#------------------------------------------------------------------------------
#$Date: 2016-03-25 16:40:09 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179983 $
#$URL: svn://www.crystallography.net/cod/cif/7/02/77/7027770.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided the Crystal Eye server at
# http://wwmm.ch.cam.ac.uk/crystaleye/, created by Nick Day at the
# Peter Murray-Rust laboratory.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_7027770
loop_
_publ_author_name
'Fässler, Thomas F.'
'Hoffmann, Rudolf'
_publ_contact_author
;
     Thomas F. Faessler
     Eidgenoessische Technische Hochschule Zuerich
     Laboratorium fuer Anorganische Chemie
     Universitaetstr.6
     ETH-Zentrum
     8092 Zuerich
     Switzerland
;
_publ_section_title
;
 Novel synthetic route to soluble polyanions: synthesis and crystal
 structure of [K(18-crown-6)]4[Pb9]·en·tol †
;
_journal_issue                   19
_journal_name_full
'Journal of the Chemical Society, Dalton Transactions'
_journal_page_first              3339
_journal_paper_doi               10.1039/a906586e
_journal_year                    1999
_chemical_formula_sum            'C28.5 H56 K2 N O12 Pb4.5'
_chemical_formula_weight         1615.3
_chemical_name_common
;
     Potassium-[18]crown-6-Salt of Nonaplumbide(4-)
;
_space_group_IT_number           11
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yb'
_symmetry_space_group_name_H-M   'P 1 21/m 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 108.13(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   14.618(2)
_cell_length_b                   14.771(2)
_cell_length_c                   21.583(3)
_cell_measurement_reflns_used    512
_cell_measurement_temperature    223(2)
_cell_measurement_theta_max      23
_cell_measurement_theta_min      3.5
_cell_volume                     4428.9(13)
_computing_cell_refinement       'Siemens SAINT'
_computing_data_collection       'Siemens SMART'
_computing_data_reduction        'Siemnes SAINT'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      223(2)
_diffrn_measured_fraction_theta_full 0.995
_diffrn_measured_fraction_theta_max 0.995
_diffrn_measurement_device       'Siemens Smart'
_diffrn_measurement_device_type  'Siemens Smart'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK/a
_diffrn_radiation_wavelength     0.71079
_diffrn_reflns_av_R_equivalents  0.0994
_diffrn_reflns_av_sigmaI/netI    0.0769
_diffrn_reflns_limit_h_max       18
_diffrn_reflns_limit_h_min       -18
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       26
_diffrn_reflns_limit_l_min       -26
_diffrn_reflns_number            39939
_diffrn_reflns_theta_full        26.45
_diffrn_reflns_theta_max         26.45
_diffrn_reflns_theta_min         0.99
_exptl_absorpt_coefficient_mu    17.289
_exptl_absorpt_correction_T_max  0.034995
_exptl_absorpt_correction_T_min  0.005537
_exptl_absorpt_correction_type   'empirical, Siemens SADABS'
_exptl_crystal_colour            'dark-red '
_exptl_crystal_density_diffrn    2.423
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       rods
_exptl_crystal_F_000             2948
_exptl_crystal_size_max          0.65
_exptl_crystal_size_mid          0.35
_exptl_crystal_size_min          0.30
_refine_diff_density_max         1.508
_refine_diff_density_min         -1.744
_refine_diff_density_rms         0.222
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.920
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     419
_refine_ls_number_reflns         9452
_refine_ls_number_restraints     16
_refine_ls_restrained_S_all      0.920
_refine_ls_R_factor_all          0.0810
_refine_ls_R_factor_gt           0.0427
_refine_ls_shift/su_max          0.031
_refine_ls_shift/su_mean         0.002
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0394P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0845
_refine_ls_wR_factor_ref         0.0972
_reflns_number_gt                5934
_reflns_number_total             9452
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            906586esup1.cif
_cod_data_source_block           k4pb9
_cod_original_cell_volume        4428.8(11)
_cod_original_sg_symbol_H-M      P2(1)/m
_cod_database_code               7027770
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z'
'-x, -y, -z'
'x, -y-1/2, z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Pb1 Pb 0.22526(3) 0.60016(3) 0.26411(2) 0.05155(12) Uani 1 1 d .
Pb2 Pb 0.12059(4) 0.7500 0.16410(3) 0.04982(16) Uani 1 2 d S
Pb3 Pb 0.32869(5) 0.7500 0.36366(3) 0.05163(16) Uani 1 2 d S
Pb4 Pb 0.28595(3) 0.63748(3) 0.14040(2) 0.04891(12) Uani 1 1 d .
Pb5 Pb 0.44260(3) 0.63238(3) 0.29243(2) 0.04897(12) Uani 1 1 d .
Pb6 Pb 0.47258(4) 0.7500 0.18309(3) 0.05033(16) Uani 1 2 d S
K1 K 0.0880(2) 0.7500 -0.02752(17) 0.0546(9) Uani 1 2 d S
O1 O -0.1235(10) 0.7716(10) -0.0776(6) 0.064(5) Uiso 0.50 1 d P
O2 O 0.0031(13) 0.5831(11) -0.0637(8) 0.061(4) Uiso 0.50 1 d P
O12 O -0.0559(16) 0.5916(12) -0.0665(9) 0.066(5) Uiso 0.50 1 d P
O3 O 0.8749(12) 0.4305(11) 0.0909(7) 0.055(4) Uiso 0.50 1 d P
O13 O 0.8168(14) 0.3923(11) 0.0855(8) 0.067(4) Uiso 0.50 1 d P
O4 O 0.7479(12) 0.2852(9) 0.0693(8) 0.068(5) Uiso 0.50 1 d P
C1 C -0.168(2) 0.6947(18) -0.0549(13) 0.068(7) Uiso 0.50 1 d PD
C11 C -0.142(2) 0.643(2) -0.0557(15) 0.071(8) Uiso 0.50 1 d PD
C2 C -0.106(3) 0.575(2) -0.0928(15) 0.079(9) Uiso 0.50 1 d PD
C12 C -0.153(2) 0.6162(18) -0.0899(14) 0.065(7) Uiso 0.50 1 d PD
C3 C 0.048(2) 0.5084(19) -0.0853(15) 0.057(8) Uiso 0.50 1 d PD
C13 C -0.026(2) 0.5147(18) -0.0974(13) 0.075(8) Uiso 0.50 1 d PD
C4 C 0.162(2) 0.5268(17) -0.0590(12) 0.061(6) Uiso 0.50 1 d PD
C14 C 0.084(3) 0.505(2) -0.0718(17) 0.076(11) Uiso 0.50 1 d PD
C5 C 0.772(2) 0.4403(19) 0.0625(14) 0.077(8) Uiso 0.50 1 d PD
C15 C 0.721(2) 0.3780(18) 0.0595(15) 0.070(8) Uiso 0.50 1 d PD
C6 C 0.724(2) 0.364(2) 0.0942(17) 0.085(9) Uiso 0.50 1 d PD
C16 C 0.695(2) 0.2844(16) 0.0870(13) 0.084(9) Uiso 0.50 1 d PD
K2 K 0.6101(2) 0.7500 0.45326(16) 0.0495(8) Uani 1 2 d S
O21 O 0.5727(9) 0.7500 0.5801(6) 0.079(4) Uani 1 2 d S
O22 O 0.6038(7) 0.5880(5) 0.5235(5) 0.083(3) Uani 1 1 d .
O23 O 0.7352(6) 0.5855(6) 0.4515(5) 0.082(3) Uani 1 1 d .
O24 O 0.7622(9) 0.7500 0.3979(6) 0.086(4) Uani 1 2 d S
C21 C 0.5190(11) 0.6727(13) 0.5797(8) 0.108(6) Uani 1 1 d .
H21A H 0.4634 0.6709 0.5400 0.129 Uiso 1 1 calc R
H21B H 0.4955 0.6725 0.6175 0.129 Uiso 1 1 calc R
C22 C 0.5813(12) 0.5931(12) 0.5819(7) 0.105(6) Uani 1 1 d .
H22A H 0.6406 0.5987 0.6187 0.127 Uiso 1 1 calc R
H22B H 0.5479 0.5379 0.5879 0.127 Uiso 1 1 calc R
C23 C 0.3368(11) 0.4884(8) 0.4805(9) 0.109(7) Uani 1 1 d .
H23A H 0.2741 0.4841 0.4466 0.131 Uiso 1 1 calc R
H23B H 0.3678 0.5449 0.4742 0.131 Uiso 1 1 calc R
C24 C 0.6760(11) 0.5130(10) 0.4539(9) 0.106(7) Uani 1 1 d .
H24A H 0.7054 0.4562 0.4461 0.128 Uiso 1 1 calc R
H24B H 0.6135 0.5197 0.4202 0.128 Uiso 1 1 calc R
C25 C 0.7512(11) 0.5901(12) 0.3913(8) 0.107(6) Uani 1 1 d .
H25A H 0.6896 0.5955 0.3564 0.129 Uiso 1 1 calc R
H25B H 0.7833 0.5348 0.3838 0.129 Uiso 1 1 calc R
C26 C 0.8127(11) 0.6703(13) 0.3907(8) 0.126(7) Uani 1 1 d .
H26A H 0.8734 0.6660 0.4264 0.152 Uiso 1 1 calc R
H26B H 0.8277 0.6726 0.3495 0.152 Uiso 1 1 calc R
K3 K 0.0472(2) 0.7500 0.32313(16) 0.0521(8) Uani 1 2 d S
O31 O -0.1379(9) 0.7500 0.2216(6) 0.083(4) Uani 1 2 d S
O32 O 0.9112(6) 0.5805(6) 0.2826(5) 0.078(3) Uani 1 1 d .
O33 O 0.0551(6) 0.5868(5) 0.4000(5) 0.072(2) Uani 1 1 d .
O34 O 0.0925(8) 0.7500 0.4704(5) 0.064(3) Uani 1 2 d S
C31 C 0.8115(11) 0.6714(11) 0.1978(7) 0.094(5) Uani 1 1 d .
H31A H 0.7823 0.6759 0.1504 0.113 Uiso 1 1 calc R
H31B H 0.7599 0.6630 0.2173 0.113 Uiso 1 1 calc R
C32 C 0.8770(12) 0.5945(11) 0.2136(7) 0.099(5) Uani 1 1 d .
H32A H 0.8435 0.5400 0.1921 0.119 Uiso 1 1 calc R
H32B H 0.9316 0.6056 0.1974 0.119 Uiso 1 1 calc R
C33 C 0.9791(10) 0.5091(8) 0.3034(7) 0.074(4) Uani 1 1 d .
H33A H 1.0347 0.5206 0.2883 0.089 Uiso 1 1 calc R
H33B H 0.9497 0.4518 0.2845 0.089 Uiso 1 1 calc R
C34 C 0.0108(11) 0.5028(8) 0.3748(8) 0.087(5) Uani 1 1 d .
H34A H -0.0445 0.4914 0.3902 0.104 Uiso 1 1 calc R
H34B H 0.0568 0.4531 0.3893 0.104 Uiso 1 1 calc R
C35 C 0.0854(9) 0.5905(9) 0.4693(6) 0.073(4) Uani 1 1 d .
H35A H 0.1221 0.5359 0.4873 0.088 Uiso 1 1 calc R
H35B H 0.0291 0.5933 0.4847 0.088 Uiso 1 1 calc R
C36 C 0.1470(9) 0.6729(8) 0.4915(6) 0.073(4) Uani 1 1 d .
H36A H 0.1730 0.6732 0.5392 0.088 Uiso 1 1 calc R
H36B H 0.2012 0.6717 0.4739 0.088 Uiso 1 1 calc R
K4 K 0.4992(3) 0.2500 0.15505(18) 0.0562(9) Uani 1 2 d S
O41 O 0.4139(8) 0.2500 0.0181(6) 0.082(4) Uani 1 2 d S
O42 O 0.4975(7) 0.4130(5) 0.0785(5) 0.084(3) Uani 1 1 d D
O43 O 0.6004(8) 0.4095(7) 0.2096(6) 0.110(4) Uani 1 1 d D
O44 O 0.6850(13) 0.2500 0.2668(7) 0.131(6) Uani 1 2 d SD
C41 C 0.4212(13) 0.3284(14) -0.0177(9) 0.137(8) Uani 1 1 d .
H41A H 0.3685 0.3297 -0.0590 0.165 Uiso 1 1 calc R
H41B H 0.4823 0.3281 -0.0275 0.165 Uiso 1 1 calc R
C42 C 0.4161(13) 0.4066(14) 0.0210(13) 0.157(12) Uani 1 1 d .
H42A H 0.4125 0.4613 -0.0053 0.189 Uiso 1 1 calc R
H42B H 0.3572 0.4033 0.0335 0.189 Uiso 1 1 calc R
C43 C 0.520(3) 0.483(2) 0.1266(15) 0.094(11) Uiso 0.50 1 d PD
H43A H 0.4671 0.4816 0.1458 0.113 Uiso 0.50 1 calc PR
H43B H 0.5125 0.5396 0.1022 0.113 Uiso 0.50 1 calc PR
C431 C 0.483(2) 0.4861(17) 0.1157(12) 0.079(10) Uiso 0.50 1 d PD
H43C H 0.4274 0.4763 0.1307 0.095 Uiso 0.50 1 calc PR
H43D H 0.4748 0.5428 0.0909 0.095 Uiso 0.50 1 calc PR
C44 C 0.607(3) 0.4931(17) 0.1813(17) 0.123(17) Uiso 0.50 1 d PD
H44A H 0.6647 0.4982 0.1676 0.147 Uiso 0.50 1 calc PR
H44B H 0.6036 0.5441 0.2095 0.147 Uiso 0.50 1 calc PR
C441 C 0.572(2) 0.4870(15) 0.1698(14) 0.076(9) Uiso 0.50 1 d PD
H44C H 0.6242 0.5015 0.1521 0.091 Uiso 0.50 1 calc PR
H44D H 0.5675 0.5373 0.1984 0.091 Uiso 0.50 1 calc PR
C45 C 0.683(3) 0.422(2) 0.253(2) 0.116(14) Uiso 0.50 1 d PD
H45A H 0.6824 0.4755 0.2796 0.140 Uiso 0.50 1 calc PR
H45B H 0.7342 0.4276 0.2331 0.140 Uiso 0.50 1 calc PR
C451 C 0.683(3) 0.392(2) 0.2759(18) 0.099(10) Uiso 0.50 1 d PD
H45C H 0.7441 0.3925 0.2659 0.119 Uiso 0.50 1 calc PR
H45D H 0.6845 0.4451 0.3038 0.119 Uiso 0.50 1 calc PR
C46 C 0.694(3) 0.3392(11) 0.2917(17) 0.116(12) Uiso 0.50 1 d PD
H46A H 0.7574 0.3428 0.3242 0.139 Uiso 0.50 1 calc PR
H46B H 0.6470 0.3440 0.3158 0.139 Uiso 0.50 1 calc PR
C461 C 0.683(4) 0.3129(19) 0.3146(14) 0.16(2) Uiso 0.50 1 d PD
H46C H 0.7398 0.3092 0.3532 0.187 Uiso 0.50 1 calc PR
H46D H 0.6243 0.3081 0.3273 0.187 Uiso 0.50 1 calc PR
N4 N 0.3748(8) 0.3486(8) 0.2113(6) 0.092(4) Uiso 1 1 d .
H4A H 0.4096 0.3909 0.2396 0.111 Uiso 1 1 calc R
H4B H 0.3287 0.3778 0.1793 0.111 Uiso 1 1 calc R
C47 C 0.3316(14) 0.2901(11) 0.2440(9) 0.143(8) Uiso 1 1 d .
H47A H 0.3573 0.3075 0.2900 0.172 Uiso 1 1 calc R
H47B H 0.2636 0.3075 0.2301 0.172 Uiso 1 1 calc R
C51 C 0.903(2) 0.7500 0.5832(17) 0.146(11) Uiso 1 2 d S
H51 H 0.8764 0.7500 0.5376 0.175 Uiso 1 2 calc SR
C52 C 0.849(3) 0.7500 0.616(2) 0.208(17) Uiso 1 2 d S
H52 H 0.7824 0.7500 0.5958 0.249 Uiso 1 2 calc SR
C53 C 0.113(3) 0.2500 0.3160(19) 0.185(14) Uiso 1 2 d S
H53 H 0.1537 0.2500 0.2896 0.222 Uiso 1 2 calc SR
C54 C 0.0004(19) 0.7500 0.6091(13) 0.110(8) Uiso 1 2 d S
H54 H 0.0394 0.7500 0.5817 0.131 Uiso 1 2 calc SR
C55 C 0.9607(18) 0.2500 0.3279(12) 0.102(7) Uiso 1 2 d S
H55 H 0.8932 0.2500 0.3105 0.123 Uiso 1 2 calc SR
C56 C 1.011(2) 0.2500 0.2883(13) 0.108(8) Uiso 1 2 d S
C57 C 0.977(2) 0.2500 0.2172(14) 0.154(11) Uiso 1 2 d S
H57A H 0.9076 0.2500 0.2020 0.230 Uiso 1 2 calc SR
H57B H 1.0011 0.1964 0.2011 0.230 Uiso 0.50 1 calc PR
H57C H 1.0011 0.3036 0.2011 0.230 Uiso 0.50 1 calc PR
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pb Pb -3.3944 10.1111 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
K K 0.2009 0.2494 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
Pb5 Pb1 Pb4 65.86(3) . .
Pb5 Pb1 Pb3 60.40(2) . 4_575
Pb4 Pb1 Pb3 104.95(2) . 4_575
Pb5 Pb1 Pb3 60.40(2) . .
Pb4 Pb1 Pb3 104.95(2) . .
Pb3 Pb1 Pb3 0.000(19) 4_575 .
Pb5 Pb1 Pb2 106.23(3) . .
Pb4 Pb1 Pb2 59.549(18) . .
Pb3 Pb1 Pb2 90.08(3) 4_575 .
Pb3 Pb1 Pb2 90.08(3) . .
Pb5 Pb1 Pb2 106.23(3) . 4_575
Pb4 Pb1 Pb2 59.549(18) . 4_575
Pb3 Pb1 Pb2 90.08(3) 4_575 4_575
Pb3 Pb1 Pb2 90.08(3) . 4_575
Pb2 Pb1 Pb2 0.00(3) . 4_575
Pb5 Pb1 K3 126.63(4) . .
Pb4 Pb1 K3 125.03(4) . .
Pb3 Pb1 K3 66.73(5) 4_575 .
Pb3 Pb1 K3 66.73(5) . .
Pb2 Pb1 K3 66.06(5) . .
Pb2 Pb1 K3 66.06(5) 4_575 .
Pb2 Pb2 Pb4 0(4) 4_575 4_575
Pb2 Pb2 Pb4 0(10) 4_575 .
Pb4 Pb2 Pb4 64.74(2) 4_575 .
Pb2 Pb2 Pb1 0(10) 4_575 4_575
Pb4 Pb2 Pb1 59.842(19) 4_575 4_575
Pb4 Pb2 Pb1 104.66(3) . 4_575
Pb2 Pb2 Pb1 0(10) 4_575 .
Pb4 Pb2 Pb1 104.66(3) 4_575 .
Pb4 Pb2 Pb1 59.844(19) . .
Pb1 Pb2 Pb1 89.73(3) 4_575 .
Pb2 Pb2 K3 0(10) 4_575 .
Pb4 Pb2 K3 125.89(4) 4_575 .
Pb4 Pb2 K3 125.89(4) . .
Pb1 Pb2 K3 66.64(4) 4_575 .
Pb1 Pb2 K3 66.64(4) . .
Pb2 Pb2 K1 0(10) 4_575 .
Pb4 Pb2 K1 71.28(5) 4_575 .
Pb4 Pb2 K1 71.28(5) . .
Pb1 Pb2 K1 125.81(3) 4_575 .
Pb1 Pb2 K1 125.81(3) . .
K3 Pb2 K1 158.38(7) . .
Pb3 Pb3 Pb5 0(7) 4_575 4_575
Pb3 Pb3 Pb5 0(10) 4_575 .
Pb5 Pb3 Pb5 67.62(2) 4_575 .
Pb3 Pb3 Pb1 0(10) 4_575 .
Pb5 Pb3 Pb1 105.87(2) 4_575 .
Pb5 Pb3 Pb1 59.054(18) . .
Pb3 Pb3 Pb1 0(10) 4_575 4_575
Pb5 Pb3 Pb1 59.054(17) 4_575 4_575
Pb5 Pb3 Pb1 105.87(2) . 4_575
Pb1 Pb3 Pb1 90.11(3) . 4_575
Pb3 Pb3 K3 0(10) 4_575 .
