#------------------------------------------------------------------------------
#$Date: 2016-03-25 16:16:36 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179961 $
#$URL: svn://www.crystallography.net/cod/cif/7/02/55/7025564.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7025564
loop_
_publ_author_name
'Norton, Kieran'
'Banerjee, Santanu'
'Das, Sayantani'
'Huebner, Louise'
'Emge, Thomas J.'
'Brennan, John G.'
_publ_section_title
;
 Lanthanide oxochalcogenido clusters.
;
_journal_issue                   29
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              6794
_journal_page_last               6800
_journal_paper_doi               10.1039/c001812k
_journal_volume                  39
_journal_year                    2010
_chemical_formula_moiety
'Ho3 O Te7 N5 C31 H30,Ho4 Te11 N7 C47 H45,2.85(N C5 H5),0.075(Te2 C12 H10)'
_chemical_formula_sum            'C93.15 H90 Ho7 N14.85 O Te18.15'
_chemical_formula_weight         4903.95
_chemical_name_systematic
;
?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                112.219(2)
_cell_angle_beta                 103.310(2)
_cell_angle_gamma                96.552(2)
_cell_formula_units_Z            2
_cell_length_a                   13.4945(10)
_cell_length_b                   21.1680(15)
_cell_length_c                   24.1226(16)
_cell_measurement_reflns_used    8483
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      23.29
_cell_measurement_theta_min      2.36
_cell_volume                     6050.9(8)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      100(2)
_diffrn_measured_fraction_theta_full 0.975
_diffrn_measured_fraction_theta_max 0.975
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0612
_diffrn_reflns_av_sigmaI/netI    0.1355
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_k_max       23
_diffrn_reflns_limit_k_min       -19
_diffrn_reflns_limit_l_max       22
_diffrn_reflns_limit_l_min       -26
_diffrn_reflns_number            28979
_diffrn_reflns_theta_full        23.39
_diffrn_reflns_theta_max         23.39
_diffrn_reflns_theta_min         1.70
_exptl_absorpt_coefficient_mu    8.855
_exptl_absorpt_correction_T_max  0.777
_exptl_absorpt_correction_T_min  0.270
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'Bruker SAINT (SADABS)'
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    2.692
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       lathe
_exptl_crystal_F_000             4347
_exptl_crystal_size_max          0.20
_exptl_crystal_size_mid          0.10
_exptl_crystal_size_min          0.03
_refine_diff_density_max         3.614
_refine_diff_density_min         -1.868
_refine_diff_density_rms         0.357
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.073
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1116
_refine_ls_number_reflns         17207
_refine_ls_number_restraints     2004
_refine_ls_restrained_S_all      1.020
_refine_ls_R_factor_all          0.1518
_refine_ls_R_factor_gt           0.0759
_refine_ls_shift/su_max          0.006
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0900P)²+1.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1725
_refine_ls_wR_factor_ref         0.2039
_reflns_number_gt                9354
_reflns_number_total             17207
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c001812k.txt
_cod_data_source_block           hotetep
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 1891 2012-01-12 08:04:46Z andrius 
;
_cod_original_cell_volume        6050.9(7)
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7025564
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ho1 Ho 0.06078(5) -0.39812(3) 0.17850(2) 0.04477(18) Uani 1 1 d . . .
Ho2 Ho -0.18244(4) -0.35642(3) 0.12678(2) 0.04088(17) Uani 1 1 d . . .
Ho3 Ho 0.03703(4) -0.30283(2) 0.08421(2) 0.03836(17) Uani 1 1 d . . .
O1 O -0.0159(5) -0.3282(3) 0.1500(3) 0.033(2) Uani 1 1 d . . .
Te1 Te -0.15321(7) -0.50490(4) 0.10183(3) 0.0503(3) Uani 1 1 d . . .
Te2 Te -0.13351(8) -0.42045(4) 0.22582(3) 0.0592(3) Uani 1 1 d . . .
Te3 Te -0.17426(6) -0.39274(4) -0.00846(3) 0.0445(3) Uani 1 1 d . . .
Te4 Te -0.17415(7) -0.25429(4) 0.06003(4) 0.0543(3) Uani 1 1 d . . .
Te5 Te 0.11529(6) -0.43839(4) 0.05022(3) 0.0448(3) Uani 1 1 d . . .
Te6 Te 0.24963(7) -0.32654(4) 0.15345(4) 0.0516(3) Uani 1 1 d . . .
Te7 Te 0.15170(8) -0.29932(4) 0.31472(4) 0.0651(3) Uani 1 1 d . . .
C1 C 0.3064(5) -0.2413(3) 0.3362(3) 0.078(3) Uani 1 1 d GU . .
C2 C 0.3257(6) -0.1984(4) 0.3064(4) 0.078(3) Uani 1 1 d GU . .
H2 H 0.2703 -0.1955 0.2757 0.094 Uiso 1 1 calc R . .
C3 C 0.4262(7) -0.1597(5) 0.3216(5) 0.083(4) Uani 1 1 d GU . .
H3 H 0.4394 -0.1304 0.3013 0.099 Uiso 1 1 calc R . .
C4 C 0.5073(6) -0.1640(5) 0.3666(5) 0.093(4) Uani 1 1 d GU . .
H4 H 0.5759 -0.1376 0.3770 0.112 Uiso 1 1 calc R . .
C5 C 0.4879(5) -0.2069(5) 0.3964(4) 0.089(4) Uani 1 1 d GU . .
H5 H 0.5434 -0.2098 0.4271 0.107 Uiso 1 1 calc R . .
C6 C 0.3875(6) -0.2455(4) 0.3811(3) 0.081(4) Uani 1 1 d GU . .
H6 H 0.3743 -0.2748 0.4015 0.097 Uiso 1 1 calc R . .
N1 N 0.1282(5) -0.5008(3) 0.1816(2) 0.075(3) Uani 1 1 d GU . .
C7 C 0.0645(6) -0.5610(4) 0.1755(3) 0.084(4) Uani 1 1 d GU . .
H7 H -0.0077 -0.5632 0.1712 0.101 Uiso 1 1 calc R . .
C8 C 0.1066(9) -0.6179(3) 0.1758(4) 0.096(4) Uani 1 1 d GU . .
H8 H 0.0631 -0.6590 0.1717 0.116 Uiso 1 1 calc R . .
C9 C 0.2123(9) -0.6146(5) 0.1821(5) 0.091(4) Uani 1 1 d GU . .
H9 H 0.2410 -0.6535 0.1822 0.109 Uiso 1 1 calc R . .
C10 C 0.2759(6) -0.5545(5) 0.1881(4) 0.088(4) Uani 1 1 d GU . .
H10 H 0.3481 -0.5523 0.1924 0.106 Uiso 1 1 calc R . .
C11 C 0.2339(5) -0.4976(4) 0.1878(3) 0.078(3) Uani 1 1 d GU . .
H11 H 0.2774 -0.4565 0.1920 0.094 Uiso 1 1 calc R . .
N2 N 0.0962(7) -0.2674(3) 0.0086(3) 0.090(3) Uani 1 1 d GU . .
C12 C 0.0409(8) -0.2378(5) -0.0276(4) 0.116(4) Uani 1 1 d GU . .
H12 H -0.0279 -0.2330 -0.0268 0.139 Uiso 1 1 calc R . .
C13 C 0.0863(11) -0.2153(6) -0.0651(5) 0.122(4) Uani 1 1 d GU . .
H13 H 0.0486 -0.1951 -0.0898 0.146 Uiso 1 1 calc R . .
C14 C 0.1870(12) -0.2224(7) -0.0663(6) 0.124(4) Uani 1 1 d GU . .
H14 H 0.2181 -0.2070 -0.0919 0.149 Uiso 1 1 calc R . .
C15 C 0.2423(9) -0.2520(7) -0.0301(6) 0.131(4) Uani 1 1 d GU . .
H15 H 0.3111 -0.2569 -0.0310 0.157 Uiso 1 1 calc R . .
C16 C 0.1969(7) -0.2745(5) 0.0073(4) 0.108(4) Uani 1 1 d GU . .
H16 H 0.2347 -0.2948 0.0320 0.130 Uiso 1 1 calc R . .
N3 N 0.1118(5) -0.1815(3) 0.1602(2) 0.057(3) Uani 1 1 d GU . .
C17 C 0.0775(6) -0.1606(4) 0.2131(3) 0.062(3) Uani 1 1 d GU . .
H17 H 0.0253 -0.1919 0.2165 0.075 Uiso 1 1 calc R . .
C18 C 0.1196(8) -0.0940(4) 0.2611(3) 0.065(3) Uani 1 1 d GU . .
H18 H 0.0962 -0.0797 0.2973 0.079 Uiso 1 1 calc R . .
C19 C 0.1959(9) -0.0482(3) 0.2561(4) 0.081(4) Uani 1 1 d GU . .
H19 H 0.2247 -0.0026 0.2889 0.097 Uiso 1 1 calc R . .
C20 C 0.2302(8) -0.0691(4) 0.2031(4) 0.107(4) Uani 1 1 d GU . .
H20 H 0.2824 -0.0378 0.1997 0.128 Uiso 1 1 calc R . .
C21 C 0.1881(6) -0.1357(4) 0.1552(3) 0.088(4) Uani 1 1 d GU . .
H21 H 0.2116 -0.1500 0.1190 0.106 Uiso 1 1 calc R . .
N4 N -0.3761(4) -0.3920(3) 0.0904(2) 0.054(3) Uani 1 1 d GU . .
C22 C -0.4354(5) -0.3657(3) 0.0526(3) 0.057(3) Uani 1 1 d GU . .
H22 H -0.4022 -0.3308 0.0429 0.068 Uiso 1 1 calc R . .
C23 C -0.5432(5) -0.3902(4) 0.0291(3) 0.063(3) Uani 1 1 d GU . .
H23 H -0.5837 -0.3722 0.0033 0.075 Uiso 1 1 calc R . .
C24 C -0.5917(4) -0.4412(4) 0.0433(4) 0.059(3) Uani 1 1 d GU . .
H24 H -0.6653 -0.4580 0.0272 0.070 Uiso 1 1 calc R . .
C25 C -0.5324(5) -0.4676(4) 0.0811(4) 0.062(3) Uani 1 1 d GU . .
H25 H -0.5655 -0.5024 0.0908 0.075 Uiso 1 1 calc R . .
C26 C -0.4246(5) -0.4430(3) 0.1046(3) 0.066(3) Uani 1 1 d GU . .
H26 H -0.3841 -0.4611 0.1304 0.079 Uiso 1 1 calc R . .
N5 N -0.1986(5) -0.2529(3) 0.2143(2) 0.051(3) Uani 1 1 d GU . .
C27 C -0.2783(5) -0.2179(4) 0.2068(3) 0.084(4) Uani 1 1 d GU . .
H27 H -0.3354 -0.2378 0.1694 0.101 Uiso 1 1 calc R . .
C28 C -0.2744(8) -0.1537(4) 0.2540(4) 0.085(4) Uani 1 1 d GU . .
H28 H -0.3289 -0.1297 0.2488 0.102 Uiso 1 1 calc R . .
C29 C -0.1909(9) -0.1245(3) 0.3086(4) 0.078(4) Uani 1 1 d GU . .
H29 H -0.1882 -0.0806 0.3409 0.094 Uiso 1 1 calc R . .
C30 C -0.1112(8) -0.1595(4) 0.3162(3) 0.066(3) Uani 1 1 d GU . .
H30 H -0.0541 -0.1395 0.3535 0.079 Uiso 1 1 calc R . .
C31 C -0.1151(5) -0.2237(4) 0.2690(3) 0.055(3) Uani 1 1 d GU . .
H31 H -0.0606 -0.2477 0.2741 0.067 Uiso 1 1 calc R . .
Ho4 Ho 0.00518(5) -0.16485(3) -0.28916(2) 0.04833(19) Uani 1 1 d . . .
Ho5 Ho 0.02857(4) -0.19088(2) -0.45852(2) 0.03986(17) Uani 1 1 d . . .
Ho6 Ho -0.23247(4) -0.34262(2) -0.54364(2) 0.03745(16) Uani 1 1 d . . .
Ho7 Ho -0.26108(5) -0.32003(2) -0.37498(2) 0.04405(18) Uani 1 1 d . . .
Te8 Te -0.06400(6) -0.29799(3) -0.41645(3) 0.0399(2) Uani 1 1 d . A .
Te9 Te -0.01707(7) -0.06950(3) -0.35840(3) 0.0465(3) Uani 1 1 d . A .
Te10 Te 0.17773(7) -0.09791(4) -0.32615(3) 0.0487(3) Uani 1 1 d . A .
Te11 Te -0.18276(7) -0.19713(3) -0.53991(3) 0.0478(3) Uani 1 1 d . A .
Te12 Te -0.07251(7) -0.29020(4) -0.59828(3) 0.0492(3) Uani 1 1 d . A .
Te13 Te -0.38250(6) -0.28179(4) -0.47446(3) 0.0483(3) Uani 1 1 d . A .
Te14 Te -0.37957(6) -0.43008(4) -0.50832(3) 0.0483(3) Uani 1 1 d . A .
Te15 Te -0.22385(7) -0.16377(4) -0.30071(4) 0.0529(3) Uani 1 1 d . A .
Te16 Te -0.12436(8) -0.23987(4) -0.23590(3) 0.0571(3) Uani 1 1 d . A .
Te17 Te -0.30196(7) -0.12200(4) -0.41711(3) 0.0506(3) Uani 1 1 d . . .
C32 C -0.4320(5) -0.0788(3) -0.4052(3) 0.052(3) Uani 1 1 d GU A .
C33 C -0.4607(6) -0.0662(4) -0.3509(3) 0.067(3) Uani 1 1 d GU . .
H33 H -0.4223 -0.0782 -0.3194 0.080 Uiso 1 1 calc R A .
C34 C -0.5456(7) -0.0362(5) -0.3425(4) 0.079(4) Uani 1 1 d GU A .
H34 H -0.5652 -0.0276 -0.3054 0.095 Uiso 1 1 calc R . .
C35 C -0.6017(6) -0.0186(5) -0.3885(6) 0.080(4) Uani 1 1 d GU . .
H35 H -0.6597 0.0019 -0.3828 0.096 Uiso 1 1 calc R A .
C36 C -0.5730(6) -0.0311(5) -0.4428(5) 0.079(3) Uani 1 1 d GU A .
H36 H -0.6114 -0.0191 -0.4743 0.094 Uiso 1 1 calc R . .
C37 C -0.4882(6) -0.0612(4) -0.4512(3) 0.066(3) Uani 1 1 d GU . .
H37 H -0.4686 -0.0698 -0.4883 0.079 Uiso 1 1 calc R A .
Te18 Te 0.16243(8) -0.22989(4) -0.23033(4) 0.0701(3) Uani 1 1 d . A .
C38 C 0.3133(5) -0.1878(3) -0.2325(3) 0.061(3) Uani 1 1 d GU . .
C39 C 0.3364(6) -0.2064(4) -0.2890(3) 0.069(3) Uani 1 1 d GU A .
H39 H 0.2846 -0.2366 -0.3272 0.083 Uiso 1 1 calc R . .
C40 C 0.4354(7) -0.1807(5) -0.2898(5) 0.076(4) Uani 1 1 d GU A .
H40 H 0.4512 -0.1934 -0.3284 0.091 Uiso 1 1 calc R . .
C41 C 0.5114(6) -0.1366(5) -0.2339(6) 0.081(4) Uani 1 1 d GU A .
H41 H 0.5790 -0.1190 -0.2344 0.098 Uiso 1 1 calc R . .
C42 C 0.4883(5) -0.1180(4) -0.1773(5) 0.087(4) Uani 1 1 d GU A .
H42 H 0.5401 -0.0878 -0.1392 0.105 Uiso 1 1 calc R . .
C43 C 0.3892(6) -0.1437(4) -0.1766(3) 0.075(4) Uani 1 1 d GU A .
H43 H 0.3735 -0.1310 -0.1379 0.090 Uiso 1 1 calc R . .
