#------------------------------------------------------------------------------
#$Date: 2016-03-25 14:24:27 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179894 $
#$URL: svn://www.crystallography.net/cod/cif/7/01/90/7019092.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7019092
loop_
_publ_author_name
'Zhu, Yan'
'Luo, Feng'
'Song, Yu-Mei'
'Huang, Hai-Xiao'
'Sun, Gong-Ming'
'Tian, Xiao-Zhao'
'Yuan, Zi-Zun'
'Liao, Zhen-Wei'
'Luo, Ming-Biao'
'Liu, Shu-Juan'
'Xu, Wen-Yuan'
'Feng, Xue-Feng'
_publ_section_title
;
 A series of 1D Dy(iii) compound showing slow magnetic relaxation:
 synthesis, structure, and magnetic studies.
;
_journal_issue                   22
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              6749
_journal_page_last               6755
_journal_paper_doi               10.1039/c2dt12313d
_journal_volume                  41
_journal_year                    2012
_chemical_formula_sum            'C130 H56 Dy4 Fe N18 O58'
_chemical_formula_weight         3503.78
_chemical_name_systematic
;
?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                86.2430(10)
_cell_angle_beta                 81.2920(10)
_cell_angle_gamma                86.1710(10)
_cell_formula_units_Z            1
_cell_length_a                   10.1915(2)
_cell_length_b                   18.7208(3)
_cell_length_c                   20.7128(4)
_cell_measurement_reflns_used    9904
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      25.43
_cell_measurement_theta_min      2.24
_cell_volume                     3891.43(12)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0409
_diffrn_reflns_av_sigmaI/netI    0.0421
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       22
_diffrn_reflns_limit_k_min       -22
_diffrn_reflns_limit_l_max       24
_diffrn_reflns_limit_l_min       -24
_diffrn_reflns_number            56992
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         1.00
_exptl_absorpt_coefficient_mu    2.078
_exptl_absorpt_correction_T_max  0.8191
_exptl_absorpt_correction_T_min  0.6813
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            Red
_exptl_crystal_density_diffrn    1.495
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Block
_exptl_crystal_F_000             1716
_exptl_crystal_size_max          0.20
_exptl_crystal_size_mid          0.15
_exptl_crystal_size_min          0.10
_platon_squeeze_details
;
;
_refine_diff_density_max         1.701
_refine_diff_density_min         -1.386
_refine_diff_density_rms         0.153
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.078
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1025
_refine_ls_number_reflns         13671
_refine_ls_number_restraints     121
_refine_ls_restrained_S_all      229.663
_refine_ls_R_factor_all          0.0761
_refine_ls_R_factor_gt           0.0591
_refine_ls_shift/su_max          0.006
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1394P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1883
_refine_ls_wR_factor_ref         0.2022
_reflns_number_gt                9645
_reflns_number_total             13671
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c2dt12313d.txt
_cod_data_source_block           3
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.1 from
2010-06-29.

'_exptl_absorpt_correction_type' value 'Multi-scan'
changed to 'multi-scan' according to
/home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 
;
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7019092
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
C1 C 0.590(14) 0.726(7) 0.621(8) 0.06(5) Uani 1 1 d . . .
C2 C 0.553(14) 0.806(7) 0.615(7) 0.05(5) Uani 1 1 d . . .
C3 C 0.638(15) 0.855(7) 0.629(8) 0.06(5) Uani 1 1 d . . .
H3 H 0.7160 0.8400 0.6451 0.076 Uiso 1 1 calc R . .
C4 C 0.607(16) 0.926(8) 0.618(9) 0.07(6) Uani 1 1 d D . .
H4 H 0.6657 0.9593 0.6261 0.090 Uiso 1 1 calc R . .
C5 C 0.494(15) 0.950(7) 0.597(8) 0.06(5) Uani 1 1 d . . .
C6 C 0.405(15) 0.903(7) 0.582(8) 0.06(5) Uani 1 1 d . . .
H6 H 0.3280 0.9191 0.5654 0.077 Uiso 1 1 calc R . .
C7 C 0.436(15) 0.831(7) 0.592(8) 0.06(5) Uani 1 1 d . . .
H7 H 0.3779 0.7980 0.5832 0.073 Uiso 1 1 calc R . .
C8 C 0.029(19) 0.740(9) 0.705(8) 0.08(6) Uani 1 1 d D . .
C9 C 0.116(18) 0.800(8) 0.723(8) 0.07(6) Uani 1 1 d . . .
C10 C 0.22(2) 0.779(11) 0.754(10) 0.10(8) Uani 1 1 d . . .
H10 H 0.2368 0.7316 0.7675 0.121 Uiso 1 1 calc R . .
C11 C 0.31(3) 0.833(12) 0.765(10) 0.14(10) Uani 1 1 d . . .
H11 H 0.3853 0.8220 0.7831 0.164 Uiso 1 1 calc R . .
C12 C 0.16(2) 0.922(10) 0.717(9) 0.11(8) Uani 1 1 d . . .
H12 H 0.1441 0.9698 0.7035 0.126 Uiso 1 1 calc R . .
C13 C 0.09(2) 0.870(9) 0.704(9) 0.09(7) Uani 1 1 d . . .
H13 H 0.0160 0.8815 0.6829 0.108 Uiso 1 1 calc R . .
C14 C 0.112(14) 0.704(7) 0.550(7) 0.05(4) Uani 1 1 d . . .
C15 C 0.086(13) 0.776(6) 0.515(6) 0.04(4) Uani 1 1 d . . .
C16 C 0.188(14) 0.809(7) 0.475(7) 0.06(5) Uani 1 1 d . . .
H16 H 0.2733 0.7870 0.4705 0.071 Uiso 1 1 calc R . .
C17 C 0.165(16) 0.873(8) 0.441(8) 0.07(5) Uani 1 1 d . . .
H17 H 0.2339 0.8948 0.4143 0.080 Uiso 1 1 calc R . .
C18 C 0.039(15) 0.903(7) 0.449(7) 0.06(5) Uani 1 1 d . . .
C19 C -0.067(15) 0.872(7) 0.489(8) 0.06(5) Uani 1 1 d . . .
H19 H -0.1518 0.8944 0.4936 0.077 Uiso 1 1 calc R . .
C20 C -0.041(13) 0.807(6) 0.521(7) 0.05(4) Uani 1 1 d . . .
H20 H -0.1102 0.7839 0.5474 0.062 Uiso 1 1 calc R . .
C21 C 0.038(15) 0.478(7) 0.709(7) 0.06(5) Uani 1 1 d . . .
C22 C -0.030(15) 0.420(7) 0.751(7) 0.06(5) Uani 1 1 d . . .
C23 C -0.167(18) 0.420(9) 0.763(10) 0.09(7) Uani 1 1 d . . .
H23 H -0.2176 0.4572 0.7445 0.108 Uiso 1 1 calc R . .
C24 C -0.230(19) 0.366(9) 0.803(10) 0.10(7) Uani 1 1 d . . .
H24 H -0.3222 0.3682 0.8137 0.123 Uiso 1 1 calc R . .
C25 C -0.154(19) 0.310(9) 0.825(9) 0.09(7) Uani 1 1 d . . .
C26 C -0.02(2) 0.306(9) 0.812(10) 0.10(8) Uani 1 1 d . . .
H26 H 0.0273 0.2668 0.8286 0.120 Uiso 1 1 calc R . .
C27 C 0.044(18) 0.362(8) 0.774(8) 0.08(6) Uani 1 1 d . . .
H27 H 0.1358 0.3596 0.7644 0.093 Uiso 1 1 calc R . .
C28 C 0.616(14) 0.676(7) 0.472(7) 0.05(5) Uani 1 1 d . . .
C29 C 0.718(14) 0.713(7) 0.426(7) 0.05(4) Uani 1 1 d . . .
C30 C 0.682(16) 0.779(7) 0.397(8) 0.07(5) Uani 1 1 d . . .
H30 H 0.5955 0.7982 0.4065 0.079 Uiso 1 1 calc R . .
C31 C 0.776(18) 0.816(8) 0.355(9) 0.08(6) Uani 1 1 d . . .
H31 H 0.7529 0.8601 0.3352 0.101 Uiso 1 1 calc R . .
C32 C 0.901(17) 0.787(8) 0.343(8) 0.07(5) Uani 1 1 d . . .
C33 C 0.941(16) 0.721(8) 0.371(8) 0.07(6) Uani 1 1 d . . .
H33 H 1.0279 0.7022 0.3614 0.085 Uiso 1 1 calc R . .
C34 C 0.849(14) 0.685(8) 0.413(7) 0.06(5) Uani 1 1 d . . .
H34 H 0.8737 0.6419 0.4337 0.070 Uiso 1 1 calc R . .
C35 C 0.440(13) 0.549(6) 0.404(7) 0.05(4) Uani 1 1 d . . .
C36 C 0.457(15) 0.605(7) 0.349(8) 0.06(5) Uani 1 1 d . . .
