#------------------------------------------------------------------------------
#$Date: 2016-03-25 13:50:30 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179866 $
#$URL: svn://www.crystallography.net/cod/cif/7/01/62/7016247.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7016247
loop_
_publ_author_name
'McLellan, R.'
'Boag, N. M.'
'Dodds, K.'
'Ellis, D.'
'Macgregor, S. A.'
'McKay, D.'
'Masters, S. L.'
'Noble-Eddy, R'
'Platt, N. P.'
'Rankin, D. W. H.'
'Robertson, H. E.'
'Rosair, G. M.'
'Welch, A. J.'
_publ_section_title
;
 New chemistry of 1,2-closo-P(2)B(10)H(10) and
 1,2-closo-As(2)B(10)H(10); in silico and gas electron diffraction
 structures, and new metalladiphospha- and metalladiarsaboranes.
;
_journal_issue                   27
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              7181
_journal_page_last               7192
_journal_paper_doi               10.1039/c1dt10540j
_journal_volume                  40
_journal_year                    2011
_chemical_formula_sum            'C5 H14 B9 Co P2'
_chemical_formula_weight         292.32
_space_group_IT_number           11
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yb'
_symmetry_space_group_name_H-M   'P 1 21/m 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 113.024(12)
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   7.220(5)
_cell_length_b                   10.652(8)
_cell_length_c                   8.821(6)
_cell_measurement_reflns_used    9300
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      31.97
_cell_measurement_theta_min      2.51
_cell_volume                     624.4(8)
_computing_cell_refinement       'Bruker SAINT'
_computing_data_collection       'Bruker APEX2'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      100(2)
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 0.925
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0312
_diffrn_reflns_av_sigmaI/netI    0.0209
_diffrn_reflns_limit_h_max       10
_diffrn_reflns_limit_h_min       -10
_diffrn_reflns_limit_k_max       14
_diffrn_reflns_limit_k_min       -15
_diffrn_reflns_limit_l_max       13
_diffrn_reflns_limit_l_min       -12
_diffrn_reflns_number            15705
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         32.59
_diffrn_reflns_theta_min         2.51
_exptl_absorpt_coefficient_mu    1.587
_exptl_absorpt_correction_T_max  0.8835
_exptl_absorpt_correction_T_min  0.3823
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'Bruker SADABS'
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.555
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       PLATE
_exptl_crystal_F_000             292
_exptl_crystal_size_max          0.75
_exptl_crystal_size_mid          0.42
_exptl_crystal_size_min          0.08
_refine_diff_density_max         0.814
_refine_diff_density_min         -0.685
_refine_diff_density_rms         0.105
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.026
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     85
_refine_ls_number_reflns         2201
_refine_ls_number_restraints     9
_refine_ls_restrained_S_all      1.025
_refine_ls_R_factor_all          0.0474
_refine_ls_R_factor_gt           0.0449
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0289P)²+2.6360P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1090
_refine_ls_wR_factor_ref         0.1104
_reflns_number_gt                2084
_reflns_number_total             2201
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c1dt10540j.txt
_cod_data_source_block           x82605_0m
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 
;
_cod_original_sg_symbol_H-M      P2(1)/m
_cod_database_code               7016247
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z'
'-x, -y, -z'
'x, -y-1/2, z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Co3 Co 0.72294(6) 0.2500 -0.05656(5) 0.01214(12) Uani 1 2 d S . .
P1 P 1.05787(13) 0.2500 0.09992(11) 0.01824(19) Uani 1 2 d S . .
P2 P 0.86582(16) 0.08222(12) 0.10653(15) 0.0238(2) Uani 0.50 1 d P . 1
B2 B 0.86582(16) 0.08222(12) 0.10653(15) 0.0238(2) Uani 0.50 1 d P . 2
H2 H 0.8735 -0.0125 0.0543 0.029 Uiso 0.50 1 calc PR . 2
B6 B 1.0679(4) 0.1640(3) 0.3100(3) 0.0185(5) Uani 1 1 d . . .
H6 H 1.2098 0.1102 0.3771 0.022 Uiso 1 1 calc R . 1
B7 B 0.6217(4) 0.1645(3) 0.1159(3) 0.0156(4) Uani 1 1 d . . .
H7 H 0.4759 0.1124 0.0589 0.019 Uiso 1 1 calc R A 1
B10 B 0.9477(6) 0.2500 0.4180(5) 0.0257(9) Uani 1 2 d S . .
H10 H 1.0137 0.2500 0.5559 0.031 Uiso 1 2 calc SR . .
B11 B 0.8282(4) 0.1137(3) 0.3074(4) 0.0252(6) Uani 1 1 d . . .
H11 H 0.8161 0.0264 0.3736 0.030 Uiso 1 1 calc R B 1
B12 B 0.6830(6) 0.2500 0.3050(5) 0.0237(9) Uani 1 2 d S . .
H12 H 0.5757 0.2500 0.3685 0.028 Uiso 1 2 calc SR . .
C30 C 0.7383(4) 0.1837(2) -0.2728(3) 0.0219(5) Uani 1 1 d U . .
H30 H 0.8404 0.1316 -0.2817 0.026 Uiso 1 1 calc R . .
C33 C 0.4525(6) 0.2500 -0.2481(5) 0.058(2) Uani 1 2 d SU . .
H33 H 0.3266 0.2500 -0.2373 0.070 Uiso 1 2 calc SR . .
