#------------------------------------------------------------------------------
#$Date: 2016-03-25 16:10:25 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179955 $
#$URL: svn://www.crystallography.net/cod/cif/7/02/50/7025086.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7025086
loop_
_publ_author_name
'Li, Ni-Ya'
'Ren, Zhi-Gang'
'Liu, Dong'
'Yuan, Rong-Xin'
'Wei, Li-Pei'
'Zhang, Liang'
'Li, Hong-Xi'
'Lang, Jian-Ping'
_publ_section_title
;
 Construction of [Ag2X2]-based complexes from reactions of Ag(I) salts
 with N-diphenylphosphanylmethyl-4-aminopyridine: isolation, structures,
 and luminescent properties.
;
_journal_issue                   17
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              4213
_journal_page_last               4222
_journal_paper_doi               10.1039/b925081f
_journal_volume                  39
_journal_year                    2010
_chemical_formula_moiety         'C72 H68 Ag2 I2 N8 P4, C2 O2, C O'
_chemical_formula_sum            'C75 H68 Ag2 I2 N8 O3 P4'
_chemical_formula_weight         1722.79
_chemical_name_systematic
;
?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                101.13(3)
_cell_angle_beta                 93.39(3)
_cell_angle_gamma                105.72(3)
_cell_formula_units_Z            1
_cell_length_a                   11.941(2)
_cell_length_b                   12.106(2)
_cell_length_c                   14.236(3)
_cell_measurement_reflns_used    7329
_cell_measurement_temperature    193(2)
_cell_measurement_theta_max      27.5476
_cell_measurement_theta_min      3.0898
_cell_volume                     1930.1(7)
_computing_cell_refinement       'CrystalClear, Ver. 1.30 (Rigaku/MSC, 2001)'
_computing_data_collection       'CrystalClear, Ver. 1.30 (Rigaku/MSC, 2001)'
_computing_data_reduction
'CrystalStructure, Ver. 3.60 (Rigaku/MSC, 2004)'
_computing_molecular_graphics    'ORTEPII (Johnson, 1976)'
_computing_publication_material  SHELXL97
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      193(2)
_diffrn_measured_fraction_theta_full 0.983
_diffrn_measured_fraction_theta_max 0.983
_diffrn_measurement_device_type  'Rigaku MercuryCCD area detector'
_diffrn_measurement_method       ω
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0608
_diffrn_reflns_av_sigmaI/netI    0.0886
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_k_min       -15
_diffrn_reflns_limit_l_max       18
_diffrn_reflns_limit_l_min       -17
_diffrn_reflns_number            18700
_diffrn_reflns_theta_full        27.48
_diffrn_reflns_theta_max         27.48
_diffrn_reflns_theta_min         3.09
_diffrn_standards_decay_%        0
_diffrn_standards_interval_count 0
_diffrn_standards_interval_time  0
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    1.439
_exptl_absorpt_correction_T_max  0.8694
_exptl_absorpt_correction_T_min  0.7148
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
'Jacobson, R. (1998) Private communication to Rigaku Company, Tokyo, Japan.'
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.482
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             858
_exptl_crystal_size_max          0.25
_exptl_crystal_size_mid          0.10
_exptl_crystal_size_min          0.10
_refine_diff_density_max         1.122
_refine_diff_density_min         -0.947
_refine_diff_density_rms         0.116
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.132
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     421
_refine_ls_number_reflns         8709
_refine_ls_number_restraints     3
_refine_ls_restrained_S_all      1.132
_refine_ls_R_factor_all          0.1140
_refine_ls_R_factor_gt           0.0813
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0813P)²+0.9375P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1872
_refine_ls_wR_factor_ref         0.2092
_reflns_number_gt                6288
_reflns_number_total             8709
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b925081f.txt
_cod_data_source_block           '[Ag2I2(dppmapy)4].3MeOH'
_cod_depositor_comments
;
The following automatic conversions were performed:
'__computing_data_collection' tag replaced with
'_computing_data_collection'.

Automatic conversion script
Id: cif_correct_tags 1440 2010-10-19 06:21:57Z saulius 
;
_cod_database_code               7025086
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
I1 I 0.09192(4) 0.38388(4) 0.04080(4) 0.05071(19) Uani 1 1 d . . .
Ag1 Ag 0.15335(5) 0.61808(5) -0.00107(5) 0.0493(2) Uani 1 1 d . . .
P1 P 0.26921(16) 0.77844(17) 0.13202(16) 0.0433(5) Uani 1 1 d . . .
