#------------------------------------------------------------------------------
#$Date: 2016-03-25 16:26:56 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179970 $
#$URL: svn://www.crystallography.net/cod/cif/7/02/64/7026492.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7026492
loop_
_publ_author_name
'Xu, Gang'
'Guo, Guo-Cong'
'Guo, Jin-Shuang'
'Guo, Sheng-Ping'
'Jiang, Xiao-Ming'
'Yang, Chen'
'Wang, Ming-Sheng'
'Zhang, Zhang-Jing'
_publ_section_title
;
 Photochromic inorganic-organic hybrid: a new approach for switchable
 photoluminescence in the solid state and partial photochromic phenomenon.
;
_journal_issue                   37
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              8688
_journal_page_last               8692
_journal_paper_doi               10.1039/c0dt00471e
_journal_volume                  39
_journal_year                    2010
_chemical_formula_moiety         '(mv)4BI6CL26 2H2O'
_chemical_formula_sum            'C48 H60 Bi6 Cl26 N8 O2'
_chemical_formula_weight         2956.62
_chemical_melting_point          ?
_chemical_name_common            '(mv)4BI6CL26 2H2O'
_chemical_name_systematic        '(mv)4BI6CL26 2H2O'
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                99.887(12)
_cell_angle_beta                 102.928(9)
_cell_angle_gamma                107.801(9)
_cell_formula_units_Z            1
_cell_length_a                   9.327(2)
_cell_length_b                   12.528(3)
_cell_length_c                   19.738(6)
_cell_measurement_reflns_used    4937
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      27.4835
_cell_measurement_theta_min      2.4340
_cell_volume                     2067.4(9)
_computing_cell_refinement       'CrystalClear (Rigaku Corp., 2002)'
_computing_data_collection       'CrystalClear (Rigaku Corp., 2002)'
_computing_data_reduction        'CrystalClear (Rigaku Corp., 2002)'
_computing_publication_material  'Siemens SHELXTLTM 5'
_computing_structure_refinement  'Siemens SHELXTLTM 5'
_computing_structure_solution    'Siemens SHELXTLTM 5'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.950
_diffrn_measured_fraction_theta_max 0.950
_diffrn_measurement_device_type  'Rigaku Mercury CCD '
_diffrn_measurement_method       'ω '
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'rotating-anode generator'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0358
_diffrn_reflns_av_sigmaI/netI    0.0464
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       -10
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_k_min       -14
_diffrn_reflns_limit_l_max       23
_diffrn_reflns_limit_l_min       -23
_diffrn_reflns_number            14435
_diffrn_reflns_theta_full        25.35
_diffrn_reflns_theta_max         25.35
_diffrn_reflns_theta_min         2.76
_exptl_absorpt_coefficient_mu    13.603
_exptl_absorpt_correction_T_max  1.0000
_exptl_absorpt_correction_T_min  0.5410
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'Sphere (Rigaku CrystalClear)'
_exptl_crystal_colour            yellowish
_exptl_crystal_density_diffrn    2.375
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Prism
_exptl_crystal_F_000             1360
_exptl_crystal_size_max          0.38
_exptl_crystal_size_mid          0.28
_exptl_crystal_size_min          0.27
_refine_diff_density_max         1.847
_refine_diff_density_min         -1.212
_refine_diff_density_rms         0.149
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.072
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     415
_refine_ls_number_reflns         7180
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.072
_refine_ls_R_factor_all          0.0446
_refine_ls_R_factor_gt           0.0321
_refine_ls_shift/su_max          0.008
_refine_ls_shift/su_mean         0.001
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0323P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0704
_refine_ls_wR_factor_ref         0.0748
_reflns_number_gt                5762
_reflns_number_total             7180
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c0dt00471e.txt
_cod_data_source_block           x_yellowish_1
_cod_depositor_comments
;
The following automatic conversions were performed:

'_chemical_melting_point' value 'not measured' was changed to '?' -
the value is undefined or not
given.

'_exptl_absorpt_correction_type' value 'Multi-scan' changed
to 'multi-scan' according to
/home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary named
'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 1891 2012-01-12 08:04:46Z andrius 
;
_cod_original_cell_volume        2067.4(10)
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7026492
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Bi1 Bi 0.108793(8) -0.435973(7) 0.281297(4) 0.01716(2) Uani 1 1 d .
Bi2 Bi 0.167726(8) -0.164905(7) 0.174714(4) 0.01764(2) Uani 1 1 d .
Bi3 Bi 0.525657(8) 0.134308(6) 0.447942(4) 0.01376(2) Uani 1 1 d .