N6A N 0.0512(9) -0.0539(7) -0.1866(6) 0.095(2) Uani 0.580(9) 1 d PGU A 1
C44A C 0.0702(13) 0.0141(7) -0.1820(7) 0.104(3) Uani 0.580(9) 1 d PGU A 1
H44A H 0.0780 0.0223 -0.2170 0.125 Uiso 0.580(9) 1 calc PR A 1
C45A C 0.0779(18) 0.0701(7) -0.1261(9) 0.110(4) Uani 0.580(9) 1 d PGU A 1
H45A H 0.0909 0.1166 -0.1229 0.131 Uiso 0.580(9) 1 calc PR A 1
C46A C 0.0666(18) 0.0581(10) -0.0748(7) 0.110(4) Uani 0.580(9) 1 d PGU A 1
H46A H 0.0718 0.0963 -0.0367 0.132 Uiso 0.580(9) 1 calc PR A 1
C47A C 0.0475(16) -0.0100(11) -0.0795(6) 0.113(4) Uani 0.580(9) 1 d PGU A 1
H47A H 0.0398 -0.0182 -0.0445 0.135 Uiso 0.580(9) 1 calc PR A 1
C48A C 0.0398(13) -0.0660(8) -0.1354(7) 0.110(4) Uani 0.580(9) 1 d PGU A 1
H48A H 0.0268 -0.1124 -0.1386 0.132 Uiso 0.580(9) 1 calc PR A 1
N6B N 0.0562(14) -0.0609(7) -0.1934(5) 0.095(2) Uani 0.420(9) 1 d PGU A 2
C44B C -0.0117(16) -0.0170(10) -0.1777(7) 0.098(4) Uani 0.420(9) 1 d PGU A 2
H44B H -0.0811 -0.0290 -0.2045 0.117 Uiso 0.420(9) 1 calc PR A 2
C45B C 0.022(2) 0.0443(10) -0.1229(8) 0.106(4) Uani 0.420(9) 1 d PGU A 2
H45B H -0.0245 0.0742 -0.1121 0.127 Uiso 0.420(9) 1 calc PR A 2
C46B C 0.123(2) 0.0617(8) -0.0836(6) 0.109(4) Uani 0.420(9) 1 d PGU A 2
H46B H 0.1464 0.1036 -0.0461 0.131 Uiso 0.420(9) 1 calc PR A 2
C47B C 0.1914(16) 0.0179(11) -0.0993(6) 0.113(5) Uani 0.420(9) 1 d PGU A 2
H47B H 0.2608 0.0299 -0.0725 0.135 Uiso 0.420(9) 1 calc PR A 2
C48B C 0.1578(14) -0.0434(10) -0.1542(6) 0.105(4) Uani 0.420(9) 1 d PGU A 2
H48B H 0.2042 -0.0733 -0.1649 0.125 Uiso 0.420(9) 1 calc PR A 2
N7 N 0.1110(4) -0.1152(2) -0.4984(2) 0.038(2) Uani 1 1 d GU A .
C49 C 0.1066(5) -0.0451(2) -0.4783(3) 0.047(3) Uani 1 1 d GU . .
H49 H 0.0765 -0.0245 -0.4457 0.057 Uiso 1 1 calc R A .
C50 C 0.1462(6) -0.0051(3) -0.5059(4) 0.055(3) Uani 1 1 d GU A .
H50 H 0.1432 0.0428 -0.4921 0.066 Uiso 1 1 calc R . .
C51 C 0.1903(7) -0.0352(4) -0.5536(4) 0.053(3) Uani 1 1 d GU . .
H51 H 0.2174 -0.0079 -0.5724 0.063 Uiso 1 1 calc R A .
C52 C 0.1947(7) -0.1054(4) -0.5738(3) 0.055(3) Uani 1 1 d GU A .
H52 H 0.2248 -0.1260 -0.6064 0.066 Uiso 1 1 calc R . .
C53 C 0.1551(5) -0.1454(3) -0.5462(3) 0.057(3) Uani 1 1 d GU . .
H53 H 0.1581 -0.1933 -0.5600 0.069 Uiso 1 1 calc R A .
N8 N 0.1709(4) -0.2504(2) -0.46987(18) 0.044(3) Uani 1 1 d GU A .
C54 C 0.1495(5) -0.3232(2) -0.4958(3) 0.045(3) Uani 1 1 d GU . .
H54 H 0.0801 -0.3490 -0.5072 0.054 Uiso 1 1 calc R A .
C55 C 0.2295(6) -0.3581(3) -0.5051(4) 0.059(3) Uani 1 1 d GU A .
H55 H 0.2149 -0.4078 -0.5228 0.071 Uiso 1 1 calc R . .
C56 C 0.3310(6) -0.3203(4) -0.4884(4) 0.067(3) Uani 1 1 d GU . .
H56 H 0.3858 -0.3441 -0.4947 0.080 Uiso 1 1 calc R A .
C57 C 0.3525(4) -0.2475(4) -0.4625(4) 0.061(3) Uani 1 1 d GU A .
H57 H 0.4219 -0.2217 -0.4511 0.073 Uiso 1 1 calc R . .
C58 C 0.2724(4) -0.2126(3) -0.4532(3) 0.045(3) Uani 1 1 d GU . .
H58 H 0.2871 -0.1629 -0.4355 0.054 Uiso 1 1 calc R A .
N9A N -0.3631(11) -0.3818(4) -0.6466(5) 0.058(3) Uani 0.577(7) 1 d PDU A 1
C59A C -0.4052(14) -0.3388(6) -0.6704(5) 0.071(3) Uani 0.577(7) 1 d PDU A 1
H59A H -0.3922 -0.2901 -0.6448 0.085 Uiso 0.577(7) 1 calc PR A 1
C60A C -0.4678(16) -0.3665(6) -0.7328(6) 0.075(3) Uani 0.577(7) 1 d PDU A 1
H60A H -0.4859 -0.3370 -0.7531 0.090 Uiso 0.577(7) 1 calc PR A 1
C61A C -0.5019(16) -0.4373(5) -0.7634(6) 0.074(4) Uani 0.577(7) 1 d PDU A 1
H61A H -0.5445 -0.4579 -0.8059 0.089 Uiso 0.577(7) 1 calc PR A 1
C62A C -0.4743(10) -0.4794(6) -0.7326(5) 0.081(4) Uani 0.577(7) 1 d PDU A 1
H62A H -0.4984 -0.5288 -0.7543 0.097 Uiso 0.577(7) 1 calc PR A 1
C63A C -0.4138(8) -0.4510(5) -0.6722(5) 0.073(4) Uani 0.577(7) 1 d PDU A 1
H63A H -0.4065 -0.4780 -0.6483 0.088 Uiso 0.577(7) 1 calc PR A 1
N9B N -0.3574(7) -0.3742(6) -0.6493(5) 0.062(3) Uani 0.423(7) 1 d PGDU A 2
C59B C -0.3342(11) -0.3454(8) -0.6892(7) 0.063(4) Uani 0.423(7) 1 d PGDU A 2
H59B H -0.2635 -0.3290 -0.6856 0.076 Uiso 0.423(7) 1 calc PR A 2
C60B C -0.4145(16) -0.3408(11) -0.7343(8) 0.069(4) Uani 0.423(7) 1 d PGDU A 2
H60B H -0.3986 -0.3211 -0.7616 0.082 Uiso 0.423(7) 1 calc PR A 2
C61B C -0.5179(14) -0.3648(13) -0.7396(9) 0.074(4) Uani 0.423(7) 1 d PGDU A 2
H61B H -0.5728 -0.3616 -0.7704 0.089 Uiso 0.423(7) 1 calc PR A 2
C62B C -0.5411(8) -0.3935(11) -0.6996(9) 0.077(4) Uani 0.423(7) 1 d PGDU A 2
H62B H -0.6118 -0.4099 -0.7032 0.093 Uiso 0.423(7) 1 calc PR A 2
C63B C -0.4608(8) -0.3982(8) -0.6545(7) 0.068(3) Uani 0.423(7) 1 d PGDU A 2
H63B H -0.4767 -0.4178 -0.6272 0.082 Uiso 0.423(7) 1 calc PR A 2
N10 N -0.1731(3) -0.4527(2) -0.5850(2) 0.037(2) Uani 1 1 d GU A .
C64 C -0.1817(5) -0.4849(3) -0.6484(2) 0.051(3) Uani 1 1 d GU . .
H64 H -0.2075 -0.4635 -0.6754 0.061 Uiso 1 1 calc R A .
C65 C -0.1525(7) -0.5483(3) -0.6725(3) 0.063(3) Uani 1 1 d GU A .
H65 H -0.1583 -0.5703 -0.7158 0.075 Uiso 1 1 calc R . .
C66 C -0.1146(7) -0.5795(3) -0.6330(4) 0.064(3) Uani 1 1 d GU . .
H66 H -0.0947 -0.6229 -0.6495 0.077 Uiso 1 1 calc R A .
C67 C -0.1061(6) -0.5474(3) -0.5696(4) 0.053(3) Uani 1 1 d GU A .
H67 H -0.0802 -0.5688 -0.5426 0.064 Uiso 1 1 calc R . .
C68 C -0.1353(5) -0.4840(3) -0.5456(3) 0.036(3) Uani 1 1 d GU . .
H68 H -0.1295 -0.4620 -0.5022 0.043 Uiso 1 1 calc R A .
N11 N -0.2348(5) -0.4240(3) -0.3610(2) 0.076(3) Uani 1 1 d GU A .
C69 C -0.3223(5) -0.4753(4) -0.3751(3) 0.089(4) Uani 1 1 d GU . .
H69 H -0.3902 -0.4688 -0.3900 0.106 Uiso 1 1 calc R A .
C70 C -0.3105(8) -0.5362(4) -0.3675(4) 0.104(4) Uani 1 1 d GU A .
H70 H -0.3703 -0.5713 -0.3772 0.125 Uiso 1 1 calc R . .
C71 C -0.2111(9) -0.5458(4) -0.3458(5) 0.106(4) Uani 1 1 d GU . .
H71 H -0.2030 -0.5874 -0.3406 0.127 Uiso 1 1 calc R A .
C72 C -0.1236(7) -0.4944(5) -0.3316(4) 0.103(4) Uani 1 1 d GU A .
H72 H -0.0557 -0.5010 -0.3167 0.124 Uiso 1 1 calc R . .
C73 C -0.1354(5) -0.4336(4) -0.3392(3) 0.091(4) Uani 1 1 d GU . .
H73 H -0.0756 -0.3985 -0.3295 0.109 Uiso 1 1 calc R A .
N12 N -0.4161(5) -0.3343(3) -0.3364(3) 0.060(3) Uani 1 1 d GU A .
C74 C -0.4048(6) -0.3045(4) -0.2725(3) 0.074(4) Uani 1 1 d GU . .
H74 H -0.3389 -0.2775 -0.2435 0.089 Uiso 1 1 calc R A .
C75 C -0.4900(8) -0.3141(6) -0.2511(4) 0.085(4) Uani 1 1 d GU A .
H75 H -0.4823 -0.2938 -0.2074 0.101 Uiso 1 1 calc R . .
C76 C -0.5865(7) -0.3536(6) -0.2935(5) 0.082(4) Uani 1 1 d GU . .
H76 H -0.6447 -0.3602 -0.2788 0.098 Uiso 1 1 calc R A .
C77 C -0.5978(5) -0.3834(5) -0.3574(5) 0.086(4) Uani 1 1 d GU A .
H77 H -0.6637 -0.4104 -0.3864 0.103 Uiso 1 1 calc R . .
C78 C -0.5126(5) -0.3738(4) -0.3789(3) 0.076(4) Uani 1 1 d GU . .
H78 H -0.5203 -0.3942 -0.4226 0.092 Uiso 1 1 calc R A .
N13 N -0.4655(9) -0.1880(6) 0.0887(5) 0.203(4) Uani 1 1 d GU . .
C79 C -0.4050(11) -0.1270(7) 0.0942(6) 0.210(4) Uani 1 1 d GU . .
H79 H -0.3587 -0.1296 0.0695 0.252 Uiso 1 1 calc R . .
C80 C -0.4123(16) -0.0622(6) 0.1358(8) 0.225(4) Uani 1 1 d GU . .
H80 H -0.3709 -0.0205 0.1395 0.270 Uiso 1 1 calc R . .
C81 C -0.4800(18) -0.0584(8) 0.1719(8) 0.219(4) Uani 1 1 d GU . .
H81 H -0.4850 -0.0142 0.2003 0.263 Uiso 1 1 calc R . .
C82 C -0.5405(14) -0.1194(10) 0.1664(7) 0.216(4) Uani 1 1 d GU . .
H82 H -0.5868 -0.1169 0.1910 0.259 Uiso 1 1 calc R . .
C83 C -0.5333(10) -0.1842(8) 0.1248(6) 0.205(4) Uani 1 1 d GU . .
H83 H -0.5746 -0.2259 0.1210 0.246 Uiso 1 1 calc R . .
N14 N -0.4389(6) -0.3426(4) -0.0954(3) 0.118(3) Uani 0.93 1 d PGU B 1
C84 C -0.4545(7) -0.2754(4) -0.0825(5) 0.115(4) Uani 0.93 1 d PGU B 1
H84 H -0.3975 -0.2361 -0.0584 0.139 Uiso 0.93 1 calc PR B 1
C85 C -0.5533(8) -0.2655(5) -0.1048(6) 0.130(4) Uani 0.93 1 d PGU B 1
H85 H -0.5640 -0.2195 -0.0959 0.156 Uiso 0.93 1 calc PR B 1
C86 C -0.6367(7) -0.3229(7) -0.1400(5) 0.120(4) Uani 0.93 1 d PGU B 1
H86 H -0.7043 -0.3162 -0.1553 0.144 Uiso 0.93 1 calc PR B 1
C87 C -0.6212(6) -0.3902(6) -0.1530(4) 0.113(4) Uani 0.93 1 d PGU B 1
H87 H -0.6782 -0.4295 -0.1771 0.135 Uiso 0.93 1 calc PR B 1
C88 C -0.5223(6) -0.4001(4) -0.1307(4) 0.107(4) Uani 0.93 1 d PGU B 1
H88 H -0.5117 -0.4461 -0.1396 0.129 Uiso 0.93 1 calc PR B 1
N15 N -0.2165(8) -0.0793(5) -0.1031(4) 0.163(4) Uani 0.93 1 d PGU C 1
C89 C -0.2319(10) -0.0115(5) -0.0848(5) 0.148(3) Uani 0.93 1 d PGU C 1
H89 H -0.2046 0.0182 -0.1016 0.178 Uiso 0.93 1 calc PR C 1
C90 C -0.2873(12) 0.0129(6) -0.0420(6) 0.155(3) Uani 0.93 1 d PGU C 1
H90 H -0.2978 0.0593 -0.0295 0.185 Uiso 0.93 1 calc PR C 1
C91 C -0.3272(11) -0.0305(8) -0.0174(6) 0.173(4) Uani 0.93 1 d PGU C 1
H91 H -0.3651 -0.0138 0.0118 0.207 Uiso 0.93 1 calc PR C 1
C92 C -0.3118(11) -0.0983(7) -0.0357(6) 0.177(4) Uani 0.93 1 d PGU C 1
H92 H -0.3391 -0.1280 -0.0189 0.213 Uiso 0.93 1 calc PR C 1
C93 C -0.2564(10) -0.1228(5) -0.0785(5) 0.175(4) Uani 0.93 1 d PGU C 1
H93 H -0.2459 -0.1691 -0.0910 0.211 Uiso 0.93 1 calc PR C 1
Te19 Te -0.26238(6) -0.209247(9) -0.059378(4) 0.061(3) Uani 0.07 1 d PDU D 2
Te20 Te -0.265720(9) -0.141464(14) -0.134317(6) 0.065(3) Uani 0.07 1 d PDU D 2
C94 C -0.40026(6) -0.290429(14) -0.094193(7) 0.1323(16) Uiso 0.07 1 d PGDU D 2
C95 C -0.49430(6) -0.27360(2) -0.086584(10) 0.1323(16) Uiso 0.07 1 d PGDU D 2
H95 H -0.4974 -0.2261 -0.0659 0.159 Uiso 0.07 1 calc PR D 2
C96 C -0.58386(6) -0.32633(3) -0.109198(13) 0.1323(16) Uiso 0.07 1 d PGDU D 2
H96 H -0.6481 -0.3148 -0.1040 0.159 Uiso 0.07 1 calc PR D 2
C97 C -0.57937(7) -0.39589(2) -0.139421(13) 0.1323(16) Uiso 0.07 1 d PGDU D 2
H97 H -0.6406 -0.4319 -0.1549 0.159 Uiso 0.07 1 calc PR D 2
C98 C -0.48533(7) -0.412721(16) -0.147031(11) 0.1323(16) Uiso 0.07 1 d PGDU D 2
H98 H -0.4823 -0.4603 -0.1677 0.159 Uiso 0.07 1 calc PR D 2
C99 C -0.39577(6) -0.359991(14) -0.124417(8) 0.1323(16) Uiso 0.07 1 d PGDU D 2
H99 H -0.3315 -0.3715 -0.1296 0.159 Uiso 0.07 1 calc PR D 2
C100 C -0.242380(15) -0.03097(2) -0.081953(10) 0.1323(16) Uiso 0.07 1 d PGDU D
2
C101 C -0.16365(2) 0.00335(2) -0.025216(12) 0.1323(16) Uiso 0.07 1 d PGDU D 2
H101 H -0.1202 -0.0222 -0.0097 0.159 Uiso 0.07 1 calc PR D 2
C102 C -0.14849(3) 0.07512(2) 0.008795(13) 0.1323(16) Uiso 0.07 1 d PGDU D 2
H102 H -0.0947 0.0986 0.0476 0.159 Uiso 0.07 1 calc PR D 2
C103 C -0.21206(3) 0.11257(2) -0.013932(15) 0.1323(16) Uiso 0.07 1 d PGDU D 2
H103 H -0.2017 0.1616 0.0093 0.159 Uiso 0.07 1 calc PR D 2
C104 C -0.29079(3) 0.07824(2) -0.070670(16) 0.1323(16) Uiso 0.07 1 d PGDU D 2
H104 H -0.3342 0.1038 -0.0862 0.159 Uiso 0.07 1 calc PR D 2
C105 C -0.305952(19) 0.00648(2) -0.104681(13) 0.1323(16) Uiso 0.07 1 d PGDU D 2
H105 H -0.3598 -0.0170 -0.1435 0.159 Uiso 0.07 1 calc PR D 2
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Te Te -0.5308 1.6751 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ho Ho -0.2175 4.6783 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O1 Ho1 N1 164.56(18) . .