C37 C 0.39(2) 0.672(8) 0.357(9) 0.09(7) Uani 1 1 d . . .
H37 H 0.3248 0.6804 0.3925 0.111 Uiso 1 1 calc R . .
C38 C 0.42(2) 0.727(12) 0.307(11) 0.12(10) Uani 1 1 d . . .
H38 H 0.3846 0.7727 0.3102 0.141 Uiso 1 1 calc R . .
C39 C 0.512(7) 0.7113(14) 0.255(2) 0.12(10) Uani 1 1 d D . .
C40 C 0.57(3) 0.648(13) 0.246(13) 0.13(11) Uani 1 1 d . . .
H40 H 0.6285 0.6396 0.2074 0.156 Uiso 1 1 calc R . .
C41 C 0.542(18) 0.593(11) 0.293(8) 0.09(7) Uani 1 1 d . . .
H41 H 0.5817 0.5470 0.2871 0.114 Uiso 1 1 calc R . .
C43 C 0.3812(19) 0.0559(6) 0.1173(8) 0.07(12) Uani 0.48(9) 1 d PD A 1
C44 C 0.2913(18) 0.0672(6) 0.1740(8) 0.10(17) Uani 0.48(9) 1 d PD A 1
C45 C 0.1933(14) 0.0179(7) 0.1931(7) 0.2(3) Uani 1 1 d D . .
C46 C 0.221(3) -0.0529(9) 0.1752(14) 0.08(14) Uani 0.48(9) 1 d PD A 1
C47 C 0.316(3) -0.0652(8) 0.1199(10) 0.09(14) Uani 0.48(9) 1 d PD A 1
C58 C 0.6931(16) -0.1169(8) 0.054(2) 0.1(2) Uani 0.48(9) 1 d PD A 1
C59 C 0.8270(16) -0.1340(8) 0.059(2) 0.10(17) Uani 0.48(9) 1 d PD A 1
C60 C 0.9054(11) -0.0788(8) 0.0701(7) 0.19(18) Uani 1 1 d D . .
C61 C 0.8447(13) -0.0100(6) 0.0777(11) 0.1(2) Uani 0.48(9) 1 d PD A 1
C62 C 0.7315(13) 0.0085(6) 0.0485(12) 0.09(16) Uani 0.48(9) 1 d PD A 1
C63 C 0.9216(16) 0.0453(9) 0.0904(16) 0.3(3) Uani 1 1 d D . .
H63 H 1.0123 0.0374 0.0915 0.321 Uiso 1 1 calc R A 1
C64 C 0.8577(16) 0.1128(9) 0.1015(13) 0.2(2) Uani 1 1 d D A .
H64 H 0.8923 0.1449 0.1259 0.284 Uiso 1 1 calc R . .
C65 C 0.6702(12) 0.0769(6) 0.0560(11) 0.2(3) Uani 1 1 d D . .
C66 C 0.7412(12) 0.1310(6) 0.0751(11) 2(6) Uani 1 1 d D A .
C67 C 0.686(2) 0.2015(8) 0.0722(15) 0.3(3) Uani 1 1 d D . .
C68 C 0.6015(19) 0.2192(6) 0.0246(8) 0.17(15) Uani 1 1 d D A .
C69 C 0.5247(18) 0.1653(8) 0.0093(11) 0.3(3) Uani 1 1 d D . .
C70 C 0.294(3) 0.1301(9) 0.2062(9) 0.2(2) Uani 1 1 d D . .
H70 H 0.2578 0.1328 0.2500 0.245 Uiso 1 1 calc R A 1
C71 C 0.353(3) 0.1890(8) 0.1713(10) 0.3(4) Uani 1 1 d D A .
H71 H 0.3296 0.2354 0.1839 0.392 Uiso 1 1 calc R . .
C72 C 0.4413(17) 0.1148(6) 0.0829(7) 0.16(15) Uani 1 1 d D A .
C73 C 0.4498(17) 0.1761(6) 0.1169(7) 0.2(2) Uani 1 1 d D . .
C74 C 0.542(2) 0.2257(9) 0.0896(9) 0.2(2) Uani 1 1 d D A .
C75 C 0.621(3) 0.1504(9) 0.0007(10) 0.2(2) Uani 1 1 d D A .
C76 C 0.27(2) 0.905(9) 0.748(9) 0.11(8) Uani 1 1 d . . .
C43' C 0.3947(18) -0.0436(16) 0.1446(8) 0.08(13) Uani 0.52(9) 1 d PD A 2
C44' C 0.2917(19) -0.0374(13) 0.1972(8) 0.09(15) Uani 0.52(9) 1 d PD A 2
C46' C 0.1606(18) 0.0394(17) 0.1312(8) 0.2(3) Uani 0.52(9) 1 d PD A 2
C47' C 0.2488(17) 0.019(2) 0.0762(8) 0.08(13) Uani 0.52(9) 1 d PD . 2
C58' C 0.8926(16) -0.064(3) 0.0041(8) 0.2(3) Uani 0.52(9) 1 d PD A 2
C59' C 0.7707(16) -0.033(2) -0.0104(8) 0.1(2) Uani 0.52(9) 1 d PD . 2
C61' C 0.7910(16) -0.095(2) 0.1136(8) 0.11(18) Uani 0.52(9) 1 d PD A 2
C62' C 0.6681(16) -0.067(3) 0.0987(8) 0.08(12) Uani 0.52(9) 1 d PD A 2
Dy1 Dy 0.4108(6) 0.6086(3) 0.5607(3) 0.049(2) Uani 1 1 d . . .
Dy2 Dy -0.1304(7) 0.6391(3) 0.6704(4) 0.058(2) Uani 1 1 d . . .
Fe1 Fe 0.5000 0.0000 0.0000 0.062(10) Uani 1 2 d S . .
N1 N 0.560(3) 0.7766(10) 0.2175(11) 0.3(2) Uani 1 1 d D . .
N2 N 0.462(15) 1.028(7) 0.585(8) 0.09(6) Uani 1 1 d . . .
N3 N 1.001(18) 0.827(9) 0.300(9) 0.12(7) Uani 1 1 d . . .
N4 N 0.35(2) 0.956(10) 0.764(10) 0.15(9) Uani 1 1 d . . .
N5 N -0.22(2) 0.250(9) 0.863(9) 0.13(8) Uani 1 1 d . . .
N6 N 0.015(14) 0.973(7) 0.415(7) 0.08(5) Uani 1 1 d . . .
N7 N 0.5477(13) 0.0956(6) 0.0350(9) 0.10(6) Uani 1 1 d D A .
N8 N 0.3773(16) -0.0070(8) 0.0851(6) 0.07(5) Uani 1 1 d D A .
N9 N 0.6562(11) -0.0465(8) 0.0338(7) 0.08(5) Uani 1 1 d D A .
O1 O -0.081(12) 0.762(6) 0.689(6) 0.08(4) Uani 1 1 d . . .
O2 O 0.066(11) 0.677(5) 0.713(5) 0.07(4) Uani 1 1 d . . .
O3 O -0.21(2) 0.650(9) 0.781(8) 0.15(8) Uani 1 1 d . . .
O4 O 0.709(11) 0.710(5) 0.627(7) 0.09(5) Uani 1 1 d . . .
O5 O -0.167(12) 0.570(6) 0.578(7) 0.09(5) Uani 1 1 d . . .
O6 O -0.031(11) 0.532(5) 0.693(6) 0.08(4) Uani 1 1 d . . .
O7 O 0.159(12) 0.469(6) 0.692(6) 0.09(5) Uani 1 1 d . . .
O8 O 0.015(10) 0.671(5) 0.579(5) 0.06(3) Uani 1 1 d . . .
O9 O 0.230(10) 0.681(5) 0.546(6) 0.08(4) Uani 1 1 d . . .
O10 O 0.293(10) 0.601(5) 0.671(5) 0.07(4) Uani 1 1 d . . .
O11 O 0.505(10) 0.684(5) 0.621(5) 0.06(3) Uani 1 1 d . . .
O12 O 0.500(9) 0.704(5) 0.486(5) 0.06(3) Uani 1 1 d . . .
O13 O 0.643(9) 0.613(5) 0.498(5) 0.06(3) Uani 1 1 d . . .
O14 O 0.400(11) 0.565(6) 0.459(5) 0.07(4) Uani 1 1 d . . .
O15 O 1.116(14) 0.804(8) 0.290(8) 0.13(6) Uani 1 1 d . . .
O16 O 0.962(19) 0.884(8) 0.274(10) 0.20(8) Uani 1 1 d . . .
O17 O 0.532(15) 1.069(6) 0.606(10) 0.13(7) Uani 1 1 d . . .
O18 O 0.368(15) 1.046(6) 0.557(8) 0.12(6) Uani 1 1 d . . .
O19 O -0.092(14) 1.007(6) 0.433(8) 0.11(6) Uani 1 1 d . . .
O20 O 0.099(14) 0.997(7) 0.374(7) 0.12(6) Uani 1 1 d . . .