Pb5 Pb3 K3 124.90(4) 4_575 .
Pb5 Pb3 K3 124.90(4) . .
Pb1 Pb3 K3 66.32(4) . .
Pb1 Pb3 K3 66.32(4) 4_575 .
Pb3 Pb3 K2 0(10) 4_575 .
Pb5 Pb3 K2 66.96(4) 4_575 .
Pb5 Pb3 K2 66.96(4) . .
Pb1 Pb3 K2 122.80(4) . .
Pb1 Pb3 K2 122.80(4) 4_575 .
K3 Pb3 K2 164.59(7) . .
Pb6 Pb4 Pb2 108.931(19) . 4_575
Pb6 Pb4 Pb2 108.931(19) . .
Pb2 Pb4 Pb2 0.00(2) 4_575 .
Pb6 Pb4 Pb1 107.53(3) . .
Pb2 Pb4 Pb1 60.61(2) 4_575 .
Pb2 Pb4 Pb1 60.61(2) . .
Pb6 Pb4 Pb4 57.349(12) . 4_575
Pb2 Pb4 Pb4 57.629(11) 4_575 4_575
Pb2 Pb4 Pb4 57.629(11) . 4_575
Pb1 Pb4 Pb4 100.198(11) . 4_575
Pb6 Pb4 Pb5 56.65(2) . .
Pb2 Pb4 Pb5 100.35(2) 4_575 .
Pb2 Pb4 Pb5 100.35(2) . .
Pb1 Pb4 Pb5 56.586(17) . .
Pb4 Pb4 Pb5 91.281(10) 4_575 .
Pb6 Pb4 K1 110.59(4) . .
Pb2 Pb4 K1 64.46(5) 4_575 .
Pb2 Pb4 K1 64.46(5) . .
Pb1 Pb4 K1 120.32(5) . .
Pb4 Pb4 K1 66.76(2) 4_575 .
Pb5 Pb4 K1 157.51(3) . .
Pb6 Pb5 Pb1 108.68(3) . .
Pb6 Pb5 Pb3 106.81(2) . 4_575
Pb1 Pb5 Pb3 60.55(2) . 4_575
Pb6 Pb5 Pb3 106.81(2) . .
Pb1 Pb5 Pb3 60.55(2) . .
Pb3 Pb5 Pb3 0.00(2) 4_575 .
Pb6 Pb5 Pb4 56.958(17) . .
Pb1 Pb5 Pb4 57.55(3) . .
Pb3 Pb5 Pb4 99.33(2) 4_575 .
Pb3 Pb5 Pb4 99.33(2) . .
Pb6 Pb5 Pb5 55.530(12) . 4_575
Pb1 Pb5 Pb5 98.891(11) . 4_575
Pb3 Pb5 Pb5 56.191(12) 4_575 4_575
Pb3 Pb5 Pb5 56.191(12) . 4_575
Pb4 Pb5 Pb5 88.718(9) . 4_575
Pb6 Pb5 K2 103.16(4) . .
Pb1 Pb5 K2 123.93(6) . .
Pb3 Pb5 K2 66.69(5) 4_575 .
Pb3 Pb5 K2 66.69(5) . .
Pb4 Pb5 K2 152.77(3) . .
Pb5 Pb5 K2 64.06(2) 4_575 .
Pb5 Pb6 Pb5 68.94(2) 4_575 .
Pb5 Pb6 Pb4 102.14(3) 4_575 .
Pb5 Pb6 Pb4 66.39(3) . .
Pb5 Pb6 Pb4 66.39(3) 4_575 4_575
Pb5 Pb6 Pb4 102.14(3) . 4_575
Pb4 Pb6 Pb4 65.30(2) . 4_575
O2 K1 O2 126.5(7) 4_575 .
O2 K1 O4 95.5(5) 4_575 2_655
O2 K1 O4 114.9(5) . 2_655
O2 K1 O4 114.9(5) 4_575 3_665
O2 K1 O4 95.5(5) . 3_665
O4 K1 O4 20.9(5) 2_655 3_665
O2 K1 O1 58.2(5) 4_575 .
O2 K1 O1 70.5(5) . .
O4 K1 O1 138.5(4) 2_655 .
O4 K1 O1 142.0(4) 3_665 .
O2 K1 O1 70.5(5) 4_575 4_575
O2 K1 O1 58.2(5) . 4_575
O4 K1 O1 142.0(4) 2_655 4_575
O4 K1 O1 138.5(4) 3_665 4_575
O1 K1 O1 12.4(6) . 4_575
O2 K1 O13 58.9(5) 4_575 2_655
O2 K1 O13 137.2(5) . 2_655
O4 K1 O13 36.7(5) 2_655 2_655
O4 K1 O13 56.8(5) 3_665 2_655
O1 K1 O13 109.8(5) . 2_655
O1 K1 O13 119.4(5) 4_575 2_655
O2 K1 O13 137.2(5) 4_575 3_665
O2 K1 O13 58.9(5) . 3_665
O4 K1 O13 56.8(5) 2_655 3_665
O4 K1 O13 36.7(5) 3_665 3_665
O1 K1 O13 119.4(5) . 3_665
O1 K1 O13 109.8(5) 4_575 3_665
O13 K1 O13 88.9(7) 2_655 3_665
O2 K1 O12 113.1(6) 4_575 .
O2 K1 O12 15.6(4) . .
O4 K1 O12 128.3(5) 2_655 .
O4 K1 O12 110.1(5) 3_665 .
O1 K1 O12 55.6(5) . .
O1 K1 O12 43.3(5) 4_575 .
O13 K1 O12 141.6(5) 2_655 .
O13 K1 O12 73.8(5) 3_665 .
O2 K1 O12 15.6(4) 4_575 4_575
O2 K1 O12 113.1(6) . 4_575
O4 K1 O12 110.1(5) 2_655 4_575
O4 K1 O12 128.3(5) 3_665 4_575
O1 K1 O12 43.3(5) . 4_575
O1 K1 O12 55.6(5) 4_575 4_575
O13 K1 O12 73.8(5) 2_655 4_575
O13 K1 O12 141.6(5) 3_665 4_575
O12 K1 O12 98.7(7) . 4_575
O2 K1 O3 139.8(5) 4_575 3_665
O2 K1 O3 40.3(5) . 3_665
O4 K1 O3 74.9(4) 2_655 3_665
O4 K1 O3 55.2(4) 3_665 3_665
O1 K1 O3 103.7(4) . 3_665
O1 K1 O3 93.0(4) 4_575 3_665
O13 K1 O3 104.4(5) 2_655 3_665
O13 K1 O3 18.6(4) 3_665 3_665
O12 K1 O3 55.2(5) . 3_665
O12 K1 O3 136.6(5) 4_575 3_665
O2 K1 O3 40.3(5) 4_575 2_655
O2 K1 O3 139.8(5) . 2_655
O4 K1 O3 55.2(4) 2_655 2_655
O4 K1 O3 74.9(4) 3_665 2_655
O1 K1 O3 93.0(4) . 2_655
O1 K1 O3 103.7(4) 4_575 2_655
O13 K1 O3 18.6(4) 2_655 2_655
O13 K1 O3 104.4(5) 3_665 2_655
O12 K1 O3 136.6(5) . 2_655
O12 K1 O3 55.2(5) 4_575 2_655
O3 K1 O3 117.4(6) 3_665 2_655
O1 O1 C1 118.1(18) 4_575 4_575
O1 O1 C11 154.0(15) 4_575 4_575
C1 O1 C11 37.4(17) 4_575 4_575
O1 O1 C1 39.3(12) 4_575 .
C1 O1 C1 79(3) 4_575 .
C11 O1 C1 115(2) 4_575 .
O1 O1 C12 165.6(10) 4_575 4_575
C1 O1 C12 57.0(18) 4_575 4_575
C11 O1 C12 28.0(13) 4_575 4_575
C1 O1 C12 133.3(19) . 4_575
O1 O1 K1 83.8(3) 4_575 .
C1 O1 K1 127.5(18) 4_575 .
C11 O1 K1 105.4(14) 4_575 .
C1 O1 K1 108.5(13) . .
C12 O1 K1 110.1(11) 4_575 .
O12 O2 C13 86(2) . .
O12 O2 C3 130(3) . .
C13 O2 C3 44.7(16) . .
O12 O2 C2 23(2) . .
C13 O2 C2 64.9(18) . .
C3 O2 C2 109.5(19) . .
O12 O2 C14 144(3) . .
C13 O2 C14 60.5(19) . .
C3 O2 C14 16.4(17) . .
C2 O2 C14 125(2) . .
O12 O2 K1 104(2) . .
C13 O2 K1 159.2(18) . .
C3 O2 K1 124.6(16) . .
C2 O2 K1 120.2(14) . .
C14 O2 K1 111.7(15) . .
C2 O12 O2 133(4) . .
C2 O12 C12 39(3) . .
O2 O12 C12 162(3) . .
C2 O12 C13 78(3) . .
O2 O12 C13 58(2) . .
C12 O12 C13 117(2) . .
C2 O12 C11 69(3) . .
O2 O12 C11 156(3) . .
C12 O12 C11 31.3(14) . .
C13 O12 C11 146(2) . .
C2 O12 K1 144(3) . .
O2 O12 K1 60.3(18) . .
C12 O12 K1 115.5(15) . .
C13 O12 K1 116.2(17) . .
C11 O12 K1 96.0(14) . .
C4 O3 O13 91(2) 3_665 .
C4 O3 C14 60(2) 3_665 3_665
O13 O3 C14 150(3) . 3_665
C4 O3 C5 49.7(19) 3_665 .
O13 O3 C5 43.1(15) . .
C14 O3 C5 109(2) 3_665 .
C4 O3 C3 79(2) 3_665 3_665
O13 O3 C3 169(2) . 3_665
C14 O3 C3 20(2) 3_665 3_665
C5 O3 C3 129(2) . 3_665
C4 O3 K1 112.4(18) 3_665 3_665
O13 O3 K1 73.9(14) . 3_665
C14 O3 K1 109.7(18) 3_665 3_665
C5 O3 K1 101.6(13) . 3_665
C3 O3 K1 104.2(14) 3_665 3_665
C5 O13 O3 94(3) . .
C5 O13 C15 58(2) . .
O3 O13 C15 151(2) . .
C5 O13 C4 52(2) . 3_665
O3 O13 C4 43.7(14) . 3_665
C15 O13 C4 107(2) . 3_665
C5 O13 C6 77(3) . .
O3 O13 C6 158(2) . .
C15 O13 C6 30.8(15) . .
C4 O13 C6 128(2) 3_665 .
C5 O13 K1 128(2) . 3_665
O3 O13 K1 87.5(15) . 3_665
C15 O13 K1 105.8(15) . 3_665
C4 O13 K1 103.8(14) 3_665 3_665
C6 O13 K1 114.3(15) . 3_665
C16 O4 O4 89.3(18) . 4_565
C16 O4 C6 61(2) . .
O4 O4 C6 148.1(16) 4_565 .
C16 O4 C16 46(2) . 4_565
O4 O4 C16 43.1(11) 4_565 4_565
C6 O4 C16 107(2) . 4_565
C16 O4 C15 81(2) . .
O4 O4 C15 164.2(13) 4_565 .
C6 O4 C15 31.7(15) . .
C16 O4 C15 126(2) 4_565 .
C16 O4 K1 168(2) . 3_665
O4 O4 K1 79.5(3) 4_565 3_665
C6 O4 K1 128.1(17) . 3_665
C16 O4 K1 122.5(12) 4_565 3_665
C15 O4 K1 110.5(16) . 3_665
C11 C1 O1 94(4) . 4_575
C11 C1 C12 29(3) . .
O1 C1 C12 85(2) 4_575 .
C11 C1 O1 116(4) . .
O1 C1 O1 22.6(13) 4_575 .
C12 C1 O1 106.8(19) . .
C11 C1 C1 153(3) . 4_575
O1 C1 C1 61.9(18) 4_575 4_575
C12 C1 C1 143.7(16) . 4_575
O1 C1 C1 39.3(12) . 4_575
C12 C11 C1 120(5) . .
C12 C11 O1 98(4) . 4_575
C1 C11 O1 49(3) . 4_575
C12 C11 C2 34(3) . .
C1 C11 C2 148(4) . .
O1 C11 C2 107(2) 4_575 .
C12 C11 O12 64(3) . .
C1 C11 O12 146(4) . .
O1 C11 O12 98(2) 4_575 .
C2 C11 O12 31.1(13) . .
O12 C2 C12 106(4) . .
O12 C2 C11 80(3) . .
C12 C2 C11 29(2) . .
O12 C2 C13 71(3) . .
C12 C2 C13 176(4) . .
C11 C2 C13 149(3) . .
O12 C2 O2 24(2) . .
C12 C2 O2 128(4) . .
C11 C2 O2 103(2) . .
C13 C2 O2 48.3(15) . .
C11 C12 C2 117(5) . .
C11 C12 O12 85(3) . .
C2 C12 O12 34(2) . .
C11 C12 C1 31(3) . .
C2 C12 C1 143(4) . .
O12 C12 C1 109(2) . .
C11 C12 O1 54(3) . 4_575
C2 C12 O1 119(3) . 4_575
O12 C12 O1 91.2(17) . 4_575
C1 C12 O1 37.9(12) . 4_575
C14 C3 C13 162(9) . .
C14 C3 O2 112(7) . .
C13 C3 O2 58(2) . .
C14 C3 O3 56(6) . 3_665
C13 C3 O3 134(3) . 3_665
O2 C3 O3 89.7(18) . 3_665
C14 C3 C4 20(6) . .
C13 C3 C4 164(3) . .
O2 C3 C4 107(2) . .
O3 C3 C4 36.1(11) 3_665 .
C3 C13 O2 78(3) . .
C3 C13 O12 113(3) . .
O2 C13 O12 35.9(12) . .
C3 C13 C2 144(3) . .
O2 C13 C2 67(2) . .
O12 C13 C2 31.9(13) . .
C3 C13 C14 6(3) . .
O2 C13 C14 75(2) . .
O12 C13 C14 110(2) . .
C2 C13 C14 142(3) . .
O3 C4 C5 88(3) 3_665 3_665
O3 C4 C14 73(3) 3_665 .
C5 C4 C14 161(4) 3_665 .
O3 C4 O13 45.3(16) 3_665 3_665
C5 C4 O13 44.6(18) 3_665 3_665
C14 C4 O13 118(3) . 3_665
O3 C4 C3 64(2) 3_665 .
C5 C4 C3 152(3) 3_665 .
C14 C4 C3 9(3) . .
O13 C4 C3 110(2) 3_665 .
C3 C14 C4 151(8) . .
C3 C14 O3 104(7) . 3_665
C4 C14 O3 47.1(19) . 3_665
C3 C14 C13 12(6) . .
C4 C14 C13 157(3) . .
O3 C14 C13 111(3) 3_665 .
C3 C14 O2 51(6) . .
C4 C14 O2 117(3) . .
O3 C14 O2 86(2) 3_665 .
C13 C14 O2 44.8(14) . .
O13 C5 C4 84(3) . 3_665
O13 C5 C15 77(3) . .
C4 C5 C15 154(4) 3_665 .
O13 C5 O3 43.4(17) . .
C4 C5 O3 42.0(17) 3_665 .
C15 C5 O3 120(3) . .
O13 C5 C6 65(2) . .
C4 C5 C6 148(3) 3_665 .
C15 C5 C6 27.2(19) . .
O3 C5 C6 106(2) . .
C6 C15 C5 108(4) . .
C6 C15 O13 84(4) . .
C5 C15 O13 45.3(17) . .
C6 C15 O4 70(3) . .
C5 C15 O4 127(3) . .
O13 C15 O4 83.3(19) . .
C6 C15 C16 49(3) . .
C5 C15 C16 151(3) . .
O13 C15 C16 108(2) . .
O4 C15 C16 36.6(13) . .
C15 C6 C16 103(4) . .
C15 C6 O4 78(4) . .
C16 C6 O4 43.0(17) . .
C15 C6 O13 66(4) . .
C16 C6 O13 123(3) . .
O4 C6 O13 81(2) . .
C15 C6 C5 45(3) . .
C16 C6 C5 143(3) . .
O4 C6 C5 104(2) . .
O13 C6 C5 37.4(13) . .
O4 C16 C16 90.7(18) . 4_565
O4 C16 C6 75(2) . .
C16 C16 C6 161(2) 4_565 .
O4 C16 O4 47.6(18) . 4_565
C16 C16 O4 43.1(11) 4_565 4_565
C6 C16 O4 122(3) . 4_565
O4 C16 C15 62.0(19) . .
C16 C16 C15 150.1(16) 4_565 .
C6 C16 C15 27.8(18) . .
O4 C16 C15 109(2) 4_565 .
O24 K2 O22 112.6(3) . .
O24 K2 O22 112.6(3) . 4_575
O22 K2 O22 114.2(4) . 4_575
O24 K2 O21 141.9(4) . .
O22 K2 O21 57.4(2) . .
O22 K2 O21 57.4(2) 4_575 .
O24 K2 O23 56.1(2) . .
O22 K2 O23 57.0(3) . .
O22 K2 O23 142.6(3) 4_575 .
O21 K2 O23 107.2(3) . .
O24 K2 O23 56.1(2) . 4_575
O22 K2 O23 142.6(3) . 4_575
O22 K2 O23 57.0(3) 4_575 4_575
O21 K2 O23 107.2(3) . 4_575
O23 K2 O23 105.7(4) . 4_575
O24 K2 Pb3 128.7(3) . .
O22 K2 Pb3 93.40(19) . .
O22 K2 Pb3 93.40(19) 4_575 .
O21 K2 Pb3 89.4(3) . .
O23 K2 Pb3 121.97(17) . .
O23 K2 Pb3 121.97(17) 4_575 .
O24 K2 Pb3 128.7(3) . 4_575
O22 K2 Pb3 93.40(19) . 4_575
O22 K2 Pb3 93.40(19) 4_575 4_575
O21 K2 Pb3 89.4(3) . 4_575
O23 K2 Pb3 121.97(17) . 4_575
O23 K2 Pb3 121.97(17) 4_575 4_575
Pb3 K2 Pb3 0.000(9) . 4_575
O24 K2 Pb5 89.0(2) . .
O22 K2 Pb5 89.11(18) . .
O22 K2 Pb5 136.00(19) 4_575 .
O21 K2 Pb5 124.7(2) . .
O23 K2 Pb5 81.35(16) . .
O23 K2 Pb5 123.2(2) 4_575 .
Pb3 K2 Pb5 46.35(4) . .
Pb3 K2 Pb5 46.35(4) 4_575 .
O24 K2 Pb5 89.0(2) . 4_575
O22 K2 Pb5 136.00(19) . 4_575
O22 K2 Pb5 89.12(18) 4_575 4_575
O21 K2 Pb5 124.7(2) . 4_575
O23 K2 Pb5 123.2(2) . 4_575
O23 K2 Pb5 81.35(16) 4_575 4_575
Pb3 K2 Pb5 46.35(4) . 4_575
Pb3 K2 Pb5 46.35(4) 4_575 4_575
Pb5 K2 Pb5 51.89(5) . 4_575
C21 O21 C21 111.2(18) . 4_575
C21 O21 K2 105.2(9) . .
C21 O21 K2 105.2(9) 4_575 .
C22 O22 C23 114.2(12) . 3_666
C22 O22 K2 119.3(9) . .
C23 O22 K2 120.3(10) 3_666 .
C24 O23 C25 111.1(12) . .
C24 O23 K2 103.4(8) . .
C25 O23 K2 104.4(8) . .
C26 O24 C26 111.5(18) 4_575 .
C26 O24 K2 123.2(9) 4_575 .
C26 O24 K2 123.2(9) . .
O21 C21 C22 108.3(12) . .
O22 C22 C21 109.1(12) . .
O22 C23 C24 107.7(11) 3_666 3_666
O23 C24 C23 108.1(12) . 3_666
O23 C25 C26 108.9(12) . .
O24 C26 C25 108.7(12) . .
O31 K3 O33 107.0(2) . 4_575
O31 K3 O33 107.0(2) . .
O33 K3 O33 112.0(4) 4_575 .
O31 K3 O34 129.6(4) . .
O33 K3 O34 56.37(19) 4_575 .
O33 K3 O34 56.37(19) . .