C34 C 0.5623(5) 0.1418(4) -0.2576(3) 0.0427(10) Uani 1 1 d U . .
H34 H 0.5238 0.0569 -0.2543 0.051 Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C33 Co3 C34 40.79(14) . . ?
C33 Co3 C34 40.79(14) . 4_565 ?
C34 Co3 C34 68.3(2) . 4_565 ?
C33 Co3 C30 67.26(15) . . ?
C34 Co3 C30 39.68(12) . . ?
C34 Co3 C30 67.18(13) 4_565 . ?
C33 Co3 C30 67.26(15) . 4_565 ?
C34 Co3 C30 67.18(13) . 4_565 ?
C34 Co3 C30 39.68(12) 4_565 4_565 ?
C30 Co3 C30 39.74(15) . 4_565 ?
C33 Co3 B7 96.19(15) . 4_565 ?
C34 Co3 B7 128.39(13) . 4_565 ?
C34 Co3 B7 98.13(12) 4_565 4_565 ?
C30 Co3 B7 163.05(11) . 4_565 ?
C30 Co3 B7 131.78(11) 4_565 4_565 ?
C33 Co3 B7 96.19(15) . . ?
C34 Co3 B7 98.13(12) . . ?
C34 Co3 B7 128.39(13) 4_565 . ?
C30 Co3 B7 131.78(11) . . ?
C30 Co3 B7 163.05(11) 4_565 . ?
B7 Co3 B7 50.56(15) 4_565 . ?
C33 Co3 P1 163.79(14) . . ?
C34 Co3 P1 129.33(13) . . ?
C34 Co3 P1 129.33(13) 4_565 . ?
C30 Co3 P1 97.57(9) . . ?
C30 Co3 P1 97.57(9) 4_565 . ?
B7 Co3 P1 98.46(9) 4_565 . ?
B7 Co3 P1 98.46(9) . . ?
C33 Co3 P2 125.44(5) . 4_565 ?
C34 Co3 P2 162.14(12) . 4_565 ?
C34 Co3 P2 93.94(14) 4_565 4_565 ?
C30 Co3 P2 132.41(8) . 4_565 ?
C30 Co3 P2 98.05(9) 4_565 4_565 ?
B7 Co3 P2 53.85(8) 4_565 4_565 ?
B7 Co3 P2 94.68(9) . 4_565 ?
P1 Co3 P2 60.19(4) . 4_565 ?
C33 Co3 B2 125.44(5) . 4_565 ?
C34 Co3 B2 162.14(12) . 4_565 ?
C34 Co3 B2 93.94(14) 4_565 4_565 ?
C30 Co3 B2 132.41(8) . 4_565 ?
C30 Co3 B2 98.05(9) 4_565 4_565 ?
B7 Co3 B2 53.85(8) 4_565 4_565 ?
B7 Co3 B2 94.68(9) . 4_565 ?
P1 Co3 B2 60.19(4) . 4_565 ?
P2 Co3 B2 0.00(7) 4_565 4_565 ?
C33 Co3 P2 125.44(5) . . ?
C34 Co3 P2 93.94(14) . . ?
C34 Co3 P2 162.14(12) 4_565 . ?
C30 Co3 P2 98.05(9) . . ?
C30 Co3 P2 132.41(8) 4_565 . ?
B7 Co3 P2 94.68(9) 4_565 . ?
B7 Co3 P2 53.85(8) . . ?
P1 Co3 P2 60.19(4) . . ?
P2 Co3 P2 103.67(8) 4_565 . ?
B2 Co3 P2 103.67(8) 4_565 . ?
B6 P1 B6 53.26(18) 4_565 . ?
B6 P1 Co3 101.72(8) 4_565 . ?
B6 P1 Co3 101.72(8) . . ?
B6 P1 P2 97.73(10) 4_565 . ?
B6 P1 P2 55.30(9) . . ?
Co3 P1 P2 60.03(5) . . ?
B6 P1 P2 55.30(9) 4_565 4_565 ?
B6 P1 P2 97.73(10) . 4_565 ?
Co3 P1 P2 60.03(5) . 4_565 ?
P2 P1 P2 103.44(9) . 4_565 ?
B6 P1 B2 55.30(9) 4_565 4_565 ?
B6 P1 B2 97.73(10) . 4_565 ?
Co3 P1 B2 60.03(5) . 4_565 ?
P2 P1 B2 103.44(9) . 4_565 ?
P2 P1 B2 0.00(6) 4_565 4_565 ?
B11 P2 B7 56.01(11) . . ?
B11 P2 B6 54.42(13) . . ?
B7 P2 B6 96.68(13) . . ?
B11 P2 Co3 104.66(12) . . ?
B7 P2 Co3 59.49(8) . . ?
B6 P2 Co3 102.42(11) . . ?
B11 P2 P1 101.16(11) . . ?
B7 P2 P1 102.28(11) . . ?
B6 P2 P1 56.46(9) . . ?
Co3 P2 P1 59.79(6) . . ?
B10 B6 B11 59.45(18) . . ?
B10 B6 B6 58.91(12) . 4_565 ?
B11 B6 B6 107.30(15) . 4_565 ?
B10 B6 P2 111.45(18) . . ?
B11 B6 P2 60.20(14) . . ?
B6 B6 P2 115.62(9) 4_565 . ?
B10 B6 P1 113.86(18) . . ?