O21 O 0.33(2) 1.021(9) 0.742(12) 0.20(10) Uani 1 1 d . . .
O22 O 0.44(2) 0.941(10) 0.795(10) 0.20(9) Uani 1 1 d . . .
O23 O -0.342(18) 0.252(10) 0.871(11) 0.21(8) Uani 1 1 d . . .
O24 O -0.15(2) 0.202(9) 0.884(12) 0.22(10) Uani 1 1 d . . .
O25 O 0.474(11) 0.486(6) 0.389(5) 0.07(4) Uani 1 1 d . . .
O26 O 0.261(11) 0.512(5) 0.569(5) 0.07(4) Uani 1 1 d . . .
O27 O -0.330(14) 0.570(7) 0.700(7) 0.10(5) Uani 1 1 d . . .
O28 O 0.622(3) 0.7610(18) 0.1624(11) 0.26(18) Uani 1 1 d D . .
O29 O 0.478(3) 0.8299(12) 0.219(2) 0.25(16) Uani 1 1 d D . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Fe Fe 0.3463 0.8444 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1892 4.4098 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O11 C1 O4 126(10) . .
O11 C1 C2 119(10) . .
O4 C1 C2 115(10) . .
C3 C2 C7 119(10) . .
C3 C2 C1 121(10) . .
C7 C2 C1 120(10) . .
C4 C3 C2 119(10) . .
C4 C3 H3 120.4 . .
C2 C3 H3 120.5 . .
C5 C4 C3 122(10) . .
C5 C4 H4 119.1 . .
C3 C4 H4 119.1 . .
C4 C5 C6 122(10) . .
C4 C5 N2 121(10) . .
C6 C5 N2 118(10) . .
C7 C6 C5 117(10) . .
C7 C6 H6 121.4 . .
C5 C6 H6 121.4 . .
C6 C7 C2 121(10) . .
C6 C7 H7 119.3 . .
C2 C7 H7 119.3 . .
O2 C8 O1 125(10) . .
O2 C8 C9 119(10) . .
O1 C8 C9 115(10) . .
O2 C8 Dy2 63(10) . .
O1 C8 Dy2 63(9) . .
C9 C8 Dy2 177(10) . .
C10 C9 C13 121(10) . .
C10 C9 C8 118(10) . .
C13 C9 C8 120(10) . .
C9 C10 C11 118(10) . .
C9 C10 H10 120.9 . .
C11 C10 H10 120.9 . .
C76 C11 C10 116(10) . .
C76 C11 H11 121.9 . .
C10 C11 H11 121.9 . .
C76 C12 C13 118(10) . .
C76 C12 H12 120.8 . .
C13 C12 H12 120.8 . .
C12 C13 C9 122(10) . .
C12 C13 H13 118.9 . .
C9 C13 H13 118.9 . .
O9 C14 O8 125(10) . .
O9 C14 C15 117(10) . .
O8 C14 C15 118(10) . .
C20 C15 C16 120(10) . .
C20 C15 C14 120(10) . .
C16 C15 C14 120(10) . .
C17 C16 C15 121(10) . .
C17 C16 H16 119.4 . .
C15 C16 H16 119.4 . .
C18 C17 C16 118(10) . .
C18 C17 H17 121.1 . .
C16 C17 H17 121.1 . .
C17 C18 C19 123(10) . .
C17 C18 N6 118(10) . .
C19 C18 N6 118(10) . .
C20 C19 C18 117(10) . .
C20 C19 H19 121.3 . .
C18 C19 H19 121.3 . .
C15 C20 C19 120(10) . .
C15 C20 H20 119.8 . .
C19 C20 H20 119.8 . .
O6 C21 O7 125(10) . .
O6 C21 C22 118(10) . .
O7 C21 C22 117(10) . .
C27 C22 C23 119(10) . .
C27 C22 C21 120(10) . .
C23 C22 C21 121(10) . .
C22 C23 C24 121(10) . .
C22 C23 H23 119.6 . .
C24 C23 H23 119.6 . .
C25 C24 C23 119(10) . .
C25 C24 H24 120.7 . .
C23 C24 H24 120.7 . .
C26 C25 C24 123(10) . .
C26 C25 N5 119(10) . .
C24 C25 N5 118(10) . .
C25 C26 C27 119(10) . .
C25 C26 H26 120.5 . .
C27 C26 H26 120.5 . .
C22 C27 C26 120(10) . .
C22 C27 H27 120.0 . .
C26 C27 H27 120.0 . .
O12 C28 O13 119(10) . .
O12 C28 C29 120(10) . .
O13 C28 C29 121(10) . .
O12 C28 Dy1 57(7) . .
O13 C28 Dy1 62(7) . .
C29 C28 Dy1 177(9) . .
C30 C29 C34 120(10) . .
C30 C29 C28 119(10) . .
C34 C29 C28 122(10) . .
C29 C30 C31 120(10) . .
C29 C30 H30 120.0 . .
C31 C30 H30 120.0 . .
C32 C31 C30 119(10) . .
C32 C31 H31 120.7 . .
C30 C31 H31 120.7 . .
C31 C32 C33 123(10) . .
C31 C32 N3 119(10) . .
C33 C32 N3 118(10) . .
C34 C33 C32 118(10) . .
C34 C33 H33 121.0 . .
C32 C33 H33 121.0 . .
C33 C34 C29 121(10) . .
C33 C34 H34 119.7 . .
C29 C34 H34 119.7 . .
O14 C35 O25 123(10) . .
O14 C35 C36 120(10) . .
O25 C35 C36 117(10) . .
C41 C36 C37 120(10) . .
C41 C36 C35 120(10) . .
C37 C36 C35 119(10) . .
C36 C37 C38 117(10) . .
C36 C37 H37 121.7 . .
C38 C37 H37 121.7 . .
C39 C38 C37 120(10) . .
C39 C38 H38 120.2 . .
C37 C38 H38 120.2 . .
C40 C39 C38 124(10) . .
C40 C39 N1 122(10) . .
C38 C39 N1 112(10) . .
C39 C40 C41 119(10) . .
C39 C40 H40 120.7 . .
C41 C40 H40 120.7 . .
C36 C41 C40 120(10) . .
C36 C41 H41 119.8 . .
C40 C41 H41 119.8 . .
C44 C43 N8 118.8(14) . .
C44 C43 C72 118.9(11) . .
N8 C43 C72 119.0(14) . .
C43 C44 C70 119.0(15) . .
C43 C44 C45 118.5(13) . .
C70 C44 C45 122.2(16) . .
C44 C45 C46 118.0(16) . .
C44 C45 C46' 81.5(14) . .
C46 C45 C46' 91.5(19) . .
C44 C45 C44' 90.3(14) . .
C46 C45 C44' 40.8(17) . .
C46' C45 C44' 118.0(15) . .
C45 C46 C47 118.0(18) . .
N8 C47 C46 119.2(15) . .
C59 C58 N9 118.1(14) . .
C60 C59 C58 118.3(15) . .
C59 C60 C61 118.2(12) . .
C59 C60 C61' 59(2) . .
C61 C60 C61' 79.9(19) . .
C59 C60 C58' 79(3) . .
C61 C60 C58' 84(2) . .
C61' C60 C58' 117.9(14) . .
C62 C61 C60 118.5(15) . .
C62 C61 C63 118.1(13) . .
C60 C61 C63 118.7(13) . .
C65 C62 C61 118.8(16) . .
C65 C62 N9 118.6(13) . .
C61 C62 N9 118.5(11) . .
C64 C63 C61 117.9(15) . .
C64 C63 H63 121.0 . .
C61 C63 H63 121.0 . .
C66 C64 C63 119(2) . .
C66 C64 H64 120.6 . .
C63 C64 H64 120.6 . .
C66 C65 C62 119.3(13) . .
C66 C65 N7 118.5(11) . .
C62 C65 N7 121.4(15) . .
C66 C65 C75 80.6(12) . .
C62 C65 C75 135.3(19) . .
N7 C65 C75 49.3(11) . .
C65 C66 C64 119.3(12) . .
C65 C66 C67 118.1(16) . .
C64 C66 C67 122.3(18) . .
C66 C67 C68 117(2) . .
C66 C67 C74 127.0(17) . .
C68 C67 C74 57.4(14) . .
C66 C67 C75 73.4(14) . .
C68 C67 C75 43.6(11) . .
C74 C67 C75 84.3(17) . .
C69 C68 C74 97.9(16) . .
C69 C68 C75 41.6(13) . .
C74 C68 C75 118.1(14) . .
C69 C68 C67 117.5(14) . .
C74 C68 C67 64.5(16) . .
C75 C68 C67 92.3(15) . .
C75 C69 N7 69.4(15) . .
C75 C69 C68 69.4(17) . .
N7 C69 C68 118.6(18) . .
C75 C69 C72 110.7(19) . .
N7 C69 C72 48.3(9) . .
C68 C69 C72 113.1(16) . .
C44 C70 C71 118.6(16) . .
C44 C70 H70 120.7 . .
C71 C70 H70 120.7 . .