O31 K3 O32 55.3(2) . 1_455
O33 K3 O32 136.7(3) 4_575 1_455
O33 K3 O32 53.7(2) . 1_455
O34 K3 O32 101.8(2) . 1_455
O31 K3 O32 55.3(2) . 4_475
O33 K3 O32 53.7(2) 4_575 4_475
O33 K3 O32 136.7(3) . 4_475
O34 K3 O32 101.8(2) . 4_475
O32 K3 O32 105.4(4) 1_455 4_475
O31 K3 Pb2 77.5(3) . .
O33 K3 Pb2 121.94(19) 4_575 .
O33 K3 Pb2 121.94(19) . .
O34 K3 Pb2 152.9(2) . .
O32 K3 Pb2 94.48(18) 1_455 .
O32 K3 Pb2 94.48(18) 4_475 .
O31 K3 Pb2 77.5(3) . 4_575
O33 K3 Pb2 121.94(19) 4_575 4_575
O33 K3 Pb2 121.94(19) . 4_575
O34 K3 Pb2 152.9(2) . 4_575
O32 K3 Pb2 94.48(18) 1_455 4_575
O32 K3 Pb2 94.48(18) 4_475 4_575
Pb2 K3 Pb2 0.000(16) . 4_575
O31 K3 Pb1 108.2(2) . 4_575
O33 K3 Pb1 78.76(18) 4_575 4_575
O33 K3 Pb1 137.8(2) . 4_575
O34 K3 Pb1 112.93(19) . 4_575
O32 K3 Pb1 141.71(19) 1_455 4_575
O32 K3 Pb1 83.47(17) 4_475 4_575
Pb2 K3 Pb1 47.31(4) . 4_575
Pb2 K3 Pb1 47.31(4) 4_575 4_575
O31 K3 Pb1 108.2(2) . .
O33 K3 Pb1 137.8(2) 4_575 .
O33 K3 Pb1 78.76(18) . .
O34 K3 Pb1 112.93(19) . .
O32 K3 Pb1 83.47(17) 1_455 .
O32 K3 Pb1 141.71(19) 4_475 .
Pb2 K3 Pb1 47.31(4) . .
Pb2 K3 Pb1 47.31(4) 4_575 .
Pb1 K3 Pb1 68.78(6) 4_575 .
O31 K3 Pb3 146.4(3) . 4_575
O33 K3 Pb3 91.17(18) 4_575 4_575
O33 K3 Pb3 91.17(18) . 4_575
O34 K3 Pb3 84.0(2) . 4_575
O32 K3 Pb3 126.07(18) 1_455 4_575
O32 K3 Pb3 126.07(18) 4_475 4_575
Pb2 K3 Pb3 68.94(7) . 4_575
Pb2 K3 Pb3 68.94(7) 4_575 4_575
Pb1 K3 Pb3 46.95(4) 4_575 4_575
Pb1 K3 Pb3 46.95(4) . 4_575
O31 K3 Pb3 146.4(3) . .
O33 K3 Pb3 91.17(18) 4_575 .
O33 K3 Pb3 91.17(18) . .
O34 K3 Pb3 84.0(2) . .
O32 K3 Pb3 126.07(18) 1_455 .
O32 K3 Pb3 126.07(18) 4_475 .
Pb2 K3 Pb3 68.94(7) . .
Pb2 K3 Pb3 68.94(7) 4_575 .
Pb1 K3 Pb3 46.95(4) 4_575 .
Pb1 K3 Pb3 46.95(4) . .
Pb3 K3 Pb3 0.000(4) 4_575 .
C31 O31 C31 113.7(16) 1_455 4_475
C31 O31 K3 123.0(8) 1_455 .
C31 O31 K3 123.0(8) 4_475 .
C33 O32 C32 114.8(11) . .
C33 O32 K3 100.6(7) . 1_655
C32 O32 K3 99.3(8) . 1_655
C35 O33 C34 113.0(10) . .
C35 O33 K3 120.8(7) . .
C34 O33 K3 124.8(8) . .
C36 O34 C36 110.8(13) 4_575 .
C36 O34 K3 105.1(7) 4_575 .
C36 O34 K3 105.1(7) . .
O31 C31 C32 109.3(12) 1_655 .
O32 C32 C31 110.4(13) . .
O32 C33 C34 109.9(11) . 1_655
O33 C34 C33 107.6(11) . 1_455
O33 C35 C36 109.1(10) . .
O34 C36 C35 109.6(10) . .
O41 K4 O43 116.0(3) . .
O41 K4 O43 116.0(3) . 4_565
O43 K4 O43 112.4(5) . 4_565
O41 K4 N4 108.1(3) . .
O43 K4 N4 73.8(3) . .
O43 K4 N4 124.2(4) 4_565 .
O41 K4 N4 108.1(3) . 4_565
O43 K4 N4 124.2(4) . 4_565
O43 K4 N4 73.8(3) 4_565 4_565
N4 K4 N4 60.8(5) . 4_565
O41 K4 O42 59.0(2) . 4_565
O43 K4 O42 146.4(3) . 4_565
O43 K4 O42 57.4(3) 4_565 4_565
N4 K4 O42 139.7(3) . 4_565
N4 K4 O42 85.8(3) 4_565 4_565
O41 K4 O42 59.0(2) . .
O43 K4 O42 57.4(3) . .
O43 K4 O42 146.4(3) 4_565 .
N4 K4 O42 85.8(3) . .
N4 K4 O42 139.7(3) 4_565 .
O42 K4 O42 111.3(4) 4_565 .
O41 K4 O44 146.1(5) . .
O43 K4 O44 56.3(3) . .
O43 K4 O44 56.3(3) 4_565 .
N4 K4 O44 101.1(4) . .
N4 K4 O44 101.1(4) 4_565 .
O42 K4 O44 107.4(3) 4_565 .
O42 K4 O44 107.4(3) . .
O41 K4 C43 81.5(4) . 4_565
O43 K4 C43 145.3(6) . 4_565
O43 K4 C43 36.8(5) 4_565 4_565
N4 K4 C43 131.8(6) . 4_565
N4 K4 C43 71.2(6) 4_565 4_565
O42 K4 C43 23.3(4) 4_565 4_565
O42 K4 C43 133.9(5) . 4_565
O44 K4 C43 92.0(5) . 4_565
O41 K4 C43 81.5(4) . .
O43 K4 C43 36.8(5) . .
O43 K4 C43 145.3(6) 4_565 .
N4 K4 C43 71.2(6) . .
N4 K4 C43 131.8(6) 4_565 .
O42 K4 C43 133.9(5) 4_565 .
O42 K4 C43 23.3(4) . .
O44 K4 C43 92.0(5) . .
C43 K4 C43 155.0(10) 4_565 .
C41 O41 C41 110(2) 4_565 .
C41 O41 K4 119.2(9) 4_565 .
C41 O41 K4 119.2(9) . .
C431 O42 C43 20.8(18) . .
C431 O42 C42 108.4(15) . .
C43 O42 C42 128.1(18) . .
C431 O42 K4 106.8(15) . .
C43 O42 K4 102.9(18) . .
C42 O42 K4 107.2(9) . .
C45 O43 C44 91.1(19) . .
C45 O43 C441 111.2(19) . .
C44 O43 C441 20.7(19) . .
C45 O43 C451 24(2) . .
C44 O43 C451 114(2) . .
C441 O43 C451 133(2) . .
C45 O43 K4 131.8(16) . .
C44 O43 K4 130.7(15) . .
C441 O43 K4 113.8(14) . .
C451 O43 K4 113.4(14) . .
C461 O44 C461 84(3) 4_565 .
C461 O44 C46 28(2) 4_565 4_565
C461 O44 C46 111(3) . 4_565
C461 O44 C46 111(3) 4_565 .
C461 O44 C46 28(2) . .
C46 O44 C46 138(3) 4_565 .
C461 O44 K4 112(2) 4_565 .
C461 O44 K4 112(2) . .
C46 O44 K4 104.7(19) 4_565 .
C46 O44 K4 104.7(19) . .
O41 C41 C42 108.2(16) . .
O42 C42 C41 112.1(14) . .
O42 C43 C44 128(3) . .
O42 C43 K4 53.8(14) . .
C44 C43 K4 93.6(19) . .
O42 C431 C441 102(2) . .
O43 C44 C43 96(2) . .
O43 C44 C45 42.2(14) . .
C43 C44 C45 138(2) . .
O43 C441 C431 120(2) . .
O43 C45 C46 102(3) . .
O43 C45 C44 46.7(13) . .
C46 C45 C44 149(3) . .
C461 C451 O43 121(3) . .
O44 C46 C45 126(3) . .
O44 C461 C451 96(2) . .
O44 C461 C461 48.2(15) . 4_565
C451 C461 C461 144.6(18) . 4_565
C47 N4 K4 110.3(10) . .
C47 C47 N4 128.6(9) 4_565 .
C52 C51 C54 123(4) . 1_655
C51 C52 C53 120(5) . 3_666
C52 C53 C56 117(4) 3_666 1_455
C55 C54 C51 120(3) 3_666 1_455
C56 C55 C54 122(3) . 3_666
C55 C56 C53 118(3) . 1_655
C55 C56 C57 128(3) . .
C53 C56 C57 114(3) 1_655 .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Pb1 Pb5 3.0799(8) .
Pb1 Pb4 3.1137(8) .
Pb1 Pb3 3.1271(8) 4_575
Pb1 Pb3 3.1271(8) .
Pb1 Pb2 3.1375(8) .
Pb1 Pb2 3.1375(8) 4_575
Pb1 K3 3.919(3) .
Pb2 Pb2 0.0000(12) 4_575
Pb2 Pb4 3.1043(8) 4_575
Pb2 Pb4 3.1043(8) .
Pb2 Pb1 3.1375(8) 4_575
Pb2 K3 3.901(4) .
Pb2 K1 4.013(4) .
Pb3 Pb3 0.0000 4_575
Pb3 Pb5 3.1223(8) 4_575
Pb3 Pb5 3.1223(8) .
Pb3 Pb1 3.1271(8) 4_575
Pb3 K3 3.931(4) .
Pb3 K2 3.963(4) .
Pb4 Pb6 3.0804(8) .
Pb4 Pb2 3.1043(8) 4_575
Pb4 Pb4 3.3240(9) 4_575
Pb4 Pb5 3.3672(13) .
Pb4 K1 4.212(3) .
Pb5 Pb6 3.0696(8) .
Pb5 Pb3 3.1223(8) 4_575
Pb5 Pb5 3.4747(9) 4_575
Pb5 K2 3.971(3) .
Pb6 Pb5 3.0696(8) 4_575
Pb6 Pb4 3.0805(8) 4_575
K1 O2 2.761(16) 4_575
K1 O2 2.761(16) .
K1 O4 2.860(18) 2_655
K1 O4 2.860(18) 3_665
K1 O1 2.957(14) .
K1 O1 2.957(14) 4_575
K1 O13 3.001(17) 2_655
K1 O13 3.001(17) 3_665
K1 O12 3.08(2) .
K1 O12 3.08(2) 4_575
K1 O3 3.119(15) 3_665
K1 O3 3.119(15) 2_655
O1 O1 0.64(3) 4_575
O1 C1 1.05(3) 4_575
O1 C11 1.40(3) 4_575
O1 C1 1.47(3) .
O1 C12 1.71(3) 4_575
O2 O12 0.85(2) .
O2 C13 1.24(3) .
O2 C3 1.43(3) .
O2 C2 1.53(4) .
O2 C14 1.70(4) .
O12 C2 0.81(3) .
O12 C12 1.39(3) .
O12 C13 1.45(3) .
O12 C11 1.55(4) .
O3 C4 0.97(2) 3_665
O3 O13 0.995(19) .
O3 C14 1.26(4) 3_665
O3 C5 1.45(3) .
O3 C3 1.48(3) 3_665
O3 K1 3.119(15) 3_665
O13 C5 0.99(3) .
O13 C15 1.36(3) .
O13 C4 1.40(3) 3_665
O13 C6 1.48(4) .
O13 K1 3.001(17) 3_665
O4 C16 0.96(3) .
O4 O4 1.04(3) 4_565
O4 C6 1.36(3) .
O4 C16 1.41(3) 4_565
O4 C15 1.42(3) .
O4 K1 2.860(18) 3_665
C1 C11 0.85(3) .
C1 O1 1.05(3) 4_575
C1 C12 1.44(4) .
C1 C1 1.63(5) 4_575
C11 C12 0.81(3) .
C11 O1 1.40(3) 4_575
C11 C2 1.48(4) .
C2 C12 0.93(3) .
C2 C13 1.50(4) .
C12 O1 1.71(3) 4_575
C3 C14 0.52(4) .
C3 C13 1.03(3) .
C3 O3 1.48(3) 3_665
C3 C4 1.61(4) .
C13 C14 1.53(4) .
C4 O3 0.97(2) 3_665
C4 C5 1.10(3) 3_665
C4 C14 1.14(4) .
C4 O13 1.40(3) 3_665
C14 O3 1.26(4) 3_665
C5 C4 1.10(3) 3_665
C5 C15 1.17(3) .
C5 C6 1.59(4) .
C15 C6 0.76(4) .
C15 C16 1.59(4) .
C6 C16 1.24(3) .
C16 C16 1.02(5) 4_565
C16 O4 1.41(3) 4_565
K2 O24 2.833(14) .
K2 O22 2.849(8) .
K2 O22 2.849(8) 4_575
K2 O21 2.953(13) .
K2 O23 3.049(8) .
K2 O23 3.049(8) 4_575
K2 Pb3 3.963(4) 4_575
K2 Pb5 3.971(3) 4_575
O21 C21 1.384(17) .
O21 C21 1.384(17) 4_575
O22 C22 1.400(18) .
O22 C23 1.443(17) 3_666
O23 C24 1.387(18) .
O23 C25 1.392(19) .
O24 C26 1.423(16) 4_575
O24 C26 1.423(16) .
C21 C22 1.48(2) .
C23 O22 1.443(17) 3_666
C23 C24 1.48(2) 3_666
C24 C23 1.48(2) 3_666
C25 C26 1.49(2) .
K3 O31 2.904(12) .
K3 O33 2.909(8) 4_575
K3 O33 2.909(8) .
K3 O34 3.038(11) .
K3 O32 3.147(9) 1_455
K3 O32 3.147(8) 4_475
K3 Pb2 3.901(4) 4_575
K3 Pb1 3.919(3) 4_575
K3 Pb3 3.931(4) 4_575
O31 C31 1.387(14) 1_455
O31 C31 1.387(14) 4_475
O32 C33 1.422(14) .
O32 C32 1.430(16) .
O32 K3 3.147(8) 1_655
O33 C35 1.422(14) .
O33 C34 1.426(14) .
O34 C36 1.384(12) 4_575
O34 C36 1.384(12) .
C31 O31 1.387(14) 1_655
C31 C32 1.46(2) .
C33 C34 1.467(18) 1_655
C34 C33 1.467(18) 1_455
C35 C36 1.502(17) .
K4 O41 2.827(13) .
K4 O43 2.836(10) .
K4 O43 2.836(10) 4_565
K4 N4 2.877(12) .
K4 N4 2.877(12) 4_565
K4 O42 2.915(9) 4_565
K4 O42 2.916(9) .
K4 O44 3.020(16) .
K4 C43 3.52(4) 4_565
K4 C43 3.52(4) .
O41 C41 1.414(19) 4_565
O41 C41 1.414(19) .
O42 C431 1.399(10) .
O42 C43 1.427(10) .
O42 C42 1.43(2) .
O43 C45 1.29(4) .
O43 C44 1.395(10) .
O43 C441 1.414(10) .
O43 C451 1.58(4) .
O44 C461 1.394(10) 4_565
O44 C461 1.394(10) .
O44 C46 1.414(10) 4_565
O44 C46 1.414(10) .
C41 C42 1.44(3) .
C43 C44 1.452(10) .
C431 C441 1.449(10) .
C44 C45 1.92(4) .
C45 C46 1.456(10) .
C451 C461 1.443(10) .
C461 C461 1.86(6) 4_565
N4 C47 1.384(19) .
C47 C47 1.19(3) 4_565
C51 C52 1.21(5) .
C51 C54 1.35(3) 1_655
C52 C53 1.40(5) 3_666
C53 C52 1.40(5) 3_666
C53 C56 1.42(4) 1_455
C54 C55 1.30(3) 3_666
C54 C51 1.35(4) 1_455
C55 C56 1.29(3) .
C55 C54 1.30(3) 3_666
C56 C53 1.42(4) 1_655
C56 C57 1.46(3) .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
Pb5 Pb1 Pb2 Pb2 0.00(2) . . . 4_575
Pb4 Pb1 Pb2 Pb2 0.000(19) . . . 4_575
Pb3 Pb1 Pb2 Pb2 0.000(19) 4_575 . . 4_575
Pb3 Pb1 Pb2 Pb2 0.000(19) . . . 4_575
K3 Pb1 Pb2 Pb2 0.00(2) . . . 4_575
Pb5 Pb1 Pb2 Pb4 -0.24(2) . . . 4_575
Pb4 Pb1 Pb2 Pb4 -48.54(2) . . . 4_575
Pb3 Pb1 Pb2 Pb4 58.82(3) 4_575 . . 4_575
Pb3 Pb1 Pb2 Pb4 58.82(3) . . . 4_575
Pb2 Pb1 Pb2 Pb4 0(34) 4_575 . . 4_575
K3 Pb1 Pb2 Pb4 123.17(5) . . . 4_575
Pb5 Pb1 Pb2 Pb4 48.30(2) . . . .
Pb3 Pb1 Pb2 Pb4 107.36(2) 4_575 . . .
Pb3 Pb1 Pb2 Pb4 107.36(2) . . . .
Pb2 Pb1 Pb2 Pb4 0(26) 4_575 . . .
K3 Pb1 Pb2 Pb4 171.71(4) . . . .
Pb5 Pb1 Pb2 Pb1 -58.87(3) . . . 4_575
Pb4 Pb1 Pb2 Pb1 -107.18(2) . . . 4_575
Pb3 Pb1 Pb2 Pb1 0.19(2) 4_575 . . 4_575
Pb3 Pb1 Pb2 Pb1 0.19(2) . . . 4_575
Pb2 Pb1 Pb2 Pb1 0(23) 4_575 . . 4_575
K3 Pb1 Pb2 Pb1 64.53(4) . . . 4_575
Pb5 Pb1 Pb2 K3 -123.41(5) . . . .
Pb4 Pb1 Pb2 K3 -171.71(4) . . . .
Pb3 Pb1 Pb2 K3 -64.35(4) 4_575 . . .
Pb3 Pb1 Pb2 K3 -64.35(4) . . . .
Pb2 Pb1 Pb2 K3 0(11) 4_575 . . .
Pb5 Pb1 Pb2 K1 77.02(6) . . . .
Pb4 Pb1 Pb2 K1 28.72(6) . . . .
Pb3 Pb1 Pb2 K1 136.09(6) 4_575 . . .
Pb3 Pb1 Pb2 K1 136.09(6) . . . .
Pb2 Pb1 Pb2 K1 0(21) 4_575 . . .
K3 Pb1 Pb2 K1 -159.57(7) . . . .
Pb5 Pb1 Pb3 Pb3 0.000(18) . . . 4_575
Pb4 Pb1 Pb3 Pb3 0.00(2) . . . 4_575
Pb2 Pb1 Pb3 Pb3 0.00(2) . . . 4_575
Pb2 Pb1 Pb3 Pb3 0.00(2) 4_575 . . 4_575
K3 Pb1 Pb3 Pb3 0.00(2) . . . 4_575
Pb5 Pb1 Pb3 Pb5 50.80(3) . . . 4_575
Pb4 Pb1 Pb3 Pb5 0.48(2) . . . 4_575
Pb3 Pb1 Pb3 Pb5 0(31) 4_575 . . 4_575
Pb2 Pb1 Pb3 Pb5 -57.91(2) . . . 4_575
Pb2 Pb1 Pb3 Pb5 -57.91(2) 4_575 . . 4_575
K3 Pb1 Pb3 Pb5 -121.65(5) . . . 4_575
Pb4 Pb1 Pb3 Pb5 -50.32(2) . . . .
Pb3 Pb1 Pb3 Pb5 0(33) 4_575 . . .
Pb2 Pb1 Pb3 Pb5 -108.71(2) . . . .
Pb2 Pb1 Pb3 Pb5 -108.71(2) 4_575 . . .
K3 Pb1 Pb3 Pb5 -172.45(4) . . . .
Pb5 Pb1 Pb3 Pb1 108.52(2) . . . 4_575
Pb4 Pb1 Pb3 Pb1 58.20(2) . . . 4_575
Pb3 Pb1 Pb3 Pb1 0(19) 4_575 . . 4_575
Pb2 Pb1 Pb3 Pb1 -0.19(2) . . . 4_575
Pb2 Pb1 Pb3 Pb1 -0.19(2) 4_575 . . 4_575
K3 Pb1 Pb3 Pb1 -63.93(5) . . . 4_575
Pb5 Pb1 Pb3 K3 172.45(4) . . . .
