#------------------------------------------------------------------------------
#$Date: 2016-03-25 14:24:27 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179894 $
#$URL: svn://www.crystallography.net/cod/cif/7/01/90/7019084.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7019084
loop_
_publ_author_name
'McCann, Malachy'
'Curran, Robert'
'Ben-Shoshan, Marcia'
'McKee, Vickie'
'Tahir, Asif Ali'
'Devereux, Michael'
'Kavanagh, Kevin'
'Creaven, Bernadette S.'
'Kellett, Andrew'
_publ_section_title
;
 Silver(i) complexes of 9-anthracenecarboxylic acid and imidazoles:
 synthesis, structure and antimicrobial activity.
;
_journal_issue                   21
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              6516
_journal_page_last               6527
_journal_paper_doi               10.1039/c2dt12166b
_journal_volume                  41
_journal_year                    2012
_chemical_formula_sum            'C106 H78 Ag6 N8 O12'
_chemical_formula_weight         2302.98
_chemical_name_systematic        ' ?'
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                111.403(2)
_cell_angle_beta                 90.095(2)
_cell_angle_gamma                101.710(2)
_cell_formula_units_Z            2
_cell_length_a                   11.7251(17)
_cell_length_b                   17.908(3)
_cell_length_c                   23.464(3)
_cell_measurement_reflns_used    8664
_cell_measurement_temperature    150(2)
_cell_measurement_theta_max      27.84
_cell_measurement_theta_min      2.29
_cell_volume                     4476.1(11)
_computing_cell_refinement       'Bruker SAINT'
_computing_data_collection       'Bruker APEX2'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      150(2)
_diffrn_measured_fraction_theta_full 0.995
_diffrn_measured_fraction_theta_max 0.995
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0421
_diffrn_reflns_av_sigmaI/netI    0.0591
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       21
_diffrn_reflns_limit_k_min       -21
_diffrn_reflns_limit_l_max       27
_diffrn_reflns_limit_l_min       -27
_diffrn_reflns_number            35083
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         1.78
_exptl_absorpt_coefficient_mu    1.357
_exptl_absorpt_correction_T_max  0.9230
_exptl_absorpt_correction_T_min  0.5930
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'SADABS v2008/1, Sheldrick, G.M., (2008)'
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.709
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       plate
_exptl_crystal_F_000             2296
_exptl_crystal_size_max          0.43
_exptl_crystal_size_mid          0.32
_exptl_crystal_size_min          0.06
_refine_diff_density_max         4.988
_refine_diff_density_min         -1.066
_refine_diff_density_rms         0.183
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.049
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1194
_refine_ls_number_reflns         15686
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.049
_refine_ls_R_factor_all          0.0856
_refine_ls_R_factor_gt           0.0666
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0927P)²+35.1311P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1746
_refine_ls_wR_factor_ref         0.1882
_reflns_number_gt                11941
_reflns_number_total             15686
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c2dt12166b.txt
_cod_data_source_block           Complex_5(rjcap19a)
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 
;
_cod_original_cell_volume        4476.2(11)
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7019084
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Ag1 Ag 0.53199(5) 0.08542(3) 0.02683(3) 0.01904(15) Uani 1 1 d .
Ag2 Ag 0.33660(6) -0.00337(4) 0.07686(3) 0.02740(17) Uani 1 1 d .
O11A O 0.4960(5) 0.1822(4) 0.1181(3) 0.0350(15) Uani 1 1 d .
O12A O 0.3125(5) 0.1221(3) 0.1250(3) 0.0272(13) Uani 1 1 d .
C11A C 0.3984(7) 0.1819(5) 0.1386(4) 0.0253(18) Uani 1 1 d .
C12A C 0.3844(7) 0.2622(5) 0.1885(4) 0.0256(18) Uani 1 1 d .
C13A C 0.4588(7) 0.2966(5) 0.2434(4) 0.0241(17) Uani 1 1 d .
C14A C 0.5468(8) 0.2595(6) 0.2552(4) 0.034(2) Uani 1 1 d .
H14A H 0.5568 0.2091 0.2252 0.041 Uiso 1 1 calc R
C15A C 0.6177(9) 0.2941(6) 0.3085(5) 0.042(2) Uani 1 1 d .
H15A H 0.6758 0.2677 0.3156 0.050 Uiso 1 1 calc R
C16A C 0.6042(9) 0.3690(6) 0.3527(5) 0.044(2) Uani 1 1 d .
H16A H 0.6550 0.3934 0.3893 0.053 Uiso 1 1 calc R
C17A C 0.5210(9) 0.4073(6) 0.3446(4) 0.041(2) Uani 1 1 d .
H17A H 0.5130 0.4575 0.3755 0.050 Uiso 1 1 calc R
C18A C 0.4445(8) 0.3717(5) 0.2888(4) 0.0306(19) Uani 1 1 d .
C19A C 0.3597(8) 0.4106(5) 0.2789(4) 0.032(2) Uani 1 1 d .
H19A H 0.3507 0.4605 0.3100 0.038 Uiso 1 1 calc R
C20A C 0.2876(7) 0.3783(5) 0.2247(4) 0.032(2) Uani 1 1 d .
C21A C 0.2017(9) 0.4196(6) 0.2134(5) 0.042(2) Uani 1 1 d .
H21A H 0.1923 0.4695 0.2443 0.051 Uiso 1 1 calc R
C22A C 0.1350(9) 0.3892(6) 0.1606(5) 0.044(2) Uani 1 1 d .
H22A H 0.0809 0.4187 0.1539 0.053 Uiso 1 1 calc R
C23A C 0.1434(9) 0.3148(6) 0.1149(5) 0.041(2) Uani 1 1 d .
H23A H 0.0926 0.2928 0.0783 0.049 Uiso 1 1 calc R
C24A C 0.2253(8) 0.2727(5) 0.1226(4) 0.032(2) Uani 1 1 d .