O1 Ho1 Te7 96.39(14) . .
N1 Ho1 Te7 99.04(11) . .
O1 Ho1 Te6 83.40(19) . .
N1 Ho1 Te6 97.49(16) . .
Te7 Ho1 Te6 87.99(3) . .
O1 Ho1 Te1 84.08(15) . .
N1 Ho1 Te1 85.18(13) . .
Te7 Ho1 Te1 132.66(3) . .
Te6 Ho1 Te1 138.55(3) . .
O1 Ho1 Te2 83.9(2) . .
N1 Ho1 Te2 98.26(16) . .
Te7 Ho1 Te2 80.37(3) . .
Te6 Ho1 Te2 161.69(3) . .
Te1 Ho1 Te2 52.50(2) . .
O1 Ho1 Te5 83.45(19) . .
N1 Ho1 Te5 85.02(14) . .
Te7 Ho1 Te5 139.85(3) . .
Te6 Ho1 Te5 51.99(2) . .
Te1 Ho1 Te5 87.39(2) . .
Te2 Ho1 Te5 138.95(2) . .
O1 Ho2 N5 96.0(2) . .
O1 Ho2 N4 175.1(2) . .
N5 Ho2 N4 87.63(17) . .
O1 Ho2 Te1 85.53(17) . .
N5 Ho2 Te1 138.07(15) . .
N4 Ho2 Te1 94.03(13) . .
O1 Ho2 Te3 83.70(18) . .
N5 Ho2 Te3 136.49(15) . .
N4 Ho2 Te3 91.41(12) . .
Te1 Ho2 Te3 85.40(3) . .
O1 Ho2 Te2 83.7(2) . .
N5 Ho2 Te2 85.34(15) . .
N4 Ho2 Te2 99.93(14) . .
Te1 Ho2 Te2 53.07(2) . .
Te3 Ho2 Te2 137.33(3) . .
O1 Ho2 Te4 83.14(19) . .
N5 Ho2 Te4 84.04(15) . .
N4 Ho2 Te4 93.96(14) . .
Te1 Ho2 Te4 137.39(3) . .
Te3 Ho2 Te4 52.62(2) . .
Te2 Ho2 Te4 162.11(2) . .
O1 Ho3 N3 91.7(2) . .
O1 Ho3 N2 177.1(3) . .
N3 Ho3 N2 86.1(2) . .
O1 Ho3 Te5 86.87(18) . .
N3 Ho3 Te5 134.76(15) . .
N2 Ho3 Te5 96.03(18) . .
O1 Ho3 Te3 85.13(15) . .
N3 Ho3 Te3 138.46(15) . .
N2 Ho3 Te3 95.11(16) . .
Te5 Ho3 Te3 86.51(2) . .
O1 Ho3 Te4 84.08(19) . .
N3 Ho3 Te4 85.49(15) . .
N2 Ho3 Te4 93.7(2) . .
Te5 Ho3 Te4 139.02(2) . .
Te3 Ho3 Te4 52.97(2) . .
O1 Ho3 Te6 82.46(18) . .
N3 Ho3 Te6 82.49(15) . .
N2 Ho3 Te6 99.2(2) . .
Te5 Ho3 Te6 52.48(2) . .
Te3 Ho3 Te6 137.55(3) . .
Te4 Ho3 Te6 161.64(3) . .
Ho3 O1 Ho1 114.5(3) . .
Ho3 O1 Ho2 114.0(3) . .
Ho1 O1 Ho2 113.3(3) . .
Te2 Te1 Ho2 65.10(3) . .
Te2 Te1 Ho1 64.18(3) . .
Ho2 Te1 Ho1 70.44(2) . .
Te2 Te1 Te5 160.04(4) . 2_545
Ho2 Te1 Te5 101.54(3) . 2_545
Ho1 Te1 Te5 98.02(3) . 2_545
Te1 Te2 Ho1 63.32(3) . .
Te1 Te2 Ho2 61.83(3) . .
Ho1 Te2 Ho2 69.02(3) . .
Te4 Te3 Ho3 65.05(2) . .
Te4 Te3 Ho2 64.90(3) . .
Ho3 Te3 Ho2 70.63(2) . .
Te4 Te3 Te5 161.49(3) . 2_545
Ho3 Te3 Te5 99.49(3) . 2_545
Ho2 Te3 Te5 101.30(3) . 2_545
Te3 Te4 Ho3 61.97(3) . .
Te3 Te4 Ho2 62.48(3) . .
Ho3 Te4 Ho2 68.74(2) . .
Te6 Te5 Ho3 65.85(3) . .
Te6 Te5 Ho1 62.92(3) . .
Ho3 Te5 Ho1 69.61(2) . .
Te6 Te5 Te5 159.92(5) . 2_545
Ho3 Te5 Te5 101.02(4) . 2_545
Ho1 Te5 Te5 98.86(4) . 2_545
Te6 Te5 Te3 119.09(3) . 2_545
Ho3 Te5 Te3 172.76(3) . 2_545
Ho1 Te5 Te3 107.28(3) . 2_545
Te5 Te5 Te3 72.72(3) 2_545 2_545
Te6 Te5 Te1 122.42(4) . 2_545
Ho3 Te5 Te1 111.11(3) . 2_545
Ho1 Te5 Te1 174.59(3) . 2_545
Te5 Te5 Te1 75.72(3) 2_545 2_545
Te3 Te5 Te1 71.35(2) 2_545 2_545
Te5 Te6 Ho1 65.09(3) . .
Te5 Te6 Ho3 61.68(3) . .
Ho1 Te6 Ho3 68.95(2) . .
C1 Te7 Ho1 112.89(17) . .
C2 C1 C6 120.0 . .
C2 C1 Te7 120.4(3) . .
C6 C1 Te7 119.6(3) . .
C1 C2 C3 120.0 . .
C1 C2 H2 120.0 . .
C3 C2 H2 120.0 . .
C2 C3 C4 120.0 . .
C2 C3 H3 120.0 . .
C4 C3 H3 120.0 . .
C5 C4 C3 120.0 . .
C5 C4 H4 120.0 . .
C3 C4 H4 120.0 . .
C4 C5 C6 120.0 . .
C4 C5 H5 120.0 . .
C6 C5 H5 120.0 . .
C5 C6 C1 120.0 . .
C5 C6 H6 120.0 . .
C1 C6 H6 120.0 . .
C7 N1 C11 120.0 . .
C7 N1 Ho1 122.7(3) . .
C11 N1 Ho1 117.3(3) . .
C8 C7 N1 120.0 . .
C8 C7 H7 120.0 . .
N1 C7 H7 120.0 . .
C7 C8 C9 120.0 . .
C7 C8 H8 120.0 . .
C9 C8 H8 120.0 . .
C10 C9 C8 120.0 . .
C10 C9 H9 120.0 . .
C8 C9 H9 120.0 . .
C11 C10 C9 120.0 . .
C11 C10 H10 120.0 . .
C9 C10 H10 120.0 . .
C10 C11 N1 120.0 . .
C10 C11 H11 120.0 . .
N1 C11 H11 120.0 . .
C12 N2 C16 120.0 . .
C12 N2 Ho3 125.7(4) . .
C16 N2 Ho3 114.2(4) . .
C13 C12 N2 120.0 . .
C13 C12 H12 120.0 . .
N2 C12 H12 120.0 . .
C14 C13 C12 120.0 . .
C14 C13 H13 120.0 . .
C12 C13 H13 120.0 . .
C13 C14 C15 120.0 . .
C13 C14 H14 120.0 . .
C15 C14 H14 120.0 . .
C16 C15 C14 120.0 . .
C16 C15 H15 120.0 . .
C14 C15 H15 120.0 . .
C15 C16 N2 120.0 . .
C15 C16 H16 120.0 . .
N2 C16 H16 120.0 . .
C17 N3 C21 120.0 . .
C17 N3 Ho3 115.2(3) . .
C21 N3 Ho3 124.7(3) . .
C18 C17 N3 120.0 . .
C18 C17 H17 120.0 . .
N3 C17 H17 120.0 . .
C19 C18 C17 120.0 . .
C19 C18 H18 120.0 . .
C17 C18 H18 120.0 . .
C18 C19 C20 120.0 . .
C18 C19 H19 120.0 . .
C20 C19 H19 120.0 . .
C19 C20 C21 120.0 . .
C19 C20 H20 120.0 . .
C21 C20 H20 120.0 . .
C20 C21 N3 120.0 . .
C20 C21 H21 120.0 . .
N3 C21 H21 120.0 . .
C22 N4 C26 120.0 . .
C22 N4 Ho2 121.1(2) . .
C26 N4 Ho2 118.7(2) . .
C23 C22 N4 120.0 . .
C23 C22 H22 120.0 . .
N4 C22 H22 120.0 . .
C24 C23 C22 120.0 . .
C24 C23 H23 120.0 . .
C22 C23 H23 120.0 . .
C23 C24 C25 120.0 . .
C23 C24 H24 120.0 . .
C25 C24 H24 120.0 . .
C24 C25 C26 120.0 . .
C24 C25 H25 120.0 . .
C26 C25 H25 120.0 . .
C25 C26 N4 120.0 . .
C25 C26 H26 120.0 . .
N4 C26 H26 120.0 . .
C27 N5 C31 120.0 . .
C27 N5 Ho2 122.2(3) . .
C31 N5 Ho2 116.9(3) . .
N5 C27 C28 120.0 . .
N5 C27 H27 120.0 . .
C28 C27 H27 120.0 . .
C29 C28 C27 120.0 . .
C29 C28 H28 120.0 . .
C27 C28 H28 120.0 . .
C28 C29 C30 120.0 . .
C28 C29 H29 120.0 . .
C30 C29 H29 120.0 . .
C31 C30 C29 120.0 . .
C31 C30 H30 120.0 . .
C29 C30 H30 120.0 . .
C30 C31 N5 120.0 . .
C30 C31 H31 120.0 . .
N5 C31 H31 120.0 . .
N6A Ho4 Te18 91.9(3) . .
N6A Ho4 Te16 89.2(3) . .
Te18 Ho4 Te16 78.21(3) . .
N6A Ho4 Te15 87.8(3) . .
Te18 Ho4 Te15 134.77(4) . .
Te16 Ho4 Te15 56.56(3) . .
N6A Ho4 Te10 89.2(3) . .
Te18 Ho4 Te10 88.79(3) . .
Te16 Ho4 Te10 166.84(3) . .
Te15 Ho4 Te10 136.41(3) . .
N6A Ho4 Te9 87.3(4) . .
Te18 Ho4 Te9 142.41(4) . .
Te16 Ho4 Te9 139.31(3) . .
Te15 Ho4 Te9 82.79(3) . .
Te10 Ho4 Te9 53.63(3) . .
N6A Ho4 Te8 176.5(3) . .
Te18 Ho4 Te8 91.24(3) . .
Te16 Ho4 Te8 90.02(2) . .
Te15 Ho4 Te8 88.98(2) . .
Te10 Ho4 Te8 92.27(3) . .
Te9 Ho4 Te8 91.01(2) . .
N8 Ho5 N7 86.19(17) . .
N8 Ho5 Te11 137.57(9) . .
N7 Ho5 Te11 89.57(11) . .
N8 Ho5 Te9 137.60(9) . .
N7 Ho5 Te9 93.04(11) . .
Te11 Ho5 Te9 84.75(3) . .
N8 Ho5 Te8 88.31(13) . .
N7 Ho5 Te8 173.81(12) . .
Te11 Ho5 Te8 92.58(3) . .
Te9 Ho5 Te8 92.94(3) . .
N8 Ho5 Te10 83.78(9) . .
N7 Ho5 Te10 89.17(9) . .
Te11 Ho5 Te10 138.40(3) . .
Te9 Ho5 Te10 53.82(2) . .
Te8 Ho5 Te10 93.06(3) . .
N8 Ho5 Te12 83.88(9) . .
N7 Ho5 Te12 84.55(9) . .
Te11 Ho5 Te12 53.69(2) . .
Te9 Ho5 Te12 138.32(3) . .
Te8 Ho5 Te12 92.05(2) . .
Te10 Ho5 Te12 166.50(3) . .
N9A Ho6 N10 88.5(3) . .
N9A Ho6 Te13 92.5(3) . .
N10 Ho6 Te13 140.73(13) . .
N9A Ho6 Te14 89.2(3) . .
N10 Ho6 Te14 82.68(12) . .
Te13 Ho6 Te14 58.10(2) . .
N9A Ho6 Te11 89.5(2) . .
N10 Ho6 Te11 136.61(13) . .
Te13 Ho6 Te11 82.66(3) . .
Te14 Ho6 Te11 140.64(3) . .
N9A Ho6 Te12 87.7(4) . .
N10 Ho6 Te12 83.02(13) . .
Te13 Ho6 Te12 136.25(3) . .
Te14 Ho6 Te12 165.45(3) . .
Te11 Ho6 Te12 53.58(2) . .
N9A Ho6 Te8 177.8(3) . .
N10 Ho6 Te8 89.30(10) . .
Te13 Ho6 Te8 89.48(2) . .
Te14 Ho6 Te8 90.94(3) . .
Te11 Ho6 Te8 91.74(2) . .
Te12 Ho6 Te8 91.56(3) . .
N11 Ho7 N12 84.1(2) . .
N11 Ho7 Te13 138.26(11) . .
N12 Ho7 Te13 92.10(14) . .
N11 Ho7 Te15 140.78(12) . .
N12 Ho7 Te15 88.35(12) . .
Te13 Ho7 Te15 80.29(3) . .
N11 Ho7 Te14 80.85(11) . .
N12 Ho7 Te14 92.29(11) . .
Te13 Ho7 Te14 57.73(2) . .
Te15 Ho7 Te14 138.01(3) . .
N11 Ho7 Te8 96.10(16) . .
N12 Ho7 Te8 177.45(11) . .
Te13 Ho7 Te8 89.48(3) . .
Te15 Ho7 Te8 89.93(3) . .
Te14 Ho7 Te8 90.25(3) . .
N11 Ho7 Te16 85.35(11) . .
N12 Ho7 Te16 88.36(12) . .
Te13 Ho7 Te16 136.20(3) . .
Te15 Ho7 Te16 55.94(2) . .
Te14 Ho7 Te16 166.04(3) . .
Te8 Ho7 Te16 89.11(3) . .
Ho5 Te8 Ho6 81.07(2) . .
Ho5 Te8 Ho7 133.91(3) . .
Ho6 Te8 Ho7 81.17(2) . .
Ho5 Te8 Ho4 80.51(2) . .
Ho6 Te8 Ho4 134.15(3) . .
Ho7 Te8 Ho4 82.17(2) . .
Te10 Te9 Ho5 64.11(2) . .
Te10 Te9 Ho4 63.10(3) . .
Ho5 Te9 Ho4 82.10(2) . .