Pb4 Pb1 Pb3 K3 122.13(5) . . . .
Pb3 Pb1 Pb3 K3 0(6) 4_575 . . .
Pb2 Pb1 Pb3 K3 63.75(5) . . . .
Pb2 Pb1 Pb3 K3 63.75(5) 4_575 . . .
Pb5 Pb1 Pb3 K2 -21.69(5) . . . .
Pb4 Pb1 Pb3 K2 -72.01(6) . . . .
Pb3 Pb1 Pb3 K2 0(26) 4_575 . . .
Pb2 Pb1 Pb3 K2 -130.40(6) . . . .
Pb2 Pb1 Pb3 K2 -130.40(6) 4_575 . . .
K3 Pb1 Pb3 K2 165.85(7) . . . .
Pb2 Pb2 Pb4 Pb6 0.000(18) 4_575 . . .
Pb4 Pb2 Pb4 Pb6 26.78(2) 4_575 . . .
Pb1 Pb2 Pb4 Pb6 -18.99(3) 4_575 . . .
Pb1 Pb2 Pb4 Pb6 -99.92(3) . . . .
K3 Pb2 Pb4 Pb6 -90.52(5) . . . .
K1 Pb2 Pb4 Pb6 104.37(4) . . . .
Pb4 Pb2 Pb4 Pb2 0(4) 4_575 . . 4_575
Pb1 Pb2 Pb4 Pb2 0(6) 4_575 . . 4_575
Pb1 Pb2 Pb4 Pb2 0(21) . . . 4_575
K3 Pb2 Pb4 Pb2 0(17) . . . 4_575
K1 Pb2 Pb4 Pb2 0(17) . . . 4_575
Pb2 Pb2 Pb4 Pb1 0.000(18) 4_575 . . .
Pb4 Pb2 Pb4 Pb1 126.70(2) 4_575 . . .
Pb1 Pb2 Pb4 Pb1 80.94(3) 4_575 . . .
K3 Pb2 Pb4 Pb1 9.40(4) . . . .
K1 Pb2 Pb4 Pb1 -155.70(3) . . . .
Pb2 Pb2 Pb4 Pb4 0.000(8) 4_575 . . 4_575
Pb1 Pb2 Pb4 Pb4 -45.767(13) 4_575 . . 4_575
Pb1 Pb2 Pb4 Pb4 -126.70(2) . . . 4_575
K3 Pb2 Pb4 Pb4 -117.30(5) . . . 4_575
K1 Pb2 Pb4 Pb4 77.59(3) . . . 4_575
Pb2 Pb2 Pb4 Pb5 0.000(15) 4_575 . . .
Pb4 Pb2 Pb4 Pb5 84.900(19) 4_575 . . .
Pb1 Pb2 Pb4 Pb5 39.13(2) 4_575 . . .
Pb1 Pb2 Pb4 Pb5 -41.805(16) . . . .
K3 Pb2 Pb4 Pb5 -32.40(5) . . . .
K1 Pb2 Pb4 Pb5 162.49(3) . . . .
Pb2 Pb2 Pb4 K1 0.000(15) 4_575 . . .
Pb4 Pb2 Pb4 K1 -77.59(3) 4_575 . . .
Pb1 Pb2 Pb4 K1 -123.36(4) 4_575 . . .
Pb1 Pb2 Pb4 K1 155.70(3) . . . .
K3 Pb2 Pb4 K1 165.10(5) . . . .
Pb5 Pb1 Pb4 Pb6 -25.954(17) . . . .
Pb3 Pb1 Pb4 Pb6 21.21(2) 4_575 . . .
Pb3 Pb1 Pb4 Pb6 21.21(2) . . . .
Pb2 Pb1 Pb4 Pb6 102.27(2) . . . .
Pb2 Pb1 Pb4 Pb6 102.27(2) 4_575 . . .
K3 Pb1 Pb4 Pb6 93.01(6) . . . .
Pb5 Pb1 Pb4 Pb2 -128.224(19) . . . 4_575
Pb3 Pb1 Pb4 Pb2 -81.06(3) 4_575 . . 4_575
Pb3 Pb1 Pb4 Pb2 -81.06(3) . . . 4_575
Pb2 Pb1 Pb4 Pb2 0.0 . . . 4_575
K3 Pb1 Pb4 Pb2 -9.26(5) . . . 4_575
Pb5 Pb1 Pb4 Pb2 -128.224(19) . . . .
Pb3 Pb1 Pb4 Pb2 -81.06(3) 4_575 . . .
Pb3 Pb1 Pb4 Pb2 -81.06(3) . . . .
Pb2 Pb1 Pb4 Pb2 0.0 4_575 . . .
K3 Pb1 Pb4 Pb2 -9.26(5) . . . .
Pb5 Pb1 Pb4 Pb4 -84.752(11) . . . 4_575
Pb3 Pb1 Pb4 Pb4 -37.591(18) 4_575 . . 4_575
Pb3 Pb1 Pb4 Pb4 -37.591(18) . . . 4_575
Pb2 Pb1 Pb4 Pb4 43.472(16) . . . 4_575
Pb2 Pb1 Pb4 Pb4 43.472(16) 4_575 . . 4_575
K3 Pb1 Pb4 Pb4 34.21(5) . . . 4_575
Pb3 Pb1 Pb4 Pb5 47.161(19) 4_575 . . .
Pb3 Pb1 Pb4 Pb5 47.161(19) . . . .
Pb2 Pb1 Pb4 Pb5 128.224(19) . . . .
Pb2 Pb1 Pb4 Pb5 128.224(19) 4_575 . . .
K3 Pb1 Pb4 Pb5 118.97(5) . . . .
Pb5 Pb1 Pb4 K1 -153.70(3) . . . .
Pb3 Pb1 Pb4 K1 -106.54(3) 4_575 . . .
Pb3 Pb1 Pb4 K1 -106.54(3) . . . .
Pb2 Pb1 Pb4 K1 -25.48(3) . . . .
Pb2 Pb1 Pb4 K1 -25.48(3) 4_575 . . .
K3 Pb1 Pb4 K1 -34.74(6) . . . .
Pb4 Pb1 Pb5 Pb6 26.236(16) . . . .
Pb3 Pb1 Pb5 Pb6 -99.19(2) 4_575 . . .
Pb3 Pb1 Pb5 Pb6 -99.19(2) . . . .
Pb2 Pb1 Pb5 Pb6 -18.62(2) . . . .
Pb2 Pb1 Pb5 Pb6 -18.62(2) 4_575 . . .
K3 Pb1 Pb5 Pb6 -90.55(6) . . . .
Pb4 Pb1 Pb5 Pb3 125.429(17) . . . 4_575
Pb3 Pb1 Pb5 Pb3 0.0 . . . 4_575
Pb2 Pb1 Pb5 Pb3 80.57(2) . . . 4_575
Pb2 Pb1 Pb5 Pb3 80.57(2) 4_575 . . 4_575
K3 Pb1 Pb5 Pb3 8.65(5) . . . 4_575
Pb4 Pb1 Pb5 Pb3 125.429(17) . . . .
Pb3 Pb1 Pb5 Pb3 0.0 4_575 . . .
Pb2 Pb1 Pb5 Pb3 80.57(2) . . . .
Pb2 Pb1 Pb5 Pb3 80.57(2) 4_575 . . .
K3 Pb1 Pb5 Pb3 8.65(5) . . . .
Pb3 Pb1 Pb5 Pb4 -125.429(18) 4_575 . . .
Pb3 Pb1 Pb5 Pb4 -125.429(18) . . . .
Pb2 Pb1 Pb5 Pb4 -44.857(17) . . . .
Pb2 Pb1 Pb5 Pb4 -44.857(17) 4_575 . . .
K3 Pb1 Pb5 Pb4 -116.78(5) . . . .
Pb4 Pb1 Pb5 Pb5 82.744(11) . . . 4_575
Pb3 Pb1 Pb5 Pb5 -42.686(13) 4_575 . . 4_575
Pb3 Pb1 Pb5 Pb5 -42.686(13) . . . 4_575
Pb2 Pb1 Pb5 Pb5 37.886(17) . . . 4_575
Pb2 Pb1 Pb5 Pb5 37.886(17) 4_575 . . 4_575
K3 Pb1 Pb5 Pb5 -34.04(5) . . . 4_575
Pb4 Pb1 Pb5 K2 147.37(3) . . . .
Pb3 Pb1 Pb5 K2 21.95(3) 4_575 . . .
Pb3 Pb1 Pb5 K2 21.95(3) . . . .
Pb2 Pb1 Pb5 K2 102.52(3) . . . .
Pb2 Pb1 Pb5 K2 102.52(3) 4_575 . . .
K3 Pb1 Pb5 K2 30.59(6) . . . .
Pb3 Pb3 Pb5 Pb6 0.00(4) 4_575 . . .
Pb5 Pb3 Pb5 Pb6 -23.95(2) 4_575 . . .
Pb1 Pb3 Pb5 Pb6 102.33(3) . . . .
Pb1 Pb3 Pb5 Pb6 22.01(2) 4_575 . . .
K3 Pb3 Pb5 Pb6 93.90(5) . . . .
K2 Pb3 Pb5 Pb6 -97.40(4) . . . .
Pb3 Pb3 Pb5 Pb1 0.00(4) 4_575 . . .
Pb5 Pb3 Pb5 Pb1 -126.278(19) 4_575 . . .
Pb1 Pb3 Pb5 Pb1 -80.32(3) 4_575 . . .
K3 Pb3 Pb5 Pb1 -8.43(4) . . . .
K2 Pb3 Pb5 Pb1 160.27(4) . . . .
Pb5 Pb3 Pb5 Pb3 0(8) 4_575 . . 4_575
Pb1 Pb3 Pb5 Pb3 0(33) . . . 4_575
Pb1 Pb3 Pb5 Pb3 0(17) 4_575 . . 4_575
K3 Pb3 Pb5 Pb3 0(31) . . . 4_575
K2 Pb3 Pb5 Pb3 0(7) . . . 4_575
Pb3 Pb3 Pb5 Pb4 0.00(4) 4_575 . . .
Pb5 Pb3 Pb5 Pb4 -82.105(17) 4_575 . . .
Pb1 Pb3 Pb5 Pb4 44.17(2) . . . .
Pb1 Pb3 Pb5 Pb4 -36.15(2) 4_575 . . .
K3 Pb3 Pb5 Pb4 35.74(5) . . . .
K2 Pb3 Pb5 Pb4 -155.56(4) . . . .
Pb3 Pb3 Pb5 Pb5 0.00(3) 4_575 . . 4_575
Pb1 Pb3 Pb5 Pb5 126.278(19) . . . 4_575
Pb1 Pb3 Pb5 Pb5 45.955(18) 4_575 . . 4_575
K3 Pb3 Pb5 Pb5 117.85(5) . . . 4_575
K2 Pb3 Pb5 Pb5 -73.45(4) . . . 4_575
Pb3 Pb3 Pb5 K2 0.00(4) 4_575 . . .
Pb5 Pb3 Pb5 K2 73.45(4) 4_575 . . .
Pb1 Pb3 Pb5 K2 -160.27(4) . . . .
Pb1 Pb3 Pb5 K2 119.41(4) 4_575 . . .
K3 Pb3 Pb5 K2 -168.70(5) . . . .
Pb2 Pb4 Pb5 Pb6 -105.94(2) 4_575 . . .
Pb2 Pb4 Pb5 Pb6 -105.94(2) . . . .
Pb1 Pb4 Pb5 Pb6 -150.027(18) . . . .
Pb4 Pb4 Pb5 Pb6 -48.642(13) 4_575 . . .
K1 Pb4 Pb5 Pb6 -60.73(13) . . . .
Pb6 Pb4 Pb5 Pb1 150.027(18) . . . .
Pb2 Pb4 Pb5 Pb1 44.090(17) 4_575 . . .
Pb2 Pb4 Pb5 Pb1 44.090(17) . . . .
Pb4 Pb4 Pb5 Pb1 101.385(12) 4_575 . . .
K1 Pb4 Pb5 Pb1 89.30(13) . . . .
Pb6 Pb4 Pb5 Pb3 104.05(2) . . . 4_575
Pb2 Pb4 Pb5 Pb3 -1.888(17) 4_575 . . 4_575
Pb2 Pb4 Pb5 Pb3 -1.888(17) . . . 4_575
Pb1 Pb4 Pb5 Pb3 -45.978(17) . . . 4_575
Pb4 Pb4 Pb5 Pb3 55.407(13) 4_575 . . 4_575
K1 Pb4 Pb5 Pb3 43.32(13) . . . 4_575
Pb6 Pb4 Pb5 Pb3 104.05(2) . . . .
Pb2 Pb4 Pb5 Pb3 -1.888(17) 4_575 . . .
Pb2 Pb4 Pb5 Pb3 -1.888(17) . . . .
Pb1 Pb4 Pb5 Pb3 -45.978(17) . . . .
Pb4 Pb4 Pb5 Pb3 55.407(13) 4_575 . . .
K1 Pb4 Pb5 Pb3 43.32(13) . . . .
Pb6 Pb4 Pb5 Pb5 48.640(13) . . . 4_575
Pb2 Pb4 Pb5 Pb5 -57.297(13) 4_575 . . 4_575
Pb2 Pb4 Pb5 Pb5 -57.297(13) . . . 4_575
Pb1 Pb4 Pb5 Pb5 -101.387(12) . . . 4_575
Pb4 Pb4 Pb5 Pb5 0.0 4_575 . . 4_575
K1 Pb4 Pb5 Pb5 -12.09(13) . . . 4_575
Pb6 Pb4 Pb5 K2 47.90(12) . . . .
Pb2 Pb4 Pb5 K2 -58.04(12) 4_575 . . .
Pb2 Pb4 Pb5 K2 -58.04(12) . . . .
Pb1 Pb4 Pb5 K2 -102.13(12) . . . .
Pb4 Pb4 Pb5 K2 -0.74(12) 4_575 . . .
K1 Pb4 Pb5 K2 -12.83(18) . . . .
Pb1 Pb5 Pb6 Pb5 88.04(2) . . . 4_575
Pb3 Pb5 Pb6 Pb5 24.15(2) 4_575 . . 4_575
Pb3 Pb5 Pb6 Pb5 24.15(2) . . . 4_575
Pb4 Pb5 Pb6 Pb5 114.467(17) . . . 4_575
K2 Pb5 Pb6 Pb5 -45.13(4) . . . 4_575
Pb1 Pb5 Pb6 Pb4 -26.424(19) . . . .
Pb3 Pb5 Pb6 Pb4 -90.32(2) 4_575 . . .
Pb3 Pb5 Pb6 Pb4 -90.32(2) . . . .
Pb5 Pb5 Pb6 Pb4 -114.467(17) 4_575 . . .
K2 Pb5 Pb6 Pb4 -159.60(4) . . . .
Pb1 Pb5 Pb6 Pb4 29.49(2) . . . 4_575
Pb3 Pb5 Pb6 Pb4 -34.40(2) 4_575 . . 4_575
Pb3 Pb5 Pb6 Pb4 -34.40(2) . . . 4_575
Pb4 Pb5 Pb6 Pb4 55.92(2) . . . 4_575
Pb5 Pb5 Pb6 Pb4 -58.55(2) 4_575 . . 4_575
K2 Pb5 Pb6 Pb4 -103.68(5) . . . 4_575
Pb2 Pb4 Pb6 Pb5 29.78(2) 4_575 . . 4_575
Pb2 Pb4 Pb6 Pb5 29.78(2) . . . 4_575
Pb1 Pb4 Pb6 Pb5 -34.39(2) . . . 4_575
Pb4 Pb4 Pb6 Pb5 56.646(16) 4_575 . . 4_575
Pb5 Pb4 Pb6 Pb5 -60.32(2) . . . 4_575
K1 Pb4 Pb6 Pb5 98.80(5) . . . 4_575
Pb2 Pb4 Pb6 Pb5 90.10(2) 4_575 . . .
Pb2 Pb4 Pb6 Pb5 90.10(2) . . . .
Pb1 Pb4 Pb6 Pb5 25.934(16) . . . .
Pb4 Pb4 Pb6 Pb5 116.97(2) 4_575 . . .
K1 Pb4 Pb6 Pb5 159.12(5) . . . .
Pb2 Pb4 Pb6 Pb4 -26.87(2) 4_575 . . 4_575
Pb2 Pb4 Pb6 Pb4 -26.87(2) . . . 4_575
Pb1 Pb4 Pb6 Pb4 -91.03(2) . . . 4_575
Pb5 Pb4 Pb6 Pb4 -116.97(2) . . . 4_575
K1 Pb4 Pb6 Pb4 42.15(5) . . . 4_575
O2 K1 O1 O1 171.5(4) 4_575 . . 4_575
O2 K1 O1 O1 7.6(4) . . . 4_575
O4 K1 O1 O1 113.5(5) 2_655 . . 4_575
O4 K1 O1 O1 80.9(6) 3_665 . . 4_575
O13 K1 O1 O1 142.0(4) 2_655 . . 4_575
O13 K1 O1 O1 41.6(4) 3_665 . . 4_575
O12 K1 O1 O1 2.4(5) . . . 4_575
O12 K1 O1 O1 177.2(6) 4_575 . . 4_575
O3 K1 O1 O1 30.9(3) 3_665 . . 4_575
O3 K1 O1 O1 150.0(3) 2_655 . . 4_575
O2 K1 O1 C1 -68(2) 4_575 . . 4_575
O2 K1 O1 C1 129(2) . . . 4_575
O4 K1 O1 C1 -126(2) 2_655 . . 4_575
O4 K1 O1 C1 -158(2) 3_665 . . 4_575
O1 K1 O1 C1 121(2) 4_575 . . 4_575
O13 K1 O1 C1 -97(2) 2_655 . . 4_575
O13 K1 O1 C1 163(2) 3_665 . . 4_575
O12 K1 O1 C1 123(2) . . . 4_575
O12 K1 O1 C1 -62(2) 4_575 . . 4_575
O3 K1 O1 C1 152(2) 3_665 . . 4_575
O3 K1 O1 C1 -89(2) 2_655 . . 4_575
O2 K1 O1 C11 -33.3(16) 4_575 . . 4_575
O2 K1 O1 C11 162.8(17) . . . 4_575
O4 K1 O1 C11 -91.3(17) 2_655 . . 4_575
O4 K1 O1 C11 -123.9(16) 3_665 . . 4_575
O1 K1 O1 C11 155.2(16) 4_575 . . 4_575
O13 K1 O1 C11 -62.8(16) 2_655 . . 4_575
O13 K1 O1 C11 -163.2(16) 3_665 . . 4_575
O12 K1 O1 C11 157.5(17) . . . 4_575
O12 K1 O1 C11 -27.7(16) 4_575 . . 4_575
O3 K1 O1 C11 -173.9(16) 3_665 . . 4_575
O3 K1 O1 C11 -54.8(16) 2_655 . . 4_575
O2 K1 O1 C1 -157.4(14) 4_575 . . .
O2 K1 O1 C1 38.7(12) . . . .
O4 K1 O1 C1 144.5(12) 2_655 . . .
O4 K1 O1 C1 112.0(13) 3_665 . . .
O1 K1 O1 C1 31.0(12) 4_575 . . .
O13 K1 O1 C1 173.1(12) 2_655 . . .
O13 K1 O1 C1 72.7(13) 3_665 . . .
O12 K1 O1 C1 33.4(12) . . . .
O12 K1 O1 C1 -151.8(15) 4_575 . . .
O3 K1 O1 C1 61.9(13) 3_665 . . .
O3 K1 O1 C1 -178.9(13) 2_655 . . .
O2 K1 O1 C12 -4.3(12) 4_575 . . 4_575
O2 K1 O1 C12 -168.2(14) . . . 4_575
O4 K1 O1 C12 -62.4(14) 2_655 . . 4_575
O4 K1 O1 C12 -95.0(14) 3_665 . . 4_575
O1 K1 O1 C12 -175.9(12) 4_575 . . 4_575
O13 K1 O1 C12 -33.8(14) 2_655 . . 4_575
O13 K1 O1 C12 -134.2(13) 3_665 . . 4_575
O12 K1 O1 C12 -173.5(14) . . . 4_575
O12 K1 O1 C12 1.3(12) 4_575 . . 4_575
O3 K1 O1 C12 -145.0(13) 3_665 . . 4_575
O3 K1 O1 C12 -25.8(13) 2_655 . . 4_575
O2 K1 O2 O12 -33(2) 4_575 . . .
