 B7 5.0(2) . . . . ?
B10 B6 B11 B2 -135.9(5) . . . . ?
B5 B6 B11 B2 -100.2(5) . . . . ?
As2 B6 B11 B2 12.1(5) . . . . ?
As1 B6 B11 B2 -32.6(5) . . . . ?
B10 B6 B11 As2 -147.97(16) . . . . ?
B5 B6 B11 As2 -112.3(2) . . . . ?
B2 B6 B11 As2 -12.1(5) . . . . ?
As1 B6 B11 As2 -44.66(13) . . . . ?
B12 B7 B11 B10 36.09(17) . . . . ?
B8 B7 B11 B10 -1.6(2) . . . . ?
B2 B7 B11 B10 -102.5(5) . . . . ?
As2 B7 B11 B10 -114.09(17) . . . . ?
Co3 B7 B11 B10 -69.1(2) . . . . ?
B8 B7 B11 B12 -37.70(17) . . . . ?
B2 B7 B11 B12 -138.6(5) . . . . ?
As2 B7 B11 B12 -150.18(16) . . . . ?
Co3 B7 B11 B12 -105.23(18) . . . . ?
B12 B7 B11 B6 98.9(2) . . . . ?
B8 B7 B11 B6 61.2(2) . . . . ?
B2 B7 B11 B6 -39.7(5) . . . . ?
As2 B7 B11 B6 -51.31(16) . . . . ?
Co3 B7 B11 B6 -6.4(2) . . . . ?
B12 B7 B11 B2 138.6(5) . . . . ?
B8 B7 B11 B2 100.9(5) . . . . ?
As2 B7 B11 B2 -11.6(5) . . . . ?
Co3 B7 B11 B2 33.3(5) . . . . ?
B12 B7 B11 As2 150.18(16) . . . . ?
B8 B7 B11 As2 112.48(19) . . . . ?
B2 B7 B11 As2 11.6(5) . . . . ?
Co3 B7 B11 As2 44.95(12) . . . . ?
B7 B2 B11 B10 99.6(3) . . . . ?
B6 B2 B11 B10 -39.2(4) . . . . ?
Co3 B2 B11 B10 64.3(7) . . . . ?
As1 B2 B11 B10 -8.8(7) . . . . ?
B7 B2 B11 B12 36.0(4) . . . . ?
B6 B2 B11 B12 -102.8(3) . . . . ?
Co3 B2 B11 B12 0.7(7) . . . . ?
As1 B2 B11 B12 -72.5(6) . . . . ?
B7 B2 B11 B6 138.8(5) . . . . ?
Co3 B2 B11 B6 103.5(7) . . . . ?
As1 B2 B11 B6 30.3(4) . . . . ?
B6 B2 B11 B7 -138.8(5) . . . . ?
Co3 B2 B11 B7 -35.3(4) . . . . ?
As1 B2 B11 B7 -108.4(7) . . . . ?
B7 B2 B11 As2 -115(2) . . . . ?
B6 B2 B11 As2 106(2) . . . . ?
Co3 B2 B11 As2 -151(2) . . . . ?
As1 B2 B11 As2 136(2) . . . . ?
B7 As2 B11 B10 97.3(2) . . . . ?
B6 As2 B11 B10 -31.19(16) . . . . ?
Co3 As2 B11 B10 61.06(17) . . . . ?
As1 As2 B11 B10 2.49(18) . . . . ?
B7 As2 B11 B12 28.24(16) . . . . ?
B6 As2 B11 B12 -100.2(2) . . . . ?
Co3 As2 B11 B12 -7.99(17) . . . . ?
As1 As2 B11 B12 -66.56(16) . . . . ?
B7 As2 B11 B6 128.48(17) . . . . ?
Co3 As2 B11 B6 92.25(11) . . . . ?
As1 As2 B11 B6 33.68(11) . . . . ?
B6 As2 B11 B7 -128.48(17) . . . . ?
Co3 As2 B11 B7 -36.23(11) . . . . ?
As1 As2 B11 B7 -94.80(11) . . . . ?
B7 As2 B11 B2 59(2) . . . . ?
B6 As2 B11 B2 -69(2) . . . . ?
Co3 As2 B11 B2 23(2) . . . . ?
As1 As2 B11 B2 -36(2) . . . . ?
B7 B8 B12 B11 -40.9(2) . . . . ?