Te10 Te9 Te17 151.96(3) . .
Ho5 Te9 Te17 97.63(2) . .
Ho4 Te9 Te17 94.74(3) . .
Te9 Te10 Ho4 63.26(3) . .
Te9 Te10 Ho5 62.07(2) . .
Ho4 Te10 Ho5 81.27(2) . .
Te12 Te11 Ho5 64.28(3) . .
Te12 Te11 Ho6 64.01(3) . .
Ho5 Te11 Ho6 82.69(3) . .
Te12 Te11 Te17 151.90(4) . .
Ho5 Te11 Te17 98.41(3) . .
Ho6 Te11 Te17 93.13(3) . .
Te11 Te12 Ho6 62.41(3) . .
Te11 Te12 Ho5 62.03(2) . .
Ho6 Te12 Ho5 81.01(2) . .
Te14 Te13 Ho7 62.21(2) . .
Te14 Te13 Ho6 61.40(3) . .
Ho7 Te13 Ho6 83.97(3) . .
Te14 Te13 Te17 159.28(4) . .
Ho7 Te13 Te17 102.08(3) . .
Ho6 Te13 Te17 105.69(3) . .
Te13 Te14 Ho6 60.50(3) . .
Te13 Te14 Ho7 60.06(2) . .
Ho6 Te14 Ho7 82.47(2) . .
Te16 Te15 Ho7 63.58(2) . .
Te16 Te15 Ho4 61.48(3) . .
Ho7 Te15 Ho4 84.83(3) . .
Te16 Te15 Te17 156.42(4) . .
Ho7 Te15 Te17 98.13(3) . .
Ho4 Te15 Te17 104.25(3) . .
Te15 Te16 Ho4 61.96(3) . .
Te15 Te16 Ho7 60.48(2) . .
Ho4 Te16 Ho7 83.55(3) . .
C32 Te17 Te13 106.11(14) . .
C32 Te17 Te15 106.7(2) . .
Te13 Te17 Te15 75.93(3) . .
C32 Te17 Te11 138.89(18) . .
Te13 Te17 Te11 72.75(3) . .
Te15 Te17 Te11 112.48(3) . .
C32 Te17 Te9 139.12(13) . .
Te13 Te17 Te9 112.51(3) . .
Te15 Te17 Te9 71.46(3) . .
Te11 Te17 Te9 68.21(2) . .
C33 C32 C37 120.0 . .
C33 C32 Te17 120.2(3) . .
C37 C32 Te17 119.8(3) . .
C32 C33 C34 120.0 . .
C32 C33 H33 120.0 . .
C34 C33 H33 120.0 . .
C35 C34 C33 120.0 . .
C35 C34 H34 120.0 . .
C33 C34 H34 120.0 . .
C36 C35 C34 120.0 . .
C36 C35 H35 120.0 . .
C34 C35 H35 120.0 . .
C35 C36 C37 120.0 . .
C35 C36 H36 120.0 . .
C37 C36 H36 120.0 . .
C36 C37 C32 120.0 . .
C36 C37 H37 120.0 . .
C32 C37 H37 120.0 . .
C38 Te18 Ho4 107.74(18) . .
C39 C38 C43 120.0 . .
C39 C38 Te18 120.4(3) . .
C43 C38 Te18 119.6(3) . .
C40 C39 C38 120.0 . .
C40 C39 H39 120.0 . .
C38 C39 H39 120.0 . .
C41 C40 C39 120.0 . .
C41 C40 H40 120.0 . .
C39 C40 H40 120.0 . .
C40 C41 C42 120.0 . .
C40 C41 H41 120.0 . .
C42 C41 H41 120.0 . .
C43 C42 C41 120.0 . .
C43 C42 H42 120.0 . .
C41 C42 H42 120.0 . .
C42 C43 C38 120.0 . .
C42 C43 H43 120.0 . .
C38 C43 H43 120.0 . .
C44A N6A C48A 120.0 . .
C44A N6A Ho4 124.9(6) . .
C48A N6A Ho4 114.4(6) . .
N6A C44A C45A 120.0 . .
N6A C44A H44A 120.0 . .
C45A C44A H44A 120.0 . .
C46A C45A C44A 120.0 . .
C46A C45A H45A 120.0 . .
C44A C45A H45A 120.0 . .
C47A C46A C45A 120.0 . .
C47A C46A H46A 120.0 . .
C45A C46A H46A 120.0 . .
C46A C47A C48A 120.0 . .
C46A C47A H47A 120.0 . .
C48A C47A H47A 120.0 . .
C47A C48A N6A 120.0 . .
C47A C48A H48A 120.0 . .
N6A C48A H48A 120.0 . .
C44B N6B C48B 120.0 . .
C45B C44B N6B 120.0 . .
C45B C44B H44B 120.0 . .
N6B C44B H44B 120.0 . .
C44B C45B C46B 120.0 . .
C44B C45B H45B 120.0 . .
C46B C45B H45B 120.0 . .
C47B C46B C45B 120.0 . .
C47B C46B H46B 120.0 . .
C45B C46B H46B 120.0 . .
C48B C47B C46B 120.0 . .
C48B C47B H47B 120.0 . .
C46B C47B H47B 120.0 . .
C47B C48B N6B 120.0 . .
C47B C48B H48B 120.0 . .
N6B C48B H48B 120.0 . .
C49 N7 C53 120.0 . .
C49 N7 Ho5 121.4(2) . .
C53 N7 Ho5 118.3(2) . .
C50 C49 N7 120.0 . .
C50 C49 H49 120.0 . .
N7 C49 H49 120.0 . .
C49 C50 C51 120.0 . .
C49 C50 H50 120.0 . .
C51 C50 H50 120.0 . .
C52 C51 C50 120.0 . .
C52 C51 H51 120.0 . .
C50 C51 H51 120.0 . .
C51 C52 C53 120.0 . .
C51 C52 H52 120.0 . .
C53 C52 H52 120.0 . .
C52 C53 N7 120.0 . .
C52 C53 H53 120.0 . .
N7 C53 H53 120.0 . .
C54 N8 C58 120.0 . .
C54 N8 Ho5 119.3(2) . .
C58 N8 Ho5 120.6(2) . .
C55 C54 N8 120.0 . .
C55 C54 H54 120.0 . .
N8 C54 H54 120.0 . .
C54 C55 C56 120.0 . .
C54 C55 H55 120.0 . .
C56 C55 H55 120.0 . .
C55 C56 C57 120.0 . .
C55 C56 H56 120.0 . .
C57 C56 H56 120.0 . .
C58 C57 C56 120.0 . .
C58 C57 H57 120.0 . .
C56 C57 H57 120.0 . .
C57 C58 N8 120.0 . .
C57 C58 H58 120.0 . .
N8 C58 H58 120.0 . .
C59A N9A C63A 118.5(11) . .
C59A N9A Ho6 125.1(6) . .
C63A N9A Ho6 114.2(9) . .
N9A C59A C60A 119.7(10) . .
N9A C59A H59A 120.1 . .
C60A C59A H59A 120.1 . .
C61A C60A C59A 117.8(12) . .
C61A C60A H60A 121.1 . .
C59A C60A H60A 121.1 . .
C60A C61A C62A 120.0(11) . .
C60A C61A H61A 120.0 . .
C62A C61A H61A 120.0 . .
C63A C62A C61A 120.9(10) . .
C63A C62A H62A 119.5 . .
C61A C62A H62A 119.5 . .
C62A C63A N9A 117.6(12) . .
C62A C63A H63A 121.2 . .
N9A C63A H63A 121.2 . .
C59B N9B C63B 120.0 . .
N9B C59B C60B 120.0 . .
N9B C59B H59B 120.0 . .
C60B C59B H59B 120.0 . .
C59B C60B C61B 120.0 . .
C59B C60B H60B 120.0 . .
C61B C60B H60B 120.0 . .
C62B C61B C60B 120.0 . .
C62B C61B H61B 120.0 . .
C60B C61B H61B 120.0 . .
C61B C62B C63B 120.0 . .
C61B C62B H62B 120.0 . .
C63B C62B H62B 120.0 . .
C62B C63B N9B 120.0 . .
C62B C63B H63B 120.0 . .
N9B C63B H63B 120.0 . .
C64 N10 C68 120.0 . .
C64 N10 Ho6 119.7(2) . .
C68 N10 Ho6 120.2(2) . .
C65 C64 N10 120.0 . .
C65 C64 H64 120.0 . .
N10 C64 H64 120.0 . .
C64 C65 C66 120.0 . .
C64 C65 H65 120.0 . .
C66 C65 H65 120.0 . .
C67 C66 C65 120.0 . .
C67 C66 H66 120.0 . .
C65 C66 H66 120.0 . .
C68 C67 C66 120.0 . .
C68 C67 H67 120.0 . .
C66 C67 H67 120.0 . .
C67 C68 N10 120.0 . .
C67 C68 H68 120.0 . .
N10 C68 H68 120.0 . .
C69 N11 C73 120.0 . .
C69 N11 Ho7 118.2(3) . .
C73 N11 Ho7 121.8(3) . .
N11 C69 C70 120.0 . .
N11 C69 H69 120.0 . .
C70 C69 H69 120.0 . .
C69 C70 C71 120.0 . .
C69 C70 H70 120.0 . .
C71 C70 H70 120.0 . .
C70 C71 C72 120.0 . .
C70 C71 H71 120.0 . .
C72 C71 H71 120.0 . .
C73 C72 C71 120.0 . .
C73 C72 H72 120.0 . .
C71 C72 H72 120.0 . .
C72 C73 N11 120.0 . .
C72 C73 H73 120.0 . .
N11 C73 H73 120.0 . .
C74 N12 C78 120.0 . .
C74 N12 Ho7 120.0(3) . .
C78 N12 Ho7 120.0(3) . .
C75 C74 N12 120.0 . .
C75 C74 H74 120.0 . .
N12 C74 H74 120.0 . .
C74 C75 C76 120.0 . .
C74 C75 H75 120.0 . .
C76 C75 H75 120.0 . .
C77 C76 C75 120.0 . .
C77 C76 H76 120.0 . .
C75 C76 H76 120.0 . .
C76 C77 C78 120.0 . .
C76 C77 H77 120.0 . .
C78 C77 H77 120.0 . .
C77 C78 N12 120.0 . .
C77 C78 H78 120.0 . .
N12 C78 H78 120.0 . .
C79 N13 C83 120.0 . .
N13 C79 C80 120.0 . .
N13 C79 H79 120.0 . .
C80 C79 H79 120.0 . .
C79 C80 C81 120.0 . .
C79 C80 H80 120.0 . .
C81 C80 H80 120.0 . .
C82 C81 C80 120.0 . .
C82 C81 H81 120.0 . .
C80 C81 H81 120.0 . .
C83 C82 C81 120.0 . .
C83 C82 H82 120.0 . .
C81 C82 H82 120.0 . .
C82 C83 N13 120.0 . .
C82 C83 H83 120.0 . .
N13 C83 H83 120.0 . .
C84 N14 C88 120.0 . .
N14 C84 C85 120.0 . .
N14 C84 H84 120.0 . .
C85 C84 H84 120.0 . .
C84 C85 C86 120.0 . .
C84 C85 H85 120.0 . .
C86 C85 H85 120.0 . .
C87 C86 C85 120.0 . .
C87 C86 H86 120.0 . .
C85 C86 H86 120.0 . .
C86 C87 C88 120.0 . .
C86 C87 H87 120.0 . .
C88 C87 H87 120.0 . .
C87 C88 N14 120.0 . .
C87 C88 H88 120.0 . .
N14 C88 H88 120.0 . .
C89 N15 C93 120.0 . .
C90 C89 N15 120.0 . .
C90 C89 H89 120.0 . .
N15 C89 H89 120.0 . .
C89 C90 C91 120.0 . .
C89 C90 H90 120.0 . .
C91 C90 H90 120.0 . .
C92 C91 C90 120.0 . .
C92 C91 H91 120.0 . .
C90 C91 H91 120.0 . .
C91 C92 C93 120.0 . .
C91 C92 H92 120.0 . .
C93 C92 H92 120.0 . .
C92 C93 N15 120.0 . .
C92 C93 H93 120.0 . .
N15 C93 H93 120.0 . .
C94 Te19 Te20 111.026(17) . .
C100 Te20 Te19 111.097(11) . .
C95 C94 C99 120.0 . .
C95 C94 Te19 120.0 . .
C99 C94 Te19 120.0 . .
C96 C95 C94 120.0 . .
C96 C95 H95 120.0 . .
C94 C95 H95 120.0 . .
C97 C96 C95 120.0 . .
C97 C96 H96 120.0 . .
C95 C96 H96 120.0 . .
C98 C97 C96 120.0 . .
C98 C97 H97 120.0 . .
C96 C97 H97 120.0 . .
C97 C98 C99 120.0 . .
C97 C98 H98 120.0 . .
C99 C98 H98 120.0 . .
C98 C99 C94 120.0 . .
C98 C99 H99 120.0 . .
C94 C99 H99 120.0 . .
C101 C100 C105 120.0 . .
C101 C100 Te20 120.0 . .
C105 C100 Te20 120.0 . .
C102 C101 C100 120.0 . .
C102 C101 H101 120.0 . .
C100 C101 H101 120.0 . .
C101 C102 C103 120.0 . .
C101 C102 H102 120.0 . .
C103 C102 H102 120.0 . .
C104 C103 C102 120.0 . .
C104 C103 H103 120.0 . .
C102 C103 H103 120.0 . .
C105 C104 C103 120.0 . .
C105 C104 H104 120.0 . .
C103 C104 H104 120.0 . .
C104 C105 C100 120.0 . .
C104 C105 H105 120.0 . .
C100 C105 H105 120.0 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ho1 O1 2.128(7) .
Ho1 N1 2.470(7) .
Ho1 Te7 3.0062(9) .
Ho1 Te6 3.1107(12) .
Ho1 Te1 3.1238(9) .
Ho1 Te2 3.1469(12) .
Ho1 Te5 3.1686(10) .
Ho2 O1 2.140(7) .
Ho2 N5 2.476(5) .
Ho2 N4 2.482(5) .
Ho2 Te1 3.0589(10) .
Ho2 Te3 3.0879(10) .
Ho2 Te2 3.1475(11) .
Ho2 Te4 3.1529(11) .
Ho3 O1 2.097(7) .
Ho3 N3 2.443(5) .
Ho3 N2 2.469(8) .
Ho3 Te5 3.0551(10) .
Ho3 Te3 3.0591(9) .
Ho3 Te4 3.1421(11) .
Ho3 Te6 3.1668(11) .
Te1 Te2 2.7737(10) .
Te1 Te5 3.5819(12) 2_545
Te3 Te4 2.7667(10) .
Te3 Te5 3.5665(12) 2_545
Te5 Te6 2.7525(9) .
Te5 Te5 3.5002(14) 2_545
Te5 Te3 3.5665(12) 2_545
Te5 Te1 3.5819(12) 2_545
Te7 C1 2.138(7) .
C1 C2 1.3900 .
C1 C6 1.3900 .
C2 C3 1.3900 .
C2 H2 0.9500 .
C3 C4 1.3900 .
C3 H3 0.9500 .
C4 C5 1.3900 .
C4 H4 0.9500 .
C5 C6 1.3900 .
C5 H5 0.9500 .
C6 H6 0.9500 .
N1 C7 1.3900 .
N1 C11 1.3900 .
C7 C8 1.3900 .
C7 H7 0.9500 .
C8 C9 1.3900 .
C8 H8 0.9500 .
C9 C10 1.3900 .
C9 H9 0.9500 .
C10 C11 1.3900 .
C10 H10 0.9500 .
C11 H11 0.9500 .
N2 C12 1.3900 .
N2 C16 1.3900 .
C12 C13 1.3900 .
C12 H12 0.9500 .
C13 C14 1.3900 .
C13 H13 0.9500 .
C14 C15 1.3900 .
C14 H14 0.9500 .
C15 C16 1.3900 .
C15 H15 0.9500 .
C16 H16 0.9500 .
N3 C17 1.3900 .
N3 C21 1.3900 .
C17 C18 1.3900 .
C17 H17 0.9500 .
C18 C19 1.3900 .
C18 H18 0.9500 .
C19 C20 1.3900 .
C19 H19 0.9500 .
C20 C21 1.3900 .
C20 H20 0.9500 .
C21 H21 0.9500 .
N4 C22 1.3900 .
N4 C26 1.3900 .
C22 C23 1.3900 .
C22 H22 0.9500 .
C23 C24 1.3900 .