C70 C71 C73 118.1(15) . .
C70 C71 H71 120.9 . .
C73 C71 H71 120.9 . .
C43 C72 C73 118.2(13) . .
C43 C72 N7 113.4(11) . .
C73 C72 N7 118.1(14) . .
C43 C72 C69 155.3(13) . .
C73 C72 C69 86.5(10) . .
N7 C72 C69 48.1(8) . .
C74 C73 C72 118.1(13) . .
C74 C73 C71 123.4(14) . .
C72 C73 C71 117.9(15) . .
C73 C74 C68 118.1(16) . .
C73 C74 C67 119.8(15) . .
C68 C74 C67 58.2(17) . .
C69 C75 N7 69.0(17) . .
C69 C75 C68 69.1(17) . .
N7 C75 C68 118.2(17) . .
C69 C75 C65 113.6(19) . .
N7 C75 C65 49.2(9) . .
C68 C75 C65 117.6(16) . .
C69 C75 C67 99.5(19) . .
N7 C75 C67 103.7(15) . .
C68 C75 C67 44.1(11) . .
C65 C75 C67 76.7(12) . .
C12 C76 N4 121(10) . .
C12 C76 C11 123(10) . .
N4 C76 C11 116(10) . .
N8 C43' C44' 118.1(18) . .
C43' C44' C45 118.0(18) . .
C47' C46' C45 118.1(18) . .
N8 C47' C46' 118.2(15) . .
N8 C47' C59' 115.1(14) . 2_655
C46' C47' C59' 126(2) . 2_655
C59' C58' C60 117.7(15) . .
N9 C59' C58' 118(2) . .
N9 C59' C47' 115.5(15) . 2_655
C58' C59' C47' 120.0(16) . 2_655
C62' C61' C60 118(2) . .
N9 C62' C61' 118.8(14) . .
O9 Dy1 O11 97(4) . .
O9 Dy1 O14 87(4) . .
O11 Dy1 O14 148(4) . .
O9 Dy1 O25 155(4) . 2_666
O11 Dy1 O25 88(4) . 2_666
O14 Dy1 O25 102(4) . 2_666
O9 Dy1 O10 81(4) . .
O11 Dy1 O10 72(4) . .
O14 Dy1 O10 139(4) . .
O25 Dy1 O10 77(4) 2_666 .
O9 Dy1 O12 76(3) . .
O11 Dy1 O12 73(4) . .
O14 Dy1 O12 77(4) . .
O25 Dy1 O12 128(4) 2_666 .
O10 Dy1 O12 136(3) . .
O9 Dy1 O26 85(4) . .
O11 Dy1 O26 144(3) . .
O14 Dy1 O26 68(4) . .
O25 Dy1 O26 77(4) 2_666 .
O10 Dy1 O26 72(4) . .
O12 Dy1 O26 141(4) . .
O9 Dy1 O13 128(3) . .
O11 Dy1 O13 79(3) . .
O14 Dy1 O13 74(4) . .
O25 Dy1 O13 77(3) 2_666 .
O10 Dy1 O13 141(4) . .
O12 Dy1 O13 53(3) . .
O26 Dy1 O13 128(3) . .
O9 Dy1 C28 102(4) . .
O11 Dy1 C28 74(4) . .
O14 Dy1 C28 75(4) . .
O25 Dy1 C28 103(4) 2_666 .
O10 Dy1 C28 146(4) . .
O12 Dy1 C28 26(3) . .
O26 Dy1 C28 142(4) . .
O13 Dy1 C28 27(3) . .
O6 Dy2 O4 152(4) . 1_455
O6 Dy2 O8 98(4) . .
O4 Dy2 O8 88(4) 1_455 .
O6 Dy2 O3 91(5) . .
O4 Dy2 O3 99(6) 1_455 .
O8 Dy2 O3 150(6) . .
O6 Dy2 O1 133(4) . .
O4 Dy2 O1 75(4) 1_455 .
O8 Dy2 O1 76(4) . .
O3 Dy2 O1 77(5) . .
O6 Dy2 O5 78(4) . .
O4 Dy2 O5 78(4) 1_455 .
O8 Dy2 O5 70(4) . .
O3 Dy2 O5 140(6) . .
O1 Dy2 O5 138(4) . .
O6 Dy2 O27 81(4) . .
O4 Dy2 O27 77(4) 1_455 .
O8 Dy2 O27 139(4) . .
O3 Dy2 O27 71(6) . .
O1 Dy2 O27 133(4) . .
O5 Dy2 O27 69(4) . .
O6 Dy2 O2 80(4) . .
O4 Dy2 O2 128(4) 1_455 .
O8 Dy2 O2 75(4) . .
O3 Dy2 O2 78(6) . .
O1 Dy2 O2 53(4) . .
O5 Dy2 O2 135(4) . .
O27 Dy2 O2 143(4) . .
O6 Dy2 C8 106(5) . .
O4 Dy2 C8 102(5) 1_455 .
O8 Dy2 C8 72(4) . .
O3 Dy2 C8 78(6) . .
O1 Dy2 C8 27(5) . .
O5 Dy2 C8 143(4) . .
O27 Dy2 C8 148(5) . .
O2 Dy2 C8 26(4) . .
N9 Fe1 N9 180.0(11) . 2_655
N9 Fe1 N8 95.8(6) . .
N9 Fe1 N8 84.2(6) 2_655 .
N9 Fe1 N8 84.2(6) . 2_655
N9 Fe1 N8 95.8(6) 2_655 2_655
N8 Fe1 N8 180.0(9) . 2_655
N9 Fe1 N7 92.1(6) . 2_655
N9 Fe1 N7 87.9(6) 2_655 2_655
N8 Fe1 N7 96.5(6) . 2_655
N8 Fe1 N7 83.5(6) 2_655 2_655
N9 Fe1 N7 87.9(6) . .
N9 Fe1 N7 92.1(6) 2_655 .
N8 Fe1 N7 83.5(6) . .
N8 Fe1 N7 96.5(6) 2_655 .
N7 Fe1 N7 180.0(9) 2_655 .
O28 N1 O29 117(3) . .
O28 N1 C39 110(3) . .
O29 N1 C39 116(3) . .
O18 N2 O17 125(10) . .
O18 N2 C5 118(10) . .
O17 N2 C5 117(10) . .
O15 N3 O16 123(10) . .
O15 N3 C32 121(10) . .
O16 N3 C32 117(10) . .
O22 N4 O21 120(10) . .
O22 N4 C76 122(10) . .
O21 N4 C76 119(10) . .
O24 N5 O23 124(10) . .
O24 N5 C25 118(10) . .
O23 N5 C25 118(10) . .
O20 N6 O19 123(10) . .
O20 N6 C18 120(10) . .
O19 N6 C18 117(10) . .
C69 N7 C65 118.6(13) . .
C69 N7 C75 41.6(12) . .
C65 N7 C75 81.5(14) . .
C69 N7 C72 83.6(11) . .
C65 N7 C72 117.0(17) . .
C75 N7 C72 118.0(12) . .
C69 N7 Fe1 127.8(14) . .
C65 N7 Fe1 102.6(8) . .
C75 N7 Fe1 128.1(13) . .
C72 N7 Fe1 106.0(9) . .
C43 N8 C47 118.4(14) . .
C43 N8 C47' 85.2(18) . .
C47 N8 C47' 85.5(19) . .
C43 N8 C43' 86.3(15) . .
C47 N8 C43' 47.5(15) . .
C47' N8 C43' 118.1(14) . .
C43 N8 Fe1 108.6(11) . .
C47 N8 Fe1 131.6(12) . .
C47' N8 Fe1 110.2(10) . .
C43' N8 Fe1 130.5(12) . .
C62' N9 C59' 119.1(14) . .
C62' N9 C62 80(2) . .
C59' N9 C62 63.8(17) . .
C62' N9 C58 58(3) . .
C59' N9 C58 98(2) . .
C62 N9 C58 118.0(17) . .
C62' N9 Fe1 127.4(11) . .
C59' N9 Fe1 109.7(13) . .
C62 N9 Fe1 106.6(10) . .
C58 N9 Fe1 134.6(13) . .
C8 O1 Dy2 90(9) . .
C8 O2 Dy2 90(10) . .
C1 O4 Dy2 152(10) . 1_655
C21 O6 Dy2 170(10) . .
C14 O8 Dy2 153(10) . .
C14 O9 Dy1 161(9) . .
C1 O11 Dy1 146(10) . .
C28 O12 Dy1 97(8) . .
C28 O13 Dy1 91(8) . .
C35 O14 Dy1 157(10) . .
C35 O25 Dy1 134(10) . 2_666
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
C1 O11 1.20(18) .
C1 O4 1.26(19) .
C1 C2 1.52(18) .
C2 C3 1.4(2) .
C2 C7 1.4(2) .
C3 C4 1.4(2) .
C3 H3 0.9300 .
C4 C5 1.3(2) .
C4 H4 0.9300 .
C5 C6 1.4(2) .
C5 N2 1.49(19) .