H24A H 0.2324 0.2234 0.0904 0.039 Uiso 1 1 calc R
C25A C 0.2986(7) 0.3019(5) 0.1777(4) 0.0283(19) Uani 1 1 d .
O11B O 0.6478(5) 0.1951(3) 0.0039(2) 0.0257(12) Uani 1 1 d .
O12B O 0.6614(5) 0.1156(3) -0.0935(2) 0.0243(12) Uani 1 1 d .
C11B C 0.6509(6) 0.1820(5) -0.0526(4) 0.0227(17) Uani 1 1 d .
C12B C 0.6405(7) 0.2506(5) -0.0740(4) 0.0211(16) Uani 1 1 d .
C13B C 0.5554(7) 0.2361(5) -0.1213(4) 0.0219(17) Uani 1 1 d .
C14B C 0.4715(7) 0.1595(5) -0.1474(4) 0.0241(17) Uani 1 1 d .
H14B H 0.4740 0.1163 -0.1334 0.029 Uiso 1 1 calc R
C15B C 0.3882(7) 0.1487(6) -0.1920(4) 0.033(2) Uani 1 1 d .
H15B H 0.3331 0.0977 -0.2087 0.039 Uiso 1 1 calc R
C16B C 0.3821(8) 0.2112(6) -0.2141(4) 0.035(2) Uani 1 1 d .
H16B H 0.3244 0.2018 -0.2459 0.041 Uiso 1 1 calc R
C17B C 0.4589(8) 0.2852(6) -0.1898(4) 0.035(2) Uani 1 1 d .
H17B H 0.4536 0.3276 -0.2042 0.042 Uiso 1 1 calc R
C18B C 0.5468(7) 0.2995(5) -0.1432(4) 0.0265(18) Uani 1 1 d .
C19B C 0.6267(8) 0.3748(5) -0.1181(4) 0.0304(19) Uani 1 1 d .
H19B H 0.6239 0.4161 -0.1341 0.037 Uiso 1 1 calc R
C20B C 0.7100(8) 0.3913(5) -0.0705(4) 0.0285(18) Uani 1 1 d .
C21B C 0.7873(8) 0.4698(5) -0.0432(4) 0.034(2) Uani 1 1 d .
H21B H 0.7846 0.5108 -0.0596 0.041 Uiso 1 1 calc R
C22B C 0.8640(9) 0.4875(6) 0.0050(4) 0.040(2) Uani 1 1 d .
H22B H 0.9127 0.5408 0.0234 0.048 Uiso 1 1 calc R
C23B C 0.8712(8) 0.4250(6) 0.0281(4) 0.040(2) Uani 1 1 d .
H23B H 0.9253 0.4372 0.0621 0.048 Uiso 1 1 calc R
C24B C 0.8028(7) 0.3489(5) 0.0025(4) 0.0272(18) Uani 1 1 d .
H24B H 0.8121 0.3079 0.0178 0.033 Uiso 1 1 calc R
C25B C 0.7173(7) 0.3286(5) -0.0465(4) 0.0220(16) Uani 1 1 d .
O11C O 0.7012(5) 0.0571(3) 0.0519(3) 0.0303(13) Uani 1 1 d .
O12C O 0.6232(5) -0.0741(4) 0.0344(3) 0.0316(14) Uani 1 1 d .
C11C C 0.6986(7) -0.0091(5) 0.0583(3) 0.0205(16) Uani 1 1 d .
C12C C 0.7945(6) -0.0122(5) 0.0997(4) 0.0208(16) Uani 1 1 d .
C13C C 0.7883(6) 0.0201(5) 0.1628(4) 0.0214(16) Uani 1 1 d .
C14C C 0.6972(7) 0.0598(5) 0.1909(4) 0.0252(18) Uani 1 1 d .
H14C H 0.6389 0.0661 0.1658 0.030 Uiso 1 1 calc R
C15C C 0.6930(7) 0.0888(6) 0.2530(4) 0.0303(19) Uani 1 1 d .
H15C H 0.6328 0.1163 0.2705 0.036 Uiso 1 1 calc R
C16C C 0.7764(8) 0.0790(6) 0.2923(4) 0.032(2) Uani 1 1 d .
H16C H 0.7716 0.0989 0.3355 0.038 Uiso 1 1 calc R
C17C C 0.8639(7) 0.0405(5) 0.2667(4) 0.0293(19) Uani 1 1 d .
H17C H 0.9191 0.0332 0.2928 0.035 Uiso 1 1 calc R
C18C C 0.8747(7) 0.0108(5) 0.2020(4) 0.0244(17) Uani 1 1 d .
C19C C 0.9653(7) -0.0267(5) 0.1768(4) 0.0264(18) Uani 1 1 d .
H19C H 1.0211 -0.0334 0.2029 0.032 Uiso 1 1 calc R
C20C C 0.9753(6) -0.0543(5) 0.1140(4) 0.0247(17) Uani 1 1 d .
C21C C 1.0697(7) -0.0912(6) 0.0871(4) 0.031(2) Uani 1 1 d .
H21C H 1.1281 -0.0962 0.1128 0.037 Uiso 1 1 calc R
C22C C 1.0770(7) -0.1193(5) 0.0248(4) 0.031(2) Uani 1 1 d .
H22C H 1.1406 -0.1432 0.0080 0.038 Uiso 1 1 calc R
C23C C 0.9905(7) -0.1133(5) -0.0149(4) 0.0293(19) Uani 1 1 d .
H23C H 0.9970 -0.1325 -0.0580 0.035 Uiso 1 1 calc R
C24C C 0.8977(7) -0.0798(5) 0.0090(4) 0.0262(18) Uani 1 1 d .
H24C H 0.8393 -0.0772 -0.0179 0.031 Uiso 1 1 calc R
C25C C 0.8872(6) -0.0491(5) 0.0728(4) 0.0226(17) Uani 1 1 d .