B9 B8 B12 B11 100.73(19) . . . . ?
B4 B8 B12 B11 65.5(3) . . . . ?
As4 B8 B12 B11 75.8(2) . . . . ?
Co3 B8 B12 B11 -5.6(3) . . . . ?
B7 B8 B12 B9 -141.6(2) . . . . ?
B4 B8 B12 B9 -35.2(2) . . . . ?
As4 B8 B12 B9 -24.95(16) . . . . ?
Co3 B8 B12 B9 -106.34(19) . . . . ?
B7 B8 B12 B10 -104.7(2) . . . . ?
B9 B8 B12 B10 36.91(17) . . . . ?
B4 B8 B12 B10 1.7(3) . . . . ?
As4 B8 B12 B10 12.0(2) . . . . ?
Co3 B8 B12 B10 -69.4(2) . . . . ?
B9 B8 B12 B7 141.6(2) . . . . ?
B4 B8 B12 B7 106.4(3) . . . . ?
As4 B8 B12 B7 116.7(2) . . . . ?
Co3 B8 B12 B7 35.27(16) . . . . ?
B10 B11 B12 B8 -100.4(2) . . . . ?
B6 B11 B12 B8 -65.1(2) . . . . ?
B7 B11 B12 B8 39.34(19) . . . . ?
B2 B11 B12 B8 2.8(5) . . . . ?
As2 B11 B12 B8 9.1(2) . . . . ?
B10 B11 B12 B9 -35.21(19) . . . . ?
B6 B11 B12 B9 0.1(3) . . . . ?
B7 B11 B12 B9 104.5(2) . . . . ?
B2 B11 B12 B9 68.0(5) . . . . ?
As2 B11 B12 B9 74.3(2) . . . . ?
B6 B11 B12 B10 35.34(18) . . . . ?
B7 B11 B12 B10 139.75(19) . . . . ?
B2 B11 B12 B10 103.2(4) . . . . ?
As2 B11 B12 B10 109.47(18) . . . . ?
B10 B11 B12 B7 -139.75(19) . . . . ?
B6 B11 B12 B7 -104.4(2) . . . . ?
B2 B11 B12 B7 -36.5(4) . . . . ?
As2 B11 B12 B7 -30.28(17) . . . . ?
B10 B9 B12 B8 138.83(19) . . . . ?
B5 B9 B12 B8 103.6(2) . . . . ?
B4 B9 B12 B8 35.7(2) . . . . ?
As4 B9 B12 B8 26.77(18) . . . . ?
B10 B9 B12 B11 35.21(18) . . . . ?
B5 B9 B12 B11 0.0(3) . . . . ?
B4 B9 B12 B11 -67.9(3) . . . . ?
B8 B9 B12 B11 -103.6(2) . . . . ?
As4 B9 B12 B11 -76.8(2) . . . . ?
B5 B9 B12 B10 -35.20(18) . . . . ?
B4 B9 B12 B10 -103.1(3) . . . . ?
B8 B9 B12 B10 -138.83(19) . . . . ?
As4 B9 B12 B10 -112.1(2) . . . . ?
B10 B9 B12 B7 103.6(2) . . . . ?
B5 B9 B12 B7 68.4(2) . . . . ?
B4 B9 B12 B7 0.5(3) . . . . ?
B8 B9 B12 B7 -35.27(18) . . . . ?
As4 B9 B12 B7 -8.5(3) . . . . ?
B5 B10 B12 B8 -1.5(2) . . . . ?
B11 B10 B12 B8 103.3(2) . . . . ?
B6 B10 B12 B8 65.9(2) . . . . ?
B9 B10 B12 B8 -37.47(18) . . . . ?
B5 B10 B12 B11 -104.8(2) . . . . ?
B6 B10 B12 B11 -37.43(19) . . . . ?
B9 B10 B12 B11 -140.8(2) . . . . ?
B5 B10 B12 B9 36.01(18) . . . . ?
B11 B10 B12 B9 140.8(2) . . . . ?
B6 B10 B12 B9 103.4(2) . . . . ?
B5 B10 B12 B7 -66.2(2) . . . . ?
B11 B10 B12 B7 38.59(18) . . . . ?
B6 B10 B12 B7 1.2(2) . . . . ?
B9 B10 B12 B7 -102.2(2) . . . . ?
B11 B7 B12 B8 -136.9(2) . . . . ?
