#------------------------------------------------------------------------------
#$Date: 2016-03-25 15:56:59 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179944 $
#$URL: svn://www.crystallography.net/cod/cif/7/02/39/7023949.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7023949
loop_
_publ_author_name
'Bonuccelli, Veronica'
'Funaioli, Tiziana'
'Leoni, Piero'
'Marchetti, Lorella'
'Zacchini, Stefano'
_publ_section_title
;
 Bridging molecular clusters and fullerene.
;
_journal_issue                   48
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              16898
_journal_page_last               16908
_journal_paper_doi               10.1039/c3dt52055b
_journal_volume                  42
_journal_year                    2013
_chemical_formula_sum            'C35 H59 O3 P3 Pt3'
_chemical_formula_weight         1206.00
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           12
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2y'
_symmetry_space_group_name_H-M   'C 1 2/m 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 93.194(2)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   19.025(3)
_cell_length_b                   15.496(2)
_cell_length_c                   13.934(2)
_cell_measurement_reflns_used    9920
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      27.847
_cell_measurement_theta_min      2.201
_cell_volume                     4101.5(10)
_computing_cell_refinement       'APEX2 (Bruker AXS, 2006)'
_computing_data_collection       'APEX2 (Bruker AXS, 2006)'
_computing_data_reduction        'SAINT (Bruker AXS, 2004)'
_computing_molecular_graphics    'ORTEPII (Johnson, 1996)'
_computing_publication_material  'XCIF (Bruker AXS, 2001)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      100(2)
_diffrn_measured_fraction_theta_full 0.960
_diffrn_measured_fraction_theta_max 0.960
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0388
_diffrn_reflns_av_unetI/netI     0.0278
_diffrn_reflns_limit_h_max       22
_diffrn_reflns_limit_h_min       -22
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       16
_diffrn_reflns_limit_l_min       -16
_diffrn_reflns_number            18478
_diffrn_reflns_theta_full        25.03
_diffrn_reflns_theta_max         25.03
_diffrn_reflns_theta_min         1.70
_exptl_absorpt_coefficient_mu    10.354
_exptl_absorpt_correction_T_max  0.3955
_exptl_absorpt_correction_T_min  0.2881
_exptl_absorpt_correction_type   empirical
_exptl_absorpt_process_details
; 
 Data were corrected for Lorentz polarization and absorption
 effects (empirical absorption correction SADABS).
 R(int) =  0.1545 (selected reflections only, before parameter refinement)
 R(int) =  0.0556 (selected reflections only, after parameter refinement)
;
_exptl_crystal_colour            pale-yellow
_exptl_crystal_density_diffrn    1.953
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       plate
_exptl_crystal_F_000             2288
_exptl_crystal_size_max          0.16
_exptl_crystal_size_mid          0.12
_exptl_crystal_size_min          0.11