C23 H23 0.9500 .
C24 C25 1.3900 .
C24 H24 0.9500 .
C25 C26 1.3900 .
C25 H25 0.9500 .
C26 H26 0.9500 .
N5 C27 1.3900 .
N5 C31 1.3900 .
C27 C28 1.3900 .
C27 H27 0.9500 .
C28 C29 1.3900 .
C28 H28 0.9500 .
C29 C30 1.3900 .
C29 H29 0.9500 .
C30 C31 1.3900 .
C30 H30 0.9500 .
C31 H31 0.9500 .
Ho4 N6A 2.566(11) .
Ho4 Te18 3.0281(12) .
Ho4 Te16 3.0285(12) .
Ho4 Te15 3.0422(12) .
Ho4 Te10 3.0635(12) .
Ho4 Te9 3.0678(10) .
Ho4 Te8 3.1268(7) .
Ho5 N8 2.426(5) .
Ho5 N7 2.446(5) .
Ho5 Te11 3.0240(10) .
Ho5 Te9 3.0277(9) .
Ho5 Te8 3.0672(10) .
Ho5 Te10 3.0829(8) .
Ho5 Te12 3.0846(8) .
Ho6 N9A 2.460(11) .
Ho6 N10 2.470(5) .
Ho6 Te13 3.0111(10) .
Ho6 Te14 3.0375(11) .
Ho6 Te11 3.0389(9) .
Ho6 Te12 3.0819(11) .
Ho6 Te8 3.0952(9) .
Ho7 N11 2.402(7) .
Ho7 N12 2.509(7) .
Ho7 Te13 3.0102(10) .
Ho7 Te15 3.0212(9) .
Ho7 Te14 3.0733(8) .
Ho7 Te8 3.0962(11) .
Ho7 Te16 3.1094(9) .
Te9 Te10 2.7659(13) .
Te9 Te17 3.6535(12) .
Te11 Te12 2.7592(12) .
Te11 Te17 3.6201(12) .
Te13 Te14 2.9371(11) .
Te13 Te17 3.0765(10) .
Te15 Te16 2.8763(13) .
Te15 Te17 3.2410(13) .
Te17 C32 2.098(6) .
C32 C33 1.3900 .
C32 C37 1.3900 .
C33 C34 1.3900 .
C33 H33 0.9500 .
C34 C35 1.3900 .
C34 H34 0.9500 .
C35 C36 1.3900 .
C35 H35 0.9500 .
C36 C37 1.3900 .
C36 H36 0.9500 .
C37 H37 0.9500 .
Te18 C38 2.147(7) .
C38 C39 1.3900 .
C38 C43 1.3900 .
C39 C40 1.3900 .
C39 H39 0.9500 .
C40 C41 1.3900 .
C40 H40 0.9500 .
C41 C42 1.3900 .
C41 H41 0.9500 .
C42 C43 1.3900 .
C42 H42 0.9500 .
C43 H43 0.9500 .
N6A C44A 1.3900 .
N6A C48A 1.3900 .
C44A C45A 1.3900 .
C44A H44A 0.9500 .
C45A C46A 1.3900 .
C45A H45A 0.9500 .
C46A C47A 1.3900 .
C46A H46A 0.9500 .
C47A C48A 1.3900 .
C47A H47A 0.9500 .
C48A H48A 0.9500 .
N6B C44B 1.3900 .
N6B C48B 1.3900 .
C44B C45B 1.3900 .
C44B H44B 0.9500 .
C45B C46B 1.3900 .
C45B H45B 0.9500 .
C46B C47B 1.3900 .
C46B H46B 0.9500 .
C47B C48B 1.3900 .
C47B H47B 0.9500 .
C48B H48B 0.9500 .
N7 C49 1.3900 .
N7 C53 1.3900 .
C49 C50 1.3900 .
C49 H49 0.9500 .
C50 C51 1.3900 .
C50 H50 0.9500 .
C51 C52 1.3900 .
C51 H51 0.9500 .
C52 C53 1.3900 .
C52 H52 0.9500 .
C53 H53 0.9500 .
N8 C54 1.3900 .
N8 C58 1.3900 .
C54 C55 1.3900 .
C54 H54 0.9500 .
C55 C56 1.3900 .
C55 H55 0.9500 .
C56 C57 1.3900 .
C56 H56 0.9500 .
C57 C58 1.3900 .
C57 H57 0.9500 .
C58 H58 0.9500 .
N9A C59A 1.359(16) .
N9A C63A 1.374(13) .
C59A C60A 1.398(15) .
C59A H59A 0.9500 .
C60A C61A 1.359(13) .
C60A H60A 0.9500 .
C61A C62A 1.392(17) .
C61A H61A 0.9500 .
C62A C63A 1.353(13) .
C62A H62A 0.9500 .
C63A H63A 0.9500 .
N9B C59B 1.3900 .
N9B C63B 1.3900 .
C59B C60B 1.3900 .
C59B H59B 0.9500 .
C60B C61B 1.3900 .
C60B H60B 0.9500 .
C61B C62B 1.3900 .
C61B H61B 0.9500 .
C62B C63B 1.3900 .
C62B H62B 0.9500 .
C63B H63B 0.9500 .
N10 C64 1.3900 .
N10 C68 1.3900 .
C64 C65 1.3900 .
C64 H64 0.9500 .
C65 C66 1.3900 .
C65 H65 0.9500 .
C66 C67 1.3900 .
C66 H66 0.9500 .
C67 C68 1.3900 .
C67 H67 0.9500 .
C68 H68 0.9500 .
N11 C69 1.3900 .
N11 C73 1.3900 .
C69 C70 1.3900 .
C69 H69 0.9500 .
C70 C71 1.3900 .
C70 H70 0.9500 .
C71 C72 1.3900 .
C71 H71 0.9500 .
C72 C73 1.3900 .
C72 H72 0.9500 .
C73 H73 0.9500 .
N12 C74 1.3900 .
N12 C78 1.3900 .
C74 C75 1.3900 .
C74 H74 0.9500 .
C75 C76 1.3900 .
C75 H75 0.9500 .
C76 C77 1.3900 .
C76 H76 0.9500 .
C77 C78 1.3900 .
C77 H77 0.9500 .
C78 H78 0.9500 .
N13 C79 1.3900 .
N13 C83 1.3900 .
C79 C80 1.3900 .
C79 H79 0.9500 .
C80 C81 1.3900 .
C80 H80 0.9500 .
C81 C82 1.3900 .
C81 H81 0.9500 .
C82 C83 1.3900 .
C82 H82 0.9500 .
C83 H83 0.9500 .
N14 C84 1.3900 .
N14 C88 1.3900 .
C84 C85 1.3900 .
C84 H84 0.9500 .
C85 C86 1.3900 .
C85 H85 0.9500 .
C86 C87 1.3900 .
C86 H86 0.9500 .
C87 C88 1.3900 .
C87 H87 0.9500 .
C88 H88 0.9500 .
N15 C89 1.3900 .
N15 C93 1.3900 .
C89 C90 1.3900 .
C89 H89 0.9500 .
C90 C91 1.3900 .
C90 H90 0.9500 .
C91 C92 1.3900 .
C91 H91 0.9500 .
C92 C93 1.3900 .
C92 H92 0.9500 .
C93 H93 0.9500 .
Te19 C94 2.1400 .
Te19 Te20 2.6958(3) .
Te20 C100 2.1400 .
C94 C95 1.3900 .
C94 C99 1.3900 .
C95 C96 1.3900 .
C95 H95 0.9500 .
C96 C97 1.3900 .
C96 H96 0.9500 .
C97 C98 1.3900 .
C97 H97 0.9500 .
C98 C99 1.3900 .
C98 H98 0.9500 .
C99 H99 0.9500 .
C100 C101 1.3900 .
C100 C105 1.3900 .
C101 C102 1.3900 .
C101 H101 0.9500 .
C102 C103 1.3900 .
C102 H102 0.9500 .
C103 C104 1.3900 .
C103 H103 0.9500 .
C104 C105 1.3900 .
C104 H104 0.9500 .
C105 H105 0.9500 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
N3 Ho3 O1 Ho1 -112.4(3) . .
N2 Ho3 O1 Ho1 -156(4) . .
Te5 Ho3 O1 Ho1 22.3(2) . .
Te3 Ho3 O1 Ho1 109.1(2) . .
Te4 Ho3 O1 Ho1 162.3(2) . .
Te6 Ho3 O1 Ho1 -30.2(2) . .
N3 Ho3 O1 Ho2 114.8(3) . .
N2 Ho3 O1 Ho2 71(4) . .
Te5 Ho3 O1 Ho2 -110.5(2) . .
Te3 Ho3 O1 Ho2 -23.7(2) . .
Te4 Ho3 O1 Ho2 29.5(2) . .
Te6 Ho3 O1 Ho2 -163.0(3) . .
N1 Ho1 O1 Ho3 -63.5(10) . .
Te7 Ho1 O1 Ho3 118.0(2) . .
Te6 Ho1 O1 Ho3 30.8(2) . .
Te1 Ho1 O1 Ho3 -109.6(2) . .
Te2 Ho1 O1 Ho3 -162.5(2) . .
Te5 Ho1 O1 Ho3 -21.6(2) . .
N1 Ho1 O1 Ho2 69.6(11) . .
Te7 Ho1 O1 Ho2 -108.9(2) . .
Te6 Ho1 O1 Ho2 163.9(3) . .
Te1 Ho1 O1 Ho2 23.5(2) . .
Te2 Ho1 O1 Ho2 -29.3(2) . .
Te5 Ho1 O1 Ho2 111.5(2) . .
N5 Ho2 O1 Ho3 -112.7(3) . .
N4 Ho2 O1 Ho3 24(3) . .
Te1 Ho2 O1 Ho3 109.4(2) . .
Te3 Ho2 O1 Ho3 23.6(2) . .
Te2 Ho2 O1 Ho3 162.7(3) . .
Te4 Ho2 O1 Ho3 -29.4(2) . .
N5 Ho2 O1 Ho1 114.0(3) . .
N4 Ho2 O1 Ho1 -109(3) . .
Te1 Ho2 O1 Ho1 -24.0(2) . .
Te3 Ho2 O1 Ho1 -109.8(2) . .
Te2 Ho2 O1 Ho1 29.3(2) . .
Te4 Ho2 O1 Ho1 -162.8(3) . .
O1 Ho2 Te1 Te2 85.48(18) . .
N5 Ho2 Te1 Te2 -8.5(2) . .
N4 Ho2 Te1 Te2 -99.40(12) . .
Te3 Ho2 Te1 Te2 169.50(3) . .
Te4 Ho2 Te1 Te2 160.29(4) . .
O1 Ho2 Te1 Ho1 15.64(18) . .
N5 Ho2 Te1 Ho1 -78.3(2) . .
N4 Ho2 Te1 Ho1 -169.24(12) . .
Te3 Ho2 Te1 Ho1 99.67(3) . .
Te2 Ho2 Te1 Ho1 -69.83(3) . .
Te4 Ho2 Te1 Ho1 90.46(4) . .
O1 Ho2 Te1 Te5 -78.86(18) . 2_545
N5 Ho2 Te1 Te5 -172.8(2) . 2_545
N4 Ho2 Te1 Te5 96.26(12) . 2_545
Te3 Ho2 Te1 Te5 5.16(3) . 2_545
Te2 Ho2 Te1 Te5 -164.34(4) . 2_545
Te4 Ho2 Te1 Te5 -4.05(5) . 2_545
O1 Ho1 Te1 Te2 -86.84(19) . .
N1 Ho1 Te1 Te2 104.26(14) . .
Te7 Ho1 Te1 Te2 6.41(5) . .
Te6 Ho1 Te1 Te2 -159.87(5) . .
Te5 Ho1 Te1 Te2 -170.52(3) . .
O1 Ho1 Te1 Ho2 -15.77(19) . .
N1 Ho1 Te1 Ho2 175.34(14) . .
Te7 Ho1 Te1 Ho2 77.48(4) . .
Te6 Ho1 Te1 Ho2 -88.80(5) . .
Te2 Ho1 Te1 Ho2 71.07(3) . .
Te5 Ho1 Te1 Ho2 -99.45(3) . .
O1 Ho1 Te1 Te5 83.69(19) . 2_545
N1 Ho1 Te1 Te5 -85.21(14) . 2_545
Te7 Ho1 Te1 Te5 176.94(4) . 2_545
Te6 Ho1 Te1 Te5 10.66(5) . 2_545
Te2 Ho1 Te1 Te5 170.53(4) . 2_545
Te5 Ho1 Te1 Te5 0.01(4) . 2_545
Ho2 Te1 Te2 Ho1 -79.31(2) . .
Te5 Te1 Te2 Ho1 -28.51(12) 2_545 .
Ho1 Te1 Te2 Ho2 79.31(2) . .
Te5 Te1 Te2 Ho2 50.80(12) 2_545 .
O1 Ho1 Te2 Te1 87.21(14) . .
N1 Ho1 Te2 Te1 -77.39(11) . .
Te7 Ho1 Te2 Te1 -175.23(4) . .
Te6 Ho1 Te2 Te1 133.51(9) . .
Te5 Ho1 Te2 Te1 14.50(5) . .
O1 Ho1 Te2 Ho2 19.12(14) . .
N1 Ho1 Te2 Ho2 -145.48(11) . .
Te7 Ho1 Te2 Ho2 116.69(3) . .
Te6 Ho1 Te2 Ho2 65.42(9) . .
Te1 Ho1 Te2 Ho2 -68.09(3) . .
Te5 Ho1 Te2 Ho2 -53.59(4) . .
O1 Ho2 Te2 Te1 -89.13(15) . .
N5 Ho2 Te2 Te1 174.33(14) . .
N4 Ho2 Te2 Te1 87.57(11) . .
Te3 Ho2 Te2 Te1 -15.54(5) . .
Te4 Ho2 Te2 Te1 -131.98(10) . .
O1 Ho2 Te2 Ho1 -19.01(15) . .
N5 Ho2 Te2 Ho1 -115.55(13) . .
N4 Ho2 Te2 Ho1 157.68(11) . .
Te1 Ho2 Te2 Ho1 70.12(3) . .
Te3 Ho2 Te2 Ho1 54.57(4) . .
Te4 Ho2 Te2 Ho1 -61.86(11) . .
O1 Ho3 Te3 Te4 86.25(18) . .
N3 Ho3 Te3 Te4 -0.9(2) . .
N2 Ho3 Te3 Te4 -90.84(19) . .
Te5 Ho3 Te3 Te4 173.41(4) . .
Te6 Ho3 Te3 Te4 159.51(5) . .
O1 Ho3 Te3 Ho2 15.67(18) . .
N3 Ho3 Te3 Ho2 -71.5(2) . .
N2 Ho3 Te3 Ho2 -161.42(19) . .
Te5 Ho3 Te3 Ho2 102.82(3) . .
Te4 Ho3 Te3 Ho2 -70.58(3) . .
Te6 Ho3 Te3 Ho2 88.92(4) . .
O1 Ho3 Te3 Te5 -83.06(18) . 2_545
N3 Ho3 Te3 Te5 -170.2(2) . 2_545
N2 Ho3 Te3 Te5 99.84(19) . 2_545
Te5 Ho3 Te3 Te5 4.09(4) . 2_545
Te4 Ho3 Te3 Te5 -169.31(4) . 2_545
Te6 Ho3 Te3 Te5 -9.81(5) . 2_545
O1 Ho2 Te3 Te4 -86.17(17) . .
N5 Ho2 Te3 Te4 5.87(19) . .
N4 Ho2 Te3 Te4 93.91(13) . .
Te1 Ho2 Te3 Te4 -172.16(3) . .
Te2 Ho2 Te3 Te4 -159.75(4) . .
O1 Ho2 Te3 Ho3 -15.38(17) . .
N5 Ho2 Te3 Ho3 76.65(19) . .
N4 Ho2 Te3 Ho3 164.70(13) . .
Te1 Ho2 Te3 Ho3 -101.37(3) . .
Te2 Ho2 Te3 Ho3 -88.96(4) . .
Te4 Ho2 Te3 Ho3 70.79(3) . .
O1 Ho2 Te3 Te5 80.81(17) . 2_545
N5 Ho2 Te3 Te5 172.85(19) . 2_545
N4 Ho2 Te3 Te5 -99.11(13) . 2_545
Te1 Ho2 Te3 Te5 -5.18(3) . 2_545
Te2 Ho2 Te3 Te5 7.23(5) . 2_545
Te4 Ho2 Te3 Te5 166.98(4) . 2_545
Ho2 Te3 Te4 Ho3 79.28(2) . .