Ag3 Ag 1.03135(5) 0.08562(3) 0.52251(3) 0.01965(15) Uani 1 1 d .
Ag4 Ag 0.84345(6) -0.00043(4) 0.42012(3) 0.02866(17) Uani 1 1 d .
O11D O 1.1490(5) 0.1940(3) 0.6072(2) 0.0238(12) Uani 1 1 d .
O12D O 1.1590(5) 0.1132(3) 0.6590(2) 0.0244(12) Uani 1 1 d .
C11D C 1.1523(6) 0.1805(5) 0.6553(3) 0.0183(16) Uani 1 1 d .
C12D C 1.1470(6) 0.2502(5) 0.7155(3) 0.0191(16) Uani 1 1 d .
C13D C 1.2307(7) 0.3248(5) 0.7326(3) 0.0219(16) Uani 1 1 d .
C14D C 1.3246(7) 0.3396(5) 0.6958(4) 0.0275(18) Uani 1 1 d .
H14D H 1.3292 0.2985 0.6570 0.033 Uiso 1 1 calc R
C15D C 1.4060(9) 0.4103(6) 0.7153(4) 0.039(2) Uani 1 1 d .
H15D H 1.4658 0.4188 0.6897 0.046 Uiso 1 1 calc R
C16D C 1.4039(9) 0.4732(6) 0.7742(5) 0.045(2) Uani 1 1 d .
H16D H 1.4629 0.5224 0.7879 0.054 Uiso 1 1 calc R
C17D C 1.3161(8) 0.4618(5) 0.8106(4) 0.039(2) Uani 1 1 d .
H17D H 1.3142 0.5036 0.8495 0.047 Uiso 1 1 calc R
C18D C 1.2283(7) 0.3886(5) 0.7911(4) 0.0273(18) Uani 1 1 d .
C19D C 1.1379(7) 0.3768(5) 0.8276(4) 0.0307(19) Uani 1 1 d .
H19D H 1.1342 0.4200 0.8654 0.037 Uiso 1 1 calc R
C20D C 1.0532(7) 0.3045(5) 0.8108(4) 0.0264(18) Uani 1 1 d .
C21D C 0.9614(8) 0.2943(5) 0.8492(4) 0.0306(19) Uani 1 1 d .
H21D H 0.9576 0.3375 0.8871 0.037 Uiso 1 1 calc R
C22D C 0.8801(8) 0.2229(6) 0.8314(4) 0.034(2) Uani 1 1 d .
H23D H 0.8197 0.2168 0.8574 0.041 Uiso 1 1 calc R
C23D C 0.8824(7) 0.1573(5) 0.7755(4) 0.0298(19) Uani 1 1 d .
H23X H 0.8243 0.1079 0.7643 0.036 Uiso 1 1 calc R
C24D C 0.9682(7) 0.1651(5) 0.7376(4) 0.0251(17) Uani 1 1 d .
H24D H 0.9687 0.1210 0.6998 0.030 Uiso 1 1 calc R
C25D C 1.0581(6) 0.2391(5) 0.7539(4) 0.0201(16) Uani 1 1 d .
O11E O 0.8763(5) 0.0719(4) 0.5752(3) 0.0385(16) Uani 1 1 d .
O12E O 0.8034(5) -0.0601(4) 0.5216(3) 0.0365(15) Uani 1 1 d .
C11E C 0.8027(6) 0.0053(5) 0.5635(3) 0.0188(16) Uani 1 1 d .
C12E C 0.7055(6) 0.0072(5) 0.6055(3) 0.0189(16) Uani 1 1 d .
C13E C 0.6117(6) 0.0426(5) 0.5999(4) 0.0225(17) Uani 1 1 d .
C14E C 0.6018(7) 0.0755(5) 0.5530(4) 0.0249(17) Uani 1 1 d .
H14E H 0.6606 0.0745 0.5251 0.030 Uiso 1 1 calc R
C15E C 0.5080(7) 0.1083(5) 0.5484(4) 0.0294(19) Uani 1 1 d .
H14X H 0.5020 0.1295 0.5171 0.035 Uiso 1 1 calc R
C16E C 0.4197(7) 0.1108(5) 0.5899(4) 0.0298(19) Uani 1 1 d .
H16E H 0.3547 0.1331 0.5858 0.036 Uiso 1 1 calc R
C17E C 0.4273(7) 0.0810(5) 0.6364(4) 0.033(2) Uani 1 1 d .
H18E H 0.3683 0.0839 0.6643 0.040 Uiso 1 1 calc R
C18E C 0.5239(7) 0.0461(5) 0.6422(4) 0.0248(17) Uani 1 1 d .
C19E C 0.5344(8) 0.0170(5) 0.6891(4) 0.0310(19) Uani 1 1 d .
H19E H 0.4759 0.0209 0.7174 0.037 Uiso 1 1 calc R
C20E C 0.6275(7) -0.0177(5) 0.6962(4) 0.0280(18) Uani 1 1 d .
C21E C 0.6392(8) -0.0475(6) 0.7437(4) 0.035(2) Uani 1 1 d .
H22E H 0.5832 -0.0425 0.7734 0.042 Uiso 1 1 calc R
C22E C 0.7291(8) -0.0832(6) 0.7475(4) 0.035(2) Uani 1 1 d .
H21E H 0.7350 -0.1030 0.7796 0.042 Uiso 1 1 calc R
C23E C 0.8150(7) -0.0912(5) 0.7039(4) 0.0307(19) Uani 1 1 d .
H23E H 0.8770 -0.1170 0.7067 0.037 Uiso 1 1 calc R
C24E C 0.8079(7) -0.0618(5) 0.6580(4) 0.0265(18) Uani 1 1 d .
H24E H 0.8660 -0.0668 0.6295 0.032 Uiso 1 1 calc R
C25E C 0.7159(6) -0.0239(5) 0.6522(4) 0.0209(16) Uani 1 1 d .