Cl1 Cl -0.09546(6) -0.52696(5) 0.34022(3) 0.03072(18) Uani 1 1 d .
Cl2 Cl -0.05577(7) -0.58731(6) 0.16262(3) 0.03522(19) Uani 1 1 d .
Cl3 Cl 0.26375(6) -0.56625(5) 0.31067(3) 0.03117(18) Uani 1 1 d .
Cl4 Cl 0.32457(6) -0.31614(5) 0.20921(3) 0.02325(16) Uani 1 1 d .
Cl5 Cl -0.05453(6) -0.28450(5) 0.23480(3) 0.02423(16) Uani 1 1 d .
Cl6 Cl 0.38459(7) -0.05644(5) 0.11872(3) 0.03261(19) Uani 1 1 d .
Cl7 Cl 0.00622(7) -0.30919(6) 0.05033(3) 0.0358(2) Uani 1 1 d .
Cl8 Cl 0.00529(7) -0.03140(5) 0.14636(4) 0.03720(19) Uani 1 1 d .
Cl9 Cl 0.34343(6) -0.01269(5) 0.31282(3) 0.03048(19) Uani 1 1 d .
Cl10 Cl 0.73142(6) 0.23158(5) 0.38896(3) 0.02591(16) Uani 1 1 d .
Cl11 Cl 0.37527(6) 0.27100(5) 0.42362(3) 0.02613(16) Uani 1 1 d .
Cl12 Cl 0.68840(5) -0.01887(4) 0.48325(3) 0.02009(15) Uani 1 1 d .
Cl13 Cl 0.70001(6) 0.28078(5) 0.57505(3) 0.03008(19) Uani 1 1 d .
C1 C 0.5015(4) -0.1589(3) -0.03028(17) 0.0663(12) Uani 1 1 d .
H1A H 0.6109 -0.1156 -0.0223 0.099 Uiso 1 1 calc R
H1B H 0.4522 -0.1081 -0.0119 0.099 Uiso 1 1 calc R
H1C H 0.4509 -0.1922 -0.0809 0.099 Uiso 1 1 calc R
C2 C 0.6159(3) -0.2643(3) 0.04854(16) 0.0563(11) Uani 1 1 d .
H2A H 0.7146 -0.2115 0.0528 0.068 Uiso 1 1 calc R
C3 C 0.6049(3) -0.3501(3) 0.08344(15) 0.0485(10) Uani 1 1 d .
H3A H 0.6958 -0.3573 0.1099 0.058 Uiso 1 1 calc R
C4 C 0.4599(3) -0.4257(2) 0.07945(12) 0.0264(7) Uani 1 1 d .
C5 C 0.3282(3) -0.4137(2) 0.03834(14) 0.0381(9) Uani 1 1 d .
H5A H 0.2286 -0.4645 0.0346 0.046 Uiso 1 1 calc R
C6 C 0.3425(3) -0.3272(2) 0.00258(14) 0.0335(8) Uani 1 1 d .
H6A H 0.2533 -0.3192 -0.0250 0.040 Uiso 1 1 calc R
C7 C 0.4431(2) -0.51832(19) 0.11935(12) 0.0244(7) Uani 1 1 d .
C8 C 0.2977(3) -0.5958(2) 0.11439(13) 0.0404(9) Uani 1 1 d .
H8A H 0.2066 -0.5916 0.0859 0.048 Uiso 1 1 calc R
C9 C 0.2878(3) -0.6793(3) 0.15173(14) 0.0446(9) Uani 1 1 d .
H9A H 0.1890 -0.7312 0.1480 0.053 Uiso 1 1 calc R
C10 C 0.4022(3) -0.7762(2) 0.23453(15) 0.0473(9) Uani 1 1 d .
H10A H 0.5054 -0.7691 0.2617 0.071 Uiso 1 1 calc R
H10B H 0.3503 -0.8521 0.2020 0.071 Uiso 1 1 calc R
H10C H 0.3419 -0.7647 0.2668 0.071 Uiso 1 1 calc R
C11 C 0.5561(3) -0.6131(2) 0.19982(18) 0.0539(10) Uani 1 1 d .
H11A H 0.6452 -0.6169 0.2303 0.065 Uiso 1 1 calc R
C12 C 0.5735(3) -0.5302(2) 0.16299(18) 0.0508(10) Uani 1 1 d .
H12A H 0.6741 -0.4807 0.1670 0.061 Uiso 1 1 calc R
C13 C 0.2366(3) 0.4725(2) 0.50641(14) 0.0365(8) Uani 1 1 d .