B2 B7 B12 B8 -99.1(5) . . . . ?
As2 B7 B12 B8 -108.3(2) . . . . ?
Co3 B7 B12 B8 -33.24(15) . . . . ?
B8 B7 B12 B11 136.9(2) . . . . ?
B2 B7 B12 B11 37.8(5) . . . . ?
As2 B7 B12 B11 28.63(15) . . . . ?
Co3 B7 B12 B11 103.69(18) . . . . ?
B8 B7 B12 B9 35.52(19) . . . . ?
B11 B7 B12 B9 -101.41(19) . . . . ?
B2 B7 B12 B9 -63.6(5) . . . . ?
As2 B7 B12 B9 -72.8(2) . . . . ?
Co3 B7 B12 B9 2.3(2) . . . . ?
B8 B7 B12 B10 100.1(2) . . . . ?
B11 B7 B12 B10 -36.88(17) . . . . ?
B2 B7 B12 B10 0.9(5) . . . . ?
As2 B7 B12 B10 -8.3(2) . . . . ?
Co3 B7 B12 B10 66.8(2) . . . . ?
C34 Co3 C30 C31 118.4(2) . . . . ?
C33 Co3 C30 C31 80.65(19) . . . . ?
C32 Co3 C30 C31 37.68(17) . . . . ?
B2 Co3 C30 C31 112.3(15) . . . . ?
B8 Co3 C30 C31 -142.28(18) . . . . ?
B4 Co3 C30 C31 -91.5(2) . . . . ?
B7 Co3 C30 C31 173.25(17) . . . . ?
As1 Co3 C30 C31 -37.3(2) . . . . ?
As2 Co3 C30 C31 99.6(3) . . . . ?
As4 Co3 C30 C31 -89.60(17) . . . . ?
C33 Co3 C30 C34 -37.77(14) . . . . ?
C31 Co3 C30 C34 -118.4(2) . . . . ?
C32 Co3 C30 C34 -80.73(17) . . . . ?
B2 Co3 C30 C34 -6.1(15) . . . . ?
B8 Co3 C30 C34 99.30(16) . . . . ?
B4 Co3 C30 C34 150.1(2) . . . . ?
B7 Co3 C30 C34 54.84(19) . . . . ?
As1 Co3 C30 C34 -155.67(11) . . . . ?
As2 Co3 C30 C34 -18.8(3) . . . . ?
As4 Co3 C30 C34 151.99(14) . . . . ?
C34 C30 C31 C32 -0.1(3) . . . . ?
Co3 C30 C31 C32 -60.0(2) . . . . ?
C34 C30 C31 Co3 59.91(18) . . . . ?
C34 Co3 C31 C32 80.1(2) . . . . ?
C30 Co3 C31 C32 118.5(3) . . . . ?
C33 Co3 C31 C32 36.7(2) . . . . ?
B2 Co3 C31 C32 -38.3(7) . . . . ?
B8 Co3 C31 C32 166.28(18) . . . . ?
B4 Co3 C31 C32 -145.6(2) . . . . ?
B7 Co3 C31 C32 100.8(4) . . . . ?
As1 Co3 C31 C32 -88.0(2) . . . . ?
As2 Co3 C31 C32 -28.6(3) . . . . ?
As4 Co3 C31 C32 -149.8(2) . . . . ?
C34 Co3 C31 C30 -38.39(18) . . . . ?
C33 Co3 C31 C30 -81.75(19) . . . . ?
C32 Co3 C31 C30 -118.5(3) . . . . ?
B2 Co3 C31 C30 -156.8(7) . . . . ?
B8 Co3 C31 C30 47.8(2) . . . . ?
B4 Co3 C31 C30 96.0(2) . . . . ?
B7 Co3 C31 C30 -17.6(4) . . . . ?
As1 Co3 C31 C30 153.58(17) . . . . ?
As2 Co3 C31 C30 -147.04(16) . . . . ?
As4 Co3 C31 C30 91.75(18) . . . . ?
C30 C31 C32 C33 -0.2(4) . . . . ?
Co3 C31 C32 C33 -59.2(2) . . . . ?
C30 C31 C32 Co3 59.1(2) . . . . ?
C34 Co3 C32 C33 37.29(17) . . . . ?
C30 Co3 C32 C33 81.87(19) . . . . ?
C31 Co3 C32 C33 120.1(3) . . . . ?