Te5 Te3 Te4 Ho3 35.18(13) 2_545 .
Ho3 Te3 Te4 Ho2 -79.28(2) . .
Te5 Te3 Te4 Ho2 -44.10(13) 2_545 .
O1 Ho3 Te4 Te3 -88.36(14) . .
N3 Ho3 Te4 Te3 179.41(16) . .
N2 Ho3 Te4 Te3 93.58(13) . .
Te5 Ho3 Te4 Te3 -10.07(5) . .
Te6 Ho3 Te4 Te3 -131.40(9) . .
O1 Ho3 Te4 Ho2 -19.12(14) . .
N3 Ho3 Te4 Ho2 -111.35(16) . .
N2 Ho3 Te4 Ho2 162.82(13) . .
Te5 Ho3 Te4 Ho2 59.17(5) . .
Te3 Ho3 Te4 Ho2 69.24(3) . .
Te6 Ho3 Te4 Ho2 -62.16(9) . .
O1 Ho2 Te4 Te3 87.30(15) . .
N5 Ho2 Te4 Te3 -175.94(13) . .
N4 Ho2 Te4 Te3 -88.75(11) . .
Te1 Ho2 Te4 Te3 11.58(5) . .
Te2 Ho2 Te4 Te3 130.20(10) . .
O1 Ho2 Te4 Ho3 18.75(15) . .
N5 Ho2 Te4 Ho3 115.51(13) . .
N4 Ho2 Te4 Ho3 -157.29(10) . .
Te1 Ho2 Te4 Ho3 -56.96(4) . .
Te3 Ho2 Te4 Ho3 -68.54(3) . .
Te2 Ho2 Te4 Ho3 61.66(11) . .
O1 Ho3 Te5 Te6 -82.90(16) . .
N3 Ho3 Te5 Te6 6.5(2) . .
N2 Ho3 Te5 Te6 97.02(16) . .
Te3 Ho3 Te5 Te6 -168.20(4) . .
Te4 Ho3 Te5 Te6 -160.17(5) . .
O1 Ho3 Te5 Ho1 -14.34(15) . .
N3 Ho3 Te5 Ho1 75.0(2) . .
N2 Ho3 Te5 Ho1 165.58(16) . .
Te3 Ho3 Te5 Ho1 -99.64(3) . .
Te4 Ho3 Te5 Ho1 -91.61(5) . .
Te6 Ho3 Te5 Ho1 68.56(3) . .
O1 Ho3 Te5 Te5 81.12(16) . 2_545
N3 Ho3 Te5 Te5 170.5(2) . 2_545
N2 Ho3 Te5 Te5 -98.97(16) . 2_545
Te3 Ho3 Te5 Te5 -4.19(4) . 2_545
Te4 Ho3 Te5 Te5 3.85(7) . 2_545
Te6 Ho3 Te5 Te5 164.01(5) . 2_545
O1 Ho3 Te5 Te3 51.4(3) . 2_545
N3 Ho3 Te5 Te3 140.7(3) . 2_545
N2 Ho3 Te5 Te3 -128.7(3) . 2_545
Te3 Ho3 Te5 Te3 -33.9(3) . 2_545
Te4 Ho3 Te5 Te3 -25.9(3) . 2_545
Te6 Ho3 Te5 Te3 134.3(3) . 2_545
O1 Ho3 Te5 Te1 159.93(16) . 2_545
N3 Ho3 Te5 Te1 -110.7(2) . 2_545
N2 Ho3 Te5 Te1 -20.16(16) . 2_545
Te3 Ho3 Te5 Te1 74.62(3) . 2_545
Te4 Ho3 Te5 Te1 82.66(5) . 2_545
Te6 Ho3 Te5 Te1 -117.18(4) . 2_545
O1 Ho1 Te5 Te6 86.72(16) . .
N1 Ho1 Te5 Te6 -103.55(14) . .
Te7 Ho1 Te5 Te6 -5.44(5) . .
Te1 Ho1 Te5 Te6 171.06(3) . .
Te2 Ho1 Te5 Te6 159.59(5) . .
O1 Ho1 Te5 Ho3 14.19(16) . .
N1 Ho1 Te5 Ho3 -176.08(14) . .
Te7 Ho1 Te5 Ho3 -77.97(5) . .
Te6 Ho1 Te5 Ho3 -72.53(3) . .
Te1 Ho1 Te5 Ho3 98.53(2) . .
Te2 Ho1 Te5 Ho3 87.06(4) . .
O1 Ho1 Te5 Te5 -84.35(16) . 2_545
N1 Ho1 Te5 Te5 85.38(14) . 2_545
Te7 Ho1 Te5 Te5 -176.51(4) . 2_545
Te6 Ho1 Te5 Te5 -171.07(5) . 2_545
Te1 Ho1 Te5 Te5 -0.01(4) . 2_545
Te2 Ho1 Te5 Te5 -11.48(6) . 2_545
O1 Ho1 Te5 Te3 -158.90(16) . 2_545
N1 Ho1 Te5 Te3 10.83(14) . 2_545
Te7 Ho1 Te5 Te3 108.94(5) . 2_545
Te6 Ho1 Te5 Te3 114.38(4) . 2_545
Te1 Ho1 Te5 Te3 -74.56(3) . 2_545
Te2 Ho1 Te5 Te3 -86.03(5) . 2_545
O1 Ho1 Te5 Te1 -84.4(4) . 2_545
N1 Ho1 Te5 Te1 85.3(4) . 2_545
Te7 Ho1 Te5 Te1 -176.6(3) . 2_545
Te6 Ho1 Te5 Te1 -171.1(4) . 2_545
Te1 Ho1 Te5 Te1 -0.1(4) . 2_545
Te2 Ho1 Te5 Te1 -11.5(4) . 2_545
Ho3 Te5 Te6 Ho1 78.48(2) . .
Te5 Te5 Te6 Ho1 26.54(15) 2_545 .
Te3 Te5 Te6 Ho1 -95.59(4) 2_545 .
Te1 Te5 Te6 Ho1 179.01(4) 2_545 .
Ho1 Te5 Te6 Ho3 -78.48(2) . .
Te5 Te5 Te6 Ho3 -51.95(15) 2_545 .
Te3 Te5 Te6 Ho3 -174.07(4) 2_545 .
Te1 Te5 Te6 Ho3 100.53(4) 2_545 .
O1 Ho1 Te6 Te5 -86.83(15) . .
N1 Ho1 Te6 Te5 77.64(11) . .
Te7 Ho1 Te6 Te5 176.49(4) . .
Te1 Ho1 Te6 Te5 -13.56(5) . .
Te2 Ho1 Te6 Te5 -133.20(9) . .
O1 Ho1 Te6 Ho3 -19.28(15) . .
N1 Ho1 Te6 Ho3 145.19(11) . .
Te7 Ho1 Te6 Ho3 -115.95(3) . .
Te1 Ho1 Te6 Ho3 54.00(4) . .
Te2 Ho1 Te6 Ho3 -65.64(9) . .
Te5 Ho1 Te6 Ho3 67.56(3) . .
O1 Ho3 Te6 Te5 91.85(15) . .
N3 Ho3 Te6 Te5 -175.38(16) . .
N2 Ho3 Te6 Te5 -90.54(14) . .
Te3 Ho3 Te6 Te5 17.60(5) . .
Te4 Ho3 Te6 Te5 135.06(9) . .
O1 Ho3 Te6 Ho1 19.62(15) . .
N3 Ho3 Te6 Ho1 112.39(16) . .
N2 Ho3 Te6 Ho1 -162.77(14) . .
Te5 Ho3 Te6 Ho1 -72.23(3) . .
Te3 Ho3 Te6 Ho1 -54.63(4) . .
Te4 Ho3 Te6 Ho1 62.84(9) . .
O1 Ho1 Te7 C1 -93.1(3) . .
N1 Ho1 Te7 C1 87.3(3) . .
Te6 Ho1 Te7 C1 -10.0(2) . .
Te1 Ho1 Te7 C1 179.1(2) . .
Te2 Ho1 Te7 C1 -175.8(2) . .
Te5 Ho1 Te7 C1 -5.7(2) . .
Ho1 Te7 C1 C2 59.0(3) . .
Ho1 Te7 C1 C6 -122.3(3) . .
C6 C1 C2 C3 0.0 . .
Te7 C1 C2 C3 178.7(3) . .
C1 C2 C3 C4 0.0 . .
C2 C3 C4 C5 0.0 . .
C3 C4 C5 C6 0.0 . .
C4 C5 C6 C1 0.0 . .
C2 C1 C6 C5 0.0 . .
Te7 C1 C6 C5 -178.7(3) . .
O1 Ho1 N1 C7 -70.6(10) . .
Te7 Ho1 N1 C7 107.9(3) . .
Te6 Ho1 N1 C7 -162.9(3) . .
Te1 Ho1 N1 C7 -24.6(3) . .
Te2 Ho1 N1 C7 26.4(3) . .
Te5 Ho1 N1 C7 -112.4(3) . .
O1 Ho1 N1 C11 107.6(10) . .
Te7 Ho1 N1 C11 -73.9(3) . .
Te6 Ho1 N1 C11 15.2(3) . .
Te1 Ho1 N1 C11 153.6(3) . .
Te2 Ho1 N1 C11 -155.4(3) . .
Te5 Ho1 N1 C11 65.8(3) . .
C11 N1 C7 C8 0.0 . .
Ho1 N1 C7 C8 178.1(3) . .
N1 C7 C8 C9 0.0 . .
C7 C8 C9 C10 0.0 . .
C8 C9 C10 C11 0.0 . .
C9 C10 C11 N1 0.0 . .
C7 N1 C11 C10 0.0 . .
Ho1 N1 C11 C10 -178.2(3) . .
O1 Ho3 N2 C12 -42(5) . .
N3 Ho3 N2 C12 -85.8(4) . .
Te5 Ho3 N2 C12 139.6(4) . .
Te3 Ho3 N2 C12 52.6(4) . .
Te4 Ho3 N2 C12 -0.6(4) . .
Te6 Ho3 N2 C12 -167.5(4) . .
O1 Ho3 N2 C16 133(4) . .
N3 Ho3 N2 C16 89.6(4) . .
Te5 Ho3 N2 C16 -45.1(4) . .
Te3 Ho3 N2 C16 -132.1(4) . .
Te4 Ho3 N2 C16 174.8(4) . .
Te6 Ho3 N2 C16 7.8(4) . .
C16 N2 C12 C13 0.0 . .
Ho3 N2 C12 C13 175.1(4) . .
N2 C12 C13 C14 0.0 . .
C12 C13 C14 C15 0.0 . .
C13 C14 C15 C16 0.0 . .
C14 C15 C16 N2 0.0 . .
C12 N2 C16 C15 0.0 . .
Ho3 N2 C16 C15 -175.7(3) . .
O1 Ho3 N3 C17 -15.6(3) . .
N2 Ho3 N3 C17 162.4(3) . .
Te5 Ho3 N3 C17 -102.9(3) . .
Te3 Ho3 N3 C17 69.0(4) . .
Te4 Ho3 N3 C17 68.3(3) . .
Te6 Ho3 N3 C17 -97.8(3) . .
O1 Ho3 N3 C21 160.4(4) . .
N2 Ho3 N3 C21 -21.6(4) . .
Te5 Ho3 N3 C21 73.1(4) . .
Te3 Ho3 N3 C21 -115.0(4) . .
Te4 Ho3 N3 C21 -115.7(4) . .
Te6 Ho3 N3 C21 78.2(3) . .
C21 N3 C17 C18 0.0 . .
Ho3 N3 C17 C18 176.2(3) . .
N3 C17 C18 C19 0.0 . .
C17 C18 C19 C20 0.0 . .
C18 C19 C20 C21 0.0 . .
C19 C20 C21 N3 0.0 . .
C17 N3 C21 C20 0.0 . .
Ho3 N3 C21 C20 -175.8(4) . .
O1 Ho2 N4 C22 -53(3) . .
N5 Ho2 N4 C22 84.8(3) . .
Te1 Ho2 N4 C22 -137.2(3) . .
Te3 Ho2 N4 C22 -51.7(3) . .
Te2 Ho2 N4 C22 169.6(3) . .
Te4 Ho2 N4 C22 0.9(3) . .
O1 Ho2 N4 C26 123(3) . .
N5 Ho2 N4 C26 -99.8(3) . .
Te1 Ho2 N4 C26 38.2(3) . .
Te3 Ho2 N4 C26 123.7(3) . .
Te2 Ho2 N4 C26 -15.0(3) . .
Te4 Ho2 N4 C26 176.3(3) . .
C26 N4 C22 C23 0.0 . .
Ho2 N4 C22 C23 175.3(2) . .
N4 C22 C23 C24 0.0 . .
C22 C23 C24 C25 0.0 . .
C23 C24 C25 C26 0.0 . .
C24 C25 C26 N4 0.0 . .
C22 N4 C26 C25 0.0 . .
Ho2 N4 C26 C25 -175.4(2) . .
O1 Ho2 N5 C27 139.7(4) . .
N4 Ho2 N5 C27 -37.0(4) . .
Te1 Ho2 N5 C27 -130.3(3) . .
Te3 Ho2 N5 C27 52.6(4) . .
Te2 Ho2 N5 C27 -137.1(3) . .
Te4 Ho2 N5 C27 57.3(3) . .
O1 Ho2 N5 C31 -29.8(3) . .
N4 Ho2 N5 C31 153.5(3) . .
Te1 Ho2 N5 C31 60.1(3) . .
Te3 Ho2 N5 C31 -116.9(3) . .
Te2 Ho2 N5 C31 53.3(3) . .
Te4 Ho2 N5 C31 -112.2(3) . .
C31 N5 C27 C28 0.0 . .
Ho2 N5 C27 C28 -169.2(3) . .
N5 C27 C28 C29 0.0 . .
C27 C28 C29 C30 0.0 . .
C28 C29 C30 C31 0.0 . .
C29 C30 C31 N5 0.0 . .
C27 N5 C31 C30 0.0 . .
Ho2 N5 C31 C30 169.8(3) . .
N8 Ho5 Te8 Ho6 -111.92(9) . .
N7 Ho5 Te8 Ho6 -84.6(10) . .
Te11 Ho5 Te8 Ho6 25.63(2) . .
Te9 Ho5 Te8 Ho6 110.50(3) . .
Te10 Ho5 Te8 Ho6 164.40(3) . .
Te12 Ho5 Te8 Ho6 -28.11(3) . .
N8 Ho5 Te8 Ho7 179.61(9) . .
N7 Ho5 Te8 Ho7 -153.1(9) . .
Te11 Ho5 Te8 Ho7 -42.84(4) . .
Te9 Ho5 Te8 Ho7 42.03(4) . .
Te10 Ho5 Te8 Ho7 95.93(4) . .
Te12 Ho5 Te8 Ho7 -96.58(4) . .
N8 Ho5 Te8 Ho4 110.26(9) . .
N7 Ho5 Te8 Ho4 137.6(10) . .
Te11 Ho5 Te8 Ho4 -112.19(2) . .
Te9 Ho5 Te8 Ho4 -27.32(3) . .
Te10 Ho5 Te8 Ho4 26.58(3) . .
Te12 Ho5 Te8 Ho4 -165.93(3) . .
N9A Ho6 Te8 Ho5 99(8) . .
N10 Ho6 Te8 Ho5 111.12(12) . .
Te13 Ho6 Te8 Ho5 -108.13(3) . .
Te14 Ho6 Te8 Ho5 -166.21(2) . .
Te11 Ho6 Te8 Ho5 -25.48(3) . .
Te12 Ho6 Te8 Ho5 28.12(2) . .
N9A Ho6 Te8 Ho7 -124(8) . .
N10 Ho6 Te8 Ho7 -111.58(12) . .
Te13 Ho6 Te8 Ho7 29.17(2) . .
Te14 Ho6 Te8 Ho7 -28.91(2) . .
Te11 Ho6 Te8 Ho7 111.82(3) . .
Te12 Ho6 Te8 Ho7 165.42(2) . .
N9A Ho6 Te8 Ho4 166(8) . .
N10 Ho6 Te8 Ho4 178.48(13) . .
Te13 Ho6 Te8 Ho4 -40.77(5) . .
Te14 Ho6 Te8 Ho4 -98.85(4) . .
Te11 Ho6 Te8 Ho4 41.87(5) . .
Te12 Ho6 Te8 Ho4 95.48(5) . .
