#------------------------------------------------------------------------------
#$Date: 2016-03-25 15:59:31 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179946 $
#$URL: svn://www.crystallography.net/cod/cif/7/02/41/7024156.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7024156
loop_
_publ_author_name
'Szłyk, Edward'
'Szczesny, Robert'
'Wojtczak, Andrzej'
_publ_section_title
;
 X-Ray structural and gas phase studies of silver(i) perfluorinated
 carboxylate complexes with 2,2'-bipyridyl as potential precursors for
 chemical vapour deposition (CVD).
;
_journal_issue                   7
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              1823
_journal_page_last               1830
_journal_paper_doi               10.1039/b911741e
_journal_volume                  39
_journal_year                    2010
_chemical_formula_sum            'C64 H32 Ag6 F41 N8 O12'
_chemical_formula_weight         2531.20
_chemical_name_common
(tetra(2,2'-bipyridine)hexasilver(i)hexa(heptafluorbutyrate))
_chemical_name_systematic
;
[tetra(2,2'-bipyridine)hexasilver(I)hexa(heptafluorbutyrate)]
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 103.15(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   16.476(3)
_cell_length_b                   29.367(6)
_cell_length_c                   17.436(3)
_cell_measurement_reflns_used    8055
_cell_measurement_temperature    292(2)
_cell_measurement_theta_max      30.91
_cell_measurement_theta_min      2.07
_cell_volume                     8215(3)
_computing_cell_refinement       'Oxford Diffraction CrysAlis'
_computing_data_collection       'Oxford Diffraction CrysAlis'
_computing_data_reduction        'Oxford Diffraction CrysAlis'
_computing_molecular_graphics    'PLATON (Spek, 1990)'
_computing_publication_material  'CIFTAB (Sheldrick, 1997)'
_computing_structure_refinement  'SHELX-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELX-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      292(2)
_diffrn_detector_area_resol_mean 8.2564
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'Oxford Sapphire CCD'
_diffrn_measurement_method       θ/2θ
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.1202
_diffrn_reflns_av_sigmaI/netI    0.0920
_diffrn_reflns_limit_h_max       18
_diffrn_reflns_limit_h_min       -18
_diffrn_reflns_limit_k_max       28
_diffrn_reflns_limit_k_min       -32
_diffrn_reflns_limit_l_max       19
_diffrn_reflns_limit_l_min       -19
_diffrn_reflns_number            48538
_diffrn_reflns_theta_full        23.50
_diffrn_reflns_theta_max         23.50
_diffrn_reflns_theta_min         2.07
_diffrn_standards_decay_%        0
_diffrn_standards_interval_count 0
_diffrn_standards_interval_time  0
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    1.557
_exptl_absorpt_correction_T_max  0.8962
_exptl_absorpt_correction_T_min  0.7756
_exptl_absorpt_correction_type   numerical
_exptl_absorpt_process_details   'Oxford Diffraction CrysAlis'
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    2.047
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       plate
_exptl_crystal_F_000             4876
_exptl_crystal_size_max          0.17
_exptl_crystal_size_mid          0.16
_exptl_crystal_size_min          0.07
_refine_diff_density_max         1.000
_refine_diff_density_min         -0.777
_refine_diff_density_rms         0.132
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.155
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1306
_refine_ls_number_reflns         12155
_refine_ls_number_restraints     1247
_refine_ls_restrained_S_all      1.134
_refine_ls_R_factor_all          0.1693
_refine_ls_R_factor_gt           0.1079
_refine_ls_shift/su_max          0.003
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0904P)²+48.7850P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2206
_refine_ls_wR_factor_ref         0.2595
_reflns_number_gt                7500
_reflns_number_total             12155
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b911741e.txt
_cod_data_source_block           szcz4
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 1891 2012-01-12 08:04:46Z andrius 
;
_cod_original_sg_symbol_H-M      P2(1)/n
_cod_database_code               7024156
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.30320(7) 0.18856(4) 0.54517(7) 0.0591(4) Uani 1 1 d . . .
Ag2 Ag 0.46336(7) 0.17998(4) 0.49988(7) 0.0601(4) Uani 1 1 d . . .
Ag3 Ag 0.62879(9) 0.24052(5) 0.50860(9) 0.0750(4) Uani 1 1 d . . .
Ag4 Ag 0.78415(8) 0.17453(4) 0.50622(8) 0.0644(4) Uani 1 1 d . . .
Ag5 Ag 0.94725(7) 0.18405(4) 0.46553(7) 0.0584(4) Uani 1 1 d . . .
Ag6 Ag 1.12513(9) 0.14974(6) 0.50926(10) 0.0927(5) Uani 1 1 d . . .
N1 N 0.2729(7) 0.1813(5) 0.4121(7) 0.057(3) Uani 1 1 d U . .
C1 C 0.2415(10) 0.2165(6) 0.3670(10) 0.073(5) Uani 1 1 d U . .
H1A H 0.2367 0.2442 0.3915 0.088 Uiso 1 1 calc R . .
C2 C 0.2162(11) 0.2143(8) 0.2878(11) 0.084(5) Uani 1 1 d U . .
H2A H 0.1961 0.2400 0.2584 0.101 Uiso 1 1 calc R . .
C3 C 0.2211(11) 0.1730(8) 0.2519(11) 0.086(6) Uani 1 1 d U . .
H3A H 0.2035 0.1699 0.1975 0.103 Uiso 1 1 calc R . .
C4 C 0.2512(11) 0.1380(7) 0.2961(10) 0.075(5) Uani 1 1 d U . .
H4A H 0.2536 0.1095 0.2734 0.090 Uiso 1 1 calc R . .
C5 C 0.2793(9) 0.1436(6) 0.3762(9) 0.060(4) Uani 1 1 d U . .
C6 C 0.3173(11) 0.1050(5) 0.4265(10) 0.061(4) Uani 1 1 d U . .
C7 C 0.2834(13) 0.0617(7) 0.4163(13) 0.092(6) Uani 1 1 d U . .
H7A H 0.2347 0.0561 0.3785 0.110 Uiso 1 1 calc R . .
C8 C 0.3235(16) 0.0272(7) 0.4635(15) 0.103(7) Uani 1 1 d U . .
H8A H 0.3005 -0.0019 0.4579 0.123 Uiso 1 1 calc R . .
C9 C 0.3997(14) 0.0347(7) 0.5212(14) 0.097(6) Uani 1 1 d U . .
H9A H 0.4276 0.0111 0.5520 0.116 Uiso 1 1 calc R . .
C10 C 0.4287(11) 0.0780(5) 0.5280(11) 0.072(5) Uani 1 1 d U . .
H10A H 0.4770 0.0848 0.5656 0.087 Uiso 1 1 calc R . .
N2 N 0.3877(8) 0.1123(4) 0.4803(8) 0.057(3) Uani 1 1 d U . .
N3 N 0.4164(7) 0.2214(5) 0.6309(7) 0.065(4) Uani 1 1 d U . .
C11 C 0.4364(11) 0.2015(7) 0.7043(9) 0.084(5) Uani 1 1 d U . .
H11A H 0.4218 0.1715 0.7110 0.101 Uiso 1 1 calc R . .
C12 C 0.4784(12) 0.2267(8) 0.7677(11) 0.095(6) Uani 1 1 d U . .
H12A H 0.4844 0.2149 0.8181 0.114 Uiso 1 1 calc R . .
C13 C 0.5107(11) 0.2673(8) 0.7590(13) 0.093(6) Uani 1 1 d U . .
H13A H 0.5447 0.2819 0.8018 0.112 Uiso 1 1 calc R . .
C14 C 0.4926(12) 0.2877(7) 0.6848(12) 0.085(5) Uani 1 1 d U . .
H14A H 0.5110 0.3170 0.6780 0.102 Uiso 1 1 calc R . .
C15 C 0.4465(8) 0.2632(5) 0.6210(10) 0.057(4) Uani 1 1 d U . .
C16 C 0.4247(8) 0.2823(5) 0.5427(11) 0.057(4) Uani 1 1 d U . .
C17 C 0.4004(12) 0.3266(7) 0.5251(15) 0.102(7) Uani 1 1 d U . .
H17A H 0.3944 0.3460 0.5656 0.122 Uiso 1 1 calc R . .
C18 C 0.3852(13) 0.3425(8) 0.4516(18) 0.110(7) Uani 1 1 d U . .
H18A H 0.3661 0.3722 0.4410 0.132 Uiso 1 1 calc R . .
C19 C 0.3973(14) 0.3159(9) 0.3929(15) 0.111(7) Uani 1 1 d U . .
H19A H 0.3877 0.3270 0.3417 0.133 Uiso 1 1 calc R . .
C20 C 0.4238(11) 0.2723(7) 0.4088(13) 0.089(6) Uani 1 1 d U . .
H20A H 0.4314 0.2535 0.3681 0.107 Uiso 1 1 calc R . .
N4 N 0.4388(7) 0.2563(4) 0.4818(8) 0.059(3) Uani 1 1 d U . .
N5 N 0.8144(7) 0.2477(4) 0.5332(8) 0.063(3) Uani 1 1 d U . .
C21 C 0.8343(10) 0.2624(8) 0.6086(11) 0.093(6) Uani 1 1 d U . .
H21A H 0.8286 0.2428 0.6489 0.111 Uiso 1 1 calc R . .
C22 C 0.8635(12) 0.3069(9) 0.6271(15) 0.115(8) Uani 1 1 d U . .
H22A H 0.8745 0.3174 0.6788 0.138 Uiso 1 1 calc R . .
C23 C 0.8754(13) 0.3347(8) 0.5666(18) 0.119(8) Uani 1 1 d U . .
H23A H 0.8969 0.3638 0.5783 0.143 Uiso 1 1 calc R . .