H13A H 0.3450 0.5230 0.5209 0.055 Uiso 1 1 calc R
H13B H 0.1732 0.5162 0.5184 0.055 Uiso 1 1 calc R
H13C H 0.2023 0.4388 0.4554 0.055 Uiso 1 1 calc R
C14 C 0.3460(3) 0.3767(2) 0.59066(14) 0.0373(9) Uani 1 1 d .
H14A H 0.4440 0.4339 0.5993 0.045 Uiso 1 1 calc R
C15 C 0.3332(3) 0.2905(2) 0.62619(14) 0.0368(8) Uani 1 1 d .
H15A H 0.4223 0.2893 0.6582 0.044 Uiso 1 1 calc R
C16 C 0.1877(2) 0.20527(19) 0.61431(13) 0.0258(7) Uani 1 1 d .
C17 C 0.0609(3) 0.2118(2) 0.56581(17) 0.0486(10) Uani 1 1 d .
H17A H -0.0385 0.1556 0.5558 0.058 Uiso 1 1 calc R
C18 C 0.0794(3) 0.2997(2) 0.53219(17) 0.0477(10) Uani 1 1 d .
H18A H -0.0081 0.3035 0.5005 0.057 Uiso 1 1 calc R
C19 C 0.1700(2) 0.10922(19) 0.65118(12) 0.0241(7) Uani 1 1 d .
C20 C 0.2985(3) 0.0967(2) 0.69531(17) 0.0454(10) Uani 1 1 d .
H20A H 0.3989 0.1495 0.7025 0.054 Uiso 1 1 calc R
C21 C 0.2811(3) 0.0083(2) 0.72863(17) 0.0469(10) Uani 1 1 d .
H21A H 0.3691 0.0018 0.7582 0.056 Uiso 1 1 calc R
C22 C 0.1204(3) -0.1650(2) 0.75369(15) 0.0390(9) Uani 1 1 d .
H22A H 0.2222 -0.1582 0.7822 0.059 Uiso 1 1 calc R
H22B H 0.0742 -0.2377 0.7176 0.059 Uiso 1 1 calc R
H22C H 0.0538 -0.1616 0.7841 0.059 Uiso 1 1 calc R
C23 C 0.0107(3) -0.0602(3) 0.67505(15) 0.0459(10) Uani 1 1 d .
H23A H -0.0886 -0.1147 0.6678 0.055 Uiso 1 1 calc R
C24 C 0.0248(3) 0.0274(2) 0.64099(14) 0.0394(9) Uani 1 1 d .
H24A H -0.0645 0.0314 0.6108 0.047 Uiso 1 1 calc R
N1 N 0.4864(2) -0.25488(19) 0.00816(11) 0.0386(7) Uani 1 1 d .
N2 N 0.4161(2) -0.68842(17) 0.19349(10) 0.0315(6) Uani 1 1 d .
N3 N 0.2203(2) 0.37967(15) 0.54406(10) 0.0253(6) Uani 1 1 d .
N4 N 0.13712(19) -0.06896(16) 0.71860(10) 0.0254(6) Uani 1 1 d .
O1W O 0.8602(5) -0.0987(4) -0.0334(2) 0.0658(16) Uani 0.50 1 d P
O2W O -0.1164(6) -0.8671(4) 0.0541(2) 0.0878(19) Uani 0.50 1 d P
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Bi Bi -4.1077 10.2566 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
Cl1 Bi1 Cl3 93.16(3) . .
Cl1 Bi1 Cl2 89.62(3) . .
Cl3 Bi1 Cl2 89.31(3) . .
Cl1 Bi1 Cl4 173.94(2) . .
Cl3 Bi1 Cl4 92.89(3) . .
Cl2 Bi1 Cl4 90.19(3) . .
Cl1 Bi1 Cl5 92.39(3) . .
Cl3 Bi1 Cl5 173.85(2) . .
Cl2 Bi1 Cl5 88.09(3) . .
Cl4 Bi1 Cl5 81.55(2) . .
Cl1 Bi1 Cl13 87.32(3) . 2_656
Cl3 Bi1 Cl13 85.94(2) . 2_656
Cl2 Bi1 Cl13 174.20(2) . 2_656
Cl4 Bi1 Cl13 93.37(3) . 2_656
Cl5 Bi1 Cl13 96.96(2) . 2_656
Cl7 Bi2 Cl8 89.36(3) . .
Cl7 Bi2 Cl6 90.65(3) . .
Cl8 Bi2 Cl6 92.08(3) . .
Cl7 Bi2 Cl5 89.35(3) . .