N11 Ho7 Te8 Ho5 177.80(11) . .
N12 Ho7 Te8 Ho5 -89(3) . .
Te13 Ho7 Te8 Ho5 39.26(3) . .
Te15 Ho7 Te8 Ho5 -41.03(4) . .
Te14 Ho7 Te8 Ho5 96.98(3) . .
Te16 Ho7 Te8 Ho5 -96.97(4) . .
N11 Ho7 Te8 Ho6 109.37(11) . .
N12 Ho7 Te8 Ho6 -157(3) . .
Te13 Ho7 Te8 Ho6 -29.18(2) . .
Te15 Ho7 Te8 Ho6 -109.47(2) . .
Te14 Ho7 Te8 Ho6 28.54(2) . .
Te16 Ho7 Te8 Ho6 -165.40(2) . .
N11 Ho7 Te8 Ho4 -113.51(11) . .
N12 Ho7 Te8 Ho4 -20(3) . .
Te13 Ho7 Te8 Ho4 107.95(2) . .
Te15 Ho7 Te8 Ho4 27.66(3) . .
Te14 Ho7 Te8 Ho4 165.67(3) . .
Te16 Ho7 Te8 Ho4 -28.28(2) . .
N6A Ho4 Te8 Ho5 88(6) . .
Te18 Ho4 Te8 Ho5 -115.57(3) . .
Te16 Ho4 Te8 Ho5 166.22(3) . .
Te15 Ho4 Te8 Ho5 109.67(3) . .
Te10 Ho4 Te8 Ho5 -26.74(3) . .
Te9 Ho4 Te8 Ho5 26.90(3) . .
N6A Ho4 Te8 Ho6 21(6) . .
Te18 Ho4 Te8 Ho6 176.85(4) . .
Te16 Ho4 Te8 Ho6 98.64(5) . .
Te15 Ho4 Te8 Ho6 42.09(5) . .
Te10 Ho4 Te8 Ho6 -94.32(5) . .
Te9 Ho4 Te8 Ho6 -40.68(5) . .
N6A Ho4 Te8 Ho7 -49(6) . .
Te18 Ho4 Te8 Ho7 107.30(3) . .
Te16 Ho4 Te8 Ho7 29.10(3) . .
Te15 Ho4 Te8 Ho7 -27.46(3) . .
Te10 Ho4 Te8 Ho7 -163.86(3) . .
Te9 Ho4 Te8 Ho7 -110.22(3) . .
N8 Ho5 Te9 Te10 0.93(19) . .
N7 Ho5 Te9 Te10 -86.75(11) . .
Te11 Ho5 Te9 Te10 -176.03(3) . .
Te8 Ho5 Te9 Te10 91.64(3) . .
Te12 Ho5 Te9 Te10 -171.96(5) . .
N8 Ho5 Te9 Ho4 -62.95(19) . .
N7 Ho5 Te9 Ho4 -150.62(11) . .
Te11 Ho5 Te9 Ho4 120.09(3) . .
Te8 Ho5 Te9 Ho4 27.76(2) . .
Te10 Ho5 Te9 Ho4 -63.88(3) . .
Te12 Ho5 Te9 Ho4 124.16(4) . .
N8 Ho5 Te9 Te17 -156.71(19) . .
N7 Ho5 Te9 Te17 115.61(11) . .
Te11 Ho5 Te9 Te17 26.32(3) . .
Te8 Ho5 Te9 Te17 -66.00(3) . .
Te10 Ho5 Te9 Te17 -157.64(4) . .
Te12 Ho5 Te9 Te17 30.40(5) . .
N6A Ho4 Te9 Te10 91.0(3) . .
Te18 Ho4 Te9 Te10 1.27(4) . .
Te16 Ho4 Te9 Te10 176.72(4) . .
Te15 Ho4 Te9 Te10 179.08(2) . .
Te8 Ho4 Te9 Te10 -92.08(3) . .
N6A Ho4 Te9 Ho5 155.9(3) . .
Te18 Ho4 Te9 Ho5 66.19(4) . .
Te16 Ho4 Te9 Ho5 -118.36(4) . .
Te15 Ho4 Te9 Ho5 -116.00(2) . .
Te10 Ho4 Te9 Ho5 64.92(2) . .
Te8 Ho4 Te9 Ho5 -27.16(3) . .
N6A Ho4 Te9 Te17 -107.1(3) . .
Te18 Ho4 Te9 Te17 163.25(4) . .
Te16 Ho4 Te9 Te17 -21.29(4) . .
Te15 Ho4 Te9 Te17 -18.93(2) . .
Te10 Ho4 Te9 Te17 161.99(3) . .
Te8 Ho4 Te9 Te17 69.91(3) . .
Ho5 Te9 Te10 Ho4 -94.29(2) . .
Te17 Te9 Te10 Ho4 -40.97(7) . .
Ho4 Te9 Te10 Ho5 94.29(2) . .
Te17 Te9 Te10 Ho5 53.32(7) . .
N6A Ho4 Te10 Te9 -87.3(3) . .
Te18 Ho4 Te10 Te9 -179.23(3) . .
Te16 Ho4 Te10 Te9 -170.57(11) . .
Te15 Ho4 Te10 Te9 -1.32(4) . .
Te8 Ho4 Te10 Te9 89.58(3) . .
N6A Ho4 Te10 Ho5 -150.3(3) . .
Te18 Ho4 Te10 Ho5 117.73(2) . .
Te16 Ho4 Te10 Ho5 126.38(11) . .
Te15 Ho4 Te10 Ho5 -64.37(4) . .
Te9 Ho4 Te10 Ho5 -63.05(2) . .
Te8 Ho4 Te10 Ho5 26.53(3) . .
N8 Ho5 Te10 Te9 -179.37(13) . .
N7 Ho5 Te10 Te9 94.38(12) . .
Te11 Ho5 Te10 Te9 5.95(5) . .
Te8 Ho5 Te10 Te9 -91.40(3) . .
Te12 Ho5 Te10 Te9 156.54(13) . .
N8 Ho5 Te10 Ho4 -115.08(13) . .
N7 Ho5 Te10 Ho4 158.67(12) . .
Te11 Ho5 Te10 Ho4 70.25(5) . .
Te9 Ho5 Te10 Ho4 64.29(3) . .
Te8 Ho5 Te10 Ho4 -27.11(3) . .
Te12 Ho5 Te10 Ho4 -139.17(13) . .
N8 Ho5 Te11 Te12 -0.33(19) . .
N7 Ho5 Te11 Te12 83.55(10) . .
Te9 Ho5 Te11 Te12 176.64(3) . .
Te8 Ho5 Te11 Te12 -90.64(3) . .
Te10 Ho5 Te11 Te12 171.82(5) . .
N8 Ho5 Te11 Ho6 64.29(19) . .
N7 Ho5 Te11 Ho6 148.16(10) . .
Te9 Ho5 Te11 Ho6 -118.74(3) . .
Te8 Ho5 Te11 Ho6 -26.03(2) . .
Te10 Ho5 Te11 Ho6 -123.57(4) . .
Te12 Ho5 Te11 Ho6 64.61(3) . .
N8 Ho5 Te11 Te17 156.39(19) . .
N7 Ho5 Te11 Te17 -119.73(10) . .
Te9 Ho5 Te11 Te17 -26.64(3) . .
Te8 Ho5 Te11 Te17 66.07(3) . .
Te10 Ho5 Te11 Te17 -31.46(5) . .
Te12 Ho5 Te11 Te17 156.72(4) . .
N9A Ho6 Te11 Te12 -87.5(4) . .
N10 Ho6 Te11 Te12 -0.17(15) . .
Te13 Ho6 Te11 Te12 179.91(3) . .
Te14 Ho6 Te11 Te12 -175.73(4) . .
Te8 Ho6 Te11 Te12 90.66(3) . .
N9A Ho6 Te11 Ho5 -152.4(4) . .
N10 Ho6 Te11 Ho5 -65.06(15) . .
Te13 Ho6 Te11 Ho5 115.02(2) . .
Te14 Ho6 Te11 Ho5 119.38(4) . .
Te12 Ho6 Te11 Ho5 -64.89(3) . .
Te8 Ho6 Te11 Ho5 25.76(3) . .
N9A Ho6 Te11 Te17 109.5(4) . .
N10 Ho6 Te11 Te17 -163.15(15) . .
Te13 Ho6 Te11 Te17 16.93(2) . .
Te14 Ho6 Te11 Te17 21.29(5) . .
Te12 Ho6 Te11 Te17 -162.98(3) . .
Te8 Ho6 Te11 Te17 -72.32(3) . .
Ho5 Te11 Te12 Ho6 94.47(2) . .
Te17 Te11 Te12 Ho6 38.36(6) . .
Ho6 Te11 Te12 Ho5 -94.47(2) . .
Te17 Te11 Te12 Ho5 -56.11(6) . .
N9A Ho6 Te12 Te11 91.1(2) . .
N10 Ho6 Te12 Te11 179.88(10) . .
Te13 Ho6 Te12 Te11 -0.13(4) . .
Te14 Ho6 Te12 Te11 169.17(11) . .
Te8 Ho6 Te12 Te11 -91.02(3) . .
N9A Ho6 Te12 Ho5 154.2(2) . .
N10 Ho6 Te12 Ho5 -117.06(10) . .
Te13 Ho6 Te12 Ho5 62.93(4) . .
Te14 Ho6 Te12 Ho5 -127.77(11) . .
Te11 Ho6 Te12 Ho5 63.06(2) . .
Te8 Ho6 Te12 Ho5 -27.96(2) . .
N8 Ho5 Te12 Te11 179.78(13) . .
N7 Ho5 Te12 Te11 -93.49(12) . .
Te9 Ho5 Te12 Te11 -5.03(5) . .
Te8 Ho5 Te12 Te11 91.70(3) . .
Te10 Ho5 Te12 Te11 -156.13(13) . .
N8 Ho5 Te12 Ho6 116.32(13) . .
N7 Ho5 Te12 Ho6 -156.94(12) . .
Te11 Ho5 Te12 Ho6 -63.46(3) . .
Te9 Ho5 Te12 Ho6 -68.49(5) . .
Te8 Ho5 Te12 Ho6 28.24(3) . .
Te10 Ho5 Te12 Ho6 140.41(13) . .
N11 Ho7 Te13 Te14 -8.0(2) . .
N12 Ho7 Te13 Te14 -91.38(11) . .
Te15 Ho7 Te13 Te14 -179.35(3) . .
Te8 Ho7 Te13 Te14 90.63(3) . .
Te16 Ho7 Te13 Te14 178.80(5) . .
N11 Ho7 Te13 Ho6 -68.7(2) . .
N12 Ho7 Te13 Ho6 -152.14(11) . .
Te15 Ho7 Te13 Ho6 119.89(3) . .
Te14 Ho7 Te13 Ho6 -60.76(3) . .
Te8 Ho7 Te13 Ho6 29.87(2) . .
Te16 Ho7 Te13 Ho6 118.04(4) . .
N11 Ho7 Te13 Te17 -173.5(2) . .
N12 Ho7 Te13 Te17 103.05(11) . .
Te15 Ho7 Te13 Te17 15.09(3) . .
Te14 Ho7 Te13 Te17 -165.56(4) . .
Te8 Ho7 Te13 Te17 -74.93(3) . .
Te16 Ho7 Te13 Te17 13.23(6) . .
N9A Ho6 Te13 Te14 87.6(3) . .
N10 Ho6 Te13 Te14 -3.17(16) . .
Te11 Ho6 Te13 Te14 176.74(3) . .
Te12 Ho6 Te13 Te14 176.85(4) . .
Te8 Ho6 Te13 Te14 -91.43(3) . .
N9A Ho6 Te13 Ho7 149.1(3) . .
N10 Ho6 Te13 Ho7 58.38(16) . .
Te14 Ho6 Te13 Ho7 61.55(2) . .
Te11 Ho6 Te13 Ho7 -121.70(2) . .
Te12 Ho6 Te13 Ho7 -121.60(4) . .
Te8 Ho6 Te13 Ho7 -29.88(2) . .
N9A Ho6 Te13 Te17 -110.0(3) . .
N10 Ho6 Te13 Te17 159.27(16) . .
Te14 Ho6 Te13 Te17 162.44(4) . .
Te11 Ho6 Te13 Te17 -20.82(3) . .
Te12 Ho6 Te13 Te17 -20.71(5) . .
Te8 Ho6 Te13 Te17 71.01(3) . .
Ho7 Te13 Te14 Ho6 -98.75(3) . .
Te17 Te13 Te14 Ho6 -55.18(11) . .
Ho6 Te13 Te14 Ho7 98.75(3) . .
Te17 Te13 Te14 Ho7 43.57(11) . .
N9A Ho6 Te14 Te13 -93.4(3) . .
N10 Ho6 Te14 Te13 177.98(11) . .
Te11 Ho6 Te14 Te13 -5.10(4) . .
Te12 Ho6 Te14 Te13 -171.30(11) . .
Te8 Ho6 Te14 Te13 88.80(3) . .
N9A Ho6 Te14 Ho7 -153.2(3) . .
N10 Ho6 Te14 Ho7 118.22(11) . .
Te13 Ho6 Te14 Ho7 -59.76(2) . .
Te11 Ho6 Te14 Ho7 -64.86(4) . .
Te12 Ho6 Te14 Ho7 128.94(11) . .
Te8 Ho6 Te14 Ho7 29.05(2) . .
N11 Ho7 Te14 Te13 174.64(17) . .
N12 Ho7 Te14 Te13 91.03(15) . .
Te15 Ho7 Te14 Te13 0.95(5) . .
Te8 Ho7 Te14 Te13 -89.22(3) . .
Te16 Ho7 Te14 Te13 -176.54(14) . .
N11 Ho7 Te14 Ho6 -125.17(16) . .
N12 Ho7 Te14 Ho6 151.23(15) . .
Te13 Ho7 Te14 Ho6 60.19(3) . .
Te15 Ho7 Te14 Ho6 61.15(5) . .
Te8 Ho7 Te14 Ho6 -29.03(3) . .
Te16 Ho7 Te14 Ho6 -116.35(14) . .
N11 Ho7 Te15 Te16 10.6(3) . .
N12 Ho7 Te15 Te16 89.14(14) . .
Te13 Ho7 Te15 Te16 -178.45(4) . .
Te14 Ho7 Te15 Te16 -179.27(5) . .
Te8 Ho7 Te15 Te16 -88.97(3) . .
N11 Ho7 Te15 Ho4 71.3(3) . .
N12 Ho7 Te15 Ho4 149.77(14) . .
Te13 Ho7 Te15 Ho4 -117.82(3) . .
Te14 Ho7 Te15 Ho4 -118.64(5) . .
Te8 Ho7 Te15 Ho4 -28.33(3) . .
Te16 Ho7 Te15 Ho4 60.64(3) . .
N11 Ho7 Te15 Te17 174.9(3) . .
N12 Ho7 Te15 Te17 -106.54(14) . .
Te13 Ho7 Te15 Te17 -14.13(3) . .
Te14 Ho7 Te15 Te17 -14.94(6) . .
Te8 Ho7 Te15 Te17 75.36(3) . .
Te16 Ho7 Te15 Te17 164.33(4) . .
N6A Ho4 Te15 Te16 -90.5(4) . .
Te18 Ho4 Te15 Te16 -0.03(4) . .
Te10 Ho4 Te15 Te16 -177.08(3) . .
Te9 Ho4 Te15 Te16 -178.15(2) . .
Te8 Ho4 Te15 Te16 90.70(3) . .
N6A Ho4 Te15 Ho7 -153.2(4) . .
Te18 Ho4 Te15 Ho7 -62.69(4) . .
Te16 Ho4 Te15 Ho7 -62.66(2) . .
Te10 Ho4 Te15 Ho7 120.25(3) . .
Te9 Ho4 Te15 Ho7 119.18(2) . .
Te8 Ho4 Te15 Ho7 28.04(3) . .
N6A Ho4 Te15 Te17 109.7(4) . .
Te18 Ho4 Te15 Te17 -159.79(3) . .
Te16 Ho4 Te15 Te17 -159.76(3) . .
Te10 Ho4 Te15 Te17 23.16(4) . .
Te9 Ho4 Te15 Te17 22.09(2) . .
Te8 Ho4 Te15 Te17 -69.06(3) . .
Ho7 Te15 Te16 Ho4 98.94(3) . .
Te17 Te15 Te16 Ho4 56.97(9) . .
Ho4 Te15 Te16 Ho7 -98.94(3) . .