O11F O 0.9952(5) 0.1870(4) 0.4901(3) 0.0417(16) Uani 1 1 d .
O12F O 0.8160(5) 0.1240(3) 0.4430(3) 0.0274(13) Uani 1 1 d .
C11F C 0.8987(7) 0.1850(5) 0.4657(3) 0.0251(18) Uani 1 1 d .
C12F C 0.8830(7) 0.2669(5) 0.4651(4) 0.0243(17) Uani 1 1 d .
C13F C 0.7978(7) 0.3054(5) 0.4985(4) 0.0260(18) Uani 1 1 d .
C14F C 0.7213(8) 0.2689(5) 0.5326(4) 0.0307(19) Uani 1 1 d .
H14F H 0.7256 0.2160 0.5318 0.037 Uiso 1 1 calc R
C15F C 0.6419(8) 0.3084(6) 0.5667(4) 0.033(2) Uani 1 1 d .
H15F H 0.5935 0.2840 0.5905 0.040 Uiso 1 1 calc R
C16F C 0.6316(8) 0.3865(6) 0.5666(4) 0.038(2) Uani 1 1 d .
H16F H 0.5743 0.4129 0.5892 0.045 Uiso 1 1 calc R
C17F C 0.7024(8) 0.4231(5) 0.5347(4) 0.035(2) Uani 1 1 d .
H17F H 0.6963 0.4757 0.5359 0.042 Uiso 1 1 calc R
C18F C 0.7870(8) 0.3828(5) 0.4990(4) 0.031(2) Uani 1 1 d .
C19F C 0.8636(8) 0.4217(5) 0.4666(4) 0.033(2) Uani 1 1 d .
H19F H 0.8582 0.4746 0.4682 0.039 Uiso 1 1 calc R
C20F C 0.9454(8) 0.3838(5) 0.4328(4) 0.032(2) Uani 1 1 d .
C21F C 1.0220(8) 0.4224(6) 0.3990(4) 0.038(2) Uani 1 1 d .
H21F H 1.0143 0.4739 0.3985 0.045 Uiso 1 1 calc R
C22F C 1.1056(9) 0.3854(7) 0.3675(5) 0.049(3) Uani 1 1 d .
H22F H 1.1567 0.4122 0.3460 0.058 Uiso 1 1 calc R
C23F C 1.1176(9) 0.3082(7) 0.3662(4) 0.043(2) Uani 1 1 d .
H23F H 1.1758 0.2832 0.3434 0.052 Uiso 1 1 calc R
C24F C 1.0468(8) 0.2689(6) 0.3974(4) 0.034(2) Uani 1 1 d .
H24F H 1.0564 0.2170 0.3964 0.041 Uiso 1 1 calc R
C25F C 0.9583(7) 0.3051(5) 0.4315(4) 0.0258(18) Uani 1 1 d .
Ag5 Ag 0.60873(6) 0.31834(4) 0.09975(3) 0.03708(19) Uani 1 1 d .
C1A C 0.7978(8) 0.2596(6) 0.1517(4) 0.039(2) Uani 1 1 d .
H1A H 0.7789 0.2088 0.1176 0.047 Uiso 1 1 calc R
N1A N 0.7505(7) 0.3223(5) 0.1588(4) 0.0402(19) Uani 1 1 d .
C2A C 0.8019(10) 0.3833(7) 0.2143(5) 0.049(3) Uani 1 1 d .
H2A H 0.7848 0.4362 0.2323 0.059 Uiso 1 1 calc R
C3A C 0.8800(9) 0.3542(6) 0.2382(5) 0.048(3) Uani 1 1 d .
H3A H 0.9282 0.3831 0.2755 0.058 Uiso 1 1 calc R
N2A N 0.8768(7) 0.2763(5) 0.1989(4) 0.0388(19) Uani 1 1 d .
C4A C 0.9496(10) 0.2217(7) 0.2063(6) 0.054(3) Uani 1 1 d .
H4A1 H 0.9304 0.2097 0.2432 0.082 Uiso 1 1 calc R
H4A2 H 1.0323 0.2489 0.2105 0.082 Uiso 1 1 calc R
H4A3 H 0.9344 0.1703 0.1702 0.082 Uiso 1 1 calc R
C1B C 0.3948(8) 0.2747(6) 0.0075(5) 0.037(2) Uani 1 1 d .
H1B H 0.3823 0.2188 0.0033 0.044 Uiso 1 1 calc R
N1B N 0.4770(7) 0.3352(5) 0.0463(4) 0.041(2) Uani 1 1 d .
C2B C 0.4635(10) 0.4037(7) 0.0353(6) 0.053(3) Uani 1 1 d .
H2B H 0.5101 0.4574 0.0556 0.064 Uiso 1 1 calc R
C3B C 0.3767(11) 0.3846(7) -0.0075(6) 0.057(3) Uani 1 1 d .
H3B H 0.3505 0.4208 -0.0230 0.068 Uiso 1 1 calc R
N2B N 0.3332(7) 0.3024(5) -0.0244(4) 0.0387(19) Uani 1 1 d .
C4B C 0.2341(11) 0.2533(8) -0.0697(5) 0.059(3) Uani 1 1 d .
H4B1 H 0.2389 0.1954 -0.0853 0.088 Uiso 1 1 calc R
H4B2 H 0.2364 0.2726 -0.1039 0.088 Uiso 1 1 calc R
H4B3 H 0.1608 0.2592 -0.0503 0.088 Uiso 1 1 calc R
Ag6 Ag 1.09942(6) 0.32242(4) 0.59376(4) 0.03891(19) Uani 1 1 d .
C1C C 1.2814(8) 0.2673(6) 0.5023(5) 0.039(2) Uani 1 1 d .