C6 C7 1.37(19) .
C6 H6 0.9300 .
C7 H7 0.9300 .
C8 O2 1.23(19) .
C8 O1 1.3(2) .
C8 C9 1.6(3) .
C8 Dy2 2.76(19) .
C9 C10 1.4(3) .
C9 C13 1.4(2) .
C10 C11 1.4(3) .
C10 H10 0.9300 .
C11 C76 1.4(3) .
C11 H11 0.9300 .
C12 C76 1.3(3) .
C12 C13 1.3(3) .
C12 H12 0.9300 .
C13 H13 0.9300 .
C14 O9 1.24(17) .
C14 O8 1.25(16) .
C14 C15 1.51(17) .
C15 C20 1.37(18) .
C15 C16 1.39(18) .
C16 C17 1.4(2) .
C16 H16 0.9300 .
C17 C18 1.4(2) .
C17 H17 0.9300 .
C18 C19 1.4(2) .
C18 N6 1.47(19) .
C19 C20 1.38(19) .
C19 H19 0.9300 .
C20 H20 0.9300 .
C21 O6 1.24(17) .
C21 O7 1.24(19) .
C21 C22 1.49(19) .
C22 C27 1.4(2) .
C22 C23 1.4(2) .
C23 C24 1.4(3) .
C23 H23 0.9300 .
C24 C25 1.4(3) .
C24 H24 0.9300 .
C25 C26 1.3(3) .
C25 N5 1.5(2) .
C26 C27 1.4(2) .
C26 H26 0.9300 .
C27 H27 0.9300 .
C28 O12 1.27(16) .
C28 O13 1.29(16) .
C28 C29 1.48(19) .
C28 Dy1 2.87(13) .
C29 C30 1.38(19) .
C29 C34 1.39(19) .
C30 C31 1.4(2) .
C30 H30 0.9300 .
C31 C32 1.3(2) .
C31 H31 0.9300 .
C32 C33 1.4(2) .
C32 N3 1.5(2) .
C33 C34 1.4(2) .
C33 H33 0.9300 .
C34 H34 0.9300 .
C35 O14 1.22(18) .
C35 O25 1.25(16) .
C35 C36 1.50(19) .
C36 C41 1.4(2) .
C36 C37 1.4(2) .
C37 C38 1.4(3) .
C37 H37 0.9300 .
C38 C39 1.3(2) .
C38 H38 0.9300 .
C39 C40 1.3(2) .
C39 N1 1.48(4) .
C40 C41 1.4(3) .
C40 H40 0.9300 .
C41 H41 0.9300 .
C43 C44 1.39(2) .
C43 N8 1.40(2) .
C43 C72 1.397(19) .
C44 C70 1.40(2) .
C44 C45 1.40(2) .
C45 C46 1.40(2) .
C45 C46' 1.40(2) .
C45 C44' 1.40(3) .
C46 C47 1.40(3) .
C47 N8 1.40(2) .
C58 C59 1.40(3) .
C58 N9 1.40(2) .
C59 C60 1.40(3) .
C60 C61 1.399(18) .
C60 C61' 1.40(2) .
C60 C58' 1.40(2) .
C61 C62 1.40(2) .
C61 C63 1.40(2) .
C62 C65 1.394(17) .
C62 N9 1.40(2) .
C63 C64 1.40(2) .
C63 H63 0.9300 .
C64 C66 1.39(3) .
C64 H64 0.9300 .
C65 C66 1.39(2) .
C65 N7 1.40(2) .
C65 C75 1.83(3) .
C66 C67 1.40(2) .
C67 C68 1.41(4) .
C67 C74 1.50(3) .
C67 C75 2.03(4) .
C68 C69 1.40(2) .
C68 C74 1.40(2) .
C68 C75 1.40(2) .
C69 C75 0.99(3) .
C69 N7 1.40(2) .
C69 C72 1.86(2) .
C70 C71 1.40(3) .
C70 H70 0.9300 .
C71 C73 1.40(3) .
C71 H71 0.9300 .
C72 C73 1.399(19) .
C72 N7 1.40(2) .
C73 C74 1.40(3) .
C75 N7 1.40(2) .
C76 N4 1.4(3) .
C43' N8 1.40(2) .
C43' C44' 1.40(2) .
C46' C47' 1.40(3) .
C47' N8 1.40(3) .
C47' C59' 1.41(2) 2_655
C58' C59' 1.40(3) .
C59' N9 1.40(2) .
C59' C47' 1.41(2) 2_655
C61' C62' 1.40(3) .
C62' N9 1.39(2) .
Dy1 O9 2.26(10) .
Dy1 O11 2.29(11) .
Dy1 O14 2.32(11) .
Dy1 O25 2.33(11) 2_666
Dy1 O10 2.41(10) .
Dy1 O12 2.43(9) .
Dy1 O26 2.43(11) .
Dy1 O13 2.53(9) .
Dy2 O6 2.24(10) .
Dy2 O4 2.29(12) 1_455
Dy2 O8 2.29(9) .
Dy2 O3 2.34(16) .
Dy2 O1 2.45(11) .
Dy2 O5 2.46(13) .
Dy2 O27 2.46(14) .
Dy2 O2 2.47(12) .
Fe1 N9 1.963(13) .
Fe1 N9 1.963(13) 2_655
Fe1 N8 2.002(13) .
Fe1 N8 2.002(13) 2_655
Fe1 N7 2.087(14) 2_655
Fe1 N7 2.087(14) .
N1 O28 1.26(3) .
N1 O29 1.26(3) .
N2 O18 1.2(2) .
N2 O17 1.2(2) .
N3 O15 1.2(2) .
N3 O16 1.2(2) .
N4 O22 1.2(3) .
N4 O21 1.3(3) .
N5 O24 1.2(3) .
N5 O23 1.2(3) .
N6 O20 1.20(19) .
N6 O19 1.24(19) .
O4 Dy2 2.29(12) 1_655
O25 Dy1 2.33(11) 2_666
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
O11 C1 C2 C3 166(15) . .
O4 C1 C2 C3 -12(22) . .
O11 C1 C2 C7 -18(22) . .
O4 C1 C2 C7 164(14) . .
C7 C2 C3 C4 -1(23) . .
C1 C2 C3 C4 175(15) . .
C2 C3 C4 C5 2(26) . .
C3 C4 C5 C6 -3(27) . .
C3 C4 C5 N2 -179(16) . .
C4 C5 C6 C7 2(24) . .
N2 C5 C6 C7 179(14) . .
C5 C6 C7 C2 -1(23) . .
C3 C2 C7 C6 1(23) . .
C1 C2 C7 C6 -175(14) . .
O2 C8 C9 C10 -8(23) . .
O1 C8 C9 C10 166(16) . .
Dy2 C8 C9 C10 -170(100) . .
O2 C8 C9 C13 169(16) . .
O1 C8 C9 C13 -17(23) . .
Dy2 C8 C9 C13 8(100) . .
C13 C9 C10 C11 -3(27) . .
C8 C9 C10 C11 175(16) . .
C9 C10 C11 C76 6(27) . .
C76 C12 C13 C9 -1(29) . .
C10 C9 C13 C12 0(28) . .
C8 C9 C13 C12 -178(17) . .
O9 C14 C15 C20 -175(14) . .
O8 C14 C15 C20 6(20) . .
O9 C14 C15 C16 8(21) . .
O8 C14 C15 C16 -171(14) . .
C20 C15 C16 C17 1(23) . .
C14 C15 C16 C17 178(14) . .
C15 C16 C17 C18 0(24) . .
C16 C17 C18 C19 0(25) . .
C16 C17 C18 N6 179(15) . .
C17 C18 C19 C20 -1(25) . .
N6 C18 C19 C20 -180(14) . .
C16 C15 C20 C19 -2(22) . .
C14 C15 C20 C19 -179(14) . .
C18 C19 C20 C15 2(23) . .
O6 C21 C22 C27 -175(15) . .
O7 C21 C22 C27 7(23) . .
O6 C21 C22 C23 9(23) . .
O7 C21 C22 C23 -169(16) . .
C27 C22 C23 C24 5(27) . .
C21 C22 C23 C24 -179(17) . .
C22 C23 C24 C25 -5(30) . .
C23 C24 C25 C26 3(32) . .
C23 C24 C25 N5 -176(18) . .
C24 C25 C26 C27 -1(31) . .
N5 C25 C26 C27 179(18) . .
C23 C22 C27 C26 -3(25) . .
C21 C22 C27 C26 -179(16) . .
C25 C26 C27 C22 1(28) . .
O12 C28 C29 C30 -2(22) . .
O13 C28 C29 C30 177(14) . .
Dy1 C28 C29 C30 -8(100) . .
O12 C28 C29 C34 176(14) . .
O13 C28 C29 C34 -5(23) . .
Dy1 C28 C29 C34 170(100) . .
C34 C29 C30 C31 1(24) . .
C28 C29 C30 C31 179(15) . .
C29 C30 C31 C32 -1(26) . .