O4 K1 O2 O12 -151.7(19) 2_655 . . .
O4 K1 O2 O12 -160.0(19) 3_665 . . .
O1 K1 O2 O12 -16.4(19) . . . .
O1 K1 O2 O12 -14.4(18) 4_575 . . .
O13 K1 O2 O12 -115(2) 2_655 . . .
O13 K1 O2 O12 -162(2) 3_665 . . .
O12 K1 O2 O12 -24.1(18) 4_575 . . .
O3 K1 O2 O12 -160(2) 3_665 . . .
O3 K1 O2 O12 -87(2) 2_655 . . .
O2 K1 O2 C13 83(5) 4_575 . . .
O4 K1 O2 C13 -35(5) 2_655 . . .
O4 K1 O2 C13 -44(5) 3_665 . . .
O1 K1 O2 C13 100(5) . . . .
O1 K1 O2 C13 102(5) 4_575 . . .
O13 K1 O2 C13 1(5) 2_655 . . .
O13 K1 O2 C13 -45(5) 3_665 . . .
O12 K1 O2 C13 116(6) . . . .
O12 K1 O2 C13 92(5) 4_575 . . .
O3 K1 O2 C13 -44(5) 3_665 . . .
O3 K1 O2 C13 29(6) 2_655 . . .
O2 K1 O2 C3 135.0(17) 4_575 . . .
O4 K1 O2 C3 16.7(19) 2_655 . . .
O4 K1 O2 C3 8.4(19) 3_665 . . .
O1 K1 O2 C3 152.1(19) . . . .
O1 K1 O2 C3 154.0(19) 4_575 . . .
O13 K1 O2 C3 54(2) 2_655 . . .
O13 K1 O2 C3 6.8(18) 3_665 . . .
O12 K1 O2 C3 168(3) . . . .
O12 K1 O2 C3 144.3(18) 4_575 . . .
O3 K1 O2 C3 8.4(17) 3_665 . . .
O3 K1 O2 C3 81.5(19) 2_655 . . .
O2 K1 O2 C2 -16(2) 4_575 . . .
O4 K1 O2 C2 -133.9(16) 2_655 . . .
O4 K1 O2 C2 -142.2(16) 3_665 . . .
O1 K1 O2 C2 1.5(16) . . . .
O1 K1 O2 C2 3.4(15) 4_575 . . .
O13 K1 O2 C2 -97.0(18) 2_655 . . .
O13 K1 O2 C2 -143.8(18) 3_665 . . .
O12 K1 O2 C2 18(2) . . . .
O12 K1 O2 C2 -6.3(18) 4_575 . . .
O3 K1 O2 C2 -142.2(18) 3_665 . . .
O3 K1 O2 C2 -69.1(19) 2_655 . . .
O2 K1 O2 C14 146.5(14) 4_575 . . .
O4 K1 O2 C14 28.2(16) 2_655 . . .
O4 K1 O2 C14 19.9(15) 3_665 . . .
O1 K1 O2 C14 163.6(16) . . . .
O1 K1 O2 C14 165.5(16) 4_575 . . .
O13 K1 O2 C14 65.1(17) 2_655 . . .
O13 K1 O2 C14 18.3(15) 3_665 . . .
O12 K1 O2 C14 180(3) . . . .
O12 K1 O2 C14 155.8(15) 4_575 . . .
O3 K1 O2 C14 19.9(15) 3_665 . . .
O3 K1 O2 C14 93.0(17) 2_655 . . .
C13 O2 O12 C2 -24(5) . . . .
C3 O2 O12 C2 -30(7) . . . .
C14 O2 O12 C2 -43(7) . . . .
K1 O2 O12 C2 137(5) . . . .
C13 O2 O12 C12 -80(10) . . . .
C3 O2 O12 C12 -86(10) . . . .
C2 O2 O12 C12 -56(9) . . . .
C14 O2 O12 C12 -99(10) . . . .
K1 O2 O12 C12 81(10) . . . .
C3 O2 O12 C13 -6(3) . . . .
C2 O2 O12 C13 24(5) . . . .
C14 O2 O12 C13 -19(4) . . . .
K1 O2 O12 C13 161.4(18) . . . .
C13 O2 O12 C11 -176(6) . . . .
C3 O2 O12 C11 178(5) . . . .
C2 O2 O12 C11 -152(10) . . . .
C14 O2 O12 C11 166(4) . . . .
K1 O2 O12 C11 -15(7) . . . .
C13 O2 O12 K1 -161.4(18) . . . .
C3 O2 O12 K1 -168(3) . . . .
C2 O2 O12 K1 -137(5) . . . .
C14 O2 O12 K1 -180(5) . . . .
O2 K1 O12 C2 28(6) 4_575 . . .
O2 K1 O12 C2 -123(6) . . . .
O4 K1 O12 C2 -90(6) 2_655 . . .
O4 K1 O12 C2 -102(6) 3_665 . . .
O1 K1 O12 C2 38(5) . . . .
O1 K1 O12 C2 39(5) 4_575 . . .
O13 K1 O12 C2 -40(6) 2_655 . . .
O13 K1 O12 C2 -107(6) 3_665 . . .
O12 K1 O12 C2 35(6) 4_575 . . .
O3 K1 O12 C2 -107(6) 3_665 . . .
O3 K1 O12 C2 -13(6) 2_655 . . .
O2 K1 O12 O2 151(2) 4_575 . . .
O4 K1 O12 O2 33(2) 2_655 . . .
O4 K1 O12 O2 21(2) 3_665 . . .
O1 K1 O12 O2 161(2) . . . .
O1 K1 O12 O2 162(2) 4_575 . . .
O13 K1 O12 O2 83(2) 2_655 . . .
O13 K1 O12 O2 16.3(19) 3_665 . . .
O12 K1 O12 O2 157.6(17) 4_575 . . .
O3 K1 O12 O2 15.6(18) 3_665 . . .
O3 K1 O12 O2 110(2) 2_655 . . .
O2 K1 O12 C12 -9.1(18) 4_575 . . .
O2 K1 O12 C12 -160(3) . . . .
O4 K1 O12 C12 -127.1(17) 2_655 . . .
O4 K1 O12 C12 -139.1(17) 3_665 . . .
O1 K1 O12 C12 0.9(16) . . . .
O1 K1 O12 C12 1.7(16) 4_575 . . .
O13 K1 O12 C12 -77.5(19) 2_655 . . .
O13 K1 O12 C12 -144.0(18) 3_665 . . .
O12 K1 O12 C12 -3(2) 4_575 . . .
O3 K1 O12 C12 -144.7(19) 3_665 . . .
O3 K1 O12 C12 -50(2) 2_655 . . .
O2 K1 O12 C13 133.6(16) 4_575 . . .
O2 K1 O12 C13 -17.6(18) . . . .
O4 K1 O12 C13 15.6(18) 2_655 . . .
O4 K1 O12 C13 3.6(17) 3_665 . . .
O1 K1 O12 C13 143.6(17) . . . .
O1 K1 O12 C13 144.3(18) 4_575 . . .
O13 K1 O12 C13 65.1(19) 2_655 . . .
O13 K1 O12 C13 -1.4(15) 3_665 . . .
O12 K1 O12 C13 140.0(14) 4_575 . . .
O3 K1 O12 C13 -2.0(15) 3_665 . . .
O3 K1 O12 C13 92.6(17) 2_655 . . .
O2 K1 O12 C11 -34.8(14) 4_575 . . .
O2 K1 O12 C11 174(3) . . . .
O4 K1 O12 C11 -152.8(13) 2_655 . . .
O4 K1 O12 C11 -164.8(13) 3_665 . . .
O1 K1 O12 C11 -24.8(13) . . . .
O1 K1 O12 C11 -24.0(13) 4_575 . . .
O13 K1 O12 C11 -103.2(15) 2_655 . . .
O13 K1 O12 C11 -169.7(15) 3_665 . . .
O12 K1 O12 C11 -28.4(16) 4_575 . . .
O3 K1 O12 C11 -170.3(15) 3_665 . . .
O3 K1 O12 C11 -75.7(15) 2_655 . . .
C4 O3 O13 C5 -15(3) 3_665 . . .
C14 O3 O13 C5 -26(6) 3_665 . . .
C3 O3 O13 C5 -46(12) 3_665 . . .
K1 O3 O13 C5 -128(2) 3_665 . . .
C4 O3 O13 C15 -5(6) 3_665 . . .
C14 O3 O13 C15 -17(8) 3_665 . . .
C5 O3 O13 C15 9(4) . . . .
C3 O3 O13 C15 -37(15) 3_665 . . .
K1 O3 O13 C15 -119(5) 3_665 . . .
C14 O3 O13 C4 -11(5) 3_665 . . 3_665
C5 O3 O13 C4 15(3) . . . 3_665
C3 O3 O13 C4 -31(11) 3_665 . . 3_665
K1 O3 O13 C4 -113.1(18) 3_665 . . 3_665
C4 O3 O13 C6 -79(7) 3_665 . . .
C14 O3 O13 C6 -90(8) 3_665 . . .
C5 O3 O13 C6 -64(6) . . . .
C3 O3 O13 C6 -110(12) 3_665 . . .
K1 O3 O13 C6 168(7) 3_665 . . .
C4 O3 O13 K1 113.1(18) 3_665 . . 3_665
C14 O3 O13 K1 102(5) 3_665 . . 3_665
C5 O3 O13 K1 128(2) . . . 3_665
C3 O3 O13 K1 82(12) 3_665 . . 3_665
O1 O1 C1 C11 13(3) 4_575 . . .
C1 O1 C1 C11 -167(3) 4_575 . . .
C11 O1 C1 C11 -159(5) 4_575 . . .
C12 O1 C1 C11 175(4) 4_575 . . .
K1 O1 C1 C11 -41(4) . . . .
C1 O1 C1 O1 180.000(12) 4_575 . . 4_575
C11 O1 C1 O1 -171.9(17) 4_575 . . 4_575
C12 O1 C1 O1 161.7(15) 4_575 . . 4_575
K1 O1 C1 O1 -54.0(18) . . . 4_575
O1 O1 C1 C12 -16.5(13) 4_575 . . .
C1 O1 C1 C12 163.5(13) 4_575 . . .
C11 O1 C1 C12 172(2) 4_575 . . .
C12 O1 C1 C12 145(3) 4_575 . . .
K1 O1 C1 C12 -70(2) . . . .
O1 O1 C1 C1 180.000(11) 4_575 . . 4_575
C11 O1 C1 C1 8.1(17) 4_575 . . 4_575
C12 O1 C1 C1 -18.3(15) 4_575 . . 4_575
K1 O1 C1 C1 126.0(18) . . . 4_575
O1 C1 C11 C12 -73(5) 4_575 . . .
O1 C1 C11 C12 -78(6) . . . .
C1 C1 C11 C12 -97(8) 4_575 . . .
C12 C1 C11 O1 73(5) . . . 4_575
O1 C1 C11 O1 -5.1(11) . . . 4_575
C1 C1 C11 O1 -24(5) 4_575 . . 4_575
O1 C1 C11 C2 -45(8) 4_575 . . .
C12 C1 C11 C2 27(5) . . . .
O1 C1 C11 C2 -50(9) . . . .
C1 C1 C11 C2 -70(11) 4_575 . . .
O1 C1 C11 O12 13(8) 4_575 . . .
C12 C1 C11 O12 86(8) . . . .
O1 C1 C11 O12 8(9) . . . .
C1 C1 C11 O12 -11(13) 4_575 . . .
C2 O12 C11 C12 -14(4) . . . .
O2 O12 C11 C12 144(6) . . . .
C13 O12 C11 C12 -30(5) . . . .
K1 O12 C11 C12 131(3) . . . .
C2 O12 C11 C1 -119(8) . . . .
O2 O12 C11 C1 39(11) . . . .
C12 O12 C11 C1 -105(8) . . . .
C13 O12 C11 C1 -135(7) . . . .
K1 O12 C11 C1 26(7) . . . .
C2 O12 C11 O1 -109(3) . . . 4_575
O2 O12 C11 O1 49(7) . . . 4_575
C12 O12 C11 O1 -95(3) . . . 4_575
C13 O12 C11 O1 -125(3) . . . 4_575
K1 O12 C11 O1 36.4(18) . . . 4_575
O2 O12 C11 C2 158(8) . . . .
C12 O12 C11 C2 14(4) . . . .
C13 O12 C11 C2 -15(4) . . . .
K1 O12 C11 C2 146(3) . . . .
O2 O12 C2 C12 -156(4) . . . .
C13 O12 C2 C12 -177(4) . . . .
C11 O12 C2 C12 12(3) . . . .
K1 O12 C2 C12 -59(7) . . . .
O2 O12 C2 C11 -168(4) . . . .
C12 O12 C2 C11 -12(3) . . . .
C13 O12 C2 C11 171(2) . . . .
K1 O12 C2 C11 -71(5) . . . .
O2 O12 C2 C13 21(5) . . . .
C12 O12 C2 C13 177(4) . . . .
C11 O12 C2 C13 -171(2) . . . .
K1 O12 C2 C13 118(5) . . . .
C12 O12 C2 O2 156(4) . . . .
C13 O12 C2 O2 -21(5) . . . .
C11 O12 C2 O2 168(4) . . . .
K1 O12 C2 O2 97(7) . . . .
C12 C11 C2 O12 156(7) . . . .
C1 C11 C2 O12 111(8) . . . .
O1 C11 C2 O12 77(3) 4_575 . . .
C1 C11 C2 C12 -45(8) . . . .
O1 C11 C2 C12 -79(5) 4_575 . . .
O12 C11 C2 C12 -156(7) . . . .
C12 C11 C2 C13 173(8) . . . .
C1 C11 C2 C13 128(8) . . . .
O1 C11 C2 C13 94(5) 4_575 . . .
O12 C11 C2 C13 16(4) . . . .
C12 C11 C2 O2 151(6) . . . .
C1 C11 C2 O2 106(8) . . . .
O1 C11 C2 O2 72(3) 4_575 . . .
O12 C11 C2 O2 -5.0(18) . . . .
C13 O2 C2 O12 153(6) . . . .
C3 O2 C2 O12 156(5) . . . .
C14 O2 C2 O12 151(5) . . . .
K1 O2 C2 O12 -49(5) . . . .
O12 O2 C2 C12 29(5) . . . .
C13 O2 C2 C12 -177(5) . . . .
C3 O2 C2 C12 -175(4) . . . .
C14 O2 C2 C12 -180(4) . . . .
K1 O2 C2 C12 -20(5) . . . .
O12 O2 C2 C11 12(4) . . . .
C13 O2 C2 C11 165(3) . . . .
C3 O2 C2 C11 168(2) . . . .
C14 O2 C2 C11 163(2) . . . .
K1 O2 C2 C11 -37(2) . . . .
O12 O2 C2 C13 -153(6) . . . .
C3 O2 C2 C13 3(2) . . . .
C14 O2 C2 C13 -2(2) . . . .
K1 O2 C2 C13 157.2(19) . . . .
C1 C11 C12 C2 155(5) . . . .
O1 C11 C12 C2 108(4) 4_575 . . .
O12 C11 C12 C2 13(4) . . . .
C1 C11 C12 O12 141(5) . . . .
O1 C11 C12 O12 95(2) 4_575 . . .
C2 C11 C12 O12 -13(4) . . . .
O1 C11 C12 C1 -46(4) 4_575 . . .
C2 C11 C12 C1 -155(5) . . . .
O12 C11 C12 C1 -141(5) . . . .
C1 C11 C12 O1 46(4) . . . 4_575
C2 C11 C12 O1 -108(4) . . . 4_575
O12 C11 C12 O1 -95(2) . . . 4_575
O12 C2 C12 C11 -24(7) . . . .
C13 C2 C12 C11 -67(61) . . . .
O2 C2 C12 C11 -36(7) . . . .
C11 C2 C12 O12 24(7) . . . .
C13 C2 C12 O12 -43(58) . . . .
O2 C2 C12 O12 -12(2) . . . .
O12 C2 C12 C1 -3(8) . . . .
C11 C2 C12 C1 22(4) . . . .
C13 C2 C12 C1 -45(64) . . . .
O2 C2 C12 C1 -15(9) . . . .
O12 C2 C12 O1 38(5) . . . 4_575
C11 C2 C12 O1 62(4) . . . 4_575
C13 C2 C12 O1 -5(63) . . . 4_575
O2 C2 C12 O1 26(6) . . . 4_575
C2 O12 C12 C11 158(6) . . . .
O2 O12 C12 C11 -128(10) . . . .
C13 O12 C12 C11 162(3) . . . .
K1 O12 C12 C11 -56(3) . . . .
O2 O12 C12 C2 74(10) . . . .
C13 O12 C12 C2 3(4) . . . .
C11 O12 C12 C2 -158(6) . . . .
K1 O12 C12 C2 146(4) . . . .
C2 O12 C12 C1 178(5) . . . .
O2 O12 C12 C1 -108(10) . . . .
C13 O12 C12 C1 -178(2) . . . .
C11 O12 C12 C1 20(3) . . . .
K1 O12 C12 C1 -36(3) . . . .
C2 O12 C12 O1 -148(5) . . . 4_575
O2 O12 C12 O1 -74(10) . . . 4_575
C13 O12 C12 O1 -144.3(19) . . . 4_575
C11 O12 C12 O1 54(3) . . . 4_575
K1 O12 C12 O1 -2.0(19) . . . 4_575
O1 C1 C12 C11 107(6) 4_575 . . .
O1 C1 C12 C11 113(6) . . . .
C1 C1 C12 C11 131(6) 4_575 . . .
C11 C1 C12 C2 -40(7) . . . .
O1 C1 C12 C2 67(6) 4_575 . . .
O1 C1 C12 C2 74(6) . . . .
C1 C1 C12 C2 91(6) 4_575 . . .
C11 C1 C12 O12 -41(5) . . . .
O1 C1 C12 O12 66(3) 4_575 . . .
O1 C1 C12 O12 72(3) . . . .
C1 C1 C12 O12 90(3) 4_575 . . .
C11 C1 C12 O1 -107(6) . . . 4_575
O1 C1 C12 O1 6.3(6) . . . 4_575
C1 C1 C12 O1 23.9(18) 4_575 . . 4_575
O12 O2 C3 C14 -154(7) . . . .
C13 O2 C3 C14 -162(9) . . . .
C2 O2 C3 C14 -166(7) . . . .
K1 O2 C3 C14 41(8) . . . .
O12 O2 C3 C13 9(4) . . . .
C2 O2 C3 C13 -3(3) . . . .
C14 O2 C3 C13 162(9) . . . .
K1 O2 C3 C13 -157(2) . . . .
O12 O2 C3 O3 154(3) . . . 3_665
C13 O2 C3 O3 145(3) . . . 3_665
C2 O2 C3 O3 141.7(18) . . . 3_665
C14 O2 C3 O3 -53(7) . . . 3_665
K1 O2 C3 O3 -12(2) . . . 3_665
O12 O2 C3 C4 -174(3) . . . .
C13 O2 C3 C4 177(4) . . . .
C2 O2 C3 C4 174(2) . . . .
C14 O2 C3 C4 -20(7) . . . .
K1 O2 C3 C4 21(3) . . . .
C14 C3 C13 O2 62(25) . . . .
O3 C3 C13 O2 -52(4) 3_665 . . .
C4 C3 C13 O2 -9(13) . . . .
C14 C3 C13 O12 57(26) . . . .
O2 C3 C13 O12 -4.3(19) . . . .
O3 C3 C13 O12 -57(5) 3_665 . . .
C4 C3 C13 O12 -13(14) . . . .
C14 C3 C13 C2 67(27) . . . .
O2 C3 C13 C2 5(5) . . . .
O3 C3 C13 C2 -47(8) 3_665 . . .
C4 C3 C13 C2 -4(17) . . . .
O2 C3 C13 C14 -62(25) . . . .
O3 C3 C13 C14 -114(27) 3_665 . . .
C4 C3 C13 C14 -71(25) . . . .
O12 O2 C13 C3 -173(3) . . . .
C2 O2 C13 C3 177(3) . . . .
C14 O2 C13 C3 -6(3) . . . .
K1 O2 C13 C3 67(6) . . . .
C3 O2 C13 O12 173(3) . . . .
C2 O2 C13 O12 -10(2) . . . .
C14 O2 C13 O12 168(2) . . . .
K1 O2 C13 O12 -119(5) . . . .