C24 C 0.8568(12) 0.3208(7) 0.4922(15) 0.101(7) Uani 1 1 d U . .
H24A H 0.8647 0.3397 0.4517 0.122 Uiso 1 1 calc R . .
C25 C 0.8255(9) 0.2776(6) 0.4772(11) 0.064(4) Uani 1 1 d U . .
C26 C 0.8059(10) 0.2603(6) 0.3943(11) 0.071(5) Uani 1 1 d U . .
C27 C 0.7602(12) 0.2864(8) 0.3337(12) 0.092(6) Uani 1 1 d U . .
H27A H 0.7410 0.3153 0.3424 0.110 Uiso 1 1 calc R . .
C28 C 0.7449(11) 0.2677(8) 0.2606(13) 0.096(6) Uani 1 1 d U . .
H28A H 0.7148 0.2847 0.2188 0.115 Uiso 1 1 calc R . .
C29 C 0.7711(12) 0.2252(8) 0.2449(12) 0.099(6) Uani 1 1 d U . .
H29A H 0.7597 0.2126 0.1947 0.118 Uiso 1 1 calc R . .
C30 C 0.8146(11) 0.2035(7) 0.3085(10) 0.077(5) Uani 1 1 d U . .
H30A H 0.8333 0.1744 0.3002 0.093 Uiso 1 1 calc R . .
N6 N 0.8337(8) 0.2184(5) 0.3804(7) 0.060(3) Uani 1 1 d U . .
N7 N 0.8545(8) 0.1048(5) 0.5148(7) 0.064(4) Uani 1 1 d U . .
C31 C 0.8178(12) 0.0736(6) 0.4651(12) 0.083(5) Uani 1 1 d U . .
H31A H 0.7726 0.0825 0.4255 0.099 Uiso 1 1 calc R . .
C32 C 0.8413(13) 0.0296(7) 0.4675(13) 0.090(6) Uani 1 1 d U . .
H32A H 0.8141 0.0079 0.4319 0.108 Uiso 1 1 calc R . .
C33 C 0.9093(15) 0.0196(7) 0.5272(15) 0.101(6) Uani 1 1 d U . .
H33A H 0.9282 -0.0103 0.5324 0.121 Uiso 1 1 calc R . .
C34 C 0.9495(15) 0.0504(8) 0.5781(14) 0.098(6) Uani 1 1 d U . .
H34A H 0.9962 0.0422 0.6166 0.118 Uiso 1 1 calc R . .
C35 C 0.9206(11) 0.0946(6) 0.5724(11) 0.072(5) Uani 1 1 d U . .
C36 C 0.9634(9) 0.1295(7) 0.6287(10) 0.069(5) Uani 1 1 d U . .
C37 C 0.9886(12) 0.1185(8) 0.7069(11) 0.094(6) Uani 1 1 d U . .
H37A H 0.9809 0.0896 0.7258 0.112 Uiso 1 1 calc R . .
C38 C 1.0255(16) 0.1526(11) 0.7548(14) 0.127(8) Uani 1 1 d U . .
H38A H 1.0449 0.1468 0.8083 0.152 Uiso 1 1 calc R . .
C39 C 1.0347(12) 0.1944(10) 0.7269(13) 0.109(7) Uani 1 1 d U . .
H39A H 1.0554 0.2181 0.7612 0.131 Uiso 1 1 calc R . .
C40 C 1.0135(10) 0.2015(8) 0.6479(10) 0.092(6) Uani 1 1 d U . .
H40A H 1.0257 0.2295 0.6284 0.111 Uiso 1 1 calc R . .
N8 N 0.9759(8) 0.1701(6) 0.5977(8) 0.073(4) Uani 1 1 d U . .
O1A O 0.1699(11) 0.0991(6) 0.6086(10) 0.140(6) Uani 1 1 d U . .
O2A O 0.2830(10) 0.1364(5) 0.6413(9) 0.122(5) Uani 1 1 d U . .
C1A C 0.2368(17) 0.1092(8) 0.6468(13) 0.103(7) Uani 1 1 d U . .
C2A C 0.261(2) 0.0763(9) 0.7242(17) 0.144(9) Uani 1 1 d U . .
F1A F 0.2205(12) 0.0973(8) 0.7843(11) 0.207(9) Uani 1 1 d U . .
F2A F 0.2292(19) 0.0359(7) 0.7031(13) 0.301(15) Uani 1 1 d U . .
C3A C 0.346(3) 0.0721(10) 0.7680(19) 0.172(10) Uani 1 1 d U . .
F3A F 0.3695(16) 0.0555(8) 0.7032(12) 0.261(13) Uani 1 1 d U . .
F4A F 0.3616(15) 0.1145(6) 0.7950(10) 0.210(9) Uani 1 1 d U . .
C4A C 0.349(4) 0.0403(17) 0.840(3) 0.204(13) Uani 1 1 d U . .
F5A F 0.435(2) 0.0373(11) 0.8566(16) 0.266(13) Uani 1 1 d U . .
F6A F 0.3282(19) 0.0520(11) 0.8924(13) 0.301(16) Uani 1 1 d U . .
F7A F 0.341(2) -0.0012(7) 0.8145(16) 0.258(12) Uani 1 1 d U . .
O1B O 0.5724(8) 0.1484(5) 0.5950(8) 0.111(5) Uani 1 1 d U A .
O2B O 0.6828(8) 0.1905(5) 0.6132(7) 0.099(4) Uani 1 1 d U A .
C1B C 0.6470(11) 0.1576(8) 0.6324(8) 0.109(7) Uani 1 1 d DU . .
C2B C 0.6721(13) 0.1325(10) 0.7085(14) 0.171(11) Uani 0.55 1 d PDU A 1
F1B F 0.7390(19) 0.1515(9) 0.7570(13) 0.221(17) Uani 0.55 1 d PDU A 1
F2B F 0.6108(18) 0.1305(10) 0.7482(14) 0.167(11) Uani 0.55 1 d PDU A 1
C3B C 0.6920(13) 0.0853(7) 0.6843(11) 0.213(12) Uani 0.55 1 d PDU A 1
F3B F 0.7378(19) 0.0871(10) 0.6296(14) 0.157(12) Uani 0.55 1 d PDU A 1
F4B F 0.6197(16) 0.0634(10) 0.650(2) 0.26(2) Uani 0.55 1 d PDU A 1
C4B C 0.7360(16) 0.0572(8) 0.7550(12) 0.235(14) Uani 0.55 1 d PDU A 1
F6B F 0.766(3) 0.0191(10) 0.733(2) 0.237(17) Uani 0.55 1 d PDU A 1
F5B F 0.684(3) 0.0454(19) 0.800(2) 0.28(2) Uani 0.55 1 d PDU A 1
F7B F 0.798(3) 0.0790(12) 0.801(2) 0.26(2) Uani 0.55 1 d PDU A 1
C2BB C 0.7015(13) 0.1340(12) 0.7008(15) 0.175(12) Uani 0.45 1 d PDU A 2
F1BB F 0.6915(19) 0.1507(10) 0.7701(8) 0.144(12) Uani 0.45 1 d PDU A 2
F2BB F 0.7833(9) 0.1370(10) 0.7006(16) 0.131(11) Uani 0.45 1 d PDU A 2
C3BB C 0.6771(15) 0.0833(8) 0.6954(14) 0.210(12) Uani 0.45 1 d PDU A 2
F3BB F 0.672(3) 0.0693(11) 0.6205(14) 0.218(19) Uani 0.45 1 d PDU A 2
F4BB F 0.6008(15) 0.0788(12) 0.710(2) 0.196(16) Uani 0.45 1 d PDU A 2
C4BB C 0.7396(17) 0.0540(9) 0.7519(17) 0.233(14) Uani 0.45 1 d PDU A 2
F6BB F 0.714(3) 0.0116(9) 0.753(3) 0.26(2) Uani 0.45 1 d PDU A 2
F5BB F 0.753(3) 0.0691(15) 0.8249(15) 0.191(17) Uani 0.45 1 d PDU A 2
F7BB F 0.813(2) 0.053(2) 0.733(3) 0.27(2) Uani 0.45 1 d PDU A 2
O1C O 0.5667(8) 0.1963(5) 0.4017(8) 0.091(4) Uani 1 1 d U . .
O2C O 0.6727(8) 0.1481(5) 0.4078(8) 0.106(5) Uani 1 1 d U . .
C1C C 0.6052(13) 0.1644(7) 0.3828(10) 0.078(5) Uani 1 1 d U . .
C2C C 0.5561(15) 0.1370(9) 0.3089(14) 0.113(7) Uani 1 1 d U . .
F1C F 0.5697(14) 0.1499(7) 0.2465(8) 0.212(10) Uani 1 1 d U . .
F2C F 0.4629(9) 0.1466(5) 0.3050(9) 0.160(6) Uani 1 1 d U . .
C3C C 0.5450(14) 0.0872(10) 0.3208(18) 0.115(7) Uani 1 1 d U . .
F3C F 0.6199(9) 0.0675(6) 0.3186(11) 0.183(8) Uani 1 1 d U . .
F4C F 0.5401(11) 0.0789(5) 0.3951(10) 0.148(6) Uani 1 1 d U . .
C4C C 0.482(2) 0.0591(13) 0.269(3) 0.160(10) Uani 1 1 d U . .
F5C F 0.4891(14) 0.0721(7) 0.1924(12) 0.202(9) Uani 1 1 d U . .
F6C F 0.4951(14) 0.0178(6) 0.2744(14) 0.215(9) Uani 1 1 d U . .
F7C F 0.4101(13) 0.0702(8) 0.2701(18) 0.268(13) Uani 1 1 d U . .
O1D O 0.9693(9) 0.1360(5) 0.3663(7) 0.102(4) Uani 1 1 d U . .
O2D O 1.0852(9) 0.1025(5) 0.4082(10) 0.128(6) Uani 1 1 d U . .