H1C H 1.2541 0.2130 0.5011 0.047 Uiso 1 1 calc R
N1C N 1.2409(7) 0.3313(5) 0.5380(4) 0.0386(19) Uani 1 1 d .
C2C C 1.3027(8) 0.3968(6) 0.5251(5) 0.039(2) Uani 1 1 d .
H2C H 1.2929 0.4517 0.5429 0.047 Uiso 1 1 calc R
C3C C 1.3782(9) 0.3710(6) 0.4836(5) 0.046(3) Uani 1 1 d .
H3C H 1.4317 0.4040 0.4674 0.055 Uiso 1 1 calc R
N2C N 1.3638(7) 0.2871(5) 0.4687(4) 0.0362(18) Uani 1 1 d .
C4C C 1.4284(10) 0.2346(7) 0.4259(5) 0.052(3) Uani 1 1 d .
H4C1 H 1.3943 0.2195 0.3840 0.079 Uiso 1 1 calc R
H4C2 H 1.4248 0.1849 0.4348 0.079 Uiso 1 1 calc R
H4C3 H 1.5101 0.2638 0.4298 0.079 Uiso 1 1 calc R
C1D C 0.8802(8) 0.2718(6) 0.6524(4) 0.035(2) Uani 1 1 d .
H2D H 0.8699 0.2181 0.6219 0.042 Uiso 1 1 calc R
N1D N 0.9635(7) 0.3337(5) 0.6547(4) 0.0405(19) Uani 1 1 d .
C2D C 0.9479(11) 0.4001(6) 0.7042(6) 0.063(3) Uani 1 1 d .
H2X H 0.9946 0.4543 0.7168 0.075 Uiso 1 1 calc R
C3D C 0.8542(10) 0.3753(6) 0.7320(5) 0.054(3) Uani 1 1 d .
H3D H 0.8244 0.4084 0.7678 0.064 Uiso 1 1 calc R
N2D N 0.8104(7) 0.2933(5) 0.6984(4) 0.0382(18) Uani 1 1 d .
C4D C 0.7056(9) 0.2425(7) 0.7097(6) 0.053(3) Uani 1 1 d .
H4D1 H 0.7048 0.1844 0.6868 0.079 Uiso 1 1 calc R
H4D2 H 0.6361 0.2561 0.6961 0.079 Uiso 1 1 calc R
H4D3 H 0.7056 0.2529 0.7537 0.079 Uiso 1 1 calc R
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O12C Ag1 O11C 156.3(2) 2_655 .
O12C Ag1 O11A 100.7(2) 2_655 .
O11C Ag1 O11A 103.0(2) . .
O12C Ag1 O11B 93.4(2) 2_655 .
O11C Ag1 O11B 87.79(19) . .
O11A Ag1 O11B 88.2(2) . .
O12C Ag1 Ag1 81.46(15) 2_655 2_655
O11C Ag1 Ag1 81.76(15) . 2_655
O11A Ag1 Ag1 134.15(16) . 2_655
O11B Ag1 Ag1 137.61(14) . 2_655
O12C Ag1 Ag2 93.83(16) 2_655 2_655
O11C Ag1 Ag2 63.59(16) . 2_655
O11A Ag1 Ag2 158.83(15) . 2_655
O11B Ag1 Ag2 75.51(13) . 2_655
Ag1 Ag1 Ag2 63.02(2) 2_655 2_655
O12C Ag1 Ag2 78.27(16) 2_655 .
O11C Ag1 Ag2 107.78(15) . .
O11A Ag1 Ag2 74.14(15) . .
O11B Ag1 Ag2 158.52(13) . .
Ag1 Ag1 Ag2 61.36(2) 2_655 .
Ag2 Ag1 Ag2 124.37(2) 2_655 .
O12B Ag2 O12A 140.4(2) 2_655 .
O12B Ag2 Ag1 80.25(14) 2_655 2_655
O12A Ag2 Ag1 136.02(15) . 2_655
O12B Ag2 Ag1 124.89(14) 2_655 .
O12A Ag2 Ag1 81.74(14) . .
Ag1 Ag2 Ag1 55.63(2) 2_655 .
C11A O11A Ag1 124.0(5) . .
C11A O11A Ag5 118.4(5) . .
Ag1 O11A Ag5 97.8(2) . .
C11A O12A Ag2 120.0(5) . .
O11A C11A O12A 127.3(7) . .
O11A C11A C12A 115.9(7) . .
O12A C11A C12A 116.7(7) . .
C13A C12A C25A 121.4(7) . .
C13A C12A C11A 119.8(7) . .
C25A C12A C11A 118.8(7) . .
C12A C13A C14A 122.9(7) . .
C12A C13A C18A 118.7(8) . .
C14A C13A C18A 118.4(8) . .
C15A C14A C13A 121.7(8) . .
C14A C15A C16A 119.5(9) . .
C17A C16A C15A 121.8(9) . .
C16A C17A C18A 119.7(9) . .
C19A C18A C13A 120.4(8) . .
C19A C18A C17A 120.8(8) . .
C13A C18A C17A 118.8(8) . .
C18A C19A C20A 121.5(8) . .
C19A C20A C25A 119.9(8) . .
C19A C20A C21A 121.8(8) . .
C25A C20A C21A 118.3(8) . .
C22A C21A C20A 121.4(9) . .
C21A C22A C23A 121.1(9) . .
C24A C23A C22A 120.3(9) . .
C23A C24A C25A 121.2(8) . .
C12A C25A C24A 124.1(8) . .
C12A C25A C20A 118.1(8) . .
C24A C25A C20A 117.7(8) . .
C11B O11B Ag1 114.8(5) . .
C11B O11B Ag5 133.7(5) . .
Ag1 O11B Ag5 98.20(19) . .
C11B O12B Ag2 124.0(5) . 2_655
O12B C11B O11B 125.3(7) . .
O12B C11B C12B 116.3(7) . .
O11B C11B C12B 118.5(7) . .