N1 N 0.2053(10) 0.5191(9) 0.5191(7) 0.091(3) Uani 1 1 d . . .
C1 C 0.2432(12) 0.6326(10) 0.5170(9) 0.090(3) Uani 1 1 d . . .
H1 H 0.2653 0.6874 0.5772 0.108 Uiso 1 1 calc R . .
O1 O 0.305(2) 0.234(2) 0.5541(18) 0.149(8) Uiso 0.50 1 d PD A 1
O1A O 0.290(2) 0.114(2) 0.528(2) 0.164(9) Uiso 0.50 1 d PD B 2
P2 P 0.22306(17) 0.60162(18) -0.16293(16) 0.0469(5) Uani 1 1 d . . .
N2 N 0.2248(6) 0.6384(5) 0.2607(5) 0.0508(16) Uani 1 1 d . . .
H2 H 0.2113 0.5853 0.2063 0.061 Uiso 1 1 calc R . .
C2 C 0.2528(9) 0.6768(8) 0.4355(7) 0.067(2) Uani 1 1 d . . .
H2A H 0.2834 0.7590 0.4400 0.081 Uiso 1 1 calc R . .
O2 O 0.481(2) 0.006(2) 0.4416(17) 0.163(9) Uiso 0.50 1 d PD . .
C3 C 0.2174(7) 0.6004(7) 0.3459(6) 0.0502(19) Uani 1 1 d . . .
N3 N -0.0803(11) 0.0466(9) -0.4030(11) 0.117(5) Uani 1 1 d . . .
N4 N 0.1160(6) 0.3698(6) -0.2284(6) 0.065(2) Uani 1 1 d . . .
H4 H 0.1520 0.3693 -0.1728 0.078 Uiso 1 1 calc R . .
C4 C 0.1775(7) 0.4793(7) 0.3444(7) 0.054(2) Uani 1 1 d . . .
H4A H 0.1541 0.4225 0.2853 0.065 Uiso 1 1 calc R . .
C5 C 0.1739(10) 0.4465(9) 0.4321(8) 0.074(3) Uani 1 1 d . . .
H5 H 0.1464 0.3648 0.4306 0.088 Uiso 1 1 calc R . .
C6 C 0.2534(7) 0.7603(7) 0.2560(6) 0.0484(18) Uani 1 1 d . . .
H6A H 0.3276 0.8042 0.2977 0.058 Uiso 1 1 calc R . .
H6B H 0.1909 0.7936 0.2804 0.058 Uiso 1 1 calc R . .
C7 C 0.2502(6) 0.9237(6) 0.1379(6) 0.0451(17) Uani 1 1 d . . .
C8 C 0.3205(8) 1.0219(7) 0.2053(7) 0.057(2) Uani 1 1 d . . .
H8 H 0.3807 1.0127 0.2472 0.069 Uiso 1 1 calc R . .
C9 C 0.3043(8) 1.1315(7) 0.2121(7) 0.065(2) Uani 1 1 d . . .
H9 H 0.3513 1.1968 0.2594 0.079 Uiso 1 1 calc R . .
C10 C 0.2198(8) 1.1452(8) 0.1500(8) 0.070(3) Uani 1 1 d . . .
H10 H 0.2092 1.2209 0.1539 0.085 Uiso 1 1 calc R . .
C11 C 0.1498(8) 1.0511(8) 0.0818(9) 0.078(3) Uani 1 1 d . . .
H11 H 0.0905 1.0620 0.0401 0.093 Uiso 1 1 calc R . .
C12 C 0.1659(7) 0.9387(7) 0.0741(8) 0.066(3) Uani 1 1 d . . .
H12 H 0.1197 0.8740 0.0258 0.079 Uiso 1 1 calc R . .
C13 C 0.4243(6) 0.8003(6) 0.1237(6) 0.0438(17) Uani 1 1 d . . .
C14 C 0.4912(7) 0.7510(7) 0.1756(6) 0.0510(19) Uani 1 1 d . . .
H14 H 0.4574 0.7102 0.2225 0.061 Uiso 1 1 calc R . .
C15 C 0.6080(8) 0.7598(8) 0.1608(8) 0.064(2) Uani 1 1 d . . .
H15 H 0.6524 0.7239 0.1963 0.077 Uiso 1 1 calc R . .
C16 C 0.6573(8) 0.8206(7) 0.0947(7) 0.062(2) Uani 1 1 d . . .
H16 H 0.7368 0.8278 0.0853 0.075 Uiso 1 1 calc R . .