C30 C31 C32 C33 1(28) . .
C30 C31 C32 N3 -179(17) . .
C31 C32 C33 C34 -1(27) . .
N3 C32 C33 C34 178(16) . .
C32 C33 C34 C29 2(25) . .
C30 C29 C34 C33 -2(24) . .
C28 C29 C34 C33 -180(15) . .
O14 C35 C36 C41 157(17) . .
O25 C35 C36 C41 -20(23) . .
O14 C35 C36 C37 -20(24) . .
O25 C35 C36 C37 162(16) . .
C41 C36 C37 C38 -6(29) . .
C35 C36 C37 C38 171(18) . .
C36 C37 C38 C39 3(32) . .
C37 C38 C39 C40 2(33) . .
C37 C38 C39 N1 -166(17) . .
C38 C39 C40 C41 -3(34) . .
N1 C39 C40 C41 163(16) . .
C37 C36 C41 C40 5(31) . .
C35 C36 C41 C40 -172(19) . .
C39 C40 C41 C36 0(35) . .
N8 C43 C44 C70 -179.7(18) . .
C72 C43 C44 C70 -20(3) . .
N8 C43 C44 C45 -5(2) . .
C72 C43 C44 C45 154.1(16) . .
C43 C44 C45 C46 28(3) . .
C70 C44 C45 C46 -158(2) . .
C43 C44 C45 C46' -59.0(19) . .
C70 C44 C45 C46' 115(2) . .
C43 C44 C45 C44' 59.2(18) . .
C70 C44 C45 C44' -126.6(19) . .
C44 C45 C46 C47 -25(3) . .
C46' C45 C46 C47 56(3) . .
C44' C45 C46 C47 -78(3) . .
C45 C46 C47 N8 0(4) . .
N9 C58 C59 C60 25(6) . .
C58 C59 C60 C61 2(5) . .
C58 C59 C60 C61' 58(3) . .
C58 C59 C60 C58' -74(4) . .
C59 C60 C61 C62 -26(3) . .
C61' C60 C61 C62 -72.5(18) . .
C58' C60 C61 C62 47(2) . .
C59 C60 C61 C63 178(3) . .
C61' C60 C61 C63 132(2) . .
C58' C60 C61 C63 -108(2) . .
C60 C61 C62 C65 179.8(16) . .
C63 C61 C62 C65 -25(3) . .
C60 C61 C62 N9 23(3) . .
C63 C61 C62 N9 178(2) . .
C62 C61 C63 C64 28(4) . .
C60 C61 C63 C64 -177(2) . .
C61 C63 C64 C66 -25(4) . .
C61 C62 C65 C66 19(3) . .
N9 C62 C65 C66 175.6(18) . .
C61 C62 C65 N7 -171.9(17) . .
N9 C62 C65 N7 -15(3) . .
C61 C62 C65 C75 126(2) . .
N9 C62 C65 C75 -77(2) . .
C62 C65 C66 C64 -16(3) . .
N7 C65 C66 C64 174.5(19) . .
C75 C65 C66 C64 -153(2) . .
C62 C65 C66 C67 170(2) . .
N7 C65 C66 C67 0(3) . .
C75 C65 C66 C67 33(2) . .
C63 C64 C66 C65 19(3) . .
C63 C64 C66 C67 -167(2) . .
C65 C66 C67 C68 -29(3) . .
C64 C66 C67 C68 157(2) . .
C65 C66 C67 C74 39(4) . .
C64 C66 C67 C74 -135(3) . .
C65 C66 C67 C75 -30.0(19) . .
C64 C66 C67 C75 156(2) . .
C66 C67 C68 C69 33(3) . .
C74 C67 C68 C69 -85.5(18) . .
C75 C67 C68 C69 34.6(15) . .
C66 C67 C68 C74 118(2) . .
C75 C67 C68 C74 120.2(16) . .
C66 C67 C68 C75 -2(2) . .
C74 C67 C68 C75 -120.2(16) . .
C74 C68 C69 C75 -124(2) . .
C67 C68 C69 C75 -59(2) . .
C74 C68 C69 N7 -73(2) . .
C75 C68 C69 N7 50.7(17) . .
C67 C68 C69 N7 -8(3) . .
C74 C68 C69 C72 -19.6(17) . .
C75 C68 C69 C72 104(2) . .
C67 C68 C69 C72 46(2) . .
C43 C44 C70 C71 21(3) . .
C45 C44 C70 C71 -153(2) . .
C44 C70 C71 C73 -25(4) . .
C44 C43 C72 C73 24(3) . .
N8 C43 C72 C73 -177.0(16) . .
C44 C43 C72 N7 168.1(17) . .
N8 C43 C72 N7 -32(2) . .
C44 C43 C72 C69 -155(3) . .
N8 C43 C72 C69 5(5) . .
C75 C69 C72 C43 -81(4) . .
N7 C69 C72 C43 -48(4) . .
C68 C69 C72 C43 -156(3) . .
C75 C69 C72 C73 101(2) . .
N7 C69 C72 C73 133.6(17) . .
C68 C69 C72 C73 25.1(16) . .
C75 C69 C72 N7 -32.9(19) . .
C68 C69 C72 N7 -108.5(18) . .
C43 C72 C73 C74 161.0(17) . .
N7 C72 C73 C74 18(2) . .
C69 C72 C73 C74 -19.6(18) . .
C43 C72 C73 C71 -27(2) . .
N7 C72 C73 C71 -170.4(16) . .
C69 C72 C73 C71 151.9(16) . .
C70 C71 C73 C74 -161(2) . .
C70 C71 C73 C72 28(3) . .
C72 C73 C74 C68 13(3) . .
C71 C73 C74 C68 -158.3(19) . .
C72 C73 C74 C67 -55(3) . .
C71 C73 C74 C67 134(2) . .
C69 C68 C74 C73 7(2) . .
C75 C68 C74 C73 -31(3) . .
C67 C68 C74 C73 -109.4(19) . .
C69 C68 C74 C67 116.8(14) . .
C75 C68 C74 C67 78(2) . .
C66 C67 C74 C73 5(4) . .
C68 C67 C74 C73 106(2) . .
C75 C67 C74 C73 70(2) . .
C66 C67 C74 C68 -101(3) . .
C75 C67 C74 C68 -36.8(10) . .
C68 C69 C75 N7 133.5(16) . .
C72 C69 C75 N7 25.7(14) . .
N7 C69 C75 C68 -133.5(16) . .
C72 C69 C75 C68 -107.8(18) . .
N7 C69 C75 C65 -21.5(16) . .
C68 C69 C75 C65 112.0(18) . .
C72 C69 C75 C65 4(2) . .
N7 C69 C75 C67 -101.1(14) . .
C68 C69 C75 C67 32.4(12) . .
C72 C69 C75 C67 -75.4(16) . .
C74 C68 C75 C69 68(3) . .
C67 C68 C75 C69 131(2) . .
C69 C68 C75 N7 -50(2) . .
C74 C68 C75 N7 18(3) . .
C67 C68 C75 N7 80(2) . .
C69 C68 C75 C65 -106(2) . .
C74 C68 C75 C65 -38(3) . .
C67 C68 C75 C65 24(2) . .
C69 C68 C75 C67 -131(2) . .
C74 C68 C75 C67 -62(2) . .
C66 C65 C75 C69 -115(2) . .
C62 C65 C75 C69 123(2) . .
N7 C65 C75 C69 27(2) . .
C66 C65 C75 N7 -141.3(16) . .
C62 C65 C75 N7 96(2) . .
C66 C65 C75 C68 -36.7(19) . .
C62 C65 C75 C68 -159.3(17) . .
N7 C65 C75 C68 105(2) . .
C66 C65 C75 C67 -19.8(12) . .
C62 C65 C75 C67 -142.3(17) . .
N7 C65 C75 C67 121.6(15) . .
C66 C67 C75 C69 132.4(19) . .
C68 C67 C75 C69 -46.0(19) . .
C74 C67 C75 C69 1.0(18) . .
C66 C67 C75 N7 61.9(16) . .
C68 C67 C75 N7 -117(2) . .
C74 C67 C75 N7 -69.6(16) . .
C66 C67 C75 C68 178(2) . .
C74 C67 C75 C68 47.0(14) . .
C66 C67 C75 C65 20.2(11) . .
C68 C67 C75 C65 -158.2(19) . .
C74 C67 C75 C65 -111.2(13) . .
C13 C12 C76 N4 -178(18) . .
C13 C12 C76 C11 4(30) . .
C10 C11 C76 C12 -7(29) . .
C10 C11 C76 N4 175(18) . .
N8 C43' C44' C45 -16(3) . .
C44 C45 C44' C43' -49(2) . .
C46 C45 C44' C43' 87(3) . .
C46' C45 C44' C43' 32(3) . .
C44 C45 C46' C47' 69(3) . .
C46 C45 C46' C47' -49(3) . .
C44' C45 C46' C47' -16(3) . .
C45 C46' C47' N8 -15(4) . .