B11 B6 P1 115.35(16) . . ?
B6 B6 P1 63.37(9) 4_565 . ?
P2 B6 P1 68.24(10) . . ?
B10 B6 H6 121.3 . . ?
B11 B6 H6 122.0 . . ?
B6 B6 H6 120.8 4_565 . ?
P2 B6 H6 116.3 . . ?
P1 B6 H6 114.1 . . ?
B12 B7 B7 59.55(11) . 4_565 ?
B12 B7 B11 58.75(17) . . ?
B7 B7 B11 107.07(14) 4_565 . ?
B12 B7 P2 111.08(18) . . ?
B7 B7 P2 116.00(9) 4_565 . ?
B11 B7 P2 59.94(14) . . ?
B12 B7 Co3 114.64(17) . . ?
B7 B7 Co3 64.72(8) 4_565 . ?
B11 B7 Co3 113.51(17) . . ?
P2 B7 Co3 66.67(9) . . ?
B12 B7 H7 121.0 . . ?
B7 B7 H7 119.7 4_565 . ?
B11 B7 H7 123.2 . . ?
P2 B7 H7 116.9 . . ?
Co3 B7 H7 114.5 . . ?
B6 B10 B6 62.2(2) . 4_565 ?
B6 B10 B11 61.12(16) . . ?
B6 B10 B11 111.3(2) 4_565 . ?
B6 B10 B11 111.3(2) . 4_565 ?
B6 B10 B11 61.12(16) 4_565 4_565 ?
B11 B10 B11 109.9(3) . 4_565 ?
B6 B10 B12 110.1(2) . . ?
B6 B10 B12 110.1(2) 4_565 . ?
B11 B10 B12 60.41(15) . . ?
B11 B10 B12 60.41(15) 4_565 . ?
B6 B10 H10 119.6 . . ?
B6 B10 H10 119.6 4_565 . ?
B11 B10 H10 120.4 . . ?
B11 B10 H10 120.4 4_565 . ?
B12 B10 H10 121.1 . . ?
B10 B11 B12 59.9(2) . . ?
B10 B11 B6 59.43(19) . . ?
B12 B11 B6 108.3(2) . . ?
B10 B11 B7 108.0(2) . . ?
B12 B11 B7 59.33(18) . . ?
B6 B11 B7 110.66(19) . . ?
B10 B11 P2 115.8(2) . . ?
B12 B11 P2 115.1(2) . . ?
B6 B11 P2 65.37(14) . . ?
B7 B11 P2 64.05(14) . . ?
B10 B11 H11 120.9 . . ?
B12 B11 H11 121.1 . . ?
B6 B11 H11 120.7 . . ?
B7 B11 H11 121.4 . . ?
P2 B11 H11 113.8 . . ?
B10 B12 B11 59.72(15) . 4_565 ?
B10 B12 B11 59.72(15) . . ?
B11 B12 B11 108.8(3) 4_565 . ?
B10 B12 B7 109.9(2) . . ?
B11 B12 B7 110.7(2) 4_565 . ?
B11 B12 B7 61.92(15) . . ?
B10 B12 B7 109.9(2) . 4_565 ?
B11 B12 B7 61.92(15) 4_565 4_565 ?
B11 B12 B7 110.7(2) . 4_565 ?
B7 B12 B7 60.9(2) . 4_565 ?
B10 B12 H12 121.5 . . ?
B11 B12 H12 120.8 4_565 . ?
B11 B12 H12 120.8 . . ?
B7 B12 H12 119.8 . . ?
B7 B12 H12 119.8 4_565 . ?
C34 C30 C30 108.6(2) . 4_565 ?
C34 C30 Co3 69.16(16) . . ?
C30 C30 Co3 70.13(7) 4_565 . ?
C34 C30 H30 125.7 . . ?
C30 C30 H30 125.7 4_565 . ?
Co3 C30 H30 126.6 . . ?
C34 C33 C34 108.5(4) 4_565 . ?
C34 C33 Co3 70.7(2) 4_565 . ?
C34 C33 Co3 70.7(2) . . ?
C34 C33 H33 125.8 4_565 . ?
C34 C33 H33 125.8 . . ?
Co3 C33 H33 124.4 . . ?
C30 C34 C33 107.2(3) . . ?
C30 C34 Co3 71.16(16) . . ?
C33 C34 Co3 68.5(2) . . ?
C30 C34 H34 126.4 . . ?
C33 C34 H34 126.4 . . ?
Co3 C34 H34 125.5 . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Co3 C33 2.022(4) . ?
Co3 C34 2.052(3) . ?
Co3 C34 2.052(3) 4_565 ?
Co3 C30 2.077(3) . ?
Co3 C30 2.077(3) 4_565 ?
Co3 B7 2.133(3) 4_565 ?
Co3 B7 2.133(3) . ?
Co3 P1 2.2675(17) . ?
Co3 P2 2.2730(17) 4_565 ?
Co3 B2 2.2730(17) 4_565 ?
Co3 P2 2.2730(17) . ?
P1 B6 2.043(3) 4_565 ?
P1 B6 2.043(3) . ?
P1 P2 2.2767(18) . ?
P1 P2 2.2767(18) 4_565 ?
P1 B2 2.2767(18) 4_565 ?
P2 B11 1.924(4) . ?
P2 B7 1.999(3) . ?
P2 B6 2.015(3) . ?
B6 B10 1.773(5) . ?