Cl8 Bi2 Cl5 90.04(3) . .
Cl6 Bi2 Cl5 177.88(2) . .
Cl7 Bi2 Cl4 90.54(3) . .
Cl8 Bi2 Cl4 175.848(19) . .
Cl6 Bi2 Cl4 92.07(3) . .
Cl5 Bi2 Cl4 85.81(3) . .
Cl7 Bi2 Cl9 178.26(2) . .
Cl8 Bi2 Cl9 91.88(3) . .
Cl6 Bi2 Cl9 90.53(3) . .
Cl5 Bi2 Cl9 89.42(3) . .
Cl4 Bi2 Cl9 88.14(2) . .
Cl11 Bi3 Cl10 92.14(3) . .
Cl11 Bi3 Cl13 90.27(3) . .
Cl10 Bi3 Cl13 90.49(3) . .
Cl11 Bi3 Cl9 88.21(2) . .
Cl10 Bi3 Cl9 88.36(3) . .
Cl13 Bi3 Cl9 178.05(2) . .
Cl11 Bi3 Cl12 91.65(3) . 2_656
Cl10 Bi3 Cl12 176.137(19) . 2_656
Cl13 Bi3 Cl12 88.73(3) . 2_656
Cl9 Bi3 Cl12 92.53(3) . 2_656
Cl11 Bi3 Cl12 176.432(19) . .
Cl10 Bi3 Cl12 90.85(3) . .
Cl13 Bi3 Cl12 87.75(2) . .
Cl9 Bi3 Cl12 93.83(2) . .
Cl12 Bi3 Cl12 85.34(2) 2_656 .
Bi2 Cl4 Bi1 95.99(2) . .
Bi2 Cl5 Bi1 96.45(3) . .
Bi3 Cl9 Bi2 177.82(3) . .
Bi3 Cl12 Bi3 94.66(2) 2_656 .
Bi3 Cl13 Bi1 177.83(3) . 2_656
N1 C1 H1A 109.5 . .
N1 C1 H1B 109.5 . .
H1A C1 H1B 109.5 . .
N1 C1 H1C 109.5 . .
H1A C1 H1C 109.5 . .
H1B C1 H1C 109.5 . .
N1 C2 C3 120.9(2) . .
N1 C2 H2A 119.6 . .
C3 C2 H2A 119.6 . .
C2 C3 C4 119.9(3) . .
C2 C3 H3A 120.0 . .
C4 C3 H3A 120.0 . .
C3 C4 C5 118.2(3) . .
C3 C4 C7 121.4(2) . .
C5 C4 C7 120.4(2) . .
C4 C5 C6 120.8(2) . .
C4 C5 H5A 119.6 . .
C6 C5 H5A 119.6 . .
N1 C6 C5 119.1(2) . .
N1 C6 H6A 120.5 . .
C5 C6 H6A 120.5 . .
C8 C7 C12 116.8(3) . .
C8 C7 C4 121.6(2) . .
C12 C7 C4 121.6(2) . .
C9 C8 C7 119.6(2) . .
C9 C8 H8A 120.2 . .
C7 C8 H8A 120.2 . .
N2 C9 C8 122.2(2) . .
N2 C9 H9A 118.9 . .
C8 C9 H9A 118.9 . .
N2 C10 H10A 109.5 . .
N2 C10 H10B 109.5 . .
H10A C10 H10B 109.5 . .
N2 C10 H10C 109.5 . .
H10A C10 H10C 109.5 . .
H10B C10 H10C 109.5 . .
N2 C11 C12 121.7(2) . .
N2 C11 H11A 119.1 . .
C12 C11 H11A 119.1 . .
C11 C12 C7 120.9(2) . .
C11 C12 H12A 119.6 . .
C7 C12 H12A 119.6 . .
N3 C13 H13A 109.5 . .
N3 C13 H13B 109.5 . .
H13A C13 H13B 109.5 . .
N3 C13 H13C 109.5 . .
H13A C13 H13C 109.5 . .
H13B C13 H13C 109.5 . .
N3 C14 C15 121.1(2) . .
N3 C14 H14A 119.5 . .
C15 C14 H14A 119.5 . .
C14 C15 C16 120.1(2) . .
C14 C15 H15A 120.0 . .
C16 C15 H15A 120.0 . .
C17 C16 C15 116.9(3) . .
C17 C16 C19 121.60(19) . .
C15 C16 C19 121.5(2) . .
C18 C17 C16 120.8(2) . .
C18 C17 H17A 119.6 . .
C16 C17 H17A 119.6 . .
N3 C18 C17 121.0(2) . .