O12 O2 C13 C2 10(2) . . . .
C3 O2 C13 C2 -177(3) . . . .
C14 O2 C13 C2 178(2) . . . .
K1 O2 C13 C2 -109(5) . . . .
O12 O2 C13 C14 -168(2) . . . .
C3 O2 C13 C14 6(3) . . . .
C2 O2 C13 C14 -178(2) . . . .
K1 O2 C13 C14 73(5) . . . .
C2 O12 C13 C3 169(4) . . . .
O2 O12 C13 C3 7(3) . . . .
C12 O12 C13 C3 167(3) . . . .
C11 O12 C13 C3 -176(3) . . . .
K1 O12 C13 C3 25(4) . . . .
C2 O12 C13 O2 162(4) . . . .
C12 O12 C13 O2 160(3) . . . .
C11 O12 C13 O2 177(4) . . . .
K1 O12 C13 O2 18.0(18) . . . .
O2 O12 C13 C2 -162(4) . . . .
C12 O12 C13 C2 -2(3) . . . .
C11 O12 C13 C2 15(3) . . . .
K1 O12 C13 C2 -144(3) . . . .
C2 O12 C13 C14 175(3) . . . .
O2 O12 C13 C14 13(3) . . . .
C12 O12 C13 C14 173(2) . . . .
C11 O12 C13 C14 -170(3) . . . .
K1 O12 C13 C14 31(2) . . . .
O12 C2 C13 C3 -17(7) . . . .
C12 C2 C13 C3 27(63) . . . .
C11 C2 C13 C3 -34(9) . . . .
O2 C2 C13 C3 -6(5) . . . .
O12 C2 C13 O2 -11(3) . . . .
C12 C2 C13 O2 33(60) . . . .
C11 C2 C13 O2 -28(5) . . . .
C12 C2 C13 O12 44(59) . . . .
C11 C2 C13 O12 -17(4) . . . .
O2 C2 C13 O12 11(3) . . . .
O12 C2 C13 C14 -8(5) . . . .
C12 C2 C13 C14 36(62) . . . .
C11 C2 C13 C14 -25(8) . . . .
O2 C2 C13 C14 3(4) . . . .
C14 C3 C4 O3 -176(18) . . . 3_665
C13 C3 C4 O3 -57(13) . . . 3_665
O2 C3 C4 O3 -65(2) . . . 3_665
C14 C3 C4 C5 169(18) . . . 3_665
C13 C3 C4 C5 -73(15) . . . 3_665
O2 C3 C4 C5 -81(6) . . . 3_665
O3 C3 C4 C5 -16(5) 3_665 . . 3_665
C13 C3 C4 C14 118(25) . . . .
O2 C3 C4 C14 110(18) . . . .
O3 C3 C4 C14 176(18) 3_665 . . .
C14 C3 C4 O13 -171(17) . . . 3_665
C13 C3 C4 O13 -53(13) . . . 3_665
O2 C3 C4 O13 -61(3) . . . 3_665
O3 C3 C4 O13 4.4(16) 3_665 . . 3_665
C13 C3 C14 C4 -130(20) . . . .
O2 C3 C14 C4 -77(18) . . . .
O3 C3 C14 C4 -3(13) 3_665 . . .
C13 C3 C14 O3 -127(23) . . . 3_665
O2 C3 C14 O3 -73(6) . . . 3_665
C4 C3 C14 O3 3(13) . . . 3_665
O2 C3 C14 C13 53(23) . . . .
O3 C3 C14 C13 127(23) 3_665 . . .
C4 C3 C14 C13 130(20) . . . .
C13 C3 C14 O2 -53(23) . . . .
O3 C3 C14 O2 73(6) 3_665 . . .
C4 C3 C14 O2 77(18) . . . .
O3 C4 C14 C3 4(17) 3_665 . . .
C5 C4 C14 C3 -16(25) 3_665 . . .
O13 C4 C14 C3 10(19) 3_665 . . .
C5 C4 C14 O3 -20(10) 3_665 . . 3_665
O13 C4 C14 O3 5(2) 3_665 . . 3_665
C3 C4 C14 O3 -4(17) . . . 3_665
O3 C4 C14 C13 -21(9) 3_665 . . .
C5 C4 C14 C13 -41(18) 3_665 . . .
O13 C4 C14 C13 -16(11) 3_665 . . .
C3 C4 C14 C13 -25(11) . . . .
O3 C4 C14 O2 -55(3) 3_665 . . .
C5 C4 C14 O2 -75(12) 3_665 . . .
O13 C4 C14 O2 -49(4) 3_665 . . .
C3 C4 C14 O2 -59(16) . . . .
O2 C13 C14 C3 -117(26) . . . .
O12 C13 C14 C3 -125(25) . . . .
C2 C13 C14 C3 -120(25) . . . .
C3 C13 C14 C4 73(25) . . . .
O2 C13 C14 C4 -44(9) . . . .
O12 C13 C14 C4 -52(10) . . . .
C2 C13 C14 C4 -48(11) . . . .
C3 C13 C14 O3 56(24) . . . 3_665
O2 C13 C14 O3 -61(3) . . . 3_665
O12 C13 C14 O3 -68(3) . . . 3_665
C2 C13 C14 O3 -64(5) . . . 3_665
C3 C13 C14 O2 117(26) . . . .
O12 C13 C14 O2 -7.6(15) . . . .
C2 C13 C14 O2 -3(3) . . . .
O12 O2 C14 C3 35(10) . . . .
C13 O2 C14 C3 14(7) . . . .
C2 O2 C14 C3 17(9) . . . .
K1 O2 C14 C3 -144(7) . . . .
O12 O2 C14 C4 -176(4) . . . .
C13 O2 C14 C4 162(4) . . . .
C3 O2 C14 C4 148(10) . . . .
C2 O2 C14 C4 165(3) . . . .
K1 O2 C14 C4 4(4) . . . .
O12 O2 C14 O3 147(4) . . . 3_665
C13 O2 C14 O3 126(3) . . . 3_665
C3 O2 C14 O3 111(8) . . . 3_665
C2 O2 C14 O3 128(2) . . . 3_665
K1 O2 C14 O3 -33(2) . . . 3_665
O12 O2 C14 C13 21(4) . . . .
C3 O2 C14 C13 -14(7) . . . .
C2 O2 C14 C13 2(3) . . . .
K1 O2 C14 C13 -158.5(18) . . . .
O3 O13 C5 C4 13(3) . . . 3_665
C15 O13 C5 C4 -162(3) . . . 3_665
C6 O13 C5 C4 172(3) . . . 3_665
K1 O13 C5 C4 -77(3) 3_665 . . 3_665
O3 O13 C5 C15 175(2) . . . .
C4 O13 C5 C15 162(3) 3_665 . . .
C6 O13 C5 C15 -26(2) . . . .
K1 O13 C5 C15 85(3) 3_665 . . .
C15 O13 C5 O3 -175(2) . . . .
C4 O13 C5 O3 -13(3) 3_665 . . .
C6 O13 C5 O3 159(2) . . . .
K1 O13 C5 O3 -90(3) 3_665 . . .
O3 O13 C5 C6 -159(2) . . . .
C15 O13 C5 C6 26(2) . . . .
C4 O13 C5 C6 -172(3) 3_665 . . .
K1 O13 C5 C6 111(2) 3_665 . . .
C4 O3 C5 O13 161(4) 3_665 . . .
C14 O3 C5 O13 167(3) 3_665 . . .
C3 O3 C5 O13 170(3) 3_665 . . .
K1 O3 C5 O13 51(2) 3_665 . . .
O13 O3 C5 C4 -161(4) . . . 3_665
C14 O3 C5 C4 6(3) 3_665 . . 3_665
C3 O3 C5 C4 9(3) 3_665 . . 3_665
K1 O3 C5 C4 -110(2) 3_665 . . 3_665
C4 O3 C5 C15 154(4) 3_665 . . .
O13 O3 C5 C15 -6(3) . . . .
C14 O3 C5 C15 160(3) 3_665 . . .
C3 O3 C5 C15 164(3) 3_665 . . .
K1 O3 C5 C15 45(3) 3_665 . . .
C4 O3 C5 C6 180(4) 3_665 . . .
O13 O3 C5 C6 19(2) . . . .
C14 O3 C5 C6 -174(2) 3_665 . . .
C3 O3 C5 C6 -171(2) 3_665 . . .
K1 O3 C5 C6 70(2) 3_665 . . .
O13 C5 C15 C6 60(5) . . . .
C4 C5 C15 C6 105(9) 3_665 . . .
O3 C5 C15 C6 65(5) . . . .
C4 C5 C15 O13 45(8) 3_665 . . .
O3 C5 C15 O13 4(2) . . . .
C6 C5 C15 O13 -60(5) . . . .
O13 C5 C15 O4 -18(4) . . . .
C4 C5 C15 O4 27(10) 3_665 . . .
O3 C5 C15 O4 -13(5) . . . .
C6 C5 C15 O4 -78(5) . . . .
O13 C5 C15 C16 27(7) . . . .
C4 C5 C15 C16 71(11) 3_665 . . .
O3 C5 C15 C16 31(8) . . . .
C6 C5 C15 C16 -34(5) . . . .
C5 O13 C15 C6 -124(4) . . . .
O3 O13 C15 C6 -135(5) . . . .
C4 O13 C15 C6 -139(4) 3_665 . . .
K1 O13 C15 C6 111(3) 3_665 . . .
O3 O13 C15 C5 -11(5) . . . .
C4 O13 C15 C5 -15(3) 3_665 . . .
C6 O13 C15 C5 124(4) . . . .
K1 O13 C15 C5 -125(2) 3_665 . . .
C5 O13 C15 O4 166(3) . . . .
O3 O13 C15 O4 155(4) . . . .
C4 O13 C15 O4 151.0(18) 3_665 . . .
C6 O13 C15 O4 -70(3) . . . .
K1 O13 C15 O4 40.7(17) 3_665 . . .
C5 O13 C15 C16 -167(3) . . . .
O3 O13 C15 C16 -178(4) . . . .
C4 O13 C15 C16 178(2) 3_665 . . .
C6 O13 C15 C16 -43(3) . . . .
K1 O13 C15 C16 68(2) 3_665 . . .
C16 O4 C15 C6 48(4) . . . .
O4 O4 C15 C6 102(6) 4_565 . . .
C16 O4 C15 C6 59(4) 4_565 . . .
K1 O4 C15 C6 -130(4) 3_665 . . .
C16 O4 C15 C5 146(4) . . . .
O4 O4 C15 C5 -160(3) 4_565 . . .
C6 O4 C15 C5 98(5) . . . .
C16 O4 C15 C5 157(3) 4_565 . . .
K1 O4 C15 C5 -32(4) 3_665 . . .
C16 O4 C15 O13 133(3) . . . .
O4 O4 C15 O13 -172(4) 4_565 . . .
C6 O4 C15 O13 86(4) . . . .
C16 O4 C15 O13 145(2) 4_565 . . .
K1 O4 C15 O13 -44.7(18) 3_665 . . .
O4 O4 C15 C16 54(6) 4_565 . . .
C6 O4 C15 C16 -48(4) . . . .
C16 O4 C15 C16 11.4(14) 4_565 . . .
K1 O4 C15 C16 -178(2) 3_665 . . .
C5 C15 C6 C16 -159(3) . . . .
O13 C15 C6 C16 -121(3) . . . .
O4 C15 C6 C16 -36(2) . . . .
C5 C15 C6 O4 -124(3) . . . .
O13 C15 C6 O4 -85.2(16) . . . .
C16 C15 C6 O4 36(2) . . . .
C5 C15 C6 O13 -38(3) . . . .
O4 C15 C6 O13 85.2(16) . . . .
C16 C15 C6 O13 121(3) . . . .
O13 C15 C6 C5 38(3) . . . .
O4 C15 C6 C5 124(3) . . . .
C16 C15 C6 C5 159(3) . . . .
C16 O4 C6 C15 -124(5) . . . .
O4 O4 C6 C15 -150(3) 4_565 . . .
C16 O4 C6 C15 -134(4) 4_565 . . .
K1 O4 C6 C15 65(4) 3_665 . . .
O4 O4 C6 C16 -26(4) 4_565 . . .
C16 O4 C6 C16 -10.1(15) 4_565 . . .
C15 O4 C6 C16 124(5) . . . .
K1 O4 C6 C16 -171(3) 3_665 . . .
C16 O4 C6 O13 170(3) . . . .
O4 O4 C6 O13 143(2) 4_565 . . .
C16 O4 C6 O13 160(2) 4_565 . . .
C15 O4 C6 O13 -67(3) . . . .
K1 O4 C6 O13 -2(3) 3_665 . . .
C16 O4 C6 C5 -161(3) . . . .
O4 O4 C6 C5 173.3(16) 4_565 . . .
C16 O4 C6 C5 -171(2) 4_565 . . .
C15 O4 C6 C5 -37(3) . . . .
K1 O4 C6 C5 28(3) 3_665 . . .
C5 O13 C6 C15 46(4) . . . .
O3 O13 C6 C15 113(7) . . . .
C4 O13 C6 C15 54(4) 3_665 . . .
K1 O13 C6 C15 -80(4) 3_665 . . .
C5 O13 C6 C16 136(4) . . . .
O3 O13 C6 C16 -157(5) . . . .
C15 O13 C6 C16 90(5) . . . .
C4 O13 C6 C16 143(3) 3_665 . . .
K1 O13 C6 C16 10(4) 3_665 . . .
C5 O13 C6 O4 127(3) . . . .
O3 O13 C6 O4 -165(6) . . . .
C15 O13 C6 O4 81(4) . . . .
C4 O13 C6 O4 135(2) 3_665 . . .
K1 O13 C6 O4 1(2) 3_665 . . .
O3 O13 C6 C5 67(6) . . . .
C15 O13 C6 C5 -46(4) . . . .
C4 O13 C6 C5 8(3) 3_665 . . .
K1 O13 C6 C5 -126(2) 3_665 . . .
O13 C5 C6 C15 -111(5) . . . .
C4 C5 C6 C15 -125(7) 3_665 . . .
O3 C5 C6 C15 -126(5) . . . .
O13 C5 C6 C16 -76(5) . . . .
C4 C5 C6 C16 -91(8) 3_665 . . .
C15 C5 C6 C16 35(5) . . . .
O3 C5 C6 C16 -91(5) . . . .
O13 C5 C6 O4 -54(3) . . . .
C4 C5 C6 O4 -68(6) 3_665 . . .
C15 C5 C6 O4 57(4) . . . .
O3 C5 C6 O4 -68(3) . . . .
C4 C5 C6 O13 -14(5) 3_665 . . .
C15 C5 C6 O13 111(5) . . . .
O3 C5 C6 O13 -14.5(16) . . . .
O4 O4 C16 C16 0.001(5) 4_565 . . 4_565
C6 O4 C16 C16 -166.5(19) . . . 4_565
C15 O4 C16 C16 167.2(13) . . . 4_565
K1 O4 C16 C16 -22(10) 3_665 . . 4_565
O4 O4 C16 C6 166.5(19) 4_565 . . .
C16 O4 C16 C6 166.5(19) 4_565 . . .
C15 O4 C16 C6 -26(2) . . . .
K1 O4 C16 C6 145(10) 3_665 . . .
C6 O4 C16 O4 -166.5(19) . . . 4_565
C16 O4 C16 O4 -0.001(7) 4_565 . . 4_565
C15 O4 C16 O4 167.2(13) . . . 4_565
K1 O4 C16 O4 -22(10) 3_665 . . 4_565
O4 O4 C16 C15 -167.2(13) 4_565 . . .
C6 O4 C16 C15 26(2) . . . .
C16 O4 C16 C15 -167.2(13) 4_565 . . .
K1 O4 C16 C15 171(11) 3_665 . . .
C15 C6 C16 O4 57(4) . . . .
O13 C6 C16 O4 -12(4) . . . .
C5 C6 C16 O4 33(5) . . . .
C15 C6 C16 C16 102(7) . . . 4_565
O4 C6 C16 C16 45(6) . . . 4_565
O13 C6 C16 C16 33(9) . . . 4_565
C5 C6 C16 C16 78(9) . . . 4_565
C15 C6 C16 O4 69(5) . . . 4_565
O4 C6 C16 O4 11.7(17) . . . 4_565
O13 C6 C16 O4 -1(5) . . . 4_565
C5 C6 C16 O4 44(7) . . . 4_565
O4 C6 C16 C15 -57(4) . . . .
O13 C6 C16 C15 -69(4) . . . .
C5 C6 C16 C15 -24(4) . . . .
C6 C15 C16 O4 -113(5) . . . .
C5 C15 C16 O4 -69(7) . . . .
O13 C15 C16 O4 -49(3) . . . .
C6 C15 C16 C16 -140(5) . . . 4_565
C5 C15 C16 C16 -95(7) . . . 4_565
O13 C15 C16 C16 -76(3) . . . 4_565
O4 C15 C16 C16 -26(3) . . . 4_565
C5 C15 C16 C6 44(6) . . . .
O13 C15 C16 C6 64(4) . . . .
O4 C15 C16 C6 113(5) . . . .
C6 C15 C16 O4 -123(5) . . . 4_565
C5 C15 C16 O4 -79(7) . . . 4_565
O13 C15 C16 O4 -59(3) . . . 4_565
O4 C15 C16 O4 -9.9(11) . . . 4_565
Pb3 Pb3 K2 O24 0(70) 4_575 . . .
Pb5 Pb3 K2 O24 -37.203(17) 4_575 . . .
Pb5 Pb3 K2 O24 37.203(17) . . . .
Pb1 Pb3 K2 O24 57.35(3) . . . .
Pb1 Pb3 K2 O24 -57.35(3) 4_575 . . .
K3 Pb3 K2 O24 180.000(1) . . . .
Pb3 Pb3 K2 O22 0.00(5) 4_575 . . .
Pb5 Pb3 K2 O22 -159.9(2) 4_575 . . .
Pb5 Pb3 K2 O22 -85.5(2) . . . .
Pb1 Pb3 K2 O22 -65.4(2) . . . .
Pb1 Pb3 K2 O22 179.9(2) 4_575 . . .
K3 Pb3 K2 O22 57.3(2) . . . .
Pb3 Pb3 K2 O22 0.00(5) 4_575 . . 4_575
Pb5 Pb3 K2 O22 85.5(2) 4_575 . . 4_575
Pb5 Pb3 K2 O22 159.9(2) . . . 4_575
Pb1 Pb3 K2 O22 -179.9(2) . . . 4_575
Pb1 Pb3 K2 O22 65.4(2) 4_575 . . 4_575
K3 Pb3 K2 O22 -57.3(2) . . . 4_575
Pb3 Pb3 K2 O21 0.00(5) 4_575 . . .
Pb5 Pb3 K2 O21 142.797(17) 4_575 . . .
Pb5 Pb3 K2 O21 -142.797(17) . . . .
Pb1 Pb3 K2 O21 -122.65(3) . . . .
Pb1 Pb3 K2 O21 122.65(3) 4_575 . . .
K3 Pb3 K2 O21 0.000(2) . . . .
Pb3 Pb3 K2 O23 0.00(5) 4_575 . . .
Pb5 Pb3 K2 O23 -107.2(3) 4_575 . . .
Pb5 Pb3 K2 O23 -32.8(3) . . . .
Pb1 Pb3 K2 O23 -12.6(3) . . . .
Pb1 Pb3 K2 O23 -127.3(3) 4_575 . . .
K3 Pb3 K2 O23 110.0(3) . . . .
Pb3 Pb3 K2 O23 0.00(6) 4_575 . . 4_575
Pb5 Pb3 K2 O23 32.8(3) 4_575 . . 4_575
Pb5 Pb3 K2 O23 107.2(3) . . . 4_575
Pb1 Pb3 K2 O23 127.3(3) . . . 4_575
Pb1 Pb3 K2 O23 12.6(3) 4_575 . . 4_575
K3 Pb3 K2 O23 -110.0(3) . . . 4_575
Pb5 Pb3 K2 Pb3 0(19) 4_575 . . 4_575
Pb5 Pb3 K2 Pb3 0(97) . . . 4_575
Pb1 Pb3 K2 Pb3 0(100) . . . 4_575
Pb1 Pb3 K2 Pb3 0(3) 4_575 . . 4_575
K3 Pb3 K2 Pb3 0(100) . . . 4_575
Pb3 Pb3 K2 Pb5 0.00(6) 4_575 . . .
Pb5 Pb3 K2 Pb5 -74.41(3) 4_575 . . .
Pb1 Pb3 K2 Pb5 20.15(4) . . . .