B6 B11 1.803(4) . ?
B6 B6 1.832(6) 4_565 ?
B6 H6 1.1200 . ?
B7 B12 1.797(4) . ?
B7 B7 1.822(6) 4_565 ?
B7 B11 1.843(4) . ?
B7 H7 1.1200 . ?
B10 B6 1.773(5) 4_565 ?
B10 B11 1.774(4) . ?
B10 B11 1.774(4) 4_565 ?
B10 B12 1.777(6) . ?
B10 H10 1.1200 . ?
B11 B12 1.786(4) . ?
B11 H11 1.1200 . ?
B12 B11 1.786(4) 4_565 ?
B12 B7 1.797(4) 4_565 ?
B12 H12 1.1200 . ?
C30 C34 1.402(4) . ?
C30 C30 1.412(5) 4_565 ?
C30 H30 0.9500 . ?
C33 C34 1.420(5) 4_565 ?
C33 C34 1.420(5) . ?
C33 H33 0.9500 . ?
C34 H34 0.9500 . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C33 Co3 P1 B6 152.76(9) . . . 4_565 ?
C34 Co3 P1 B6 -160.68(15) . . . 4_565 ?
C34 Co3 P1 B6 106.20(16) 4_565 . . 4_565 ?
C30 Co3 P1 B6 172.81(12) . . . 4_565 ?
C30 Co3 P1 B6 132.71(12) 4_565 . . 4_565 ?
B7 Co3 P1 B6 -1.66(12) 4_565 . . 4_565 ?
B7 Co3 P1 B6 -52.82(12) . . . 4_565 ?
P2 Co3 P1 B6 37.74(10) 4_565 . . 4_565 ?
B2 Co3 P1 B6 37.74(10) 4_565 . . 4_565 ?
P2 Co3 P1 B6 -92.23(11) . . . 4_565 ?
C33 Co3 P1 B6 -152.76(9) . . . . ?
C34 Co3 P1 B6 -106.20(16) . . . . ?
C34 Co3 P1 B6 160.68(15) 4_565 . . . ?
C30 Co3 P1 B6 -132.71(12) . . . . ?
C30 Co3 P1 B6 -172.81(12) 4_565 . . . ?
B7 Co3 P1 B6 52.82(12) 4_565 . . . ?
B7 Co3 P1 B6 1.66(12) . . . . ?
P2 Co3 P1 B6 92.23(11) 4_565 . . . ?
B2 Co3 P1 B6 92.23(11) 4_565 . . . ?
P2 Co3 P1 B6 -37.74(10) . . . . ?
C33 Co3 P1 P2 -115.02(4) . . . . ?
C34 Co3 P1 P2 -68.46(14) . . . . ?
C34 Co3 P1 P2 -161.58(13) 4_565 . . . ?
C30 Co3 P1 P2 -94.97(9) . . . . ?
C30 Co3 P1 P2 -135.07(8) 4_565 . . . ?
B7 Co3 P1 P2 90.56(9) 4_565 . . . ?
B7 Co3 P1 P2 39.40(8) . . . . ?
P2 Co3 P1 P2 129.97(9) 4_565 . . . ?
B2 Co3 P1 P2 129.97(9) 4_565 . . . ?
C33 Co3 P1 P2 115.02(4) . . . 4_565 ?
C34 Co3 P1 P2 161.58(13) . . . 4_565 ?
C34 Co3 P1 P2 68.46(14) 4_565 . . 4_565 ?
C30 Co3 P1 P2 135.07(8) . . . 4_565 ?
C30 Co3 P1 P2 94.97(9) 4_565 . . 4_565 ?
B7 Co3 P1 P2 -39.40(8) 4_565 . . 4_565 ?
B7 Co3 P1 P2 -90.56(9) . . . 4_565 ?
B2 Co3 P1 P2 0.0 4_565 . . 4_565 ?
P2 Co3 P1 P2 -129.97(9) . . . 4_565 ?
C33 Co3 P1 B2 115.02(4) . . . 4_565 ?
C34 Co3 P1 B2 161.58(13) . . . 4_565 ?
C34 Co3 P1 B2 68.46(14) 4_565 . . 4_565 ?
C30 Co3 P1 B2 135.07(8) . . . 4_565 ?
C30 Co3 P1 B2 94.97(9) 4_565 . . 4_565 ?
B7 Co3 P1 B2 -39.40(8) 4_565 . . 4_565 ?
B7 Co3 P1 B2 -90.56(9) . . . 4_565 ?
P2 Co3 P1 B2 0.0 4_565 . . 4_565 ?
P2 Co3 P1 B2 -129.97(9) . . . 4_565 ?
C33 Co3 P2 B11 -103.55(19) . . . . ?
C34 Co3 P2 B11 -131.61(14) . . . . ?
C34 Co3 P2 B11 -138.3(4) 4_565 . . . ?
C30 Co3 P2 B11 -171.31(12) . . . . ?
C30 Co3 P2 B11 166.01(14) 4_565 . . . ?
B7 Co3 P2 B11 -2.54(12) 4_565 . . . ?
B7 Co3 P2 B11 -34.42(13) . . . . ?
P1 Co3 P2 B11 94.54(11) . . . . ?
P2 Co3 P2 B11 51.35(12) 4_565 . . . ?
B2 Co3 P2 B11 51.35(12) 4_565 . . . ?