C45 C46' C47' C59' 177(3) . 2_655
C59 C60 C58' C59' 75(4) . .
C61 C60 C58' C59' -45(4) . .
C61' C60 C58' C59' 30(5) . .
C60 C58' C59' N9 -27(6) . .
C60 C58' C59' C47' -178(3) . 2_655
C59 C60 C61' C62' -82(3) . .
C61 C60 C61' C62' 50(3) . .
C58' C60 C61' C62' -27(5) . .
C60 C61' C62' N9 23(6) . .
O12 C28 Dy1 O9 9(10) . .
O13 C28 Dy1 O9 -169(8) . .
C29 C28 Dy1 O9 16(100) . .
O12 C28 Dy1 O11 -85(9) . .
O13 C28 Dy1 O11 97(9) . .
C29 C28 Dy1 O11 -78(100) . .
O12 C28 Dy1 O14 93(9) . .
O13 C28 Dy1 O14 -86(9) . .
C29 C28 Dy1 O14 99(100) . .
O12 C28 Dy1 O25 -168(9) . 2_666
O13 C28 Dy1 O25 14(9) . 2_666
C29 C28 Dy1 O25 -162(100) . 2_666
O12 C28 Dy1 O10 -82(11) . .
O13 C28 Dy1 O10 99(9) . .
C29 C28 Dy1 O10 -76(100) . .
O13 C28 Dy1 O12 -178(15) . .
C29 C28 Dy1 O12 6(100) . .
O12 C28 Dy1 O26 106(9) . .
O13 C28 Dy1 O26 -72(11) . .
C29 C28 Dy1 O26 113(100) . .
O12 C28 Dy1 O13 178(15) . .
C29 C28 Dy1 O13 -175(100) . .
O2 C8 Dy2 O6 1(10) . .
O1 C8 Dy2 O6 -173(9) . .
C9 C8 Dy2 O6 162(100) . .
O2 C8 Dy2 O4 -176(9) . 1_455
O1 C8 Dy2 O4 11(10) . 1_455
C9 C8 Dy2 O4 -14(100) . 1_455
O2 C8 Dy2 O8 -92(9) . .
O1 C8 Dy2 O8 95(9) . .
C9 C8 Dy2 O8 69(100) . .
O2 C8 Dy2 O3 88(10) . .
O1 C8 Dy2 O3 -86(10) . .
C9 C8 Dy2 O3 -111(100) . .
O2 C8 Dy2 O1 173(16) . .
C9 C8 Dy2 O1 -25(100) . .
O2 C8 Dy2 O5 -90(11) . .
O1 C8 Dy2 O5 97(11) . .
C9 C8 Dy2 O5 71(100) . .
O2 C8 Dy2 O27 100(12) . .
O1 C8 Dy2 O27 -73(13) . .
C9 C8 Dy2 O27 -98(100) . .
O1 C8 Dy2 O2 -173(16) . .
C9 C8 Dy2 O2 161(100) . .
C40 C39 N1 O28 25(16) . .
C38 C39 N1 O28 -166(13) . .
C40 C39 N1 O29 161(16) . .
C38 C39 N1 O29 -31(14) . .
C4 C5 N2 O18 170(17) . .
C6 C5 N2 O18 -7(23) . .
C4 C5 N2 O17 -12(24) . .
C6 C5 N2 O17 171(16) . .
C31 C32 N3 O15 177(19) . .
C33 C32 N3 O15 -3(28) . .
C31 C32 N3 O16 -3(28) . .
C33 C32 N3 O16 177(19) . .
C12 C76 N4 O22 176(20) . .
C11 C76 N4 O22 -6(30) . .
C12 C76 N4 O21 -7(31) . .
C11 C76 N4 O21 171(20) . .
C26 C25 N5 O24 3(30) . .
C24 C25 N5 O24 -178(21) . .
C26 C25 N5 O23 -176(21) . .
C24 C25 N5 O23 4(30) . .
C17 C18 N6 O20 11(24) . .
C19 C18 N6 O20 -170(17) . .
C17 C18 N6 O19 -165(16) . .
C19 C18 N6 O19 14(23) . .
C75 C69 N7 C65 30(2) . .
C68 C69 N7 C65 -21(3) . .
C72 C69 N7 C65 -117(2) . .
C68 C69 N7 C75 -50.7(19) . .
C72 C69 N7 C75 -147(2) . .
C75 C69 N7 C72 147(2) . .
C68 C69 N7 C72 96.5(18) . .
C75 C69 N7 Fe1 -108(2) . .
C68 C69 N7 Fe1 -158.3(13) . .
C72 C69 N7 Fe1 105.3(14) . .
C66 C65 N7 C69 25(3) . .
C62 C65 N7 C69 -144.6(19) . .
C75 C65 N7 C69 -19.5(15) . .
C66 C65 N7 C75 45(2) . .
C62 C65 N7 C75 -125(2) . .
C66 C65 N7 C72 -73(2) . .
C62 C65 N7 C72 117.8(19) . .
C75 C65 N7 C72 -117.2(15) . .
C66 C65 N7 Fe1 171.9(15) . .
C62 C65 N7 Fe1 2(2) . .
C75 C65 N7 Fe1 127.3(13) . .
C68 C75 N7 C69 50(2) . .
C65 C75 N7 C69 154(2) . .
C67 C75 N7 C69 95(2) . .
C69 C75 N7 C65 -154(2) . .
C68 C75 N7 C65 -103(2) . .
C67 C75 N7 C65 -58.6(14) . .
C69 C75 N7 C72 -38(2) . .
C68 C75 N7 C72 13(3) . .
C65 C75 N7 C72 116(2) . .
C67 C75 N7 C72 58(2) . .
C69 C75 N7 Fe1 107(2) . .
C68 C75 N7 Fe1 157.1(15) . .
C65 C75 N7 Fe1 -99.4(15) . .
C67 C75 N7 Fe1 -158.0(11) . .
C43 C72 N7 C69 160.3(17) . .
C73 C72 N7 C69 -55.1(17) . .
C43 C72 N7 C65 -80.9(18) . .
C73 C72 N7 C65 63.7(17) . .
C69 C72 N7 C65 118.8(16) . .
C43 C72 N7 C75 -175.7(18) . .
C73 C72 N7 C75 -31(2) . .
C69 C72 N7 C75 24.1(16) . .
C43 C72 N7 Fe1 32.7(17) . .
C73 C72 N7 Fe1 177.4(11) . .
C69 C72 N7 Fe1 -127.5(15) . .
N9 Fe1 N7 C69 149.0(14) . .
N9 Fe1 N7 C69 -31.0(14) 2_655 .
N8 Fe1 N7 C69 -114.9(15) . .
N8 Fe1 N7 C69 65.1(15) 2_655 .
N7 Fe1 N7 C69 -3(100) 2_655 .
N9 Fe1 N7 C65 6.5(12) . .
N9 Fe1 N7 C65 -173.5(12) 2_655 .
N8 Fe1 N7 C65 102.6(12) . .
N8 Fe1 N7 C65 -77.4(12) 2_655 .
N7 Fe1 N7 C65 -146(100) 2_655 .
N9 Fe1 N7 C75 95.5(17) . .
N9 Fe1 N7 C75 -84.5(17) 2_655 .
N8 Fe1 N7 C75 -168.4(17) . .
N8 Fe1 N7 C75 11.6(17) 2_655 .
N7 Fe1 N7 C75 -57(100) 2_655 .
N9 Fe1 N7 C72 -116.7(11) . .
N9 Fe1 N7 C72 63.3(11) 2_655 .
N8 Fe1 N7 C72 -20.6(11) . .
N8 Fe1 N7 C72 159.4(11) 2_655 .
N7 Fe1 N7 C72 91(100) 2_655 .
C44 C43 N8 C47 -20(3) . .
C72 C43 N8 C47 -179.4(18) . .
C44 C43 N8 C47' 62.4(19) . .
C72 C43 N8 C47' -97.1(19) . .
C44 C43 N8 C43' -56.3(18) . .
C72 C43 N8 C43' 144.3(18) . .
C44 C43 N8 Fe1 172.1(13) . .
C72 C43 N8 Fe1 13(2) . .
C46 C47 N8 C43 23(3) . .
C46 C47 N8 C47' -59(3) . .
C46 C47 N8 C43' 76(3) . .
C46 C47 N8 Fe1 -173(2) . .
C46' C47' N8 C43 -52(3) . .
C59' C47' N8 C43 117(3) 2_655 .
C46' C47' N8 C47 67(3) . .
C59' C47' N8 C47 -124(3) 2_655 .
C46' C47' N8 C43' 31(4) . .
C59' C47' N8 C43' -160(3) 2_655 .
C46' C47' N8 Fe1 -160(2) . .
C59' C47' N8 Fe1 9(4) 2_655 .
C44' C43' N8 C43 67(2) . .
C44' C43' N8 C47 -68(2) . .
C44' C43' N8 C47' -16(4) . .
C44' C43' N8 Fe1 178.3(17) . .
N9 Fe1 N8 C43 92.2(12) . .