N3 C18 H18A 119.5 . .
C17 C18 H18A 119.5 . .
C24 C19 C20 117.0(3) . .
C24 C19 C16 121.1(2) . .
C20 C19 C16 121.9(2) . .
C21 C20 C19 121.5(2) . .
C21 C20 H20A 119.3 . .
C19 C20 H20A 119.3 . .
N4 C21 C20 120.0(2) . .
N4 C21 H21A 120.0 . .
C20 C21 H21A 120.0 . .
N4 C22 H22A 109.5 . .
N4 C22 H22B 109.5 . .
H22A C22 H22B 109.5 . .
N4 C22 H22C 109.5 . .
H22A C22 H22C 109.5 . .
H22B C22 H22C 109.5 . .
N4 C23 C24 121.4(2) . .
N4 C23 H23A 119.3 . .
C24 C23 H23A 119.3 . .
C23 C24 C19 120.3(2) . .
C23 C24 H24A 119.8 . .
C19 C24 H24A 119.8 . .
C6 N1 C2 121.1(3) . .
C6 N1 C1 118.9(2) . .
C2 N1 C1 120.0(2) . .
C11 N2 C9 118.8(3) . .
C11 N2 C10 120.1(2) . .
C9 N2 C10 121.1(2) . .
C18 N3 C14 120.0(2) . .
C18 N3 C13 119.7(2) . .
C14 N3 C13 120.22(19) . .
C21 N4 C23 119.8(2) . .
C21 N4 C22 119.5(2) . .
C23 N4 C22 120.7(2) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Bi1 Cl1 2.5299(8) .
Bi1 Cl3 2.5458(8) .
Bi1 Cl2 2.5542(9) .
Bi1 Cl4 2.9148(8) .
Bi1 Cl5 2.9161(8) .
Bi1 Cl13 2.9537(10) 2_656
Bi2 Cl7 2.5923(9) .
Bi2 Cl8 2.6263(9) .
Bi2 Cl6 2.6448(8) .
Bi2 Cl5 2.7857(8) .
Bi2 Cl4 2.8081(8) .
Bi2 Cl9 2.8386(9) .
Bi3 Cl11 2.5651(8) .
Bi3 Cl10 2.5653(8) .
Bi3 Cl13 2.6599(9) .
Bi3 Cl9 2.7866(9) .
Bi3 Cl12 2.8364(8) 2_656
Bi3 Cl12 2.8704(8) .
Cl12 Bi3 2.8364(8) 2_656
Cl13 Bi1 2.9537(10) 2_656
C1 N1 1.516(4) .
C1 H1A 0.9600 .
C1 H1B 0.9600 .
C1 H1C 0.9600 .
C2 N1 1.340(4) .
C2 C3 1.363(5) .
C2 H2A 0.9300 .
C3 C4 1.370(3) .
C3 H3A 0.9300 .
C4 C5 1.378(4) .
C4 C7 1.500(4) .
C5 C6 1.381(4) .
C5 H5A 0.9300 .
C6 N1 1.338(3) .
C6 H6A 0.9300 .
C7 C8 1.377(3) .
C7 C12 1.389(4) .
C8 C9 1.372(4) .
C8 H8A 0.9300 .
C9 N2 1.341(3) .
C9 H9A 0.9300 .
C10 N2 1.465(4) .
C10 H10A 0.9600 .
C10 H10B 0.9600 .
C10 H10C 0.9600 .
C11 N2 1.321(3) .
C11 C12 1.357(5) .
C11 H11A 0.9300 .
C12 H12A 0.9300 .
C13 N3 1.472(4) .
C13 H13A 0.9600 .
C13 H13B 0.9600 .
C13 H13C 0.9600 .
C14 N3 1.334(3) .
C14 C15 1.376(4) .
C14 H14A 0.9300 .
C15 C16 1.386(3) .
C15 H15A 0.9300 .
C16 C17 1.379(4) .
C16 C19 1.496(4) .
C17 C18 1.367(4) .
C17 H17A 0.9300 .
C18 N3 1.328(3) .
C18 H18A 0.9300 .
C19 C24 1.373(3) .
C19 C20 1.384(4) .
C20 C21 1.369(4) .
C20 H20A 0.9300 .
C21 N4 1.341(3) .
C21 H21A 0.9300 .
C22 N4 1.473(4) .
C22 H22A 0.9600 .
C22 H22B 0.9600 .
C22 H22C 0.9600 .
C23 N4 1.341(3) .
C23 C24 1.370(4) .
C23 H23A 0.9300 .
C24 H24A 0.9300 .