C33 Co3 P2 B7 -69.13(19) . . . . ?
C34 Co3 P2 B7 -97.19(14) . . . . ?
C34 Co3 P2 B7 -103.9(4) 4_565 . . . ?
C30 Co3 P2 B7 -136.89(12) . . . . ?
C30 Co3 P2 B7 -159.57(14) 4_565 . . . ?
B7 Co3 P2 B7 31.88(11) 4_565 . . . ?
P1 Co3 P2 B7 128.96(11) . . . . ?
P2 Co3 P2 B7 85.77(11) 4_565 . . . ?
B2 Co3 P2 B7 85.77(11) 4_565 . . . ?
C33 Co3 P2 B6 -159.62(18) . . . . ?
C34 Co3 P2 B6 172.32(13) . . . . ?
C34 Co3 P2 B6 165.6(4) 4_565 . . . ?
C30 Co3 P2 B6 132.62(12) . . . . ?
C30 Co3 P2 B6 109.94(15) 4_565 . . . ?
B7 Co3 P2 B6 -58.61(12) 4_565 . . . ?
B7 Co3 P2 B6 -90.49(13) . . . . ?
P1 Co3 P2 B6 38.47(9) . . . . ?
P2 Co3 P2 B6 -4.72(11) 4_565 . . . ?
B2 Co3 P2 B6 -4.72(11) 4_565 . . . ?
C33 Co3 P2 P1 161.91(16) . . . . ?
C34 Co3 P2 P1 133.85(10) . . . . ?
C34 Co3 P2 P1 127.1(4) 4_565 . . . ?
C30 Co3 P2 P1 94.15(9) . . . . ?
C30 Co3 P2 P1 71.47(12) 4_565 . . . ?
B7 Co3 P2 P1 -97.08(8) 4_565 . . . ?
B7 Co3 P2 P1 -128.96(11) . . . . ?
P2 Co3 P2 P1 -43.19(6) 4_565 . . . ?
B2 Co3 P2 P1 -43.19(6) 4_565 . . . ?
B6 P1 P2 B11 -1.47(13) 4_565 . . . ?
B6 P1 P2 B11 32.62(14) . . . . ?
Co3 P1 P2 B11 -100.59(11) . . . . ?
P2 P1 P2 B11 -57.54(11) 4_565 . . . ?
B2 P1 P2 B11 -57.54(11) 4_565 . . . ?
B6 P1 P2 B7 55.83(12) 4_565 . . . ?
B6 P1 P2 B7 89.92(13) . . . . ?
Co3 P1 P2 B7 -43.28(9) . . . . ?
P2 P1 P2 B7 -0.23(11) 4_565 . . . ?
B2 P1 P2 B7 -0.23(11) 4_565 . . . ?
B6 P1 P2 B6 -34.09(13) 4_565 . . . ?
Co3 P1 P2 B6 -133.20(11) . . . . ?
P2 P1 P2 B6 -90.15(11) 4_565 . . . ?
B2 P1 P2 B6 -90.15(11) 4_565 . . . ?
B6 P1 P2 Co3 99.12(9) 4_565 . . . ?
B6 P1 P2 Co3 133.20(11) . . . . ?
P2 P1 P2 Co3 43.05(7) 4_565 . . . ?
B2 P1 P2 Co3 43.05(7) 4_565 . . . ?
B11 P2 B6 B10 -31.32(17) . . . . ?
B7 P2 B6 B10 7.80(19) . . . . ?
Co3 P2 B6 B10 67.96(17) . . . . ?
P1 P2 B6 B10 108.12(18) . . . . ?
B7 P2 B6 B11 39.12(16) . . . . ?
Co3 P2 B6 B11 99.28(14) . . . . ?
P1 P2 B6 B11 139.44(17) . . . . ?
B11 P2 B6 B6 -96.05(14) . . . 4_565 ?
B7 P2 B6 B6 -56.93(10) . . . 4_565 ?
Co3 P2 B6 B6 3.23(8) . . . 4_565 ?
P1 P2 B6 B6 43.40(6) . . . 4_565 ?
B11 P2 B6 P1 -139.44(17) . . . . ?
B7 P2 B6 P1 -100.32(11) . . . . ?
Co3 P2 B6 P1 -40.17(8) . . . . ?
B6 P1 B6 B10 31.4(2) 4_565 . . . ?
Co3 P1 B6 B10 -64.56(19) . . . . ?
P2 P1 B6 B10 -104.7(2) . . . . ?
P2 P1 B6 B10 -3.69(19) 4_565 . . . ?
B2 P1 B6 B10 -3.69(19) 4_565 . . . ?
B6 P1 B6 B11 97.5(2) 4_565 . . . ?
Co3 P1 B6 B11 1.5(2) . . . . ?
P2 P1 B6 B11 -38.64(18) . . . . ?
P2 P1 B6 B11 62.4(2) 4_565 . . . ?
B2 P1 B6 B11 62.4(2) 4_565 . . . ?
Co3 P1 B6 B6 -95.97(5) . . . 4_565 ?
P2 P1 B6 B6 -136.13(7) . . . 4_565 ?
P2 P1 B6 B6 -35.10(5) 4_565 . . 4_565 ?
B2 P1 B6 B6 -35.10(5) 4_565 . . 4_565 ?
B6 P1 B6 P2 136.13(7) 4_565 . . . ?
Co3 P1 B6 P2 40.16(8) . . . . ?