C1D C 1.0232(13) 0.1087(5) 0.3582(8) 0.073(5) Uani 1 1 d DU . .
C2D C 1.0185(7) 0.0815(5) 0.2860(9) 0.108(7) Uani 1 1 d DU . .
F1D F 1.0615(11) 0.0422(4) 0.2977(8) 0.180(7) Uani 1 1 d DU . .
F2D F 1.0437(8) 0.1044(4) 0.2290(6) 0.141(5) Uani 1 1 d DU . .
C3D C 0.9290(8) 0.0639(4) 0.2521(7) 0.144(9) Uani 1 1 d DU . .
F3D F 0.8796(9) 0.1007(5) 0.2291(9) 0.214(10) Uani 1 1 d DU . .
F4D F 0.9033(11) 0.0434(6) 0.3114(7) 0.232(11) Uani 1 1 d DU . .
C4D C 0.9165(9) 0.0312(4) 0.1813(7) 0.179(11) Uani 1 1 d DU . .
F5D F 0.9446(12) 0.0486(6) 0.1233(7) 0.228(11) Uani 1 1 d DU . .
F6D F 0.9534(14) -0.0078(4) 0.2003(10) 0.239(11) Uani 1 1 d DU . .
F7D F 0.8366(9) 0.0231(7) 0.1538(11) 0.286(14) Uani 1 1 d DU . .
O1E O 0.6306(8) 0.3141(5) 0.5599(7) 0.093(4) Uani 1 1 d U . .
O2E O 0.6246(10) 0.3233(5) 0.4352(8) 0.112(5) Uani 1 1 d U . .
C1E C 0.6257(11) 0.3370(5) 0.4980(11) 0.065(4) Uani 1 1 d U . .
C2E C 0.615(2) 0.3879(10) 0.5079(19) 0.149(9) Uani 1 1 d U . .
F1E F 0.5696(12) 0.3978(6) 0.5740(12) 0.192(8) Uani 1 1 d U . .
F2E F 0.5577(13) 0.4066(6) 0.4448(11) 0.199(9) Uani 1 1 d U . .
C3E C 0.675(3) 0.4178(12) 0.531(2) 0.197(12) Uani 1 1 d U . .
F3E F 0.7269(12) 0.3965(5) 0.5988(12) 0.183(7) Uani 1 1 d U . .
F4E F 0.7122(16) 0.4089(8) 0.4650(15) 0.252(12) Uani 1 1 d U . .
C4E C 0.660(4) 0.4673(13) 0.566(3) 0.216(15) Uani 1 1 d U . .
F5E F 0.606(2) 0.4851(7) 0.5126(19) 0.313(18) Uani 1 1 d U . .
F6E F 0.658(3) 0.4728(11) 0.6235(16) 0.160(14) Uani 0.50 1 d PU . .
F7E F 0.727(2) 0.4849(8) 0.548(2) 0.296(15) Uani 1 1 d U . .
O1F O 1.1588(16) 0.2336(8) 0.5367(12) 0.195(10) Uani 1 1 d U . .
O2F O 1.0475(18) 0.2457(9) 0.4619(13) 0.217(11) Uani 1 1 d U . .
C1F C 1.113(2) 0.2584(12) 0.4982(17) 0.188(11) Uani 1 1 d DU . .
C2F C 1.1578(9) 0.2981(8) 0.4947(8) 0.212(11) Uani 1 1 d DU . .
F1F F 1.1589(10) 0.3170(5) 0.4246(7) 0.161(6) Uani 1 1 d DU . .
F2F F 1.2341(9) 0.3020(10) 0.5418(11) 0.167(13) Uani 0.50 1 d PDU . .
C3F C 1.1000(9) 0.3334(5) 0.5194(8) 0.240(13) Uani 1 1 d DU B .
F3F F 1.0848(9) 0.3191(5) 0.5898(7) 0.156(6) Uani 1 1 d DU . .
F4F F 1.0272(8) 0.3342(8) 0.4661(10) 0.362(17) Uani 1 1 d DU . .
C4F C 1.1387(10) 0.3805(5) 0.5301(10) 0.302(16) Uani 1 1 d DU . .
F5F F 1.113(2) 0.4048(8) 0.5829(18) 0.26(2) Uani 0.50 1 d PDU B 1
F6F F 1.2206(10) 0.3788(9) 0.552(3) 0.32(2) Uani 0.50 1 d PDU B 1
F7F F 1.121(2) 0.4045(7) 0.4639(14) 0.249(18) Uani 0.50 1 d PDU B 1
F5FB F 1.0826(17) 0.4122(6) 0.532(3) 0.244(19) Uani 0.50 1 d PDU B 2
F6FB F 1.194(2) 0.3836(10) 0.5985(15) 0.30(2) Uani 0.50 1 d PDU B 2
F7FB F 1.178(2) 0.3922(10) 0.4755(17) 0.27(2) Uani 0.50 1 d PDU B 2
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
N1 Ag1 N3 131.0(5) . .
N1 Ag1 O2A 129.4(5) . .
N3 Ag1 O2A 92.0(5) . .
N1 Ag1 Ag2 73.7(3) . .
N3 Ag1 Ag2 64.4(3) . .
O2A Ag1 Ag2 114.7(4) . .
N1 Ag1 Ag6 77.2(3) . 1_455
N3 Ag1 Ag6 151.1(3) . 1_455
O2A Ag1 Ag6 67.7(4) . 1_455
Ag2 Ag1 Ag6 142.04(6) . 1_455
N4 Ag2 N2 138.1(4) . .
N4 Ag2 O1B 124.7(5) . .
N2 Ag2 O1B 93.7(5) . .
N4 Ag2 Ag1 79.1(3) . .
N2 Ag2 Ag1 68.2(3) . .
O1B Ag2 Ag1 115.8(4) . .
N4 Ag2 Ag3 65.7(3) . .
N2 Ag2 Ag3 153.4(3) . .
O1B Ag2 Ag3 71.4(3) . .
Ag1 Ag2 Ag3 137.89(6) . .
O1C Ag3 O1E 142.5(5) . .
O1C Ag3 O2B 107.1(5) . .
O1E Ag3 O2B 108.1(5) . .
O1C Ag3 Ag4 81.9(3) . .
O1E Ag3 Ag4 128.4(3) . .
O2B Ag3 Ag4 58.2(4) . .
O1C Ag3 Ag2 55.8(3) . .
O1E Ag3 Ag2 117.7(3) . .
O2B Ag3 Ag2 81.9(4) . .
Ag4 Ag3 Ag2 109.47(5) . .
N5 Ag4 N7 138.2(5) . .
N5 Ag4 O2C 125.1(5) . .
N7 Ag4 O2C 92.9(5) . .
N5 Ag4 Ag5 77.7(3) . .
N7 Ag4 Ag5 68.4(3) . .
O2C Ag4 Ag5 117.5(4) . .
N5 Ag4 Ag3 63.8(3) . .
N7 Ag4 Ag3 155.4(3) . .
O2C Ag4 Ag3 73.5(3) . .
Ag5 Ag4 Ag3 135.90(6) . .
N8 Ag5 O1D 127.7(5) . .
N8 Ag5 N6 132.1(4) . .
O1D Ag5 N6 91.5(4) . .
N8 Ag5 O2F 99.9(6) . .
O1D Ag5 O2F 102.0(7) . .
N6 Ag5 O2F 96.4(8) . .
N8 Ag5 Ag4 74.3(3) . .
O1D Ag5 Ag4 115.3(4) . .
N6 Ag5 Ag4 63.3(3) . .
O2F Ag5 Ag4 136.9(8) . .
N8 Ag5 Ag6 73.8(3) . .
O1D Ag5 Ag6 71.3(3) . .
N6 Ag5 Ag6 153.3(3) . .
O2F Ag5 Ag6 68.6(8) . .
Ag4 Ag5 Ag6 142.36(6) . .
O2D Ag6 O1A 100.5(7) . 1_655
O2D Ag6 O1F 140.0(7) . .
O1A Ag6 O1F 118.0(7) 1_655 .
O2D Ag6 Ag5 85.0(4) . .
O1A Ag6 Ag5 122.5(5) 1_655 .
O1F Ag6 Ag5 83.3(6) . .
O2D Ag6 Ag1 119.3(4) . 1_655
O1A Ag6 Ag1 87.6(4) 1_655 1_655
O1F Ag6 Ag1 56.4(5) . 1_655
Ag5 Ag6 Ag1 138.73(7) . 1_655
C5 N1 C1 116.4(15) . .
C5 N1 Ag1 123.7(11) . .
C1 N1 Ag1 119.7(11) . .
N1 C1 C2 123.7(18) . .
N1 C1 H1A 118.2 . .
C2 C1 H1A 118.2 . .
C1 C2 C3 118.1(19) . .
C1 C2 H2A 120.9 . .
C3 C2 H2A 120.9 . .
C4 C3 C2 118.4(18) . .
C4 C3 H3A 120.8 . .
C2 C3 H3A 120.8 . .
C3 C4 C5 119.9(19) . .
C3 C4 H4A 120.1 . .
C5 C4 H4A 120.1 . .
N1 C5 C4 123.3(17) . .
N1 C5 C6 116.0(13) . .
C4 C5 C6 120.6(16) . .
N2 C6 C7 119.9(18) . .
N2 C6 C5 118.5(13) . .
C7 C6 C5 121.5(17) . .
C8 C7 C6 118(2) . .
C8 C7 H7A 120.8 . .
C6 C7 H7A 120.8 . .
C7 C8 C9 121.9(18) . .
C7 C8 H8A 119.0 . .
C9 C8 H8A 119.0 . .
C10 C9 C8 116.1(18) . .
C10 C9 H9A 121.9 . .
C8 C9 H9A 121.9 . .
C9 C10 N2 121.1(18) . .