_refine_diff_density_max         5.830
_refine_diff_density_min         -1.700
_refine_diff_density_rms         0.271
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.083
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     224
_refine_ls_number_reflns         3632
_refine_ls_number_restraints     270
_refine_ls_restrained_S_all      1.058
_refine_ls_R_factor_all          0.0523
_refine_ls_R_factor_gt           0.0475
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0757P)²+122.9937P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1245
_refine_ls_wR_factor_ref         0.1286
_reflns_number_gt                3339
_reflns_number_total             3632
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c3dt52055b.txt
_cod_data_source_block           c2m
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 1891 2012-01-12 08:04:46Z andrius 
;
_cod_original_cell_volume        4101.4(11)
_cod_original_sg_symbol_H-M      C2/m
_cod_database_code               7023949
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z'
'-x, -y, -z'
'x, -y, z'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
C1 C 0.3164(7) 0.2049(9) 0.2488(11) 0.044(3) Uani 1 1 d U
C2 C 0.0395(8) 0.0000 0.2546(12) 0.027(2) Uani 1 2 d SU
C3 C -0.0245(8) 0.0000 0.2575(12) 0.028(2) Uani 1 2 d SU
C4 C -0.1023(8) 0.0000 0.2592(12) 0.0293(19) Uani 1 2 d SU
C5 C -0.1445(8) 0.0000 0.1745(12) 0.029(2) Uani 1 2 d SU
H5 H -0.1239 0.0000 0.1139 0.035 Uiso 1 2 calc SR
C6 C -0.2190(8) 0.0000 0.1801(11) 0.027(2) Uani 1 2 d SU
H6 H -0.2489 0.0000 0.1232 0.032 Uiso 1 2 calc SR
C7 C -0.2471(8) 0.0000 0.2693(11) 0.0254(19) Uani 1 2 d SU
C8 C -0.2051(8) 0.0000 0.3519(12) 0.029(2) Uani 1 2 d SU
H8 H -0.2258 0.0000 0.4124 0.034 Uiso 1 2 calc SR
C9 C -0.1326(9) 0.0000 0.3481(12) 0.030(2) Uani 1 2 d SU
H9 H -0.1035 0.0000 0.4058 0.036 Uiso 1 2 calc SR
C10 C -0.3244(8) 0.0000 0.2765(11) 0.023(2) Uani 1 2 d SU
H10 H -0.3412 0.0000 0.3395 0.028 Uiso 1 2 calc SR
C11 C 0.4201(8) 0.0000 0.3479(11) 0.026(3) Uani 1 2 d SU
C12 C 0.4672(7) 0.0800(10) 0.3500(10) 0.043(3) Uani 1 1 d U
H12A H 0.4379 0.1319 0.3441 0.064 Uiso 1 1 calc R
H12B H 0.4984 0.0775 0.2964 0.064 Uiso 1 1 calc R
H12C H 0.4955 0.0817 0.4109 0.064 Uiso 1 1 calc R
C13 C 0.3752(8) 0.0000 0.4369(11) 0.029(3) Uani 1 2 d SU
H13A H 0.3368 -0.0418 0.4275 0.043 Uiso 0.50 1 calc PR
H13B H 0.3556 0.0577 0.4458 0.043 Uiso 0.50 1 calc PR
H13C H 0.4049 -0.0159 0.4940 0.043 Uiso 0.50 1 calc PR
C14 C 0.3954(9) 0.0000 0.1190(11) 0.030(3) Uani 1 2 d SU
C15 C 0.4414(7) 0.0783(9) 0.1071(9) 0.037(3) Uani 1 1 d U
H15A H 0.4155 0.1304 0.1238 0.055 Uiso 1 1 calc R
H15B H 0.4545 0.0822 0.0402 0.055 Uiso 1 1 calc RD
H15C H 0.4840 0.0732 0.1495 0.055 Uiso 1 1 calc R
C16 C 0.3344(9) 0.0000 0.0459(12) 0.032(3) Uani 1 2 d SU
H16A H 0.2983 0.0403 0.0660 0.048 Uiso 0.50 1 calc PR
H16B H 0.3145 -0.0582 0.0406 0.048 Uiso 0.50 1 calc PR
H16C H 0.3507 0.0180 -0.0165 0.048 Uiso 0.50 1 calc PR
C17 C 0.1310(6) 0.2018(8) 0.3681(8) 0.030(2) Uani 1 1 d U
C18 C 0.1514(6) 0.2980(8) 0.3652(9) 0.033(2) Uani 1 1 d U