C13B C12B C25B 120.6(7) . .
C13B C12B C11B 119.7(7) . .
C25B C12B C11B 119.7(7) . .
C12B C13B C18B 120.3(7) . .
C12B C13B C14B 122.0(7) . .
C18B C13B C14B 117.7(7) . .
C15B C14B C13B 120.2(7) . .
C14B C15B C16B 121.6(8) . .
C17B C16B C15B 119.9(8) . .
C16B C17B C18B 120.6(8) . .
C19B C18B C17B 121.3(8) . .
C19B C18B C13B 118.7(8) . .
C17B C18B C13B 120.0(8) . .
C20B C19B C18B 122.2(8) . .
C19B C20B C21B 121.7(8) . .
C19B C20B C25B 119.7(7) . .
C21B C20B C25B 118.6(8) . .
C22B C21B C20B 121.9(8) . .
C21B C22B C23B 119.1(8) . .
C24B C23B C22B 121.2(9) . .
C23B C24B C25B 121.6(8) . .
C24B C25B C12B 124.2(7) . .
C24B C25B C20B 117.5(7) . .
C12B C25B C20B 118.4(7) . .
C11C O11C Ag1 119.4(5) . .
C11C O12C Ag1 123.0(5) . 2_655
O11C C11C O12C 126.6(7) . .
O11C C11C C12C 117.7(7) . .
O12C C11C C12C 115.6(7) . .
C13C C12C C25C 122.1(7) . .
C13C C12C C11C 119.0(7) . .
C25C C12C C11C 118.9(7) . .
C12C C13C C14C 122.9(7) . .
C12C C13C C18C 118.8(7) . .
C14C C13C C18C 118.3(7) . .
C15C C14C C13C 120.9(7) . .
C14C C15C C16C 121.6(8) . .
C17C C16C C15C 118.8(8) . .
C16C C17C C18C 122.1(8) . .
C19C C18C C17C 121.5(7) . .
C19C C18C C13C 120.2(7) . .
C17C C18C C13C 118.3(7) . .
C20C C19C C18C 120.8(7) . .
C19C C20C C21C 121.9(7) . .
C19C C20C C25C 120.5(7) . .
C21C C20C C25C 117.6(7) . .
C22C C21C C20C 121.0(8) . .
C21C C22C C23C 120.9(8) . .
C24C C23C C22C 119.9(8) . .
C23C C24C C25C 121.3(7) . .
C24C C25C C12C 123.2(7) . .
C24C C25C C20C 119.4(7) . .
C12C C25C C20C 117.3(7) . .
O11E Ag3 O12E 158.7(2) . 2_756
O11E Ag3 O11F 99.5(2) . .
O12E Ag3 O11F 101.7(2) 2_756 .
O11E Ag3 O11D 94.7(2) . .
O12E Ag3 O11D 88.4(2) 2_756 .
O11F Ag3 O11D 86.8(2) . .
O11E Ag3 Ag3 81.64(16) . 2_756
O12E Ag3 Ag3 81.96(15) 2_756 2_756
O11F Ag3 Ag3 135.33(17) . 2_756
O11D Ag3 Ag3 137.87(13) . 2_756
O11E Ag3 Ag4 92.74(18) . 2_756
O12E Ag3 Ag4 67.54(18) 2_756 2_756
O11F Ag3 Ag4 159.45(16) . 2_756
O11D Ag3 Ag4 75.78(13) . 2_756
Ag3 Ag3 Ag4 62.59(2) 2_756 2_756
O11E Ag3 Ag4 79.45(18) . .
O12E Ag3 Ag4 104.29(17) 2_756 .
O11F Ag3 Ag4 74.89(16) . .
O11D Ag3 Ag4 159.39(13) . .
Ag3 Ag3 Ag4 61.33(2) 2_756 .
Ag4 Ag3 Ag4 123.92(2) 2_756 .
O12D Ag4 O12F 140.9(2) 2_756 .
O12D Ag4 Ag3 80.22(14) 2_756 2_756
O12F Ag4 Ag3 136.96(15) . 2_756
O12D Ag4 Ag3 126.81(14) 2_756 .
O12F Ag4 Ag3 82.41(14) . .
Ag3 Ag4 Ag3 56.08(2) 2_756 .
C11D O11D Ag3 115.0(5) . .
C11D O11D Ag6 127.2(5) . .
Ag3 O11D Ag6 100.93(18) . .
C11D O12D Ag4 124.2(5) . 2_756
O11D C11D O12D 125.7(7) . .
O11D C11D C12D 118.1(7) . .
O12D C11D C12D 116.2(6) . .
C25D C12D C13D 120.8(7) . .
C25D C12D C11D 119.2(7) . .
C13D C12D C11D 120.0(7) . .
C12D C13D C18D 119.3(7) . .
C12D C13D C14D 123.5(7) . .
C18D C13D C14D 117.1(7) . .
C15D C14D C13D 121.5(8) . .
C14D C15D C16D 121.1(9) . .
C17D C16D C15D 119.4(9) . .
C16D C17D C18D 120.9(8) . .
C19D C18D C17D 121.3(8) . .
C19D C18D C13D 118.6(8) . .
C17D C18D C13D 120.0(8) . .
C20D C19D C18D 122.7(8) . .
C19D C20D C25D 119.0(7) . .
C19D C20D C21D 121.3(8) . .
C25D C20D C21D 119.6(8) . .
C22D C21D C20D 119.8(8) . .
C21D C22D C23D 121.9(8) . .
C24D C23D C22D 119.8(8) . .
C23D C24D C25D 121.2(8) . .
C12D C25D C20D 119.4(7) . .
C12D C25D C24D 123.0(7) . .
C20D C25D C24D 117.6(7) . .
C11E O11E Ag3 123.7(5) . .
C11E O12E Ag3 121.2(5) . 2_756
O12E C11E O11E 126.1(7) . .