N9 Fe1 N8 C43 -87.8(12) 2_655 .
N8 Fe1 N8 C43 -39(100) 2_655 .
N7 Fe1 N8 C43 -174.9(12) 2_655 .
N7 Fe1 N8 C43 5.1(12) . .
N9 Fe1 N8 C47 -74(2) . .
N9 Fe1 N8 C47 106(2) 2_655 .
N8 Fe1 N8 C47 156(100) 2_655 .
N7 Fe1 N8 C47 19(2) 2_655 .
N7 Fe1 N8 C47 -161(2) . .
N9 Fe1 N8 C47' -176.1(19) . .
N9 Fe1 N8 C47' 3.9(19) 2_655 .
N8 Fe1 N8 C47' 53(100) 2_655 .
N7 Fe1 N8 C47' -83.3(19) 2_655 .
N7 Fe1 N8 C47' 96.7(19) . .
N9 Fe1 N8 C43' -9(2) . .
N9 Fe1 N8 C43' 171(2) 2_655 .
N8 Fe1 N8 C43' -140(100) 2_655 .
N7 Fe1 N8 C43' 84(2) 2_655 .
N7 Fe1 N8 C43' -96(2) . .
C61' C62' N9 C59' -20(5) . .
C61' C62' N9 C62 -73(4) . .
C61' C62' N9 C58 60(4) . .
C61' C62' N9 Fe1 -176(3) . .
C58' C59' N9 C62' 23(5) . .
C47' C59' N9 C62' 175(3) 2_655 .
C58' C59' N9 C62 83(3) . .
C47' C59' N9 C62 -125(4) 2_655 .
C58' C59' N9 C58 -35(4) . .
C47' C59' N9 C58 117(4) 2_655 .
C58' C59' N9 Fe1 -178(3) . .
C47' C59' N9 Fe1 -26(4) 2_655 .
C65 C62 N9 C62' -107(2) . .
C61 C62 N9 C62' 50(2) . .
C65 C62 N9 C59' 123(2) . .
C61 C62 N9 C59' -80(2) . .
C65 C62 N9 C58 -152(2) . .
C61 C62 N9 C58 5(3) . .
C65 C62 N9 Fe1 19(2) . .
C61 C62 N9 Fe1 175.8(15) . .
C59 C58 N9 C62' -84(4) . .
C59 C58 N9 C59' 36(4) . .
C59 C58 N9 C62 -29(5) . .
C59 C58 N9 Fe1 163(3) . .
N9 Fe1 N9 C62' 124(21) 2_655 .
N8 Fe1 N9 C62' -7(3) . .
N8 Fe1 N9 C62' 173(3) 2_655 .
N7 Fe1 N9 C62' -104(3) 2_655 .
N7 Fe1 N9 C62' 76(3) . .
N9 Fe1 N9 C59' -33(20) 2_655 .
N8 Fe1 N9 C59' -164.1(19) . .
N8 Fe1 N9 C59' 15.9(19) 2_655 .
N7 Fe1 N9 C59' 99.1(19) 2_655 .
N7 Fe1 N9 C59' -80.9(19) . .
N9 Fe1 N9 C62 34(18) 2_655 .
N8 Fe1 N9 C62 -96.6(12) . .
N8 Fe1 N9 C62 83.4(12) 2_655 .
N7 Fe1 N9 C62 166.6(12) 2_655 .
N7 Fe1 N9 C62 -13.4(12) . .
N9 Fe1 N9 C58 -157(21) 2_655 .
N8 Fe1 N9 C58 72(3) . .
N8 Fe1 N9 C58 -108(3) 2_655 .
N7 Fe1 N9 C58 -24(3) 2_655 .
N7 Fe1 N9 C58 156(3) . .
O2 C8 O1 Dy2 -7(17) . .
C9 C8 O1 Dy2 179(12) . .
O6 Dy2 O1 C8 10(12) . .
O4 Dy2 O1 C8 -169(10) 1_455 .
O8 Dy2 O1 C8 -78(10) . .
O3 Dy2 O1 C8 88(11) . .
O5 Dy2 O1 C8 -116(10) . .
O27 Dy2 O1 C8 136(10) . .
O2 Dy2 O1 C8 4(9) . .
O1 C8 O2 Dy2 7(17) . .
C9 C8 O2 Dy2 -179(13) . .
O6 Dy2 O2 C8 -179(10) . .
O4 Dy2 O2 C8 5(11) 1_455 .
O8 Dy2 O2 C8 80(9) . .
O3 Dy2 O2 C8 -87(10) . .
O1 Dy2 O2 C8 -4(9) . .
O5 Dy2 O2 C8 120(10) . .
O27 Dy2 O2 C8 -119(10) . .
O11 C1 O4 Dy2 -34(36) . 1_655
C2 C1 O4 Dy2 143(19) . 1_655
O7 C21 O6 Dy2 -55(68) . .
C22 C21 O6 Dy2 127(55) . .
O4 Dy2 O6 C21 177(56) 1_455 .
O8 Dy2 O6 C21 78(60) . .
O3 Dy2 O6 C21 -73(60) . .
O1 Dy2 O6 C21 0(62) . .
O5 Dy2 O6 C21 146(60) . .
O27 Dy2 O6 C21 -143(60) . .
O2 Dy2 O6 C21 5(60) . .
C8 Dy2 O6 C21 4(61) . .
O9 C14 O8 Dy2 85(23) . .
C15 C14 O8 Dy2 -96(22) . .
O6 Dy2 O8 C14 -99(19) . .
O4 Dy2 O8 C14 109(19) 1_455 .
O3 Dy2 O8 C14 6(24) . .
O1 Dy2 O8 C14 34(19) . .
O5 Dy2 O8 C14 -173(20) . .
O27 Dy2 O8 C14 176(18) . .
O2 Dy2 O8 C14 -21(19) . .
C8 Dy2 O8 C14 6(19) . .
O8 C14 O9 Dy1 -2(43) . .
C15 C14 O9 Dy1 179(25) . .
O11 Dy1 O9 C14 -114(32) . .
O14 Dy1 O9 C14 98(32) . .
O25 Dy1 O9 C14 -15(38) 2_666 .
O10 Dy1 O9 C14 -43(32) . .
O12 Dy1 O9 C14 175(33) . .
O26 Dy1 O9 C14 30(32) . .
O13 Dy1 O9 C14 165(31) . .
C28 Dy1 O9 C14 171(32) . .
O4 C1 O11 Dy1 -83(24) . .
C2 C1 O11 Dy1 100(18) . .
O9 Dy1 O11 C1 -103(17) . .
O14 Dy1 O11 C1 -7(20) . .
O25 Dy1 O11 C1 102(17) 2_666 .
O10 Dy1 O11 C1 179(17) . .
O12 Dy1 O11 C1 -30(16) . .
O26 Dy1 O11 C1 166(15) . .
O13 Dy1 O11 C1 25(16) . .
C28 Dy1 O11 C1 -2(16) . .
O13 C28 O12 Dy1 2(15) . .
C29 C28 O12 Dy1 -180(12) . .
O9 Dy1 O12 C28 -171(10) . .
O11 Dy1 O12 C28 87(9) . .
O14 Dy1 O12 C28 -81(9) . .
O25 Dy1 O12 C28 15(11) 2_666 .
O10 Dy1 O12 C28 128(9) . .
O26 Dy1 O12 C28 -107(10) . .
O13 Dy1 O12 C28 -1(8) . .
O12 C28 O13 Dy1 -1(14) . .
C29 C28 O13 Dy1 180(13) . .
O9 Dy1 O13 C28 13(10) . .
O11 Dy1 O13 C28 -76(9) . .
O14 Dy1 O13 C28 87(9) . .
O25 Dy1 O13 C28 -166(9) 2_666 .
O10 Dy1 O13 C28 -118(9) . .
O12 Dy1 O13 C28 1(8) . .
O26 Dy1 O13 C28 132(8) . .
O25 C35 O14 Dy1 100(25) . .
C36 C35 O14 Dy1 -78(28) . .
O9 Dy1 O14 C35 128(25) . .
O11 Dy1 O14 C35 30(28) . .
O25 Dy1 O14 C35 -75(25) 2_666 .
O10 Dy1 O14 C35 -159(22) . .
O12 Dy1 O14 C35 52(24) . .
O26 Dy1 O14 C35 -146(25) . .
O13 Dy1 O14 C35 -3(24) . .
C28 Dy1 O14 C35 25(24) . .
O14 C35 O25 Dy1 -40(21) . 2_666
C36 C35 O25 Dy1 137(12) . 2_666
loop_
_platon_squeeze_void_nr
_platon_squeeze_void_average_x
_platon_squeeze_void_average_y
_platon_squeeze_void_average_z
_platon_squeeze_void_volume
_platon_squeeze_void_count_electrons
_platon_squeeze_void_content
1 -0.037 0.500 0.000 768 323 ' '
2 0.106 0.577 0.435 26 6 ' '
3 0.894 0.423 0.565 26 8 ' '