P2 P1 B6 P2 101.03(10) 4_565 . . . ?
B2 P1 B6 P2 101.03(10) 4_565 . . . ?
B11 P2 B7 B12 30.06(17) . . . . ?
B6 P2 B7 B12 -8.18(18) . . . . ?
Co3 P2 B7 B12 -108.68(17) . . . . ?
P1 P2 B7 B12 -65.23(16) . . . . ?
B11 P2 B7 B7 95.45(14) . . . 4_565 ?
B6 P2 B7 B7 57.21(11) . . . 4_565 ?
Co3 P2 B7 B7 -43.29(5) . . . 4_565 ?
P1 P2 B7 B7 0.16(8) . . . 4_565 ?
B6 P2 B7 B11 -38.24(16) . . . . ?
Co3 P2 B7 B11 -138.74(16) . . . . ?
P1 P2 B7 B11 -95.29(14) . . . . ?
B11 P2 B7 Co3 138.74(16) . . . . ?
B6 P2 B7 Co3 100.50(12) . . . . ?
P1 P2 B7 Co3 43.45(7) . . . . ?
C33 Co3 B7 B12 -126.50(18) . . . . ?
C34 Co3 B7 B12 -167.6(2) . . . . ?
C34 Co3 B7 B12 -98.8(2) 4_565 . . . ?
C30 Co3 B7 B12 168.62(17) . . . . ?
C30 Co3 B7 B12 -138.7(3) 4_565 . . . ?
B7 Co3 B7 B12 -33.56(19) 4_565 . . . ?
P1 Co3 B7 B12 60.47(17) . . . . ?
P2 Co3 B7 B12 -0.05(18) 4_565 . . . ?
B2 Co3 B7 B12 -0.05(18) 4_565 . . . ?
P2 Co3 B7 B12 103.48(19) . . . . ?
C33 Co3 B7 B7 -92.93(7) . . . 4_565 ?
C34 Co3 B7 B7 -134.01(14) . . . 4_565 ?
C34 Co3 B7 B7 -65.28(16) 4_565 . . 4_565 ?
C30 Co3 B7 B7 -157.82(15) . . . 4_565 ?
C30 Co3 B7 B7 -105.1(4) 4_565 . . 4_565 ?
P1 Co3 B7 B7 94.03(4) . . . 4_565 ?
P2 Co3 B7 B7 33.51(5) 4_565 . . 4_565 ?
B2 Co3 B7 B7 33.51(5) 4_565 . . 4_565 ?
P2 Co3 B7 B7 137.04(6) . . . 4_565 ?
C33 Co3 B7 B11 168.53(18) . . . . ?
C34 Co3 B7 B11 127.4(2) . . . . ?
C34 Co3 B7 B11 -163.8(2) 4_565 . . . ?
C30 Co3 B7 B11 103.6(2) . . . . ?
C30 Co3 B7 B11 156.4(3) 4_565 . . . ?
B7 Co3 B7 B11 -98.54(18) 4_565 . . . ?
P1 Co3 B7 B11 -4.51(19) . . . . ?
P2 Co3 B7 B11 -65.03(18) 4_565 . . . ?
B2 Co3 B7 B11 -65.03(18) 4_565 . . . ?
P2 Co3 B7 B11 38.50(16) . . . . ?
C33 Co3 B7 P2 130.03(9) . . . . ?
C34 Co3 B7 P2 88.95(16) . . . . ?
C34 Co3 B7 P2 157.68(15) 4_565 . . . ?
C30 Co3 B7 P2 65.15(15) . . . . ?
C30 Co3 B7 P2 117.9(3) 4_565 . . . ?
B7 Co3 B7 P2 -137.04(6) 4_565 . . . ?
P1 Co3 B7 P2 -43.01(8) . . . . ?
P2 Co3 B7 P2 -103.52(9) 4_565 . . . ?
B2 Co3 B7 P2 -103.52(9) 4_565 . . . ?
B11 B6 B10 B6 -139.38(18) . . . 4_565 ?
P2 B6 B10 B6 -107.79(15) . . . 4_565 ?
P1 B6 B10 B6 -33.0(2) . . . 4_565 ?
B6 B6 B10 B11 139.38(18) 4_565 . . . ?
P2 B6 B10 B11 31.59(17) . . . . ?
P1 B6 B10 B11 106.42(18) . . . . ?
B11 B6 B10 B11 -101.7(3) . . . 4_565 ?
B6 B6 B10 B11 37.71(14) 4_565 . . 4_565 ?
P2 B6 B10 B11 -70.1(2) . . . 4_565 ?
P1 B6 B10 B11 4.7(3) . . . 4_565 ?
B11 B6 B10 B12 -36.62(17) . . . . ?
B6 B6 B10 B12 102.76(18) 4_565 . . . ?
P2 B6 B10 B12 -5.0(2) . . . . ?
P1 B6 B10 B12 69.8(2) . . . . ?
B6 B10 B11 B12 -139.9(2) . . . . ?
B6 B10 B11 B12 -101.7(2) 4_565 . . . ?
B11 B10 B11 B12 -36.0(3) 4_565 . . . ?
B6 B10 B11 B6 38.2(2) 4_565 . . . ?
B11 B10 B11 B6 103.9(3) 4_565 . . . ?
B12 B10 B11 B6 139.9(2) . . . . ?
B6 B10 B11 B7 -103.8(2) . . . . ?