Te17 Te15 Te16 Ho7 -41.96(9) . .
N6A Ho4 Te16 Te15 87.9(3) . .
Te18 Ho4 Te16 Te15 179.98(3) . .
Te10 Ho4 Te16 Te15 171.14(11) . .
Te9 Ho4 Te16 Te15 2.81(4) . .
Te8 Ho4 Te16 Te15 -88.76(3) . .
N6A Ho4 Te16 Ho7 147.8(3) . .
Te18 Ho4 Te16 Ho7 -120.13(3) . .
Te15 Ho4 Te16 Ho7 59.89(2) . .
Te10 Ho4 Te16 Ho7 -128.97(11) . .
Te9 Ho4 Te16 Ho7 62.70(4) . .
Te8 Ho4 Te16 Ho7 -28.87(3) . .
N11 Ho7 Te16 Te15 -173.29(16) . .
N12 Ho7 Te16 Te15 -89.12(14) . .
Te13 Ho7 Te16 Te15 2.20(5) . .
Te14 Ho7 Te16 Te15 177.98(14) . .
Te8 Ho7 Te16 Te15 90.52(3) . .
N11 Ho7 Te16 Ho4 125.37(16) . .
N12 Ho7 Te16 Ho4 -150.45(14) . .
Te13 Ho7 Te16 Ho4 -59.13(5) . .
Te15 Ho7 Te16 Ho4 -61.34(3) . .
Te14 Ho7 Te16 Ho4 116.64(14) . .
Te8 Ho7 Te16 Ho4 29.18(3) . .
Te14 Te13 Te17 C32 -156.5(2) . .
Ho7 Te13 Te17 C32 -117.9(2) . .
Ho6 Te13 Te17 C32 155.1(2) . .
Te14 Te13 Te17 Te15 -52.85(11) . .
Ho7 Te13 Te17 Te15 -14.27(3) . .
Ho6 Te13 Te17 Te15 -101.33(3) . .
Te14 Te13 Te17 Te11 66.53(11) . .
Ho7 Te13 Te17 Te11 105.10(3) . .
Ho6 Te13 Te17 Te11 18.05(3) . .
Te14 Te13 Te17 Te9 9.85(13) . .
Ho7 Te13 Te17 Te9 48.42(4) . .
Ho6 Te13 Te17 Te9 -38.63(4) . .
Te16 Te15 Te17 C32 154.18(16) . .
Ho7 Te15 Te17 C32 116.96(14) . .
Ho4 Te15 Te17 C32 -156.35(14) . .
Te16 Te15 Te17 Te13 51.26(9) . .
Ho7 Te15 Te17 Te13 14.04(3) . .
Ho4 Te15 Te17 Te13 100.73(3) . .
Te16 Te15 Te17 Te11 -12.98(10) . .
Ho7 Te15 Te17 Te11 -50.20(4) . .
Ho4 Te15 Te17 Te11 36.49(3) . .
Te16 Te15 Te17 Te9 -68.76(9) . .
Ho7 Te15 Te17 Te9 -105.98(3) . .
Ho4 Te15 Te17 Te9 -19.29(2) . .
Te12 Te11 Te17 C32 -146.1(2) . .
Ho5 Te11 Te17 C32 164.8(2) . .
Ho6 Te11 Te17 C32 -112.1(2) . .
Te12 Te11 Te17 Te13 -51.18(7) . .
Ho5 Te11 Te17 Te13 -100.29(3) . .
Ho6 Te11 Te17 Te13 -17.22(3) . .
Te12 Te11 Te17 Te15 15.00(8) . .
Ho5 Te11 Te17 Te15 -34.11(3) . .
Ho6 Te11 Te17 Te15 48.96(3) . .
Te12 Te11 Te17 Te9 72.59(7) . .
Ho5 Te11 Te17 Te9 23.48(2) . .
Ho6 Te11 Te17 Te9 106.55(3) . .
Te10 Te9 Te17 C32 148.8(3) . .
Ho5 Te9 Te17 C32 -164.5(3) . .
Ho4 Te9 Te17 C32 112.9(3) . .
Te10 Te9 Te17 Te13 -10.88(9) . .
Ho5 Te9 Te17 Te13 35.84(4) . .
Ho4 Te9 Te17 Te13 -46.80(4) . .
Te10 Te9 Te17 Te15 54.50(8) . .
Ho5 Te9 Te17 Te15 101.22(3) . .
Ho4 Te9 Te17 Te15 18.58(2) . .
Te10 Te9 Te17 Te11 -70.12(8) . .
Ho5 Te9 Te17 Te11 -23.41(2) . .
Ho4 Te9 Te17 Te11 -106.05(2) . .
Te13 Te17 C32 C33 86.6(3) . .
Te15 Te17 C32 C33 6.8(3) . .
Te11 Te17 C32 C33 168.6(3) . .
Te9 Te17 C32 C33 -73.9(4) . .
Te13 Te17 C32 C37 -94.8(3) . .
Te15 Te17 C32 C37 -174.6(3) . .
Te11 Te17 C32 C37 -12.8(4) . .
Te9 Te17 C32 C37 104.7(4) . .
C37 C32 C33 C34 0.0 . .
Te17 C32 C33 C34 178.6(3) . .
C32 C33 C34 C35 0.0 . .
C33 C34 C35 C36 0.0 . .
C34 C35 C36 C37 0.0 . .
C35 C36 C37 C32 0.0 . .
C33 C32 C37 C36 0.0 . .
Te17 C32 C37 C36 -178.6(3) . .
N6A Ho4 Te18 C38 -81.9(4) . .
Te16 Ho4 Te18 C38 -170.78(16) . .
Te15 Ho4 Te18 C38 -170.75(16) . .
Te10 Ho4 Te18 C38 7.21(16) . .
Te9 Ho4 Te18 C38 6.20(16) . .
Te8 Ho4 Te18 C38 99.46(16) . .
Ho4 Te18 C38 C39 -70.1(3) . .
Ho4 Te18 C38 C43 112.0(3) . .
C43 C38 C39 C40 0.0 . .
Te18 C38 C39 C40 -177.8(3) . .
C38 C39 C40 C41 0.0 . .
C39 C40 C41 C42 0.0 . .
C40 C41 C42 C43 0.0 . .
C41 C42 C43 C38 0.0 . .
C39 C38 C43 C42 0.0 . .
Te18 C38 C43 C42 177.9(3) . .
Te18 Ho4 N6A C44A 133.1(7) . .
Te16 Ho4 N6A C44A -148.7(8) . .
Te15 Ho4 N6A C44A -92.2(8) . .
Te10 Ho4 N6A C44A 44.3(8) . .
Te9 Ho4 N6A C44A -9.3(7) . .
Te8 Ho4 N6A C44A -71(6) . .
Te18 Ho4 N6A C48A -56.7(6) . .
Te16 Ho4 N6A C48A 21.5(6) . .
Te15 Ho4 N6A C48A 78.0(6) . .
Te10 Ho4 N6A C48A -145.5(6) . .
Te9 Ho4 N6A C48A 160.9(6) . .
Te8 Ho4 N6A C48A 99(6) . .
C48A N6A C44A C45A 0.0 . .
Ho4 N6A C44A C45A 169.7(7) . .
N6A C44A C45A C46A 0.0 . .
C44A C45A C46A C47A 0.0 . .
C45A C46A C47A C48A 0.0 . .
C46A C47A C48A N6A 0.0 . .
C44A N6A C48A C47A 0.0 . .
Ho4 N6A C48A C47A -170.7(6) . .
C48B N6B C44B C45B 0.0 . .
N6B C44B C45B C46B 0.0 . .
C44B C45B C46B C47B 0.0 . .
C45B C46B C47B C48B 0.0 . .
C46B C47B C48B N6B 0.0 . .
C44B N6B C48B C47B 0.0 . .
N8 Ho5 N7 C49 -146.8(3) . .
Te11 Ho5 N7 C49 75.4(2) . .
Te9 Ho5 N7 C49 -9.3(2) . .
Te8 Ho5 N7 C49 -174.2(9) . .
Te10 Ho5 N7 C49 -63.0(2) . .
Te12 Ho5 N7 C49 129.0(2) . .
N8 Ho5 N7 C53 38.7(3) . .
Te11 Ho5 N7 C53 -99.1(3) . .
Te9 Ho5 N7 C53 176.2(3) . .
Te8 Ho5 N7 C53 11.3(11) . .
Te10 Ho5 N7 C53 122.5(3) . .
Te12 Ho5 N7 C53 -45.5(3) . .
C53 N7 C49 C50 0.0 . .
Ho5 N7 C49 C50 -174.4(3) . .
N7 C49 C50 C51 0.0 . .
C49 C50 C51 C52 0.0 . .
C50 C51 C52 C53 0.0 . .
C51 C52 C53 N7 0.0 . .
C49 N7 C53 C52 0.0 . .
Ho5 N7 C53 C52 174.5(3) . .
N7 Ho5 N8 C54 -136.2(3) . .
Te11 Ho5 N8 C54 -51.0(3) . .
Te9 Ho5 N8 C54 133.5(3) . .
Te8 Ho5 N8 C54 41.0(3) . .
Te10 Ho5 N8 C54 134.2(3) . .
Te12 Ho5 N8 C54 -51.3(3) . .
N7 Ho5 N8 C58 41.1(3) . .
Te11 Ho5 N8 C58 126.3(2) . .
Te9 Ho5 N8 C58 -49.3(3) . .
Te8 Ho5 N8 C58 -141.8(2) . .
Te10 Ho5 N8 C58 -48.5(2) . .
Te12 Ho5 N8 C58 126.0(2) . .
C58 N8 C54 C55 0.0 . .
Ho5 N8 C54 C55 177.3(3) . .
N8 C54 C55 C56 0.0 . .
C54 C55 C56 C57 0.0 . .
C55 C56 C57 C58 0.0 . .
C56 C57 C58 N8 0.0 . .
C54 N8 C58 C57 0.0 . .
Ho5 N8 C58 C57 -177.2(3) . .
N10 Ho6 N9A C59A -154.3(15) . .
Te13 Ho6 N9A C59A 65.0(15) . .
Te14 Ho6 N9A C59A 123.0(15) . .
Te11 Ho6 N9A C59A -17.7(15) . .
Te12 Ho6 N9A C59A -71.2(15) . .
Te8 Ho6 N9A C59A -142(7) . .
N10 Ho6 N9A C63A 43.1(11) . .
Te13 Ho6 N9A C63A -97.6(10) . .
Te14 Ho6 N9A C63A -39.5(11) . .
Te11 Ho6 N9A C63A 179.8(11) . .
Te12 Ho6 N9A C63A 126.2(11) . .
Te8 Ho6 N9A C63A 55(9) . .
C63A N9A C59A C60A -27(3) . .
Ho6 N9A C59A C60A 171.2(14) . .
N9A C59A C60A C61A 13(3) . .
C59A C60A C61A C62A 0(3) . .
C60A C61A C62A C63A 0(3) . .
C61A C62A C63A N9A -13(2) . .
C59A N9A C63A C62A 26(2) . .
Ho6 N9A C63A C62A -169.8(10) . .
C63B N9B C59B C60B 0.0 . .
N9B C59B C60B C61B 0.0 . .
C59B C60B C61B C62B 0.0 . .
C60B C61B C62B C63B 0.0 . .
C61B C62B C63B N9B 0.0 . .
C59B N9B C63B C62B 0.0 . .
N9A Ho6 N10 C64 30.0(4) . .
Te13 Ho6 N10 C64 122.2(3) . .
Te14 Ho6 N10 C64 119.5(3) . .
Te11 Ho6 N10 C64 -57.7(3) . .
Te12 Ho6 N10 C64 -57.8(3) . .
Te8 Ho6 N10 C64 -149.5(3) . .
N9A Ho6 N10 C68 -147.3(4) . .
Te13 Ho6 N10 C68 -55.2(3) . .
Te14 Ho6 N10 C68 -57.9(2) . .
Te11 Ho6 N10 C68 124.9(3) . .
Te12 Ho6 N10 C68 124.8(2) . .
Te8 Ho6 N10 C68 33.1(2) . .
C68 N10 C64 C65 0.0 . .
Ho6 N10 C64 C65 -177.4(3) . .
N10 C64 C65 C66 0.0 . .
C64 C65 C66 C67 0.0 . .
C65 C66 C67 C68 0.0 . .
C66 C67 C68 N10 0.0 . .
C64 N10 C68 C67 0.0 . .
Ho6 N10 C68 C67 177.3(3) . .
N12 Ho7 N11 C69 37.0(2) . .
Te13 Ho7 N11 C69 -49.5(3) . .
Te15 Ho7 N11 C69 117.0(2) . .
Te14 Ho7 N11 C69 -56.3(2) . .
Te8 Ho7 N11 C69 -145.6(2) . .
Te16 Ho7 N11 C69 125.8(2) . .
N12 Ho7 N11 C73 -142.9(2) . .
Te13 Ho7 N11 C73 130.7(2) . .
Te15 Ho7 N11 C73 -62.8(3) . .
Te14 Ho7 N11 C73 123.9(2) . .
Te8 Ho7 N11 C73 34.58(19) . .
Te16 Ho7 N11 C73 -54.02(19) . .
C73 N11 C69 C70 0.0 . .
Ho7 N11 C69 C70 -179.8(3) . .
N11 C69 C70 C71 0.0 . .
C69 C70 C71 C72 0.0 . .
C70 C71 C72 C73 0.0 . .
C71 C72 C73 N11 0.0 . .
C69 N11 C73 C72 0.0 . .
Ho7 N11 C73 C72 179.8(3) . .
N11 Ho7 N12 C74 88.2(4) . .
Te13 Ho7 N12 C74 -133.5(4) . .
Te15 Ho7 N12 C74 -53.2(4) . .
Te14 Ho7 N12 C74 168.8(3) . .
Te8 Ho7 N12 C74 -5(3) . .
Te16 Ho7 N12 C74 2.7(4) . .
N11 Ho7 N12 C78 -89.9(3) . .
Te13 Ho7 N12 C78 48.4(3) . .
Te15 Ho7 N12 C78 128.6(3) . .
Te14 Ho7 N12 C78 -9.4(3) . .
Te8 Ho7 N12 C78 176(36) . .
Te16 Ho7 N12 C78 -175.4(3) . .
C78 N12 C74 C75 0.0 . .
Ho7 N12 C74 C75 -178.1(3) . .
N12 C74 C75 C76 0.0 . .
C74 C75 C76 C77 0.0 . .
C75 C76 C77 C78 0.0 . .
C76 C77 C78 N12 0.0 . .
C74 N12 C78 C77 0.0 . .
Ho7 N12 C78 C77 178.1(3) . .
C83 N13 C79 C80 0.0 . .
N13 C79 C80 C81 0.0 . .
C79 C80 C81 C82 0.0 . .
C80 C81 C82 C83 0.0 . .
C81 C82 C83 N13 0.0 . .
C79 N13 C83 C82 0.0 . .
C88 N14 C84 C85 0.0 . .
N14 C84 C85 C86 0.0 . .
C84 C85 C86 C87 0.0 . .
C85 C86 C87 C88 0.0 . .
C86 C87 C88 N14 0.0 . .
C84 N14 C88 C87 0.0 . .
C93 N15 C89 C90 0.0 . .
N15 C89 C90 C91 0.0 . .
C89 C90 C91 C92 0.0 . .
C90 C91 C92 C93 0.0 . .
C91 C92 C93 N15 0.0 . .
C89 N15 C93 C92 0.0 . .
C94 Te19 Te20 C100 126.12(2) . .
Te20 Te19 C94 C95 -75.94(2) . .
Te20 Te19 C94 C99 104.06(2) . .
C99 C94 C95 C96 0.0 . .
Te19 C94 C95 C96 180.0 . .
C94 C95 C96 C97 0.0 . .
C95 C96 C97 C98 0.0 . .
C96 C97 C98 C99 0.0 . .
C97 C98 C99 C94 0.0 . .
C95 C94 C99 C98 0.0 . .
Te19 C94 C99 C98 180.0 . .
Te19 Te20 C100 C101 45.72(2) . .
Te19 Te20 C100 C105 -134.28(2) . .
C105 C100 C101 C102 0.0 . .
Te20 C100 C101 C102 180.0 . .
C100 C101 C102 C103 0.0 . .
C101 C102 C103 C104 0.0 . .
C102 C103 C104 C105 0.0 . .
C103 C104 C105 C100 0.0 . .
C101 C100 C105 C104 0.0 . .
Te20 C100 C105 C104 180.0 . .