C17 C 0.5929(7) 0.8721(7) 0.0408(7) 0.064(2) Uani 1 1 d . . .
H17 H 0.6276 0.9136 -0.0053 0.077 Uiso 1 1 calc R . .
C18 C 0.4769(7) 0.8615(7) 0.0561(7) 0.057(2) Uani 1 1 d . . .
H18 H 0.4323 0.8964 0.0199 0.068 Uiso 1 1 calc R . .
C19 C -0.0431(12) 0.0585(11) -0.3124(16) 0.114(6) Uani 1 1 d . . .
H19 H -0.0637 -0.0098 -0.2862 0.137 Uiso 1 1 calc R . .
C20 C 0.0248(8) 0.1636(9) -0.2502(10) 0.086(4) Uani 1 1 d . . .
H20 H 0.0502 0.1654 -0.1853 0.103 Uiso 1 1 calc R . .
C21 C 0.0538(7) 0.2658(8) -0.2874(8) 0.060(2) Uani 1 1 d . . .
C22 C 0.0161(9) 0.2528(8) -0.3824(8) 0.072(3) Uani 1 1 d . . .
H22 H 0.0345 0.3187 -0.4117 0.087 Uiso 1 1 calc R . .
C23 C -0.0489(11) 0.1440(10) -0.4359(10) 0.100(4) Uani 1 1 d . . .
H23 H -0.0729 0.1388 -0.5018 0.120 Uiso 1 1 calc R . .
C24 C 0.1246(7) 0.4819(7) -0.2549(6) 0.052(2) Uani 1 1 d . . .
H24A H 0.0459 0.4939 -0.2606 0.062 Uiso 1 1 calc R . .
H24B H 0.1549 0.4815 -0.3181 0.062 Uiso 1 1 calc R . .
C25 C 0.2238(7) 0.7289(7) -0.2137(6) 0.0518(19) Uani 1 1 d . . .
C26 C 0.1191(9) 0.7481(9) -0.2404(10) 0.098(4) Uani 1 1 d . . .
H26 H 0.0475 0.6940 -0.2332 0.117 Uiso 1 1 calc R . .
C27 C 0.1165(10) 0.8445(10) -0.2774(11) 0.102(4) Uani 1 1 d . . .
H27 H 0.0435 0.8559 -0.2961 0.122 Uiso 1 1 calc R . .
C28 C 0.2175(9) 0.9231(8) -0.2874(8) 0.074(3) Uani 1 1 d . . .
H28 H 0.2153 0.9891 -0.3136 0.088 Uiso 1 1 calc R . .
C29 C 0.3207(9) 0.9078(7) -0.2604(8) 0.073(3) Uani 1 1 d . . .
H29 H 0.3915 0.9637 -0.2666 0.088 Uiso 1 1 calc R . .
C30 C 0.3244(8) 0.8108(7) -0.2234(7) 0.061(2) Uani 1 1 d . . .
H30 H 0.3982 0.8010 -0.2045 0.074 Uiso 1 1 calc R . .
C31 C 0.3657(6) 0.5791(6) -0.1771(6) 0.0415(16) Uani 1 1 d . . .
C32 C 0.4401(7) 0.5884(6) -0.0967(6) 0.0508(19) Uani 1 1 d . . .
H32 H 0.4144 0.6041 -0.0350 0.061 Uiso 1 1 calc R . .
C33 C 0.5526(7) 0.5753(7) -0.1030(7) 0.055(2) Uani 1 1 d . . .
H33 H 0.6032 0.5841 -0.0463 0.066 Uiso 1 1 calc R . .
C34 C 0.5883(7) 0.5497(7) -0.1912(7) 0.055(2) Uani 1 1 d . . .
H34 H 0.6638 0.5391 -0.1963 0.066 Uiso 1 1 calc R . .
C35 C 0.5146(8) 0.5388(7) -0.2748(7) 0.061(2) Uani 1 1 d . . .
H35 H 0.5408 0.5219 -0.3362 0.073 Uiso 1 1 calc R . .
C36 C 0.4023(7) 0.5529(7) -0.2681(6) 0.055(2) Uani 1 1 d . . .
H36 H 0.3518 0.5447 -0.3247 0.066 Uiso 1 1 calc R . .
C37 C 0.392(2) 0.288(2) 0.4984(18) 0.091(7) Uiso 0.50 1 d PD A 1
C37A C 0.253(4) 0.193(4) 0.477(3) 0.199(19) Uiso 0.50 1 d PD B 2
C38 C 0.511(3) -0.090(2) 0.387(2) 0.135(11) Uiso 0.50 1 d PD . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
I I -0.4742 1.8119 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_3
Ag1 I1 Ag1 85.96(4) 2_565
P1 Ag1 P2 118.56(7) .