C9 C10 H10A 119.4 . .
N2 C10 H10A 119.4 . .
C6 N2 C10 122.4(14) . .
C6 N2 Ag2 126.2(11) . .
C10 N2 Ag2 111.2(11) . .
C15 N3 C11 119.1(14) . .
C15 N3 Ag1 124.1(10) . .
C11 N3 Ag1 114.3(11) . .
N3 C11 C12 119.2(19) . .
N3 C11 H11A 120.4 . .
C12 C11 H11A 120.4 . .
C13 C12 C11 122(2) . .
C13 C12 H12A 118.9 . .
C11 C12 H12A 118.9 . .
C12 C13 C14 119.0(18) . .
C12 C13 H13A 120.5 . .
C14 C13 H13A 120.5 . .
C13 C14 C15 118.7(18) . .
C13 C14 H14A 120.6 . .
C15 C14 H14A 120.6 . .
N3 C15 C14 121.1(16) . .
N3 C15 C16 117.1(14) . .
C14 C15 C16 121.8(16) . .
N4 C16 C17 116.5(18) . .
N4 C16 C15 117.9(13) . .
C17 C16 C15 125.1(19) . .
C18 C17 C16 122(2) . .
C18 C17 H17A 119.1 . .
C16 C17 H17A 119.1 . .
C17 C18 C19 120(2) . .
C17 C18 H18A 119.9 . .
C19 C18 H18A 119.9 . .
C18 C19 C20 119(2) . .
C18 C19 H19A 120.3 . .
C20 C19 H19A 120.3 . .
N4 C20 C19 121(2) . .
N4 C20 H20A 119.6 . .
C19 C20 H20A 119.6 . .
C20 N4 C16 121.3(15) . .
C20 N4 Ag2 117.9(13) . .
C16 N4 Ag2 119.7(10) . .
C21 N5 C25 116.7(16) . .
C21 N5 Ag4 120.4(14) . .
C25 N5 Ag4 122.2(11) . .
N5 C21 C22 121(2) . .
N5 C21 H21A 119.5 . .
C22 C21 H21A 119.5 . .
C23 C22 C21 118(2) . .
C23 C22 H22A 120.8 . .
C21 C22 H22A 120.8 . .
C24 C23 C22 122(2) . .
C24 C23 H23A 119.2 . .
C22 C23 H23A 119.2 . .
C23 C24 C25 118(2) . .
C23 C24 H24A 121.2 . .
C25 C24 H24A 121.2 . .
N5 C25 C24 124.7(18) . .
N5 C25 C26 116.1(14) . .
C24 C25 C26 119.2(18) . .
N6 C26 C27 120.9(18) . .
N6 C26 C25 118.3(14) . .
C27 C26 C25 120.8(19) . .
C28 C27 C26 116(2) . .
C28 C27 H27A 121.8 . .
C26 C27 H27A 121.8 . .
C27 C28 C29 123.9(18) . .
C27 C28 H28A 118.0 . .
C29 C28 H28A 118.0 . .
C30 C29 C28 114(2) . .
C30 C29 H29A 123.1 . .
C28 C29 H29A 123.1 . .
N6 C30 C29 127(2) . .
N6 C30 H30A 116.3 . .
C29 C30 H30A 116.3 . .
C30 N6 C26 117.5(14) . .
C30 N6 Ag5 116.9(11) . .
C26 N6 Ag5 122.2(10) . .
C31 N7 C35 121.0(16) . .
C31 N7 Ag4 114.9(12) . .
C35 N7 Ag4 123.4(12) . .
N7 C31 C32 124(2) . .
N7 C31 H31A 117.9 . .
C32 C31 H31A 117.9 . .
C31 C32 C33 113.9(19) . .
C31 C32 H32A 123.0 . .
C33 C32 H32A 123.0 . .
C34 C33 C32 124(2) . .
C34 C33 H33A 118.1 . .
C32 C33 H33A 118.1 . .
C33 C34 C35 119(2) . .
C33 C34 H34A 120.7 . .
C35 C34 H34A 120.7 . .
N7 C35 C34 118(2) . .
N7 C35 C36 121.8(15) . .
C34 C35 C36 119.9(18) . .
N8 C36 C37 125(2) . .
N8 C36 C35 116.2(15) . .
C37 C36 C35 119(2) . .
C38 C37 C36 115(2) . .
C38 C37 H37A 122.3 . .
C36 C37 H37A 122.3 . .
C39 C38 C37 122(2) . .
C39 C38 H38A 119.2 . .
C37 C38 H38A 119.2 . .
C38 C39 C40 119(2) . .
C38 C39 H39A 120.5 . .
C40 C39 H39A 120.5 . .
N8 C40 C39 122(2) . .
N8 C40 H40A 118.8 . .
C39 C40 H40A 118.8 . .
C40 N8 C36 116.3(17) . .
C40 N8 Ag5 120.1(14) . .
C36 N8 Ag5 123.3(12) . .
C1A O1A Ag6 111.3(15) . 1_455
C1A O2A Ag1 137.2(16) . .
O2A C1A O1A 134(2) . .
O2A C1A C2A 117(2) . .
O1A C1A C2A 109(2) . .
F2A C2A C3A 110(3) . .
F2A C2A F1A 111(3) . .
C3A C2A F1A 101(3) . .
F2A C2A C1A 107(2) . .
C3A C2A C1A 121(3) . .
F1A C2A C1A 106(2) . .
F4A C3A F3A 124(4) . .
F4A C3A C2A 101(3) . .
F3A C3A C2A 91(3) . .
F4A C3A C4A 108(3) . .
F3A C3A C4A 120(3) . .
C2A C3A C4A 109(4) . .
F6A C4A F7A 124(7) . .
F6A C4A F5A 111(5) . .
F7A C4A F5A 92(3) . .
F6A C4A C3A 122(4) . .
F7A C4A C3A 107(3) . .
F5A C4A C3A 93(5) . .
C1B O1B Ag2 140.2(13) . .
C1B O2B Ag3 125.9(10) . .
O2B C1B O1B 119.7(14) . .
O2B C1B C2BB 110.3(15) . .
O1B C1B C2BB 130(2) . .
O2B C1B C2B 125.6(15) . .
O1B C1B C2B 112.9(16) . .
C2BB C1B C2B 20.6(10) . .
F1B C2B F2B 107.3(11) . .
F1B C2B C1B 112.0(18) . .
F2B C2B C1B 112.9(18) . .
F1B C2B C3B 111(2) . .
F2B C2B C3B 109.8(19) . .
C1B C2B C3B 103.9(14) . .
F3B C3B F4B 106.3(10) . .
F3B C3B C2B 110.7(16) . .
F4B C3B C2B 109.4(16) . .
F3B C3B C4B 110.8(11) . .
F4B C3B C4B 108.0(11) . .
C2B C3B C4B 111.4(17) . .
F7B C4B F6B 107.4(11) . .
F7B C4B F5B 106.8(10) . .
F6B C4B F5B 106.5(11) . .
F7B C4B C3B 113.1(10) . .
F6B C4B C3B 111.4(9) . .
F5B C4B C3B 111.3(10) . .
F1BB C2BB F2BB 107.7(11) . .
F1BB C2BB C1B 112(2) . .
F2BB C2BB C1B 112.8(19) . .
F1BB C2BB C3BB 109(2) . .
F2BB C2BB C3BB 108(2) . .
C1B C2BB C3BB 107.5(15) . .
F4BB C3BB F3BB 107.6(10) . .
F4BB C3BB C4BB 110.1(12) . .
F3BB C3BB C4BB 109.7(12) . .
F4BB C3BB C2BB 109.0(18) . .
F3BB C3BB C2BB 108.1(18) . .
C4BB C3BB C2BB 112.3(18) . .
F6BB C4BB F5BB 107.0(11) . .
F6BB C4BB F7BB 106.7(11) . .
F5BB C4BB F7BB 106.7(11) . .
F6BB C4BB C3BB 111.6(10) . .
F5BB C4BB C3BB 112.1(10) . .
F7BB C4BB C3BB 112.3(10) . .
C1C O1C Ag3 119.2(12) . .
C1C O2C Ag4 129.9(13) . .
O2C C1C O1C 134.9(17) . .
O2C C1C C2C 110.7(19) . .
O1C C1C C2C 114.4(18) . .
F1C C2C C3C 119(2) . .
F1C C2C F2C 107(2) . .
C3C C2C F2C 92(2) . .
F1C C2C C1C 114(2) . .
C3C C2C C1C 116(2) . .
F2C C2C C1C 105.2(18) . .
F4C C3C F3C 102(2) . .
F4C C3C C4C 108(3) . .
F3C C3C C4C 105(2) . .
F4C C3C C2C 110(2) . .
F3C C3C C2C 106(2) . .
C4C C3C C2C 124(3) . .
F6C C4C F7C 114(4) . .
F6C C4C F5C 107(3) . .
F7C C4C F5C 103(3) . .
F6C C4C C3C 115(3) . .
F7C C4C C3C 112(3) . .
F5C C4C C3C 104(3) . .
C1D O1D Ag5 136.2(11) . .
C1D O2D Ag6 122.3(11) . .
O2D C1D O1D 122.3(14) . .
O2D C1D C2D 114.2(13) . .
O1D C1D C2D 123.4(16) . .
F2D C2D F1D 107.6(9) . .
F2D C2D C1D 113.3(11) . .
F1D C2D C1D 114.1(11) . .
F2D C2D C3D 108.3(11) . .
F1D C2D C3D 101.2(14) . .
C1D C2D C3D 111.5(11) . .
F4D C3D F3D 108.1(9) . .
F4D C3D C4D 109.2(8) . .
F3D C3D C4D 107.3(9) . .
F4D C3D C2D 107.2(10) . .
F3D C3D C2D 107.6(9) . .