H18A H 0.1186 0.3286 0.3204 0.049 Uiso 1 1 calc R
H18B H 0.1994 0.3036 0.3439 0.049 Uiso 1 1 calc R
H18C H 0.1490 0.3229 0.4296 0.049 Uiso 1 1 calc R
C19 C 0.1763(7) 0.1572(8) 0.4478(9) 0.035(2) Uani 1 1 d U
H19A H 0.2261 0.1695 0.4393 0.053 Uiso 1 1 calc R
H19B H 0.1684 0.0948 0.4445 0.053 Uiso 1 1 calc R
H19C H 0.1634 0.1788 0.5105 0.053 Uiso 1 1 calc R
C20 C 0.0540(6) 0.1908(9) 0.3895(9) 0.037(3) Uani 1 1 d U
H20A H 0.0242 0.2194 0.3393 0.056 Uiso 1 1 calc R
H20B H 0.0456 0.2167 0.4520 0.056 Uiso 1 1 calc R
H20C H 0.0424 0.1292 0.3908 0.056 Uiso 1 1 calc R
C21 C 0.1154(7) 0.2017(9) 0.1414(9) 0.037(2) Uani 1 1 d U
C22 C 0.1614(8) 0.2824(9) 0.1165(10) 0.046(3) Uani 1 1 d U
H22A H 0.2113 0.2690 0.1301 0.069 Uiso 1 1 calc R
H22B H 0.1482 0.3317 0.1557 0.069 Uiso 1 1 calc R
H22C H 0.1533 0.2967 0.0483 0.069 Uiso 1 1 calc R
C23 C 0.1253(7) 0.1374(9) 0.0578(9) 0.041(3) Uani 1 1 d U
H23A H 0.0978 0.0851 0.0680 0.061 Uiso 1 1 calc R
H23B H 0.1752 0.1224 0.0557 0.061 Uiso 1 1 calc R
H23C H 0.1091 0.1642 -0.0032 0.061 Uiso 1 1 calc R
C24 C 0.0401(7) 0.2250(10) 0.1462(10) 0.046(3) Uani 1 1 d U
H24A H 0.0153 0.1784 0.1778 0.069 Uiso 1 1 calc R
H24B H 0.0192 0.2333 0.0810 0.069 Uiso 1 1 calc R
H24C H 0.0361 0.2785 0.1829 0.069 Uiso 1 1 calc R
O1 O 0.3465(5) 0.2689(7) 0.2491(9) 0.061(3) Uani 1 1 d U
O2 O -0.3687(5) 0.0000 0.2102(8) 0.028(2) Uani 1 2 d SU
P1 P 0.35537(18) 0.0000 0.2402(3) 0.0198(7) Uani 1 2 d S
P2 P 0.15246(13) 0.14578(16) 0.2535(2) 0.0218(5) Uani 1 1 d .
Pt1 Pt 0.14097(3) 0.0000 0.25428(5) 0.02346(17) Uani 1 2 d S
Pt2 Pt 0.267686(18) 0.10274(2) 0.24841(3) 0.02135(16) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O1 C1 Pt2 179.7(14) . .
C3 C2 Pt1 178.2(15) . .
C2 C3 C4 179.1(18) . .
C5 C4 C9 120.5(15) . .
C5 C4 C3 121.0(15) . .
C9 C4 C3 118.5(14) . .
C4 C5 C6 118.9(15) . .
C4 C5 H5 120.6 . .
C6 C5 H5 120.6 . .
C7 C6 C5 119.1(15) . .
C7 C6 H6 120.5 . .
C5 C6 H6 120.5 . .
C8 C7 C6 121.4(15) . .
C8 C7 C10 118.7(14) . .
C6 C7 C10 119.8(14) . .
C7 C8 C9 120.4(16) . .
C7 C8 H8 119.8 . .
C9 C8 H8 119.8 . .
C8 C9 C4 119.7(15) . .
C8 C9 H9 120.1 . .
C4 C9 H9 120.1 . .
O2 C10 C7 126.7(14) . .
O2 C10 H10 116.6 . .
C7 C10 H10 116.6 . .
C12 C11 C12 108.3(15) . 6
C12 C11 C13 109.5(9) . .
C12 C11 C13 109.5(9) 6 .
C12 C11 P1 111.8(8) . .
C12 C11 P1 111.8(8) 6 .
C13 C11 P1 105.9(10) . .
C11 C12 H12A 109.5 . .
C11 C12 H12B 109.5 . .
H12A C12 H12B 109.5 . .
C11 C12 H12C 109.5 . .
H12A C12 H12C 109.5 . .
H12B C12 H12C 109.5 . .
C11 C13 H13A 109.5 . .
C11 C13 H13B 109.5 . .
H13A C13 H13B 109.5 . .
C11 C13 H13C 109.5 . .
H13A C13 H13C 109.5 . .
H13B C13 H13C 109.5 . .
C16 C14 C15 110.8(9) . .
C16 C14 C15 110.8(9) . 6
C15 C14 C15 106.8(14) . 6
C16 C14 P1 105.8(11) . .
C15 C14 P1 111.3(8) . .
C15 C14 P1 111.3(8) 6 .
C14 C15 H15A 109.5 . .
C14 C15 H15B 109.5 . .
H15A C15 H15B 109.5 . .
C14 C15 H15C 109.5 . .
H15A C15 H15C 109.5 . .
H15B C15 H15C 109.5 . .
C14 C16 H16A 109.5 . .
C14 C16 H16B 109.5 . .
H16A C16 H16B 109.5 . .
C14 C16 H16C 109.5 . .
H16A C16 H16C 109.5 . .