P1 Ag1 I1 115.46(6) .
P2 Ag1 I1 107.54(6) .
P1 Ag1 I1 114.62(6) 2_565
P2 Ag1 I1 103.33(6) 2_565
I1 Ag1 I1 94.04(4) 2_565
C13 P1 C7 104.1(3) .
C13 P1 C6 103.6(4) .
C7 P1 C6 101.9(4) .
C13 P1 Ag1 110.0(3) .
C7 P1 Ag1 117.3(3) .
C6 P1 Ag1 118.1(3) .
C1 N1 C5 114.4(9) .
N1 C1 C2 125.4(11) .
N1 C1 H1 117.3 .
C2 C1 H1 117.3 .
C31 P2 C25 105.4(3) .
C31 P2 C24 103.4(4) .
C25 P2 C24 101.5(4) .
C31 P2 Ag1 119.3(3) .
C25 P2 Ag1 112.2(3) .
C24 P2 Ag1 113.2(3) .
C3 N2 C6 123.3(7) .
C3 N2 H2 118.3 .
C6 N2 H2 118.3 .
C1 C2 C3 119.4(9) .
C1 C2 H2A 120.3 .
C3 C2 H2A 120.3 .
N2 C3 C2 122.7(7) .
N2 C3 C4 120.0(8) .
C2 C3 C4 117.3(8) .
C19 N3 C23 114.7(12) .
C21 N4 C24 121.7(8) .
C21 N4 H4 119.1 .
C24 N4 H4 119.1 .
C5 C4 C3 117.3(9) .
C5 C4 H4A 121.3 .
C3 C4 H4A 121.3 .
N1 C5 C4 126.2(9) .
N1 C5 H5 116.9 .
C4 C5 H5 116.9 .
N2 C6 P1 111.2(6) .
N2 C6 H6A 109.4 .
P1 C6 H6A 109.4 .
N2 C6 H6B 109.4 .
P1 C6 H6B 109.4 .
H6A C6 H6B 108.0 .
C12 C7 C8 119.0(7) .
C12 C7 P1 119.9(6) .
C8 C7 P1 121.1(6) .
C9 C8 C7 121.4(9) .
C9 C8 H8 119.3 .
C7 C8 H8 119.3 .
C10 C9 C8 119.2(9) .
C10 C9 H9 120.4 .
C8 C9 H9 120.4 .
C9 C10 C11 121.2(8) .
C9 C10 H10 119.4 .
C11 C10 H10 119.4 .
C10 C11 C12 120.1(9) .
C10 C11 H11 120.0 .
C12 C11 H11 120.0 .
C7 C12 C11 119.1(9) .
C7 C12 H12 120.5 .
C11 C12 H12 120.5 .
C14 C13 C18 118.1(7) .
C14 C13 P1 122.7(6) .
C18 C13 P1 119.0(6) .
C13 C14 C15 121.5(8) .
C13 C14 H14 119.3 .
C15 C14 H14 119.3 .
C16 C15 C14 119.2(9) .
C16 C15 H15 120.4 .
C14 C15 H15 120.4 .
C15 C16 C17 121.2(8) .
C15 C16 H16 119.4 .
C17 C16 H16 119.4 .
C18 C17 C16 118.6(9) .
C18 C17 H17 120.7 .
C16 C17 H17 120.7 .
C17 C18 C13 121.4(9) .
C17 C18 H18 119.3 .
C13 C18 H18 119.3 .
N3 C19 C20 125.7(13) .
N3 C19 H19 117.1 .
C20 C19 H19 117.1 .
C21 C20 C19 117.7(13) .
C21 C20 H20 121.1 .
C19 C20 H20 121.1 .
N4 C21 C22 124.3(9) .
N4 C21 C20 119.3(10) .
C22 C21 C20 116.4(10) .
C21 C22 C23 120.1(11) .
C21 C22 H22 120.0 .
C23 C22 H22 120.0 .
N3 C23 C22 125.4(14) .
N3 C23 H23 117.3 .
C22 C23 H23 117.3 .
N4 C24 P2 109.8(6) .
N4 C24 H24A 109.7 .
P2 C24 H24A 109.7 .
N4 C24 H24B 109.7 .
P2 C24 H24B 109.7 .
H24A C24 H24B 108.2 .