C4D C3D C2D 117.2(9) . .
F6D C4D F5D 108.2(9) . .
F6D C4D F7D 107.7(10) . .
F5D C4D F7D 106.8(9) . .
F6D C4D C3D 112.0(9) . .
F5D C4D C3D 111.7(9) . .
F7D C4D C3D 110.2(8) . .
C1E O1E Ag3 100.0(11) . .
O2E C1E O1E 127.4(17) . .
O2E C1E C2E 118(2) . .
O1E C1E C2E 115(2) . .
C3E C2E F2E 108(3) . .
C3E C2E C1E 126(4) . .
F2E C2E C1E 112(2) . .
C3E C2E F1E 96(3) . .
F2E C2E F1E 100(3) . .
C1E C2E F1E 111(2) . .
C2E C3E F3E 103(3) . .
C2E C3E F4E 93(3) . .
F3E C3E F4E 107(4) . .
C2E C3E C4E 123(5) . .
F3E C3E C4E 101(3) . .
F4E C3E C4E 126(3) . .
F6E C4E F5E 119(8) . .
F6E C4E F7E 113(5) . .
F5E C4E F7E 99(4) . .
F6E C4E C3E 123(5) . .
F5E C4E C3E 104(4) . .
F7E C4E C3E 93(5) . .
C1F O1F Ag6 115(2) . .
C1F O2F Ag5 139(2) . .
O1F C1F O2F 121(3) . .
O1F C1F C2F 106(2) . .
O2F C1F C2F 132(3) . .
F2F C2F F1F 108.4(11) . .
F2F C2F C1F 118.4(15) . .
F1F C2F C1F 120.2(15) . .
F2F C2F C3F 109.0(14) . .
F1F C2F C3F 96.6(14) . .
C1F C2F C3F 101(2) . .
F4F C3F F3F 108.1(10) . .
F4F C3F C4F 110.7(10) . .
F3F C3F C4F 109.0(9) . .
F4F C3F C2F 109.4(12) . .
F3F C3F C2F 107.3(10) . .
C4F C3F C2F 112.3(12) . .
F7FB C4F F5F 131.2(14) . .
F7FB C4F F6F 64.9(16) . .
F5F C4F F6F 107.3(10) . .
F7FB C4F F5FB 107.1(10) . .
F5F C4F F5FB 41.9(17) . .
F6F C4F F5FB 134.4(14) . .
F7FB C4F F7F 43.6(16) . .
F5F C4F F7F 106.1(9) . .
F6F C4F F7F 106.0(9) . .
F5FB C4F F7F 68.1(16) . .
F7FB C4F F6FB 106.4(9) . .
F5F C4F F6FB 66.4(16) . .
F6F C4F F6FB 45.3(15) . .
F5FB C4F F6FB 105.8(9) . .
F7F C4F F6FB 135.5(14) . .
F7FB C4F C3F 114.4(9) . .
F5F C4F C3F 112.9(9) . .
F6F C4F C3F 112.1(9) . .
F5FB C4F C3F 111.7(9) . .
F7F C4F C3F 112.0(9) . .
F6FB C4F C3F 110.9(9) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ag1 N1 2.270(12) .
Ag1 N3 2.318(12) .
Ag1 O2A 2.349(14) .
Ag1 Ag2 2.9323(18) .
Ag1 Ag6 3.076(2) 1_455
Ag2 N4 2.286(12) .
Ag2 N2 2.330(12) .
Ag2 O1B 2.342(12) .
Ag2 Ag3 3.2286(19) .
Ag3 O1C 2.311(13) .
Ag3 O1E 2.335(13) .
Ag3 O2B 2.354(12) .
Ag3 Ag4 3.2183(19) .
Ag4 N5 2.232(13) .
Ag4 N7 2.342(13) .
Ag4 O2C 2.342(12) .
Ag4 Ag5 2.9445(18) .
Ag5 N8 2.282(15) .
Ag5 O1D 2.324(12) .
Ag5 N6 2.336(11) .
Ag5 O2F 2.461(19) .
Ag5 Ag6 3.028(2) .
Ag6 O2D 2.222(15) .
Ag6 O1A 2.274(17) 1_655
Ag6 O1F 2.55(3) .
Ag6 Ag1 3.076(2) 1_655
N1 C5 1.289(18) .
N1 C1 1.331(19) .
C1 C2 1.35(2) .
C1 H1A 0.9300 .
C2 C3 1.38(3) .
C2 H2A 0.9300 .
C3 C4 1.31(2) .
C3 H3A 0.9300 .
C4 C5 1.38(2) .
C4 H4A 0.9300 .
C5 C6 1.48(2) .
C6 N2 1.332(19) .
C6 C7 1.38(2) .
C7 C8 1.38(3) .
C7 H7A 0.9300 .
C8 C9 1.44(3) .
C8 H8A 0.9300 .
C9 C10 1.36(2) .
C9 H9A 0.9300 .
C10 N2 1.381(19) .
C10 H10A 0.9300 .
N3 C15 1.349(18) .
N3 C11 1.38(2) .
C11 C12 1.38(2) .
C11 H11A 0.9300 .
C12 C13 1.33(3) .
C12 H12A 0.9300 .
C13 C14 1.39(3) .
C13 H13A 0.9300 .
C14 C15 1.40(2) .
C14 H14A 0.9300 .
C15 C16 1.44(2) .
C16 N4 1.369(19) .
C16 C17 1.38(2) .
C17 C18 1.33(3) .
C17 H17A 0.9300 .
C18 C19 1.34(3) .
C18 H18A 0.9300 .
C19 C20 1.36(3) .
C19 H19A 0.9300 .
C20 N4 1.33(2) .
C20 H20A 0.9300 .
N5 C21 1.35(2) .
N5 C25 1.36(2) .
C21 C22 1.40(3) .
C21 H21A 0.9300 .
C22 C23 1.38(3) .
C22 H22A 0.9300 .
C23 C24 1.33(3) .
C23 H23A 0.9300 .
C24 C25 1.37(2) .
C24 H24A 0.9300 .
C25 C26 1.50(2) .
C26 N6 1.36(2) .
C26 C27 1.38(2) .
C27 C28 1.36(3) .
C27 H27A 0.9300 .
C28 C29 1.37(3) .
C28 H28A 0.9300 .
C29 C30 1.34(2) .
C29 H29A 0.9300 .
C30 N6 1.297(19) .
C30 H30A 0.9300 .
N7 C31 1.31(2) .
N7 C35 1.34(2) .
C31 C32 1.35(2) .
C31 H31A 0.9300 .
C32 C33 1.38(3) .
C32 H32A 0.9300 .
C33 C34 1.33(3) .
C33 H33A 0.9300 .
C34 C35 1.38(2) .
C34 H34A 0.9300 .
C35 C36 1.48(3) .
C36 N8 1.34(2) .
C36 C37 1.37(2) .
C37 C38 1.36(3) .
C37 H37A 0.9300 .
C38 C39 1.34(3) .
C38 H38A 0.9300 .
C39 C40 1.36(3) .
C39 H39A 0.9300 .
C40 N8 1.32(2) .
C40 H40A 0.9300 .
O1A C1A 1.19(2) .
O1A Ag6 2.274(17) 1_455
O2A C1A 1.12(2) .
C1A C2A 1.63(3) .
C2A F2A 1.31(3) .
C2A C3A 1.44(4) .
C2A F1A 1.49(3) .
C3A F4A 1.34(3) .
C3A F3A 1.37(3) .
C3A C4A 1.56(5) .
C4A F6A 1.09(4) .
C4A F7A 1.30(5) .
C4A F5A 1.38(6) .
O1B C1B 1.282(19) .
O2B C1B 1.22(2) .
C1B C2BB 1.49(3) .
C1B C2B 1.49(3) .
C2B F1B 1.349(10) .
C2B F2B 1.349(10) .
C2B C3B 1.51(3) .
C3B F3B 1.346(10) .
C3B F4B 1.366(10) .
C3B C4B 1.522(16) .
C4B F7B 1.311(10) .
C4B F6B 1.316(10) .
C4B F5B 1.324(10) .
C2BB F1BB 1.349(10) .
C2BB F2BB 1.352(10) .
C2BB C3BB 1.54(3) .
C3BB F4BB 1.347(10) .
C3BB F3BB 1.354(10) .
C3BB C4BB 1.519(17) .
C4BB F6BB 1.318(10) .
C4BB F5BB 1.318(10) .
C4BB F7BB 1.318(10) .
O1C C1C 1.22(2) .
O2C C1C 1.20(2) .
C1C C2C 1.58(3) .
C2C F1C 1.22(3) .
C2C C3C 1.49(3) .
C2C F2C 1.55(3) .
C3C F4C 1.34(3) .
C3C F3C 1.37(3) .
C3C C4C 1.47(4) .
C4C F6C 1.23(3) .
C4C F7C 1.24(3) .
C4C F5C 1.41(4) .
O1D C1D 1.229(17) .
O2D C1D 1.19(2) .
C1D C2D 1.478(18) .
C2D F2D 1.342(9) .
C2D F1D 1.345(9) .
C2D C3D 1.547(16) .
C3D F4D 1.347(8) .
C3D F3D 1.358(9) .
C3D C4D 1.540(13) .
C4D F6D 1.302(9) .
C4D F5D 1.308(9) .
C4D F7D 1.317(10) .
O1E C1E 1.258(19) .
O2E C1E 1.163(19) .
C1E C2E 1.52(3) .
C2E C3E 1.32(4) .
C2E F2E 1.39(3) .
C2E F1E 1.53(4) .
C3E F3E 1.43(4) .
C3E F4E 1.45(5) .
C3E C4E 1.62(6) .
C4E F6E 1.02(6) .
C4E F5E 1.25(5) .
C4E F7E 1.33(6) .
O1F C1F 1.15(4) .