B6 B10 B11 B7 -65.7(3) 4_565 . . . ?
B11 B10 B11 B7 0.1(4) 4_565 . . . ?
B12 B10 B11 B7 36.1(2) . . . . ?
B6 B10 B11 P2 -34.56(18) . . . . ?
B6 B10 B11 P2 3.6(3) 4_565 . . . ?
B11 B10 B11 P2 69.4(3) 4_565 . . . ?
B12 B10 B11 P2 105.3(2) . . . . ?
B6 B6 B11 B10 -35.73(15) 4_565 . . . ?
P2 B6 B11 B10 -145.82(19) . . . . ?
P1 B6 B11 B10 -103.9(2) . . . . ?
B10 B6 B11 B12 35.9(2) . . . . ?
B6 B6 B11 B12 0.2(2) 4_565 . . . ?
P2 B6 B11 B12 -109.9(2) . . . . ?
P1 B6 B11 B12 -67.9(3) . . . . ?
B10 B6 B11 B7 99.2(3) . . . . ?
B6 B6 B11 B7 63.5(2) 4_565 . . . ?
P2 B6 B11 B7 -46.58(18) . . . . ?
P1 B6 B11 B7 -4.6(3) . . . . ?
B10 B6 B11 P2 145.82(19) . . . . ?
B6 B6 B11 P2 110.09(10) 4_565 . . . ?
P1 B6 B11 P2 41.93(17) . . . . ?
B12 B7 B11 B10 -36.3(2) . . . . ?
B7 B7 B11 B10 -0.1(2) 4_565 . . . ?
P2 B7 B11 B10 110.6(2) . . . . ?
Co3 B7 B11 B10 69.2(2) . . . . ?
B7 B7 B11 B12 36.24(15) 4_565 . . . ?
P2 B7 B11 B12 146.86(19) . . . . ?
Co3 B7 B11 B12 105.5(2) . . . . ?
B12 B7 B11 B6 -99.6(3) . . . . ?
B7 B7 B11 B6 -63.4(2) 4_565 . . . ?
P2 B7 B11 B6 47.25(19) . . . . ?
Co3 B7 B11 B6 5.9(3) . . . . ?
B12 B7 B11 P2 -146.86(19) . . . . ?
B7 B7 B11 P2 -110.62(10) 4_565 . . . ?
Co3 B7 B11 P2 -41.33(15) . . . . ?
B7 P2 B11 B10 -98.4(2) . . . . ?
B6 P2 B11 B10 32.50(18) . . . . ?
Co3 P2 B11 B10 -62.4(2) . . . . ?
P1 P2 B11 B10 -1.0(2) . . . . ?
B7 P2 B11 B12 -31.29(18) . . . . ?
B6 P2 B11 B12 99.6(2) . . . . ?
Co3 P2 B11 B12 4.7(2) . . . . ?
P1 P2 B11 B12 66.1(2) . . . . ?
B7 P2 B11 B6 -130.9(2) . . . . ?
Co3 P2 B11 B6 -94.94(14) . . . . ?
P1 P2 B11 B6 -33.53(14) . . . . ?
B6 P2 B11 B7 130.9(2) . . . . ?
Co3 P2 B11 B7 35.97(13) . . . . ?
P1 P2 B11 B7 97.38(13) . . . . ?
B6 B10 B12 B11 -103.6(2) . . . 4_565 ?
B6 B10 B12 B11 -36.92(18) 4_565 . . 4_565 ?
B11 B10 B12 B11 -140.6(3) . . . 4_565 ?
B6 B10 B12 B11 36.92(18) . . . . ?
B6 B10 B12 B11 103.6(2) 4_565 . . . ?
B11 B10 B12 B11 140.6(3) 4_565 . . . ?
B6 B10 B12 B7 -0.7(2) . . . . ?
B6 B10 B12 B7 65.99(18) 4_565 . . . ?
B11 B10 B12 B7 -37.66(17) . . . . ?
B11 B10 B12 B7 102.9(2) 4_565 . . . ?
B6 B10 B12 B7 -65.99(18) . . . 4_565 ?
B6 B10 B12 B7 0.7(2) 4_565 . . 4_565 ?
B11 B10 B12 B7 -102.9(2) . . . 4_565 ?
B11 B10 B12 B7 37.66(17) 4_565 . . 4_565 ?
B6 B11 B12 B10 -35.8(2) . . . . ?
B7 B11 B12 B10 -139.4(2) . . . . ?
P2 B11 B12 B10 -106.5(2) . . . . ?
B10 B11 B12 B11 35.4(3) . . . 4_565 ?
B6 B11 B12 B11 -0.4(4) . . . 4_565 ?
B7 B11 B12 B11 -104.0(3) . . . 4_565 ?
P2 B11 B12 B11 -71.1(3) . . . 4_565 ?
B10 B11 B12 B7 139.4(2) . . . . ?
B6 B11 B12 B7 103.6(2) . . . . ?
P2 B11 B12 B7 32.88(18) . . . . ?
B10 B11 B12 B7 101.6(2) . . . 4_565 ?
B6 B11 B12 B7 65.9(3) . . . 4_565 ?
B7 B11 B12 B7 -37.76(18) . . . 4_565 ?
P2 B11 B12 B7 -4.9(3) . . . 4_565 ?
B7 B7 B12 B10 -102.32(17) 4_565 . . . ?