B2 Co3 C32 C33 -83.0(4) . . . . ?
B8 Co3 C32 C33 82.0(4) . . . . ?
B4 Co3 C32 C33 167.0(2) . . . . ?
B7 Co3 C32 C33 -29.4(3) . . . . ?
As1 Co3 C32 C33 -142.94(16) . . . . ?
As2 Co3 C32 C33 -78.86(16) . . . . ?
As4 Co3 C32 C33 157.94(14) . . . . ?
C34 Co3 C32 C31 -82.8(2) . . . . ?
C30 Co3 C32 C31 -38.2(2) . . . . ?
C33 Co3 C32 C31 -120.1(3) . . . . ?
B2 Co3 C32 C31 156.9(4) . . . . ?
B8 Co3 C32 C31 -38.1(5) . . . . ?
B4 Co3 C32 C31 46.9(3) . . . . ?
B7 Co3 C32 C31 -149.50(19) . . . . ?
As1 Co3 C32 C31 97.0(2) . . . . ?
As2 Co3 C32 C31 161.07(19) . . . . ?
As4 Co3 C32 C31 37.9(2) . . . . ?
C31 C32 C33 C34 0.4(4) . . . . ?
Co3 C32 C33 C34 -58.77(19) . . . . ?
C31 C32 C33 Co3 59.2(2) . . . . ?
C34 Co3 C33 C32 -119.7(2) . . . . ?
C30 Co3 C33 C32 -81.00(19) . . . . ?
C31 Co3 C33 C32 -37.02(18) . . . . ?
B2 Co3 C33 C32 106.9(4) . . . . ?
B8 Co3 C33 C32 -153.82(17) . . . . ?
B4 Co3 C33 C32 -46.5(7) . . . . ?
B7 Co3 C33 C32 160.96(17) . . . . ?
As1 Co3 C33 C32 47.22(19) . . . . ?
As2 Co3 C33 C32 105.84(16) . . . . ?
As4 Co3 C33 C32 -54.4(3) . . . . ?
C30 Co3 C33 C34 38.66(16) . . . . ?
C31 Co3 C33 C34 82.63(18) . . . . ?
C32 Co3 C33 C34 119.7(2) . . . . ?
B2 Co3 C33 C34 -133.5(4) . . . . ?
B8 Co3 C33 C34 -34.2(2) . . . . ?
B4 Co3 C33 C34 73.1(7) . . . . ?
B7 Co3 C33 C34 -79.38(17) . . . . ?
As1 Co3 C33 C34 166.87(12) . . . . ?
As2 Co3 C33 C34 -134.51(15) . . . . ?
As4 Co3 C33 C34 65.2(3) . . . . ?
C32 C33 C34 C30 -0.5(3) . . . . ?
Co3 C33 C34 C30 -60.13(17) . . . . ?
C32 C33 C34 Co3 59.7(2) . . . . ?
C31 C30 C34 C33 0.3(3) . . . . ?
Co3 C30 C34 C33 61.06(17) . . . . ?
C31 C30 C34 Co3 -60.72(19) . . . . ?
C30 Co3 C34 C33 -118.2(2) . . . . ?
C31 Co3 C34 C33 -80.21(17) . . . . ?
C32 Co3 C34 C33 -36.91(16) . . . . ?
B2 Co3 C34 C33 60.0(5) . . . . ?
B8 Co3 C34 C33 156.13(16) . . . . ?
B4 Co3 C34 C33 -161.5(2) . . . . ?
B7 Co3 C34 C33 106.61(16) . . . . ?
As1 Co3 C34 C33 -37.7(4) . . . . ?
As2 Co3 C34 C33 54.11(16) . . . . ?
As4 Co3 C34 C33 -154.38(14) . . . . ?
C33 Co3 C34 C30 118.2(2) . . . . ?
C31 Co3 C34 C30 37.95(16) . . . . ?
C32 Co3 C34 C30 81.25(17) . . . . ?
B2 Co3 C34 C30 178.1(5) . . . . ?
B8 Co3 C34 C30 -85.70(17) . . . . ?
B4 Co3 C34 C30 -43.3(3) . . . . ?
B7 Co3 C34 C30 -135.23(16) . . . . ?
As1 Co3 C34 C30 80.5(3) . . . . ?
As2 Co3 C34 C30 172.27(13) . . . . ?
As4 Co3 C34 C30 -36.22(18) . . . . ?