Pb1 Pb3 K2 Pb5 -94.56(3) 4_575 . . .
K3 Pb3 K2 Pb5 142.797(17) . . . .
Pb3 Pb3 K2 Pb5 0.00(5) 4_575 . . 4_575
Pb5 Pb3 K2 Pb5 74.41(3) . . . 4_575
Pb1 Pb3 K2 Pb5 94.56(3) . . . 4_575
Pb1 Pb3 K2 Pb5 -20.15(4) 4_575 . . 4_575
K3 Pb3 K2 Pb5 -142.797(17) . . . 4_575
Pb6 Pb5 K2 O24 -48.99(11) . . . .
Pb1 Pb5 K2 O24 -172.61(11) . . . .
Pb3 Pb5 K2 O24 -151.86(12) 4_575 . . .
Pb3 Pb5 K2 O24 -151.86(12) . . . .
Pb4 Pb5 K2 O24 -88.69(15) . . . .
Pb5 Pb5 K2 O24 -89.51(12) 4_575 . . .
Pb6 Pb5 K2 O22 -161.6(2) . . . .
Pb1 Pb5 K2 O22 74.8(2) . . . .
Pb3 Pb5 K2 O22 95.5(2) 4_575 . . .
Pb3 Pb5 K2 O22 95.5(2) . . . .
Pb4 Pb5 K2 O22 158.7(2) . . . .
Pb5 Pb5 K2 O22 157.9(2) 4_575 . . .
Pb6 Pb5 K2 O22 73.3(4) . . . 4_575
Pb1 Pb5 K2 O22 -50.3(4) . . . 4_575
Pb3 Pb5 K2 O22 -29.5(4) 4_575 . . 4_575
Pb3 Pb5 K2 O22 -29.5(4) . . . 4_575
Pb4 Pb5 K2 O22 33.6(4) . . . 4_575
Pb5 Pb5 K2 O22 32.8(4) 4_575 . . 4_575
Pb6 Pb5 K2 O21 150.17(16) . . . .
Pb1 Pb5 K2 O21 26.55(17) . . . .
Pb3 Pb5 K2 O21 47.31(17) 4_575 . . .
Pb3 Pb5 K2 O21 47.31(17) . . . .
Pb4 Pb5 K2 O21 110.47(18) . . . .
Pb5 Pb5 K2 O21 109.65(17) 4_575 . . .
Pb6 Pb5 K2 O23 -104.8(2) . . . .
Pb1 Pb5 K2 O23 131.6(2) . . . .
Pb3 Pb5 K2 O23 152.3(2) 4_575 . . .
Pb3 Pb5 K2 O23 152.3(2) . . . .
Pb4 Pb5 K2 O23 -144.5(2) . . . .
Pb5 Pb5 K2 O23 -145.3(2) 4_575 . . .
Pb6 Pb5 K2 O23 -1.7(3) . . . 4_575
Pb1 Pb5 K2 O23 -125.3(3) . . . 4_575
Pb3 Pb5 K2 O23 -104.5(3) 4_575 . . 4_575
Pb3 Pb5 K2 O23 -104.5(3) . . . 4_575
Pb4 Pb5 K2 O23 -41.4(3) . . . 4_575
Pb5 Pb5 K2 O23 -42.2(2) 4_575 . . 4_575
Pb6 Pb5 K2 Pb3 102.87(3) . . . .
Pb1 Pb5 K2 Pb3 -20.75(3) . . . .
Pb3 Pb5 K2 Pb3 0.0 4_575 . . .
Pb4 Pb5 K2 Pb3 63.17(11) . . . .
Pb5 Pb5 K2 Pb3 62.34(2) 4_575 . . .
Pb6 Pb5 K2 Pb3 102.87(3) . . . 4_575
Pb1 Pb5 K2 Pb3 -20.75(3) . . . 4_575
Pb3 Pb5 K2 Pb3 0.0 . . . 4_575
Pb4 Pb5 K2 Pb3 63.17(11) . . . 4_575
Pb5 Pb5 K2 Pb3 62.34(2) 4_575 . . 4_575
Pb6 Pb5 K2 Pb5 40.52(4) . . . 4_575
Pb1 Pb5 K2 Pb5 -83.10(4) . . . 4_575
Pb3 Pb5 K2 Pb5 -62.34(2) 4_575 . . 4_575
Pb3 Pb5 K2 Pb5 -62.34(2) . . . 4_575
Pb4 Pb5 K2 Pb5 0.82(13) . . . 4_575
O24 K2 O21 C21 -121.2(10) . . . .
O22 K2 O21 C21 -35.7(9) . . . .
O22 K2 O21 C21 153.2(11) 4_575 . . .
O23 K2 O21 C21 -64.7(10) . . . .
O23 K2 O21 C21 -177.8(9) 4_575 . . .
Pb3 K2 O21 C21 58.8(10) . . . .
Pb3 K2 O21 C21 58.8(10) 4_575 . . .
Pb5 K2 O21 C21 26.7(10) . . . .
Pb5 K2 O21 C21 90.9(9) 4_575 . . .
O24 K2 O21 C21 121.2(10) . . . 4_575
O22 K2 O21 C21 -153.2(11) . . . 4_575
O22 K2 O21 C21 35.7(9) 4_575 . . 4_575
O23 K2 O21 C21 177.8(9) . . . 4_575
O23 K2 O21 C21 64.7(10) 4_575 . . 4_575
Pb3 K2 O21 C21 -58.8(10) . . . 4_575
Pb3 K2 O21 C21 -58.8(10) 4_575 . . 4_575
Pb5 K2 O21 C21 -90.9(9) . . . 4_575
Pb5 K2 O21 C21 -26.7(10) 4_575 . . 4_575
O24 K2 O22 C22 141.1(9) . . . .
O22 K2 O22 C22 11.1(11) 4_575 . . .
O21 K2 O22 C22 2.9(9) . . . .
O23 K2 O22 C22 149.4(10) . . . .
O23 K2 O22 C22 77.9(11) 4_575 . . .
Pb3 K2 O22 C22 -84.2(9) . . . .
Pb3 K2 O22 C22 -84.2(9) 4_575 . . .
Pb5 K2 O22 C22 -130.3(9) . . . .
Pb5 K2 O22 C22 -105.1(9) 4_575 . . .
O24 K2 O22 C23 -9.8(9) . . . 3_666
O22 K2 O22 C23 -139.8(8) 4_575 . . 3_666
O21 K2 O22 C23 -148.0(9) . . . 3_666
O23 K2 O22 C23 -1.5(8) . . . 3_666
O23 K2 O22 C23 -73.0(10) 4_575 . . 3_666
Pb3 K2 O22 C23 125.0(8) . . . 3_666
Pb3 K2 O22 C23 125.0(8) 4_575 . . 3_666
Pb5 K2 O22 C23 78.8(8) . . . 3_666
Pb5 K2 O22 C23 104.0(8) 4_575 . . 3_666
O24 K2 O23 C24 -153.9(10) . . . .
O22 K2 O23 C24 35.4(9) . . . .
O22 K2 O23 C24 122.9(10) 4_575 . . .
O21 K2 O23 C24 64.5(9) . . . .
O23 K2 O23 C24 178.6(8) 4_575 . . .
Pb3 K2 O23 C24 -35.9(10) . . . .
Pb3 K2 O23 C24 -35.9(10) 4_575 . . .
Pb5 K2 O23 C24 -59.2(9) . . . .
Pb5 K2 O23 C24 -91.5(9) 4_575 . . .
O24 K2 O23 C25 -37.6(9) . . . .
O22 K2 O23 C25 151.7(9) . . . .
O22 K2 O23 C25 -120.8(9) 4_575 . . .
O21 K2 O23 C25 -179.2(9) . . . .
O23 K2 O23 C25 -65.1(9) 4_575 . . .
Pb3 K2 O23 C25 80.4(9) . . . .
Pb3 K2 O23 C25 80.4(9) 4_575 . . .
Pb5 K2 O23 C25 57.1(9) . . . .
Pb5 K2 O23 C25 24.8(9) 4_575 . . .
O22 K2 O24 C26 -146.7(10) . . . 4_575
O22 K2 O24 C26 -15.9(12) 4_575 . . 4_575
O21 K2 O24 C26 -81.3(11) . . . 4_575
O23 K2 O24 C26 -155.1(12) . . . 4_575
O23 K2 O24 C26 -7.5(10) 4_575 . . 4_575
Pb3 K2 O24 C26 98.7(11) . . . 4_575
Pb3 K2 O24 C26 98.7(11) 4_575 . . 4_575
Pb5 K2 O24 C26 124.6(11) . . . 4_575
Pb5 K2 O24 C26 72.7(11) 4_575 . . 4_575
O22 K2 O24 C26 15.9(12) . . . .
O22 K2 O24 C26 146.7(10) 4_575 . . .
O21 K2 O24 C26 81.3(11) . . . .
O23 K2 O24 C26 7.5(10) . . . .
O23 K2 O24 C26 155.1(12) 4_575 . . .
Pb3 K2 O24 C26 -98.7(11) . . . .
Pb3 K2 O24 C26 -98.7(11) 4_575 . . .
Pb5 K2 O24 C26 -72.7(11) . . . .
Pb5 K2 O24 C26 -124.6(11) 4_575 . . .
C21 O21 C21 C22 -178.5(8) 4_575 . . .
K2 O21 C21 C22 68.1(13) . . . .
C23 O22 C22 C21 -178.9(12) 3_666 . . .
K2 O22 C22 C21 28.5(15) . . . .
O21 C21 C22 O22 -67.4(16) . . . .
C25 O23 C24 C23 179.3(11) . . . 3_666
K2 O23 C24 C23 -69.3(11) . . . 3_666
C24 O23 C25 C26 178.5(11) . . . .
K2 O23 C25 C26 67.7(12) . . . .
C26 O24 C26 C25 -173.7(9) 4_575 . . .
K2 O24 C26 C25 21.9(17) . . . .
O23 C25 C26 O24 -62.8(16) . . . .
Pb2 Pb2 K3 O31 0.00(2) 4_575 . . .
Pb4 Pb2 K3 O31 138.63(3) 4_575 . . .
Pb4 Pb2 K3 O31 -138.63(3) . . . .
Pb1 Pb2 K3 O31 129.78(2) 4_575 . . .
Pb1 Pb2 K3 O31 -129.78(2) . . . .
K1 Pb2 K3 O31 0.0 . . . .
Pb2 Pb2 K3 O33 0.00(3) 4_575 . . 4_575
Pb4 Pb2 K3 O33 36.3(2) 4_575 . . 4_575
Pb4 Pb2 K3 O33 119.0(2) . . . 4_575
Pb1 Pb2 K3 O33 27.4(2) 4_575 . . 4_575
Pb1 Pb2 K3 O33 127.8(2) . . . 4_575
K1 Pb2 K3 O33 -102.4(2) . . . 4_575
Pb2 Pb2 K3 O33 0.00(2) 4_575 . . .
Pb4 Pb2 K3 O33 -119.0(2) 4_575 . . .
Pb4 Pb2 K3 O33 -36.3(2) . . . .
Pb1 Pb2 K3 O33 -127.8(2) 4_575 . . .
Pb1 Pb2 K3 O33 -27.4(2) . . . .
K1 Pb2 K3 O33 102.4(2) . . . .
Pb2 Pb2 K3 O34 0(81) 4_575 . . .
Pb4 Pb2 K3 O34 -41.37(3) 4_575 . . .
Pb4 Pb2 K3 O34 41.37(3) . . . .
Pb1 Pb2 K3 O34 -50.22(2) 4_575 . . .
Pb1 Pb2 K3 O34 50.22(2) . . . .
K1 Pb2 K3 O34 180.000(2) . . . .
Pb2 Pb2 K3 O32 0.00(2) 4_575 . . 1_455
Pb4 Pb2 K3 O32 -168.43(18) 4_575 . . 1_455
Pb4 Pb2 K3 O32 -85.70(19) . . . 1_455
Pb1 Pb2 K3 O32 -177.28(19) 4_575 . . 1_455
Pb1 Pb2 K3 O32 -76.85(18) . . . 1_455
K1 Pb2 K3 O32 52.93(18) . . . 1_455
Pb2 Pb2 K3 O32 0.00(3) 4_575 . . 4_475
Pb4 Pb2 K3 O32 85.70(19) 4_575 . . 4_475
Pb4 Pb2 K3 O32 168.43(18) . . . 4_475
Pb1 Pb2 K3 O32 76.85(18) 4_575 . . 4_475
Pb1 Pb2 K3 O32 177.28(19) . . . 4_475
K1 Pb2 K3 O32 -52.93(18) . . . 4_475
Pb4 Pb2 K3 Pb2 0(24) 4_575 . . 4_575
Pb4 Pb2 K3 Pb2 0(65) . . . 4_575
Pb1 Pb2 K3 Pb2 0(33) 4_575 . . 4_575
Pb1 Pb2 K3 Pb2 0(74) . . . 4_575
K1 Pb2 K3 Pb2 0(100) . . . 4_575
Pb2 Pb2 K3 Pb1 0.00(2) 4_575 . . 4_575
Pb4 Pb2 K3 Pb1 8.85(4) 4_575 . . 4_575
Pb4 Pb2 K3 Pb1 91.58(3) . . . 4_575
Pb1 Pb2 K3 Pb1 100.43(4) . . . 4_575
K1 Pb2 K3 Pb1 -129.78(2) . . . 4_575
Pb2 Pb2 K3 Pb1 0.00(3) 4_575 . . .
Pb4 Pb2 K3 Pb1 -91.58(3) 4_575 . . .
Pb4 Pb2 K3 Pb1 -8.85(4) . . . .
Pb1 Pb2 K3 Pb1 -100.43(4) 4_575 . . .
K1 Pb2 K3 Pb1 129.78(2) . . . .
Pb2 Pb2 K3 Pb3 0(81) 4_575 . . 4_575
Pb4 Pb2 K3 Pb3 -41.37(3) 4_575 . . 4_575
Pb4 Pb2 K3 Pb3 41.37(3) . . . 4_575
Pb1 Pb2 K3 Pb3 -50.22(2) 4_575 . . 4_575
Pb1 Pb2 K3 Pb3 50.22(2) . . . 4_575
K1 Pb2 K3 Pb3 180.0 . . . 4_575
Pb2 Pb2 K3 Pb3 0(81) 4_575 . . .
Pb4 Pb2 K3 Pb3 -41.37(3) 4_575 . . .
Pb4 Pb2 K3 Pb3 41.37(3) . . . .
Pb1 Pb2 K3 Pb3 -50.22(2) 4_575 . . .
Pb1 Pb2 K3 Pb3 50.22(2) . . . .
K1 Pb2 K3 Pb3 180.0 . . . .
Pb5 Pb1 K3 O31 145.07(17) . . . .
Pb4 Pb1 K3 O31 60.88(18) . . . .
Pb3 Pb1 K3 O31 153.25(18) 4_575 . . .
Pb3 Pb1 K3 O31 153.25(18) . . . .
Pb2 Pb1 K3 O31 52.15(18) . . . .
Pb2 Pb1 K3 O31 52.15(18) 4_575 . . .
Pb5 Pb1 K3 O33 -0.1(3) . . . 4_575
Pb4 Pb1 K3 O33 -84.3(3) . . . 4_575
Pb3 Pb1 K3 O33 8.0(3) 4_575 . . 4_575
Pb3 Pb1 K3 O33 8.0(3) . . . 4_575
Pb2 Pb1 K3 O33 -93.1(3) . . . 4_575
Pb2 Pb1 K3 O33 -93.1(3) 4_575 . . 4_575
Pb5 Pb1 K3 O33 -110.54(18) . . . .
Pb4 Pb1 K3 O33 165.26(18) . . . .
Pb3 Pb1 K3 O33 -102.36(19) 4_575 . . .
Pb3 Pb1 K3 O33 -102.36(19) . . . .
Pb2 Pb1 K3 O33 156.53(19) . . . .
Pb2 Pb1 K3 O33 156.53(19) 4_575 . . .
Pb5 Pb1 K3 O34 -64.75(16) . . . .
Pb4 Pb1 K3 O34 -148.94(15) . . . .
Pb3 Pb1 K3 O34 -56.57(16) 4_575 . . .
Pb3 Pb1 K3 O34 -56.57(16) . . . .
Pb2 Pb1 K3 O34 -157.67(16) . . . .
Pb2 Pb1 K3 O34 -157.67(16) 4_575 . . .
Pb5 Pb1 K3 O32 -164.80(18) . . . 1_455
Pb4 Pb1 K3 O32 111.00(19) . . . 1_455
Pb3 Pb1 K3 O32 -156.62(19) 4_575 . . 1_455
Pb3 Pb1 K3 O32 -156.62(19) . . . 1_455
Pb2 Pb1 K3 O32 102.27(19) . . . 1_455
Pb2 Pb1 K3 O32 102.27(19) 4_575 . . 1_455
Pb5 Pb1 K3 O32 88.6(3) . . . 4_475
Pb4 Pb1 K3 O32 4.4(3) . . . 4_475
Pb3 Pb1 K3 O32 96.7(3) 4_575 . . 4_475
Pb3 Pb1 K3 O32 96.7(3) . . . 4_475
Pb2 Pb1 K3 O32 -4.4(3) . . . 4_475
Pb2 Pb1 K3 O32 -4.4(3) 4_575 . . 4_475
Pb5 Pb1 K3 Pb2 92.92(5) . . . .
Pb4 Pb1 K3 Pb2 8.73(5) . . . .
Pb3 Pb1 K3 Pb2 101.10(3) 4_575 . . .
Pb3 Pb1 K3 Pb2 101.10(3) . . . .
Pb2 Pb1 K3 Pb2 0.0 4_575 . . .
Pb5 Pb1 K3 Pb2 92.92(5) . . . 4_575
Pb4 Pb1 K3 Pb2 8.73(5) . . . 4_575
Pb3 Pb1 K3 Pb2 101.10(3) 4_575 . . 4_575
Pb3 Pb1 K3 Pb2 101.10(3) . . . 4_575
Pb2 Pb1 K3 Pb2 0.0 . . . 4_575
Pb5 Pb1 K3 Pb1 42.08(6) . . . 4_575
Pb4 Pb1 K3 Pb1 -42.11(6) . . . 4_575
Pb3 Pb1 K3 Pb1 50.26(3) 4_575 . . 4_575
Pb3 Pb1 K3 Pb1 50.26(3) . . . 4_575
Pb2 Pb1 K3 Pb1 -50.84(3) . . . 4_575
Pb2 Pb1 K3 Pb1 -50.84(3) 4_575 . . 4_575
Pb5 Pb1 K3 Pb3 -8.18(5) . . . 4_575
Pb4 Pb1 K3 Pb3 -92.37(5) . . . 4_575
Pb3 Pb1 K3 Pb3 0.0 . . . 4_575
Pb2 Pb1 K3 Pb3 -101.10(3) . . . 4_575
Pb2 Pb1 K3 Pb3 -101.10(3) 4_575 . . 4_575
Pb5 Pb1 K3 Pb3 -8.18(5) . . . .
Pb4 Pb1 K3 Pb3 -92.37(5) . . . .
Pb3 Pb1 K3 Pb3 0.0 4_575 . . .
Pb2 Pb1 K3 Pb3 -101.10(3) . . . .
Pb2 Pb1 K3 Pb3 -101.10(3) 4_575 . . .
Pb3 Pb3 K3 O31 0.00(12) 4_575 . . .
Pb5 Pb3 K3 O31 42.72(3) 4_575 . . .
Pb5 Pb3 K3 O31 -42.72(3) . . . .
Pb1 Pb3 K3 O31 -50.61(2) . . . .
Pb1 Pb3 K3 O31 50.61(2) 4_575 . . .
K2 Pb3 K3 O31 180.0 . . . .
Pb3 Pb3 K3 O33 0.00(12) 4_575 . . 4_575
Pb5 Pb3 K3 O33 -81.3(2) 4_575 . . 4_575
Pb5 Pb3 K3 O33 -166.72(18) . . . 4_575
Pb1 Pb3 K3 O33 -174.61(19) . . . 4_575
Pb1 Pb3 K3 O33 -73.39(19) 4_575 . . 4_575
K2 Pb3 K3 O33 56.00(19) . . . 4_575
Pb3 Pb3 K3 O33 0.00(12) 4_575 . . .
Pb5 Pb3 K3 O33 166.72(18) 4_575 . . .
Pb5 Pb3 K3 O33 81.3(2) . . . .
Pb1 Pb3 K3 O33 73.39(19) . . . .
Pb1 Pb3 K3 O33 174.61(19) 4_575 . . .