B11 B7 B12 B10 36.72(16) . . . . ?
P2 B7 B12 B10 6.3(2) . . . . ?
Co3 B7 B12 B10 -66.87(18) . . . . ?
B7 B7 B12 B11 -38.19(14) 4_565 . . 4_565 ?
B11 B7 B12 B11 100.8(3) . . . 4_565 ?
P2 B7 B12 B11 70.4(2) . . . 4_565 ?
Co3 B7 B12 B11 -2.7(3) . . . 4_565 ?
B7 B7 B12 B11 -139.04(17) 4_565 . . . ?
P2 B7 B12 B11 -30.47(16) . . . . ?
Co3 B7 B12 B11 -103.60(18) . . . . ?
B11 B7 B12 B7 139.04(17) . . . 4_565 ?
P2 B7 B12 B7 108.57(13) . . . 4_565 ?
Co3 B7 B12 B7 35.4(2) . . . 4_565 ?
C33 Co3 C30 C34 -38.7(2) . . . . ?
C34 Co3 C30 C34 -83.1(3) 4_565 . . . ?
C30 Co3 C30 C34 -120.0(2) 4_565 . . . ?
B7 Co3 C30 C34 -51.8(4) 4_565 . . . ?
B7 Co3 C30 C34 38.7(3) . . . . ?
P1 Co3 C30 C34 147.3(2) . . . . ?
P2 Co3 C30 C34 -156.6(2) 4_565 . . . ?
B2 Co3 C30 C34 -156.6(2) 4_565 . . . ?
P2 Co3 C30 C34 86.5(2) . . . . ?
C33 Co3 C30 C30 81.29(7) . . . 4_565 ?
C34 Co3 C30 C30 120.0(2) . . . 4_565 ?
C34 Co3 C30 C30 36.88(15) 4_565 . . 4_565 ?
B7 Co3 C30 C30 68.2(3) 4_565 . . 4_565 ?
B7 Co3 C30 C30 158.71(14) . . . 4_565 ?
P1 Co3 C30 C30 -92.75(3) . . . 4_565 ?
P2 Co3 C30 C30 -36.66(7) 4_565 . . 4_565 ?
B2 Co3 C30 C30 -36.66(7) 4_565 . . 4_565 ?
P2 Co3 C30 C30 -153.56(6) . . . 4_565 ?
C34 Co3 C33 C34 -118.6(4) . . . 4_565 ?
C30 Co3 C33 C34 -80.9(2) . . . 4_565 ?
C30 Co3 C33 C34 -37.66(19) 4_565 . . 4_565 ?
B7 Co3 C33 C34 95.3(2) 4_565 . . 4_565 ?
B7 Co3 C33 C34 146.2(2) . . . 4_565 ?
P1 Co3 C33 C34 -59.28(19) . . . 4_565 ?
P2 Co3 C33 C34 45.9(3) 4_565 . . 4_565 ?
B2 Co3 C33 C34 45.9(3) 4_565 . . 4_565 ?
P2 Co3 C33 C34 -164.47(14) . . . 4_565 ?
C34 Co3 C33 C34 118.6(4) 4_565 . . . ?
C30 Co3 C33 C34 37.66(19) . . . . ?
C30 Co3 C33 C34 80.9(2) 4_565 . . . ?
B7 Co3 C33 C34 -146.2(2) 4_565 . . . ?
B7 Co3 C33 C34 -95.3(2) . . . . ?
P1 Co3 C33 C34 59.28(19) . . . . ?
P2 Co3 C33 C34 164.47(14) 4_565 . . . ?
B2 Co3 C33 C34 164.47(14) 4_565 . . . ?
P2 Co3 C33 C34 -45.9(3) . . . . ?
C30 C30 C34 C33 0.0(3) 4_565 . . . ?
Co3 C30 C34 C33 59.2(2) . . . . ?
C30 C30 C34 Co3 -59.24(10) 4_565 . . . ?
C34 C33 C34 C30 0.0(5) 4_565 . . . ?
Co3 C33 C34 C30 -61.0(2) . . . . ?
C34 C33 C34 Co3 61.0(3) 4_565 . . . ?
C33 Co3 C34 C30 118.1(3) . . . . ?
C34 Co3 C34 C30 79.9(2) 4_565 . . . ?
C30 Co3 C34 C30 36.93(18) 4_565 . . . ?
B7 Co3 C34 C30 163.00(16) 4_565 . . . ?
B7 Co3 C34 C30 -151.88(19) . . . . ?
P1 Co3 C34 C30 -43.9(3) . . . . ?
P2 Co3 C34 C30 72.7(5) 4_565 . . . ?
B2 Co3 C34 C30 72.7(5) 4_565 . . . ?
P2 Co3 C34 C30 -97.86(19) . . . . ?
C34 Co3 C34 C33 -38.1(2) 4_565 . . . ?
C30 Co3 C34 C33 -118.1(3) . . . . ?
C30 Co3 C34 C33 -81.1(2) 4_565 . . . ?
B7 Co3 C34 C33 44.9(3) 4_565 . . . ?
B7 Co3 C34 C33 90.1(2) . . . . ?
P1 Co3 C34 C33 -161.92(18) . . . . ?
P2 Co3 C34 C33 -45.3(4) 4_565 . . . ?
B2 Co3 C34 C33 -45.3(4) 4_565 . . . ?
P2 Co3 C34 C33 144.1(2) . . . . ?