H16B C16 H16C 109.5 . .
C20 C17 C19 108.4(10) . .
C20 C17 C18 111.1(10) . .
C19 C17 C18 108.9(10) . .
C20 C17 P2 111.8(8) . .
C19 C17 P2 105.5(8) . .
C18 C17 P2 111.0(8) . .
C17 C18 H18A 109.5 . .
C17 C18 H18B 109.5 . .
H18A C18 H18B 109.5 . .
C17 C18 H18C 109.5 . .
H18A C18 H18C 109.5 . .
H18B C18 H18C 109.5 . .
C17 C19 H19A 109.5 . .
C17 C19 H19B 109.5 . .
H19A C19 H19B 109.5 . .
C17 C19 H19C 109.5 . .
H19A C19 H19C 109.5 . .
H19B C19 H19C 109.5 . .
C17 C20 H20A 109.5 . .
C17 C20 H20B 109.5 . .
H20A C20 H20B 109.5 . .
C17 C20 H20C 109.5 . .
H20A C20 H20C 109.5 . .
H20B C20 H20C 109.5 . .
C24 C21 C23 110.4(11) . .
C24 C21 C22 111.6(12) . .
C23 C21 C22 104.6(11) . .
C24 C21 P2 113.0(9) . .
C23 C21 P2 105.7(9) . .
C22 C21 P2 111.1(9) . .
C21 C22 H22A 109.5 . .
C21 C22 H22B 109.5 . .
H22A C22 H22B 109.5 . .
C21 C22 H22C 109.5 . .
H22A C22 H22C 109.5 . .
H22B C22 H22C 109.5 . .
C21 C23 H23A 109.5 . .
C21 C23 H23B 109.5 . .
H23A C23 H23B 109.5 . .
C21 C23 H23C 109.5 . .
H23A C23 H23C 109.5 . .
H23B C23 H23C 109.5 . .
C21 C24 H24A 109.5 . .
C21 C24 H24B 109.5 . .
H24A C24 H24B 109.5 . .
C21 C24 H24C 109.5 . .
H24A C24 H24C 109.5 . .
H24B C24 H24C 109.5 . .
C14 P1 C11 115.6(7) . .
C14 P1 Pt2 111.8(4) . 6
C11 P1 Pt2 113.6(3) . 6
C14 P1 Pt2 111.8(4) . .
C11 P1 Pt2 113.6(3) . .
Pt2 P1 Pt2 86.97(12) 6 .
C17 P2 C21 113.6(5) . .
C17 P2 Pt1 115.4(4) . .
C21 P2 Pt1 115.4(4) . .
C17 P2 Pt2 114.4(4) . .
C21 P2 Pt2 114.9(4) . .
Pt1 P2 Pt2 78.66(8) . .
C2 Pt1 P2 95.54(7) . .
C2 Pt1 P2 95.54(7) . 6
P2 Pt1 P2 168.90(13) . 6
C2 Pt1 Pt2 146.58(3) . .
P2 Pt1 Pt2 51.08(7) . .
P2 Pt1 Pt2 117.83(7) 6 .
C2 Pt1 Pt2 146.58(3) . 6
P2 Pt1 Pt2 117.83(7) . 6
P2 Pt1 Pt2 51.08(7) 6 6
Pt2 Pt1 Pt2 66.75(2) . 6
C1 Pt2 P2 103.4(4) . .
C1 Pt2 P1 103.2(4) . .
P2 Pt2 P1 153.34(9) . .
C1 Pt2 Pt1 153.6(4) . .
P2 Pt2 Pt1 50.26(7) . .
P1 Pt2 Pt1 103.12(6) . .
C1 Pt2 Pt2 149.7(4) . 6
P2 Pt2 Pt2 106.88(7) . 6
P1 Pt2 Pt2 46.51(6) . 6
Pt1 Pt2 Pt2 56.626(11) . 6
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
C1 O1 1.145(17) .
C1 Pt2 1.834(14) .
C2 C3 1.22(2) .
C2 Pt1 1.931(15) .
C3 C4 1.48(2) .
C4 C5 1.39(2) .
C4 C9 1.39(2) .
C5 C6 1.42(2) .
C5 H5 0.9500 .
C6 C7 1.38(2) .
C6 H6 0.9500 .
C7 C8 1.36(2) .