O2F C1F 1.19(3) .
C1F C2F 1.39(2) .
C2F F2F 1.341(10) .
C2F F1F 1.345(10) .
C2F C3F 1.53(2) .
C3F F4F 1.341(9) .
C3F F3F 1.372(10) .
C3F C4F 1.516(11) .
C4F F7FB 1.310(9) .
C4F F5F 1.313(9) .
C4F F6F 1.317(9) .
C4F F5FB 1.318(9) .
C4F F7F 1.328(9) .
C4F F6FB 1.331(9) .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
N1 Ag1 Ag2 N4 84.4(5) . .
N3 Ag1 Ag2 N4 -69.6(5) . .
O2A Ag1 Ag2 N4 -149.3(5) . .
Ag6 Ag1 Ag2 N4 125.8(4) 1_455 .
N1 Ag1 Ag2 N2 -68.9(5) . .
N3 Ag1 Ag2 N2 137.2(5) . .
O2A Ag1 Ag2 N2 57.5(5) . .
Ag6 Ag1 Ag2 N2 -27.5(4) 1_455 .
N1 Ag1 Ag2 O1B -152.2(6) . .
N3 Ag1 Ag2 O1B 53.9(6) . .
O2A Ag1 Ag2 O1B -25.9(6) . .
Ag6 Ag1 Ag2 O1B -110.8(4) 1_455 .
N1 Ag1 Ag2 Ag3 117.4(4) . .
N3 Ag1 Ag2 Ag3 -36.6(4) . .
O2A Ag1 Ag2 Ag3 -116.3(4) . .
Ag6 Ag1 Ag2 Ag3 158.80(9) 1_455 .
N4 Ag2 Ag3 O1C -103.5(6) . .
N2 Ag2 Ag3 O1C 53.6(8) . .
O1B Ag2 Ag3 O1C 112.3(6) . .
Ag1 Ag2 Ag3 O1C -139.4(4) . .
N4 Ag2 Ag3 O1E 33.1(5) . .
N2 Ag2 Ag3 O1E -169.8(8) . .
O1B Ag2 Ag3 O1E -111.1(6) . .
Ag1 Ag2 Ag3 O1E -2.8(3) . .
N4 Ag2 Ag3 O2B 139.4(5) . .
N2 Ag2 Ag3 O2B -63.5(8) . .
O1B Ag2 Ag3 O2B -4.8(6) . .
Ag1 Ag2 Ag3 O2B 103.4(4) . .
N4 Ag2 Ag3 Ag4 -168.6(4) . .
N2 Ag2 Ag3 Ag4 -11.5(7) . .
O1B Ag2 Ag3 Ag4 47.2(4) . .
Ag1 Ag2 Ag3 Ag4 155.44(7) . .
O1C Ag3 Ag4 N5 140.5(5) . .
O1E Ag3 Ag4 N5 -14.9(6) . .
O2B Ag3 Ag4 N5 -103.5(6) . .
Ag2 Ag3 Ag4 N5 -170.2(4) . .
O1C Ag3 Ag4 N7 -62.5(8) . .
O1E Ag3 Ag4 N7 142.1(8) . .
O2B Ag3 Ag4 N7 53.5(9) . .
Ag2 Ag3 Ag4 N7 -13.2(8) . .
O1C Ag3 Ag4 O2C -3.9(5) . .
O1E Ag3 Ag4 O2C -159.4(6) . .
O2B Ag3 Ag4 O2C 112.1(6) . .
Ag2 Ag3 Ag4 O2C 45.4(4) . .
O1C Ag3 Ag4 Ag5 108.7(3) . .
O1E Ag3 Ag4 Ag5 -46.7(4) . .
O2B Ag3 Ag4 Ag5 -135.3(4) . .
Ag2 Ag3 Ag4 Ag5 158.04(7) . .
N5 Ag4 Ag5 N8 84.9(6) . .
N7 Ag4 Ag5 N8 -70.0(5) . .
O2C Ag4 Ag5 N8 -151.7(6) . .
Ag3 Ag4 Ag5 N8 113.8(4) . .
N5 Ag4 Ag5 O1D -150.3(5) . .
N7 Ag4 Ag5 O1D 54.8(5) . .
O2C Ag4 Ag5 O1D -27.0(6) . .
Ag3 Ag4 Ag5 O1D -121.4(4) . .
N5 Ag4 Ag5 N6 -72.1(5) . .
N7 Ag4 Ag5 N6 133.0(5) . .
O2C Ag4 Ag5 N6 51.2(5) . .
Ag3 Ag4 Ag5 N6 -43.2(4) . .
N5 Ag4 Ag5 O2F -2.8(9) . .
N7 Ag4 Ag5 O2F -157.8(9) . .
O2C Ag4 Ag5 O2F 120.5(9) . .
Ag3 Ag4 Ag5 O2F 26.1(8) . .
N5 Ag4 Ag5 Ag6 117.9(4) . .
N7 Ag4 Ag5 Ag6 -37.1(3) . .
O2C Ag4 Ag5 Ag6 -118.8(4) . .
Ag3 Ag4 Ag5 Ag6 146.77(9) . .
N8 Ag5 Ag6 O2D 130.5(7) . .
O1D Ag5 Ag6 O2D -10.0(6) . .
N6 Ag5 Ag6 O2D -62.5(9) . .
O2F Ag5 Ag6 O2D -121.6(7) . .
Ag4 Ag5 Ag6 O2D 97.5(5) . .
N8 Ag5 Ag6 O1A 31.2(7) . 1_655
O1D Ag5 Ag6 O1A -109.3(7) . 1_655
N6 Ag5 Ag6 O1A -161.8(9) . 1_655
O2F Ag5 Ag6 O1A 139.1(8) . 1_655
Ag4 Ag5 Ag6 O1A -1.8(6) . 1_655
N8 Ag5 Ag6 O1F -87.9(6) . .
O1D Ag5 Ag6 O1F 131.6(6) . .
N6 Ag5 Ag6 O1F 79.1(8) . .
O2F Ag5 Ag6 O1F 20.0(7) . .
Ag4 Ag5 Ag6 O1F -120.9(4) . .
N8 Ag5 Ag6 Ag1 -99.3(4) . 1_655
O1D Ag5 Ag6 Ag1 120.2(4) . 1_655
N6 Ag5 Ag6 Ag1 67.7(8) . 1_655
O2F Ag5 Ag6 Ag1 8.5(5) . 1_655
Ag4 Ag5 Ag6 Ag1 -132.35(10) . 1_655
N3 Ag1 N1 C5 105.1(13) . .
O2A Ag1 N1 C5 -35.4(15) . .
Ag2 Ag1 N1 C5 73.4(11) . .
Ag6 Ag1 N1 C5 -81.9(12) 1_455 .
N3 Ag1 N1 C1 -79.4(13) . .
O2A Ag1 N1 C1 140.0(12) . .
Ag2 Ag1 N1 C1 -111.1(12) . .
Ag6 Ag1 N1 C1 93.6(12) 1_455 .
C5 N1 C1 C2 1(2) . .
Ag1 N1 C1 C2 -175.2(13) . .
N1 C1 C2 C3 2(3) . .
C1 C2 C3 C4 -1(3) . .
C2 C3 C4 C5 -2(3) . .
C1 N1 C5 C4 -4(2) . .
Ag1 N1 C5 C4 171.7(12) . .
C1 N1 C5 C6 177.8(14) . .
Ag1 N1 C5 C6 -6.6(19) . .
C3 C4 C5 N1 5(3) . .
C3 C4 C5 C6 -177.0(17) . .
N1 C5 C6 N2 -47(2) . .
C4 C5 C6 N2 134.2(15) . .
N1 C5 C6 C7 135.6(16) . .
C4 C5 C6 C7 -43(2) . .
N2 C6 C7 C8 1(3) . .
C5 C6 C7 C8 177.9(17) . .
C6 C7 C8 C9 -1(3) . .
C7 C8 C9 C10 2(3) . .
C8 C9 C10 N2 -2(3) . .
C7 C6 N2 C10 -1(2) . .
C5 C6 N2 C10 -178.0(14) . .
C7 C6 N2 Ag2 173.6(12) . .
C5 C6 N2 Ag2 -3.5(19) . .
C9 C10 N2 C6 1(3) . .
C9 C10 N2 Ag2 -173.8(15) . .
N4 Ag2 N2 C6 27.5(15) . .
O1B Ag2 N2 C6 -174.8(12) . .
Ag1 Ag2 N2 C6 68.9(11) . .
Ag3 Ag2 N2 C6 -120.5(11) . .
N4 Ag2 N2 C10 -157.5(10) . .
O1B Ag2 N2 C10 0.2(11) . .
Ag1 Ag2 N2 C10 -116.1(11) . .
Ag3 Ag2 N2 C10 54.5(14) . .
N1 Ag1 N3 C15 48.8(15) . .
O2A Ag1 N3 C15 -160.7(13) . .
Ag2 Ag1 N3 C15 82.8(12) . .
Ag6 Ag1 N3 C15 -116.9(11) 1_455 .
N1 Ag1 N3 C11 -149.3(12) . .
O2A Ag1 N3 C11 1.3(13) . .
Ag2 Ag1 N3 C11 -115.3(13) . .
Ag6 Ag1 N3 C11 45.0(16) 1_455 .
C15 N3 C11 C12 8(3) . .
Ag1 N3 C11 C12 -155.4(14) . .
N3 C11 C12 C13 -10(3) . .
C11 C12 C13 C14 8(3) . .
C12 C13 C14 C15 -5(3) . .
C11 N3 C15 C14 -4(2) . .
Ag1 N3 C15 C14 156.7(12) . .
C11 N3 C15 C16 179.1(14) . .
Ag1 N3 C15 C16 -19.8(19) . .
C13 C14 C15 N3 3(3) . .