O12E C11E C12E 117.7(7) . .
O11E C11E C12E 116.2(7) . .
C13E C12E C25E 122.0(7) . .
C13E C12E C11E 120.5(7) . .
C25E C12E C11E 117.4(7) . .
C12E C13E C18E 118.8(7) . .
C12E C13E C14E 122.1(7) . .
C18E C13E C14E 119.2(7) . .
C15E C14E C13E 120.3(7) . .
C14E C15E C16E 120.6(8) . .
C17E C16E C15E 120.7(8) . .
C16E C17E C18E 120.0(8) . .
C19E C18E C13E 119.8(7) . .
C19E C18E C17E 121.1(8) . .
C13E C18E C17E 119.1(8) . .
C18E C19E C20E 122.6(8) . .
C19E C20E C21E 123.2(8) . .
C19E C20E C25E 118.1(7) . .
C21E C20E C25E 118.7(8) . .
C22E C21E C20E 121.0(8) . .
C21E C22E C23E 120.9(8) . .
C24E C23E C22E 119.8(8) . .
C23E C24E C25E 121.5(8) . .
C12E C25E C24E 123.2(7) . .
C12E C25E C20E 118.7(7) . .
C24E C25E C20E 118.0(7) . .
C11F O11F Ag3 124.1(6) . .
C11F O11F Ag6 120.1(5) . .
Ag3 O11F Ag6 97.6(2) . .
C11F O12F Ag4 120.6(5) . .
O12F C11F O11F 127.2(8) . .
O12F C11F C12F 117.9(7) . .
O11F C11F C12F 114.9(7) . .
C13F C12F C25F 120.5(7) . .
C13F C12F C11F 120.7(7) . .
C25F C12F C11F 118.8(7) . .
C12F C13F C18F 119.9(8) . .
C12F C13F C14F 121.8(7) . .
C18F C13F C14F 118.3(8) . .
C15F C14F C13F 121.1(8) . .
C14F C15F C16F 120.0(8) . .
C17F C16F C15F 120.6(8) . .
C16F C17F C18F 120.2(8) . .
C13F C18F C19F 119.7(8) . .
C13F C18F C17F 119.8(8) . .
C19F C18F C17F 120.5(8) . .
C20F C19F C18F 120.8(8) . .
C19F C20F C21F 121.1(8) . .
C19F C20F C25F 120.6(8) . .
C21F C20F C25F 118.3(8) . .
C22F C21F C20F 120.4(9) . .
C21F C22F C23F 121.0(9) . .
C24F C23F C22F 120.9(10) . .
C23F C24F C25F 120.4(9) . .
C12F C25F C24F 122.6(8) . .
C12F C25F C20F 118.4(8) . .
C24F C25F C20F 119.0(8) . .
N1B Ag5 N1A 170.8(3) . .
N1B Ag5 O11B 90.4(2) . .
N1A Ag5 O11B 96.1(2) . .
N1B Ag5 O11A 100.9(3) . .
N1A Ag5 O11A 87.1(3) . .
O11B Ag5 O11A 75.53(17) . .
N1A C1A N2A 111.3(9) . .
C1A N1A C2A 105.8(9) . .
C1A N1A Ag5 123.7(7) . .
C2A N1A Ag5 130.0(7) . .
C3A C2A N1A 108.4(10) . .
C2A C3A N2A 107.3(9) . .
C1A N2A C3A 107.2(8) . .
C1A N2A C4A 127.0(9) . .
C3A N2A C4A 125.8(9) . .
N2B C1B N1B 111.4(9) . .
C1B N1B C2B 103.5(9) . .
C1B N1B Ag5 124.9(6) . .
C2B N1B Ag5 131.0(8) . .
C3B C2B N1B 111.1(10) . .
C2B C3B N2B 105.7(9) . .
C1B N2B C3B 108.2(9) . .
C1B N2B C4B 126.0(9) . .
C3B N2B C4B 125.8(9) . .
N1C Ag6 N1D 171.2(3) . .
N1C Ag6 O11D 91.8(2) . .
N1D Ag6 O11D 95.4(2) . .
N1C Ag6 O11F 84.1(3) . .
N1D Ag6 O11F 102.8(3) . .
O11D Ag6 O11F 73.58(17) . .
N2C C1C N1C 113.0(8) . .
C1C N1C C2C 104.4(8) . .
C1C N1C Ag6 123.9(6) . .
C2C N1C Ag6 131.4(7) . .
C3C C2C N1C 109.7(9) . .
C2C C3C N2C 107.1(9) . .
C1C N2C C3C 105.8(8) . .
C1C N2C C4C 128.5(8) . .
C3C N2C C4C 125.7(9) . .
N1D C1D N2D 111.8(8) . .
C1D N1D C2D 106.7(9) . .
C1D N1D Ag6 123.1(6) . .
C2D N1D Ag6 130.0(8) . .
C3D C2D N1D 108.3(10) . .
C2D C3D N2D 107.2(9) . .
C1D N2D C3D 106.0(8) . .
C1D N2D C4D 128.0(9) . .
C3D N2D C4D 125.9(9) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ag1 O12C 2.246(5) 2_655
Ag1 O11C 2.272(5) .
Ag1 O11A 2.316(6) .
Ag1 O11B 2.384(5) .
Ag1 Ag1 2.7860(12) 2_655
Ag1 Ag2 2.9623(9) 2_655
Ag1 Ag2 3.0079(9) .
Ag2 O12B 2.188(5) 2_655
Ag2 O12A 2.193(5) .
Ag2 Ag1 2.9623(9) 2_655
O11A C11A 1.242(10) .
O11A Ag5 2.708(6) .
O12A C11A 1.255(10) .
C11A C12A 1.528(11) .
C12A C13A 1.413(12) .
C12A C25A 1.415(12) .
C13A C14A 1.413(12) .
C13A C18A 1.421(11) .