C7 C10 1.48(2) .
C8 C9 1.38(2) .
C8 H8 0.9500 .
C9 H9 0.9500 .
C10 O2 1.215(18) .
C10 H10 0.9500 .
C11 C12 1.528(16) .
C11 C12 1.528(16) 6
C11 C13 1.54(2) .
C11 P1 1.888(15) .
C12 H12A 0.9800 .
C12 H12B 0.9800 .
C12 H12C 0.9800 .
C13 H13A 0.9800 .
C13 H13B 0.9800 .
C13 H13C 0.9800 .
C14 C16 1.50(2) .
C14 C15 1.512(16) .
C14 C15 1.512(16) 6
C14 P1 1.890(16) .
C15 H15A 0.9800 .
C15 H15B 0.9800 .
C15 H15C 0.9800 .
C16 H16A 0.9800 .
C16 H16B 0.9800 .
C16 H16C 0.9800 .
C17 C20 1.522(16) .
C17 C19 1.532(16) .
C17 C18 1.540(17) .
C17 P2 1.883(11) .
C18 H18A 0.9800 .
C18 H18B 0.9800 .
C18 H18C 0.9800 .
C19 H19A 0.9800 .
C19 H19B 0.9800 .
C19 H19C 0.9800 .
C20 H20A 0.9800 .
C20 H20B 0.9800 .
C20 H20C 0.9800 .
C21 C24 1.481(19) .
C21 C23 1.553(18) .
C21 C22 1.576(19) .
C21 P2 1.889(13) .
C22 H22A 0.9800 .
C22 H22B 0.9800 .
C22 H22C 0.9800 .
C23 H23A 0.9800 .
C23 H23B 0.9800 .
C23 H23C 0.9800 .
C24 H24A 0.9800 .
C24 H24B 0.9800 .
C24 H24C 0.9800 .
P1 Pt2 2.313(3) 6
P1 Pt2 2.313(3) .
P2 Pt1 2.270(3) .
P2 Pt2 2.296(3) .
Pt1 P2 2.270(3) 6
Pt1 Pt2 2.8940(7) .
Pt1 Pt2 2.8940(7) 6
Pt2 Pt2 3.1840(9) 6
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
Pt1 C2 C3 C4 180.00(7) . .
C2 C3 C4 C5 0.00(9) . .
C2 C3 C4 C9 180.00(9) . .
C9 C4 C5 C6 0.000(1) . .
C3 C4 C5 C6 180.000(1) . .
C4 C5 C6 C7 0.000(1) . .
C5 C6 C7 C8 0.000(2) . .
C5 C6 C7 C10 180.0 . .
C6 C7 C8 C9 0.000(2) . .
C10 C7 C8 C9 180.000(2) . .
C7 C8 C9 C4 0.000(2) . .
C5 C4 C9 C8 0.000(2) . .
C3 C4 C9 C8 180.000(2) . .
C8 C7 C10 O2 180.000(1) . .
C6 C7 C10 O2 0.000(2) . .
C16 C14 P1 C11 180.0 . .
C15 C14 P1 C11 -59.5(9) . .
C15 C14 P1 C11 59.5(9) 6 .
C16 C14 P1 Pt2 47.84(18) . 6
C15 C14 P1 Pt2 168.3(8) . 6
C15 C14 P1 Pt2 -72.6(11) 6 6
C16 C14 P1 Pt2 -47.84(18) . .
C15 C14 P1 Pt2 72.6(11) . .
C15 C14 P1 Pt2 -168.3(8) 6 .
C12 C11 P1 C14 60.8(10) . .
C12 C11 P1 C14 -60.8(10) 6 .
C13 C11 P1 C14 180.000(1) . .
C12 C11 P1 Pt2 -167.9(9) . 6
C12 C11 P1 Pt2 70.5(11) 6 6
C13 C11 P1 Pt2 -48.69(19) . 6
C12 C11 P1 Pt2 -70.5(11) . .
C12 C11 P1 Pt2 167.9(9) 6 .
C13 C11 P1 Pt2 48.69(19) . .
C20 C17 P2 C21 72.6(10) . .
C19 C17 P2 C21 -169.8(8) . .
C18 C17 P2 C21 -52.0(10) . .
C20 C17 P2 Pt1 -64.1(9) . .
C19 C17 P2 Pt1 53.5(9) . .