C13 C14 C15 C16 179.3(16) . .
N3 C15 C16 N4 -51.7(18) . .
C14 C15 C16 N4 131.9(16) . .
N3 C15 C16 C17 136.7(17) . .
C14 C15 C16 C17 -40(2) . .
N4 C16 C17 C18 5(3) . .
C15 C16 C17 C18 176.6(18) . .
C16 C17 C18 C19 -3(3) . .
C17 C18 C19 C20 1(4) . .
C18 C19 C20 N4 -1(3) . .
C19 C20 N4 C16 3(3) . .
C19 C20 N4 Ag2 170.7(15) . .
C17 C16 N4 C20 -5(2) . .
C15 C16 N4 C20 -177.0(14) . .
C17 C16 N4 Ag2 -172.3(12) . .
C15 C16 N4 Ag2 15.3(16) . .
N2 Ag2 N4 C20 -73.9(14) . .
O1B Ag2 N4 C20 133.4(12) . .
Ag1 Ag2 N4 C20 -112.6(12) . .
Ag3 Ag2 N4 C20 91.0(12) . .
N2 Ag2 N4 C16 94.1(11) . .
O1B Ag2 N4 C16 -58.6(12) . .
Ag1 Ag2 N4 C16 55.4(10) . .
Ag3 Ag2 N4 C16 -101.0(10) . .
N7 Ag4 N5 C21 -73.2(14) . .
O2C Ag4 N5 C21 135.6(12) . .
Ag5 Ag4 N5 C21 -109.4(12) . .
Ag3 Ag4 N5 C21 92.7(12) . .
N7 Ag4 N5 C25 97.1(12) . .
O2C Ag4 N5 C25 -54.1(13) . .
Ag5 Ag4 N5 C25 61.0(11) . .
Ag3 Ag4 N5 C25 -97.0(11) . .
C25 N5 C21 C22 1(2) . .
Ag4 N5 C21 C22 172.0(14) . .
N5 C21 C22 C23 -3(3) . .
C21 C22 C23 C24 3(3) . .
C22 C23 C24 C25 0(3) . .
C21 N5 C25 C24 1(2) . .
Ag4 N5 C25 C24 -169.2(13) . .
C21 N5 C25 C26 178.1(14) . .
Ag4 N5 C25 C26 7.4(18) . .
C23 C24 C25 N5 -2(3) . .
C23 C24 C25 C26 -178.5(18) . .
N5 C25 C26 N6 -45(2) . .
C24 C25 C26 N6 132.2(17) . .
N5 C25 C26 C27 135.0(17) . .
C24 C25 C26 C27 -48(2) . .
N6 C26 C27 C28 0(3) . .
C25 C26 C27 C28 -179.4(16) . .
C26 C27 C28 C29 1(3) . .
C27 C28 C29 C30 -1(3) . .
C28 C29 C30 N6 0(3) . .
C29 C30 N6 C26 1(3) . .
C29 C30 N6 Ag5 -158.4(17) . .
C27 C26 N6 C30 -1(2) . .
C25 C26 N6 C30 178.5(15) . .
C27 C26 N6 Ag5 157.3(13) . .
C25 C26 N6 Ag5 -23.0(19) . .
N8 Ag5 N6 C30 -148.1(12) . .
O1D Ag5 N6 C30 0.1(13) . .
O2F Ag5 N6 C30 102.3(14) . .
Ag4 Ag5 N6 C30 -117.6(13) . .
Ag6 Ag5 N6 C30 48.8(17) . .
N8 Ag5 N6 C26 53.3(15) . .
O1D Ag5 N6 C26 -158.5(13) . .
O2F Ag5 N6 C26 -56.2(13) . .
Ag4 Ag5 N6 C26 83.8(12) . .
Ag6 Ag5 N6 C26 -109.7(12) . .
N5 Ag4 N7 C31 -154.4(12) . .
O2C Ag4 N7 C31 2.4(13) . .
Ag5 Ag4 N7 C31 -116.1(13) . .
Ag3 Ag4 N7 C31 57.4(16) . .
N5 Ag4 N7 C35 34.7(16) . .
O2C Ag4 N7 C35 -168.6(13) . .
Ag5 Ag4 N7 C35 73.0(13) . .
Ag3 Ag4 N7 C35 -113.5(13) . .
C35 N7 C31 C32 1(3) . .
Ag4 N7 C31 C32 -170.3(15) . .
N7 C31 C32 C33 -1(3) . .
C31 C32 C33 C34 -1(3) . .
C32 C33 C34 C35 2(3) . .
C31 N7 C35 C34 0(3) . .
Ag4 N7 C35 C34 170.7(13) . .
C31 N7 C35 C36 179.3(16) . .
Ag4 N7 C35 C36 -10(2) . .
C33 C34 C35 N7 -2(3) . .
C33 C34 C35 C36 179.4(18) . .
N7 C35 C36 N8 -43(2) . .
C34 C35 C36 N8 136.3(17) . .
N7 C35 C36 C37 138.4(17) . .
C34 C35 C36 C37 -43(2) . .
N8 C36 C37 C38 3(3) . .
C35 C36 C37 C38 -178.5(19) . .
C36 C37 C38 C39 1(4) . .
C37 C38 C39 C40 -6(4) . .
C38 C39 C40 N8 7(3) . .
C39 C40 N8 C36 -3(3) . .
C39 C40 N8 Ag5 -177.4(15) . .
C37 C36 N8 C40 -2(2) . .
C35 C36 N8 C40 179.4(15) . .
C37 C36 N8 Ag5 172.2(13) . .
C35 C36 N8 Ag5 -6.7(19) . .
O1D Ag5 N8 C40 134.4(13) . .
N6 Ag5 N8 C40 -87.3(14) . .
O2F Ag5 N8 C40 20.8(15) . .
Ag4 Ag5 N8 C40 -115.4(13) . .
Ag6 Ag5 N8 C40 84.8(13) . .
O1D Ag5 N8 C36 -39.3(14) . .
N6 Ag5 N8 C36 98.9(13) . .
O2F Ag5 N8 C36 -153.0(14) . .
Ag4 Ag5 N8 C36 70.9(11) . .
Ag6 Ag5 N8 C36 -88.9(12) . .
N1 Ag1 O2A C1A -33(3) . .
N3 Ag1 O2A C1A 176(3) . .
Ag2 Ag1 O2A C1A -122(3) . .
Ag6 Ag1 O2A C1A 17(3) 1_455 .
Ag1 O2A C1A O1A -13(6) . .
Ag1 O2A C1A C2A 170.2(18) . .
Ag6 O1A C1A O2A -5(4) 1_455 .
Ag6 O1A C1A C2A 172.1(17) 1_455 .
O2A C1A C2A F2A -147(3) . .
O1A C1A C2A F2A 35(4) . .
O2A C1A C2A C3A -20(4) . .
O1A C1A C2A C3A 162(3) . .
O2A C1A C2A F1A 94(3) . .
O1A C1A C2A F1A -84(3) . .
F2A C2A C3A F4A -170(3) . .
F1A C2A C3A F4A -52(3) . .
C1A C2A C3A F4A 64(4) . .
F2A C2A C3A F3A 65(3) . .
F1A C2A C3A F3A -177(2) . .
C1A C2A C3A F3A -60(3) . .
F2A C2A C3A C4A -57(4) . .
F1A C2A C3A C4A 61(3) . .
C1A C2A C3A C4A 178(3) . .
F4A C3A C4A F6A 35(9) . .
F3A C3A C4A F6A -177(6) . .
C2A C3A C4A F6A -74(8) . .
F4A C3A C4A F7A -175(5) . .
F3A C3A C4A F7A -27(8) . .
C2A C3A C4A F7A 76(5) . .
F4A C3A C4A F5A -82(4) . .
F3A C3A C4A F5A 66(6) . .
C2A C3A C4A F5A 169(3) . .
N4 Ag2 O1B C1B -30(2) . .
N2 Ag2 O1B C1B 168(2) . .
Ag1 Ag2 O1B C1B -125(2) . .
Ag3 Ag2 O1B C1B 10(2) . .
O1C Ag3 O2B C1B -44.8(19) . .
O1E Ag3 O2B C1B 122.1(17) . .
Ag4 Ag3 O2B C1B -113.4(18) . .
Ag2 Ag3 O2B C1B 5.6(17) . .
Ag3 O2B C1B O1B -1(3) . .
Ag3 O2B C1B C2BB 179.4(11) . .
Ag3 O2B C1B C2B -164.9(15) . .
Ag2 O1B C1B O2B -9(4) . .
Ag2 O1B C1B C2BB 170.0(15) . .
Ag2 O1B C1B C2B 156.4(16) . .
O2B C1B C2B F1B 2(3) . .
O1B C1B C2B F1B -162(2) . .
C2BB C1B C2B F1B 49(4) . .
O2B C1B C2B F2B 124(2) . .
O1B C1B C2B F2B -41(3) . .
C2BB C1B C2B F2B 170(5) . .
O2B C1B C2B C3B -117(2) . .
O1B C1B C2B C3B 78(2) . .
C2BB C1B C2B C3B -71(4) . .
F1B C2B C3B F3B -76(3) . .
F2B C2B C3B F3B 165.4(18) . .
C1B C2B C3B F3B 44.4(17) . .
F1B C2B C3B F4B 167.0(19) . .
F2B C2B C3B F4B 49(2) . .
C1B C2B C3B F4B -72.4(17) . .
F1B C2B C3B C4B 48(2) . .
F2B C2B C3B C4B -71(2) . .
C1B C2B C3B C4B 168.2(14) . .
F3B C3B C4B F7B 76(3) . .
F4B C3B C4B F7B -168(3) . .
C2B C3B C4B F7B -48(3) . .
F3B C3B C4B F6B -45(3) . .
F4B C3B C4B F6B 71(3) . .