C14A C15A 1.364(13) .
C15A C16A 1.404(14) .
C16A C17A 1.350(14) .
C17A C18A 1.442(13) .
C18A C19A 1.388(12) .
C19A C20A 1.388(13) .
C20A C25A 1.441(12) .
C20A C21A 1.441(13) .
C21A C22A 1.333(14) .
C22A C23A 1.395(14) .
C23A C24A 1.383(13) .
C24A C25A 1.415(12) .
O11B C11B 1.262(10) .
O11B Ag5 2.632(6) .
O12B C11B 1.256(10) .
O12B Ag2 2.188(5) 2_655
C11B C12B 1.511(11) .
C12B C13B 1.407(11) .
C12B C25B 1.417(11) .
C13B C18B 1.425(11) .
C13B C14B 1.436(11) .
C14B C15B 1.364(11) .
C15B C16B 1.409(13) .
C16B C17B 1.362(13) .
C17B C18B 1.417(12) .
C18B C19B 1.395(12) .
C19B C20B 1.388(12) .
C20B C21B 1.426(12) .
C20B C25B 1.444(11) .
C21B C22B 1.344(13) .
C22B C23B 1.427(14) .
C23B C24B 1.349(12) .
C24B C25B 1.415(11) .
O11C C11C 1.242(9) .
O12C C11C 1.248(9) .
O12C Ag1 2.246(5) 2_655
C11C C12C 1.508(10) .
C12C C13C 1.387(11) .
C12C C25C 1.416(11) .
C13C C14C 1.432(11) .
C13C C18C 1.440(11) .
C14C C15C 1.361(12) .
C15C C16C 1.423(12) .
C16C C17C 1.369(13) .
C17C C18C 1.431(12) .
C18C C19C 1.389(12) .
C19C C20C 1.385(12) .
C20C C21C 1.434(11) .
C20C C25C 1.452(11) .
C21C C22C 1.369(12) .
C22C C23C 1.423(12) .
C23C C24C 1.372(11) .
C24C C25C 1.409(12) .
Ag3 O11E 2.222(6) .
Ag3 O12E 2.248(6) 2_756
Ag3 O11F 2.319(6) .
Ag3 O11D 2.389(5) .
Ag3 Ag3 2.7889(12) 2_756
Ag3 Ag4 2.9489(9) 2_756
Ag3 Ag4 2.9838(9) .
Ag4 O12D 2.183(5) 2_756
Ag4 O12F 2.185(5) .
Ag4 Ag3 2.9488(9) 2_756
O11D C11D 1.241(9) .
O11D Ag6 2.607(5) .
O12D C11D 1.257(9) .
O12D Ag4 2.183(5) 2_756
C11D C12D 1.517(10) .
C12D C25D 1.408(11) .
C12D C13D 1.409(11) .
C13D C18D 1.435(11) .
C13D C14D 1.442(11) .
C14D C15D 1.345(12) .
C15D C16D 1.433(13) .
C16D C17D 1.369(14) .
C17D C18D 1.414(12) .
C18D C19D 1.394(12) .
C19D C20D 1.386(12) .
C20D C25D 1.430(11) .
C20D C21D 1.431(12) .
C21D C22D 1.353(13) .
C22D C23D 1.411(12) .
C23D C24D 1.363(11) .
C24D C25D 1.440(11) .
O11E C11E 1.259(9) .
O12E C11E 1.225(10) .
O12E Ag3 2.248(6) 2_756
C11E C12E 1.507(10) .
C12E C13E 1.404(11) .
C12E C25E 1.413(11) .
C13E C18E 1.426(11) .
C13E C14E 1.441(11) .
C14E C15E 1.368(11) .
C15E C16E 1.418(12) .
C16E C17E 1.387(13) .
C17E C18E 1.429(12) .
C18E C19E 1.394(12) .
C19E C20E 1.399(12) .
C20E C21E 1.418(12) .
C20E C25E 1.457(11) .
C21E C22E 1.357(13) .
C22E C23E 1.427(13) .
C23E C24E 1.369(12) .
C24E C25E 1.416(11) .
O11F C11F 1.254(10) .
O11F Ag6 2.788(7) .
O12F C11F 1.250(10) .
C11F C12F 1.521(11) .
C12F C13F 1.406(12) .
C12F C25F 1.419(12) .
C13F C18F 1.411(11) .
C13F C14F 1.422(12) .
C14F C15F 1.366(12) .
C15F C16F 1.429(13) .
C16F C17F 1.348(13) .
C17F C18F 1.436(13) .
C18F C19F 1.417(13) .
C19F C20F 1.372(13) .
C20F C21F 1.437(13) .
C20F C25F 1.438(12) .
C21F C22F 1.361(15) .
C22F C23F 1.408(15) .
C23F C24F 1.365(13) .
C24F C25F 1.426(12) .
Ag5 N1B 2.124(9) .
Ag5 N1A 2.136(8) .
C1A N1A 1.309(13) .
C1A N2A 1.349(12) .
N1A C2A 1.394(13) .
C2A C3A 1.351(15) .
C3A N2A 1.356(13) .
N2A C4A 1.474(13) .
C1B N2B 1.319(12) .
C1B N1B 1.337(13) .
N1B C2B 1.380(13) .
C2B C3B 1.327(17) .
C3B N2B 1.362(14) .
N2B C4B 1.468(14) .
Ag6 N1C 2.131(8) .
Ag6 N1D 2.134(8) .
C1C N2C 1.323(12) .
C1C N1C 1.326(12) .
N1C C2C 1.382(12) .
C2C C3C 1.336(14) .
C3C N2C 1.387(12) .
N2C C4C 1.437(13) .
C1D N1D 1.304(12) .
C1D N2D 1.346(12) .
N1D C2D 1.370(13) .
C2D C3D 1.360(17) .
C3D N2D 1.374(13) .
N2D C4D 1.459(13) .