C18 C17 P2 Pt1 171.3(7) . .
C20 C17 P2 Pt2 -152.8(7) . .
C19 C17 P2 Pt2 -35.1(9) . .
C18 C17 P2 Pt2 82.6(8) . .
C24 C21 P2 C17 -48.1(11) . .
C23 C21 P2 C17 -168.9(8) . .
C22 C21 P2 C17 78.2(10) . .
C24 C21 P2 Pt1 88.6(10) . .
C23 C21 P2 Pt1 -32.2(10) . .
C22 C21 P2 Pt1 -145.1(8) . .
C24 C21 P2 Pt2 177.5(8) . .
C23 C21 P2 Pt2 56.7(9) . .
C22 C21 P2 Pt2 -56.2(10) . .
C3 C2 Pt1 P2 -90.27(10) . .
C3 C2 Pt1 P2 90.27(11) . 6
C3 C2 Pt1 Pt2 -92.7(8) . .
C3 C2 Pt1 Pt2 92.7(8) . 6
C17 P2 Pt1 C2 70.0(6) . .
C21 P2 Pt1 C2 -65.9(7) . .
Pt2 P2 Pt1 C2 -178.3(5) . .
C17 P2 Pt1 P2 -112.8(8) . 6
C21 P2 Pt1 P2 111.3(8) . 6
Pt2 P2 Pt1 P2 -1.1(8) . 6
C17 P2 Pt1 Pt2 -111.7(4) . .
C21 P2 Pt1 Pt2 112.4(5) . .
C17 P2 Pt1 Pt2 -111.9(4) . 6
C21 P2 Pt1 Pt2 112.2(5) . 6
Pt2 P2 Pt1 Pt2 -0.13(10) . 6
O1 C1 Pt2 P2 19(100) . .
O1 C1 Pt2 P1 -162(100) . .
O1 C1 Pt2 Pt1 17(100) . .
O1 C1 Pt2 Pt2 -159(100) . 6
C17 P2 Pt2 C1 -65.8(6) . .
C21 P2 Pt2 C1 68.3(7) . .
Pt1 P2 Pt2 C1 -178.8(5) . .
C17 P2 Pt2 P1 116.4(5) . .
C21 P2 Pt2 P1 -109.5(5) . .
Pt1 P2 Pt2 P1 3.5(3) . .
C17 P2 Pt2 Pt1 113.0(4) . .
C21 P2 Pt2 Pt1 -112.9(5) . .
C17 P2 Pt2 Pt2 113.1(4) . 6
C21 P2 Pt2 Pt2 -112.8(5) . 6
Pt1 P2 Pt2 Pt2 0.11(8) . 6
C14 P1 Pt2 C1 -69.9(7) . .
C11 P1 Pt2 C1 63.3(6) . .
Pt2 P1 Pt2 C1 177.8(5) 6 .
C14 P1 Pt2 P2 107.9(5) . .
C11 P1 Pt2 P2 -119.0(5) . .
Pt2 P1 Pt2 P2 -4.4(3) 6 .
C14 P1 Pt2 Pt1 110.6(4) . .
C11 P1 Pt2 Pt1 -116.2(4) . .
Pt2 P1 Pt2 Pt1 -1.70(11) 6 .
C14 P1 Pt2 Pt2 112.3(4) . 6
C11 P1 Pt2 Pt2 -114.5(4) . 6
C2 Pt1 Pt2 C1 5.8(14) . .
P2 Pt1 Pt2 C1 2.7(11) . .
P2 Pt1 Pt2 C1 -177.6(11) 6 .
Pt2 Pt1 Pt2 C1 -177.5(11) 6 .
C2 Pt1 Pt2 P2 3.2(9) . .
P2 Pt1 Pt2 P2 179.76(17) 6 .
Pt2 Pt1 Pt2 P2 179.87(9) 6 .
C2 Pt1 Pt2 P1 -175.2(9) . .
P2 Pt1 Pt2 P1 -178.40(13) . .
P2 Pt1 Pt2 P1 1.36(13) 6 .
Pt2 Pt1 Pt2 P1 1.47(10) 6 .
C2 Pt1 Pt2 Pt2 -176.7(9) . 6
P2 Pt1 Pt2 Pt2 -179.87(9) . 6
P2 Pt1 Pt2 Pt2 -0.11(8) 6 6