C2B C3B C4B F6B -169(3) . .
F3B C3B C4B F5B -164(3) . .
F4B C3B C4B F5B -48(3) . .
C2B C3B C4B F5B 72(3) . .
O2B C1B C2BB F1BB 90(2) . .
O1B C1B C2BB F1BB -90(3) . .
C2B C1B C2BB F1BB -52(4) . .
O2B C1B C2BB F2BB -32(3) . .
O1B C1B C2BB F2BB 149(2) . .
C2B C1B C2BB F2BB -173(5) . .
O2B C1B C2BB C3BB -150.9(19) . .
O1B C1B C2BB C3BB 30(3) . .
C2B C1B C2BB C3BB 68(4) . .
F1BB C2BB C3BB F4BB 52(2) . .
F2BB C2BB C3BB F4BB 168.6(18) . .
C1B C2BB C3BB F4BB -69.5(16) . .
F1BB C2BB C3BB F3BB 168.6(18) . .
F2BB C2BB C3BB F3BB -75(2) . .
C1B C2BB C3BB F3BB 47.1(17) . .
F1BB C2BB C3BB C4BB -70.3(19) . .
F2BB C2BB C3BB C4BB 46(2) . .
C1B C2BB C3BB C4BB 168.3(14) . .
F4BB C3BB C4BB F6BB 52(3) . .
F3BB C3BB C4BB F6BB -66(3) . .
C2BB C3BB C4BB F6BB 173(3) . .
F4BB C3BB C4BB F5BB -68(3) . .
F3BB C3BB C4BB F5BB 173(3) . .
C2BB C3BB C4BB F5BB 53(3) . .
F4BB C3BB C4BB F7BB 172(3) . .
F3BB C3BB C4BB F7BB 53(3) . .
C2BB C3BB C4BB F7BB -67(3) . .
O1E Ag3 O1C C1C 151.2(14) . .
O2B Ag3 O1C C1C -49.5(16) . .
Ag4 Ag3 O1C C1C 3.6(14) . .
Ag2 Ag3 O1C C1C -116.7(16) . .
N5 Ag4 O2C C1C -32(2) . .
N7 Ag4 O2C C1C 166.8(19) . .
Ag5 Ag4 O2C C1C -126.1(18) . .
Ag3 Ag4 O2C C1C 7.6(18) . .
Ag4 O2C C1C O1C -8(4) . .
Ag4 O2C C1C C2C 172.6(15) . .
Ag3 O1C C1C O2C 1(3) . .
Ag3 O1C C1C C2C -179.9(15) . .
O2C C1C C2C F1C -87(3) . .
O1C C1C C2C F1C 93(3) . .
O2C C1C C2C C3C 56(3) . .
O1C C1C C2C C3C -123(2) . .
O2C C1C C2C F2C 156.1(19) . .
O1C C1C C2C F2C -23(3) . .
F1C C2C C3C F4C 173(2) . .
F2C C2C C3C F4C -77(2) . .
C1C C2C C3C F4C 31(3) . .
F1C C2C C3C F3C 64(3) . .
F2C C2C C3C F3C 174.0(19) . .
C1C C2C C3C F3C -78(3) . .
F1C C2C C3C C4C -57(4) . .
F2C C2C C3C C4C 53(3) . .
C1C C2C C3C C4C 161(3) . .
F4C C3C C4C F6C -67(4) . .
F3C C3C C4C F6C 41(5) . .
C2C C3C C4C F6C 162(3) . .
F4C C3C C4C F7C 66(5) . .
F3C C3C C4C F7C 174(4) . .
C2C C3C C4C F7C -66(5) . .
F4C C3C C4C F5C 177(2) . .
F3C C3C C4C F5C -75(3) . .
C2C C3C C4C F5C 45(4) . .
N8 Ag5 O1D C1D -38(2) . .
N6 Ag5 O1D C1D 171.7(19) . .
O2F Ag5 O1D C1D 75(2) . .
Ag4 Ag5 O1D C1D -127.3(18) . .
Ag6 Ag5 O1D C1D 12.6(18) . .
O1A Ag6 O2D C1D 139.4(18) 1_655 .
O1F Ag6 O2D C1D -56(2) . .
Ag5 Ag6 O2D C1D 17.3(17) . .
Ag1 Ag6 O2D C1D -127.4(16) 1_655 .
Ag6 O2D C1D O1D -14(3) . .
Ag6 O2D C1D C2D 164.4(10) . .
Ag5 O1D C1D O2D -3(3) . .
Ag5 O1D C1D C2D 178.4(11) . .
O2D C1D C2D F2D -96.5(17) . .
O1D C1D C2D F2D 82(2) . .
O2D C1D C2D F1D 27(2) . .
O1D C1D C2D F1D -154.5(17) . .
O2D C1D C2D C3D 141.0(17) . .
O1D C1D C2D C3D -40.5(19) . .
F2D C2D C3D F4D -176.5(12) . .
F1D C2D C3D F4D 70.6(13) . .
C1D C2D C3D F4D -51.2(12) . .
F2D C2D C3D F3D -60.5(14) . .
F1D C2D C3D F3D -173.4(11) . .
C1D C2D C3D F3D 64.9(11) . .
F2D C2D C3D C4D 60.5(13) . .
F1D C2D C3D C4D -52.5(12) . .
C1D C2D C3D C4D -174.2(9) . .
F4D C3D C4D F6D -55.1(15) . .
F3D C3D C4D F6D -172.0(14) . .
C2D C3D C4D F6D 66.9(14) . .
F4D C3D C4D F5D -176.7(14) . .
F3D C3D C4D F5D 66.3(15) . .
C2D C3D C4D F5D -54.7(14) . .
F4D C3D C4D F7D 64.7(15) . .
F3D C3D C4D F7D -52.2(15) . .
C2D C3D C4D F7D -173.2(13) . .
O1C Ag3 O1E C1E -40.1(15) . .
O2B Ag3 O1E C1E 160.7(11) . .
Ag4 Ag3 O1E C1E 97.3(11) . .
Ag2 Ag3 O1E C1E -109.1(11) . .
Ag3 O1E C1E O2E -3(2) . .
Ag3 O1E C1E C2E 172.8(18) . .
O2E C1E C2E C3E -98(4) . .
O1E C1E C2E C3E 86(4) . .
O2E C1E C2E F2E 37(4) . .
O1E C1E C2E F2E -139(2) . .
O2E C1E C2E F1E 148(2) . .
O1E C1E C2E F1E -28(3) . .
F2E C2E C3E F3E 177(3) . .
C1E C2E C3E F3E -47(5) . .
F1E C2E C3E F3E 75(3) . .
F2E C2E C3E F4E -75(4) . .
C1E C2E C3E F4E 61(4) . .
F1E C2E C3E F4E -177(3) . .
F2E C2E C3E C4E 63(5) . .
C1E C2E C3E C4E -161(3) . .
F1E C2E C3E C4E -39(5) . .
C2E C3E C4E F6E 83(8) . .
F3E C3E C4E F6E -31(8) . .
F4E C3E C4E F6E -152(6) . .
C2E C3E C4E F5E -57(6) . .
F3E C3E C4E F5E -171(4) . .
F4E C3E C4E F5E 67(7) . .
C2E C3E C4E F7E -157(4) . .
F3E C3E C4E F7E 89(4) . .
F4E C3E C4E F7E -32(6) . .
O2D Ag6 O1F C1F 43(3) . .
O1A Ag6 O1F C1F -154(2) 1_655 .
Ag5 Ag6 O1F C1F -31(3) . .
Ag1 Ag6 O1F C1F 140(3) 1_655 .
N8 Ag5 O2F C1F 28(5) . .
O1D Ag5 O2F C1F -104(5) . .
N6 Ag5 O2F C1F 163(5) . .
Ag4 Ag5 O2F C1F 106(5) . .
Ag6 Ag5 O2F C1F -40(5) . .
Ag6 O1F C1F O2F 16(5) . .
Ag6 O1F C1F C2F -154.0(16) . .
Ag5 O2F C1F O1F 24(8) . .
Ag5 O2F C1F C2F -170(2) . .
O1F C1F C2F F2F -9(4) . .
O2F C1F C2F F2F -177(4) . .
O1F C1F C2F F1F 128(2) . .
O2F C1F C2F F1F -40(6) . .
O1F C1F C2F C3F -128(3) . .
O2F C1F C2F C3F 64(5) . .
F2F C2F C3F F4F 171.2(14) . .
F1F C2F C3F F4F 59.1(16) . .
C1F C2F C3F F4F -63.4(14) . .
F2F C2F C3F F3F -71.8(15) . .
F1F C2F C3F F3F 176.1(12) . .
C1F C2F C3F F3F 53.5(13) . .
F2F C2F C3F C4F 47.9(15) . .
F1F C2F C3F C4F -64.3(13) . .
C1F C2F C3F C4F 173.2(12) . .
F4F C3F C4F F7FB -80(2) . .
F3F C3F C4F F7FB 161(2) . .
C2F C3F C4F F7FB 42(2) . .
F4F C3F C4F F5F 87(2) . .
F3F C3F C4F F5F -32(2) . .
C2F C3F C4F F5F -150.3(19) . .
F4F C3F C4F F6F -152(2) . .
F3F C3F C4F F6F 90(2) . .
C2F C3F C4F F6F -29(2) . .
F4F C3F C4F F5FB 42(2) . .
F3F C3F C4F F5FB -77(2) . .
C2F C3F C4F F5FB 164(2) . .
F4F C3F C4F F7F -33(2) . .
F3F C3F C4F F7F -151.2(19) . .
C2F C3F C4F F7F 90.1(18) . .
F4F C3F C4F F6FB 159(2) . .
F3F C3F C4F F6FB 41(2) . .
C2F C3F C4F F6FB -78(2) . .