C30 C25 C26 117.3(8) .
C30 C25 P2 123.2(6) .
C26 C25 P2 119.5(6) .
C27 C26 C25 121.0(9) .
C27 C26 H26 119.5 .
C25 C26 H26 119.5 .
C28 C27 C26 120.4(10) .
C28 C27 H27 119.8 .
C26 C27 H27 119.8 .
C29 C28 C27 119.9(9) .
C29 C28 H28 120.0 .
C27 C28 H28 120.0 .
C28 C29 C30 120.3(9) .
C28 C29 H29 119.9 .
C30 C29 H29 119.9 .
C25 C30 C29 121.1(9) .
C25 C30 H30 119.4 .
C29 C30 H30 119.4 .
C32 C31 C36 119.0(7) .
C32 C31 P2 119.5(6) .
C36 C31 P2 121.5(6) .
C31 C32 C33 122.0(8) .
C31 C32 H32 119.0 .
C33 C32 H32 119.0 .
C34 C33 C32 119.1(8) .
C34 C33 H33 120.5 .
C32 C33 H33 120.5 .
C33 C34 C35 120.5(8) .
C33 C34 H34 119.8 .
C35 C34 H34 119.8 .
C34 C35 C36 120.2(8) .
C34 C35 H35 119.9 .
C36 C35 H35 119.9 .
C31 C36 C35 119.2(8) .
C31 C36 H36 120.4 .
C35 C36 H36 120.4 .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
I1 Ag1 2.9170(10) .
I1 Ag1 2.9427(10) 2_565
Ag1 P1 2.467(2) .
Ag1 P2 2.486(2) .
Ag1 I1 2.9427(10) 2_565
P1 C13 1.813(7) .
P1 C7 1.821(8) .
P1 C6 1.834(8) .
N1 C1 1.332(13) .
N1 C5 1.339(13) .
C1 C2 1.367(14) .
C1 H1 0.9500 .
O1 C37 1.432(10) .
O1A C37A 1.445(10) .
P2 C31 1.814(7) .
P2 C25 1.822(8) .
P2 C24 1.833(9) .
N2 C3 1.377(10) .
N2 C6 1.438(9) .
N2 H2 0.8800 .
C2 C3 1.389(12) .
C2 H2A 0.9500 .
O2 C38 1.418(10) .
C3 C4 1.408(10) .
N3 C19 1.31(2) .
N3 C23 1.320(17) .
N4 C21 1.362(11) .
N4 C24 1.456(10) .
N4 H4 0.8800 .
C4 C5 1.382(13) .
C4 H4A 0.9500 .
C5 H5 0.9500 .
C6 H6A 0.9900 .
C6 H6B 0.9900 .
C7 C12 1.388(11) .
C7 C8 1.400(11) .
C8 C9 1.378(11) .
C8 H8 0.9500 .
C9 C10 1.367(13) .
C9 H9 0.9500 .
C10 C11 1.378(14) .
C10 H10 0.9500 .
C11 C12 1.410(12) .
C11 H11 0.9500 .
C12 H12 0.9500 .
C13 C14 1.378(10) .
C13 C18 1.402(11) .
C14 C15 1.402(11) .
C14 H14 0.9500 .
C15 C16 1.369(12) .
C15 H15 0.9500 .
C16 C17 1.393(13) .
C16 H16 0.9500 .
C17 C18 1.391(11) .
C17 H17 0.9500 .
C18 H18 0.9500 .
C19 C20 1.408(19) .
C19 H19 0.9500 .
C20 C21 1.404(12) .
C20 H20 0.9500 .
C21 C22 1.364(14) .
C22 C23 1.381(14) .
C22 H22 0.9500 .
C23 H23 0.9500 .
C24 H24A 0.9900 .
C24 H24B 0.9900 .
C25 C30 1.369(10) .
C25 C26 1.378(12) .
C26 C27 1.377(13) .
C26 H26 0.9500 .
C27 C28 1.353(13) .
C27 H27 0.9500 .
C28 C29 1.339(13) .
C28 H28 0.9500 .
C29 C30 1.387(12) .
C29 H29 0.9500 .
C30 H30 0.9500 .
C31 C32 1.373(11) .
C31 C36 1.398(11) .
C32 C33 1.401(10) .
C32 H32 0.9500 .
C33 C34 1.356(12) .
C33 H33 0.9500 .
C34 C35 1.399(13) .
C34 H34 0.9500 .
C35 C36 1.403(11) .
C35 H35 0.9500 .
C36 H36 0.9500 .