K2 Pb3 K3 O33 -56.00(19) . . . .
Pb3 Pb3 K3 O34 0(70) 4_575 . . .
Pb5 Pb3 K3 O34 -137.28(3) 4_575 . . .
Pb5 Pb3 K3 O34 137.28(3) . . . .
Pb1 Pb3 K3 O34 129.39(2) . . . .
Pb1 Pb3 K3 O34 -129.39(2) 4_575 . . .
K2 Pb3 K3 O34 0.000(1) . . . .
Pb3 Pb3 K3 O32 0.00(12) 4_575 . . 1_455
Pb5 Pb3 K3 O32 122.5(2) 4_575 . . 1_455
Pb5 Pb3 K3 O32 37.1(3) . . . 1_455
Pb1 Pb3 K3 O32 29.2(2) . . . 1_455
Pb1 Pb3 K3 O32 130.4(2) 4_575 . . 1_455
K2 Pb3 K3 O32 -100.2(2) . . . 1_455
Pb3 Pb3 K3 O32 0.00(12) 4_575 . . 4_475
Pb5 Pb3 K3 O32 -37.1(3) 4_575 . . 4_475
Pb5 Pb3 K3 O32 -122.5(2) . . . 4_475
Pb1 Pb3 K3 O32 -130.4(2) . . . 4_475
Pb1 Pb3 K3 O32 -29.2(2) 4_575 . . 4_475
K2 Pb3 K3 O32 100.2(2) . . . 4_475
Pb3 Pb3 K3 Pb2 0.00(12) 4_575 . . .
Pb5 Pb3 K3 Pb2 42.72(3) 4_575 . . .
Pb5 Pb3 K3 Pb2 -42.72(3) . . . .
Pb1 Pb3 K3 Pb2 -50.61(2) . . . .
Pb1 Pb3 K3 Pb2 50.61(2) 4_575 . . .
K2 Pb3 K3 Pb2 180.0 . . . .
Pb3 Pb3 K3 Pb2 0.00(12) 4_575 . . 4_575
Pb5 Pb3 K3 Pb2 42.72(3) 4_575 . . 4_575
Pb5 Pb3 K3 Pb2 -42.72(3) . . . 4_575
Pb1 Pb3 K3 Pb2 -50.61(2) . . . 4_575
Pb1 Pb3 K3 Pb2 50.61(2) 4_575 . . 4_575
K2 Pb3 K3 Pb2 180.0 . . . 4_575
Pb3 Pb3 K3 Pb1 0.00(12) 4_575 . . 4_575
Pb5 Pb3 K3 Pb1 -7.89(4) 4_575 . . 4_575
Pb5 Pb3 K3 Pb1 -93.33(3) . . . 4_575
Pb1 Pb3 K3 Pb1 -101.23(4) . . . 4_575
K2 Pb3 K3 Pb1 129.39(2) . . . 4_575
Pb3 Pb3 K3 Pb1 0.00(12) 4_575 . . .
Pb5 Pb3 K3 Pb1 93.33(3) 4_575 . . .
Pb5 Pb3 K3 Pb1 7.89(4) . . . .
Pb1 Pb3 K3 Pb1 101.23(4) 4_575 . . .
K2 Pb3 K3 Pb1 -129.39(2) . . . .
Pb5 Pb3 K3 Pb3 0(49) 4_575 . . 4_575
Pb5 Pb3 K3 Pb3 0(100) . . . 4_575
Pb1 Pb3 K3 Pb3 0(100) . . . 4_575
Pb1 Pb3 K3 Pb3 0(38) 4_575 . . 4_575
K2 Pb3 K3 Pb3 0(100) . . . 4_575
O33 K3 O31 C31 -146.4(12) 4_575 . . 1_455
O33 K3 O31 C31 -26.2(13) . . . 1_455
O34 K3 O31 C31 -86.3(12) . . . 1_455
O32 K3 O31 C31 -10.9(11) 1_455 . . 1_455
O32 K3 O31 C31 -161.7(14) 4_475 . . 1_455
Pb2 K3 O31 C31 93.7(12) . . . 1_455
Pb2 K3 O31 C31 93.7(12) 4_575 . . 1_455
Pb1 K3 O31 C31 130.2(12) 4_575 . . 1_455
Pb1 K3 O31 C31 57.2(13) . . . 1_455
Pb3 K3 O31 C31 93.7(12) 4_575 . . 1_455
Pb3 K3 O31 C31 93.7(12) . . . 1_455
O33 K3 O31 C31 26.2(13) 4_575 . . 4_475
O33 K3 O31 C31 146.4(12) . . . 4_475
O34 K3 O31 C31 86.3(12) . . . 4_475
O32 K3 O31 C31 161.7(14) 1_455 . . 4_475
O32 K3 O31 C31 10.9(11) 4_475 . . 4_475
Pb2 K3 O31 C31 -93.7(12) . . . 4_475
Pb2 K3 O31 C31 -93.7(12) 4_575 . . 4_475
Pb1 K3 O31 C31 -57.2(13) 4_575 . . 4_475
Pb1 K3 O31 C31 -130.2(12) . . . 4_475
Pb3 K3 O31 C31 -93.7(12) 4_575 . . 4_475
Pb3 K3 O31 C31 -93.7(12) . . . 4_475
O31 K3 O33 C35 -132.6(8) . . . .
O33 K3 O33 C35 -15.6(10) 4_575 . . .
O34 K3 O33 C35 -5.9(8) . . . .
O32 K3 O33 C35 -148.2(9) 1_455 . . .
O32 K3 O33 C35 -75.5(9) 4_475 . . .
Pb2 K3 O33 C35 141.8(8) . . . .
Pb2 K3 O33 C35 141.8(8) 4_575 . . .
Pb1 K3 O33 C35 82.0(9) 4_575 . . .
Pb1 K3 O33 C35 121.7(8) . . . .
Pb3 K3 O33 C35 76.1(8) 4_575 . . .
Pb3 K3 O33 C35 76.1(8) . . . .
O31 K3 O33 C34 32.7(10) . . . .
O33 K3 O33 C34 149.7(9) 4_575 . . .
O34 K3 O33 C34 159.4(11) . . . .
O32 K3 O33 C34 17.1(9) 1_455 . . .
O32 K3 O33 C34 89.8(10) 4_475 . . .
Pb2 K3 O33 C34 -52.9(10) . . . .
Pb2 K3 O33 C34 -52.9(10) 4_575 . . .
Pb1 K3 O33 C34 -112.7(9) 4_575 . . .
Pb1 K3 O33 C34 -73.0(10) . . . .
Pb3 K3 O33 C34 -118.6(10) 4_575 . . .
Pb3 K3 O33 C34 -118.6(10) . . . .
O31 K3 O34 C36 -121.5(7) . . . 4_575
O33 K3 O34 C36 -36.9(7) 4_575 . . 4_575
O33 K3 O34 C36 154.0(9) . . . 4_575
O32 K3 O34 C36 -175.8(7) 1_455 . . 4_575
O32 K3 O34 C36 -67.1(8) 4_475 . . 4_575
Pb2 K3 O34 C36 58.5(7) . . . 4_575
Pb2 K3 O34 C36 58.5(7) 4_575 . . 4_575
Pb1 K3 O34 C36 20.7(8) 4_575 . . 4_575
Pb1 K3 O34 C36 96.4(7) . . . 4_575
Pb3 K3 O34 C36 58.5(7) 4_575 . . 4_575
Pb3 K3 O34 C36 58.5(7) . . . 4_575
O31 K3 O34 C36 121.5(8) . . . .
O33 K3 O34 C36 -154.0(9) 4_575 . . .
O33 K3 O34 C36 36.9(7) . . . .
O32 K3 O34 C36 67.1(8) 1_455 . . .
O32 K3 O34 C36 175.8(7) 4_475 . . .
Pb2 K3 O34 C36 -58.5(8) . . . .
Pb2 K3 O34 C36 -58.5(8) 4_575 . . .
Pb1 K3 O34 C36 -96.4(7) 4_575 . . .
Pb1 K3 O34 C36 -20.7(8) . . . .
Pb3 K3 O34 C36 -58.5(8) 4_575 . . .
Pb3 K3 O34 C36 -58.5(8) . . . .
C33 O32 C32 C31 -177.4(11) . . . .
K3 O32 C32 C31 -71.1(12) 1_655 . . .
O31 C31 C32 O32 66.4(17) 1_655 . . .
C32 O32 C33 C34 178.5(11) . . . 1_655
K3 O32 C33 C34 73.1(11) 1_655 . . 1_655
C35 O33 C34 C33 177.5(11) . . . 1_455
K3 O33 C34 C33 11.2(15) . . . 1_455
C34 O33 C35 C36 169.5(11) . . . .
K3 O33 C35 C36 -23.6(13) . . . .
C36 O34 C36 C35 178.6(8) 4_575 . . .
K3 O34 C36 C35 -68.3(11) . . . .
O33 C35 C36 O34 64.4(14) . . . .
O43 K4 O41 C41 137.1(12) . . . 4_565
O43 K4 O41 C41 2.1(13) 4_565 . . 4_565
N4 K4 O41 C41 -142.6(12) . . . 4_565
N4 K4 O41 C41 -78.2(13) 4_565 . . 4_565
O42 K4 O41 C41 -4.9(12) 4_565 . . 4_565
O42 K4 O41 C41 144.1(13) . . . 4_565
O44 K4 O41 C41 69.6(12) . . . 4_565
C43 K4 O41 C41 -11.2(13) 4_565 . . 4_565
C43 K4 O41 C41 150.5(14) . . . 4_565
O43 K4 O41 C41 -2.1(13) . . . .
O43 K4 O41 C41 -137.1(12) 4_565 . . .
N4 K4 O41 C41 78.2(13) . . . .
N4 K4 O41 C41 142.6(12) 4_565 . . .
O42 K4 O41 C41 -144.1(13) 4_565 . . .
O42 K4 O41 C41 4.9(12) . . . .
O44 K4 O41 C41 -69.6(12) . . . .
C43 K4 O41 C41 -150.5(14) 4_565 . . .
C43 K4 O41 C41 11.2(13) . . . .
O41 K4 O42 C431 142.7(15) . . . .
O43 K4 O42 C431 -44.7(14) . . . .
O43 K4 O42 C431 -126.3(15) 4_565 . . .
N4 K4 O42 C431 28.7(14) . . . .
N4 K4 O42 C431 61.3(16) 4_565 . . .
O42 K4 O42 C431 171.0(13) 4_565 . . .
O44 K4 O42 C431 -71.6(15) . . . .
C43 K4 O42 C431 177.7(16) 4_565 . . .
C43 K4 O42 C431 -21(2) . . . .
O41 K4 O42 C43 163.9(17) . . . .
O43 K4 O42 C43 -23.6(16) . . . .
O43 K4 O42 C43 -105.1(17) 4_565 . . .
N4 K4 O42 C43 49.9(16) . . . .
N4 K4 O42 C43 82.5(17) 4_565 . . .
O42 K4 O42 C43 -167.8(15) 4_565 . . .
O44 K4 O42 C43 -50.4(16) . . . .
C43 K4 O42 C43 -161(2) 4_565 . . .
O41 K4 O42 C42 26.6(11) . . . .
O43 K4 O42 C42 -160.8(12) . . . .
O43 K4 O42 C42 117.7(12) 4_565 . . .
N4 K4 O42 C42 -87.4(11) . . . .
N4 K4 O42 C42 -54.8(12) 4_565 . . .
O42 K4 O42 C42 55.0(12) 4_565 . . .
O44 K4 O42 C42 172.3(11) . . . .
C43 K4 O42 C42 61.6(14) 4_565 . . .
C43 K4 O42 C42 -137(2) . . . .
O41 K4 O43 C45 -135(3) . . . .
O43 K4 O43 C45 1(3) 4_565 . . .
N4 K4 O43 C45 122(3) . . . .
N4 K4 O43 C45 86(3) 4_565 . . .
O42 K4 O43 C45 -63(3) 4_565 . . .
O42 K4 O43 C45 -142(3) . . . .
O44 K4 O43 C45 6(3) . . . .
C43 K4 O43 C45 -21(3) 4_565 . . .
C43 K4 O43 C45 -158(3) . . . .
O41 K4 O43 C44 8(3) . . . .
O43 K4 O43 C44 145(3) 4_565 . . .
N4 K4 O43 C44 -95(3) . . . .
N4 K4 O43 C44 -130(3) 4_565 . . .
O42 K4 O43 C44 80(3) 4_565 . . .
O42 K4 O43 C44 1(3) . . . .
O44 K4 O43 C44 150(3) . . . .
C43 K4 O43 C44 122(3) 4_565 . . .
C43 K4 O43 C44 -14(3) . . . .
O41 K4 O43 C441 22.1(19) . . . .
O43 K4 O43 C441 158.7(17) 4_565 . . .
N4 K4 O43 C441 -80.5(18) . . . .
N4 K4 O43 C441 -116.2(18) 4_565 . . .
O42 K4 O43 C441 94.4(19) 4_565 . . .
O42 K4 O43 C441 15.0(18) . . . .
O44 K4 O43 C441 163.8(19) . . . .
C43 K4 O43 C441 136.5(19) 4_565 . . .
C43 K4 O43 C441 0(2) . . . .
O41 K4 O43 C451 -153.2(18) . . . .
O43 K4 O43 C451 -16.6(19) 4_565 . . .
N4 K4 O43 C451 104.2(18) . . . .
N4 K4 O43 C451 68.4(18) 4_565 . . .
O42 K4 O43 C451 -80.9(19) 4_565 . . .
O42 K4 O43 C451 -160.3(18) . . . .
O44 K4 O43 C451 -11.6(18) . . . .
C43 K4 O43 C451 -39(2) 4_565 . . .
C43 K4 O43 C451 -176(2) . . . .
O41 K4 O44 C461 -134.2(19) . . . 4_565
O43 K4 O44 C461 139(2) . . . 4_565
O43 K4 O44 C461 -47.0(18) 4_565 . . 4_565
N4 K4 O44 C461 76.8(19) . . . 4_565
N4 K4 O44 C461 15(2) 4_565 . . 4_565
O42 K4 O44 C461 -74(2) 4_565 . . 4_565
O42 K4 O44 C461 165.8(19) . . . 4_565
C43 K4 O44 C461 -57(2) 4_565 . . 4_565
C43 K4 O44 C461 148(2) . . . 4_565
O41 K4 O44 C461 134.2(19) . . . .
O43 K4 O44 C461 47.0(19) . . . .
O43 K4 O44 C461 -139(2) 4_565 . . .
N4 K4 O44 C461 -15(2) . . . .
N4 K4 O44 C461 -76.8(19) 4_565 . . .
O42 K4 O44 C461 -165.8(19) 4_565 . . .
O42 K4 O44 C461 74(2) . . . .
C43 K4 O44 C461 -148(2) 4_565 . . .
C43 K4 O44 C461 57(2) . . . .
O41 K4 O44 C46 -105(2) . . . 4_565
O43 K4 O44 C46 167(2) . . . 4_565
O43 K4 O44 C46 -18(2) 4_565 . . 4_565
N4 K4 O44 C46 106(2) . . . 4_565
N4 K4 O44 C46 44(2) 4_565 . . 4_565
O42 K4 O44 C46 -45(2) 4_565 . . 4_565
O42 K4 O44 C46 -165(2) . . . 4_565
C43 K4 O44 C46 -28(2) 4_565 . . 4_565
C43 K4 O44 C46 177(2) . . . 4_565
O41 K4 O44 C46 105(2) . . . .
O43 K4 O44 C46 18(2) . . . .
O43 K4 O44 C46 -167(2) 4_565 . . .
N4 K4 O44 C46 -44(2) . . . .
N4 K4 O44 C46 -106(2) 4_565 . . .
O42 K4 O44 C46 165(2) 4_565 . . .
O42 K4 O44 C46 45(2) . . . .
C43 K4 O44 C46 -177(2) 4_565 . . .
C43 K4 O44 C46 28(2) . . . .
C41 O41 C41 C42 -178.4(10) 4_565 . . .
K4 O41 C41 C42 -36(2) . . . .
C431 O42 C42 C41 -175(2) . . . .
C43 O42 C42 C41 177(3) . . . .
K4 O42 C42 C41 -60.4(18) . . . .
O41 C41 C42 O42 66(2) . . . .
C431 O42 C43 C44 166(11) . . . .
C42 O42 C43 C44 -173(3) . . . .
K4 O42 C43 C44 62(4) . . . .
C431 O42 C43 K4 103(8) . . . .
C42 O42 C43 K4 124(2) . . . .
O41 K4 C43 O42 -13.9(14) . . . .
O43 K4 C43 O42 146(2) . . . .
O43 K4 C43 O42 110.2(13) 4_565 . . .
N4 K4 C43 O42 -126.4(16) . . . .
N4 K4 C43 O42 -120.6(14) 4_565 . . .
O42 K4 C43 O42 16(2) 4_565 . . .
O44 K4 C43 O42 132.6(15) . . . .
C43 K4 C43 O42 33(4) 4_565 . . .
O41 K4 C43 C44 -149(2) . . . .
O43 K4 C43 C44 10(2) . . . .
O43 K4 C43 C44 -25(3) 4_565 . . .
N4 K4 C43 C44 98(2) . . . .
N4 K4 C43 C44 104(2) 4_565 . . .
O42 K4 C43 C44 -120(2) 4_565 . . .
O42 K4 C43 C44 -135(3) . . . .
O44 K4 C43 C44 -3(2) . . . .
C43 K4 C43 C44 -102(3) 4_565 . . .
C43 O42 C431 C441 -15(7) . . . .
C42 O42 C431 C441 -177.4(19) . . . .
K4 O42 C431 C441 67(2) . . . .
C45 O43 C44 C43 175(3) . . . .
C441 O43 C44 C43 -18(7) . . . .
C451 O43 C44 C43 -178(2) . . . .
K4 O43 C44 C43 21(4) . . . .
C441 O43 C44 C45 167(9) . . . .
C451 O43 C44 C45 8(3) . . . .
K4 O43 C44 C45 -154(3) . . . .
O42 C43 C44 O43 -59(5) . . . .
K4 C43 C44 O43 -13(3) . . . .
O42 C43 C44 C45 -53(7) . . . .
K4 C43 C44 C45 -8(5) . . . .
C45 O43 C441 C431 177(3) . . . .
C44 O43 C441 C431 163(12) . . . .
C451 O43 C441 C431 -171(3) . . . .
K4 O43 C441 C431 15(4) . . . .
O42 C431 C441 O43 -58(4) . . . .
C44 O43 C45 C46 180(3) . . . .
C441 O43 C45 C46 175(3) . . . .
C451 O43 C45 C46 17(6) . . . .
K4 O43 C45 C46 -27(4) . . . .
C441 O43 C45 C44 -5(4) . . . .
C451 O43 C45 C44 -163(8) . . . .
K4 O43 C45 C44 153(3) . . . .
C43 C44 C45 O43 -8(5) . . . .
O43 C44 C45 C46 -1(6) . . . .
C43 C44 C45 C46 -8(11) . . . .
C45 O43 C451 C461 -166(10) . . . .
C44 O43 C451 C461 175(4) . . . .
C441 O43 C451 C461 165(3) . . . .
K4 O43 C451 C461 -21(4) . . . .
C461 O44 C46 C45 -170(5) 4_565 . . .
C461 O44 C46 C45 -157(11) . . . .
C46 O44 C46 C45 178(3) 4_565 . . .
K4 O44 C46 C45 -49(5) . . . .
O43 C45 C46 O44 53(5) . . . .
C44 C45 C46 O44 53(9) . . . .
C461 O44 C461 C451 -179.2(18) 4_565 . . .
C46 O44 C461 C451 175(3) 4_565 . . .
C46 O44 C461 C451 12(6) . . . .
K4 O44 C461 C451 -68(3) . . . .
C46 O44 C461 C461 -6(3) 4_565 . . 4_565
C46 O44 C461 C461 -168(6) . . . 4_565
K4 O44 C461 C461 111(3) . . . 4_565
O43 C451 C461 O44 60(4) . . . .
O43 C451 C461 C461 59(6) . . . 4_565
O41 K4 N4 C47 109.8(11) . . . .
O43 K4 N4 C47 -137.6(12) . . . .
O43 K4 N4 C47 -31.2(13) 4_565 . . .
N4 K4 N4 C47 8.8(12) 4_565 . . .
O42 K4 N4 C47 46.8(13) 4_565 . . .
O42 K4 N4 C47 165.2(12) . . . .
O44 K4 N4 C47 -87.8(11) . . . .
C43 K4 N4 C47 15.1(14) 4_565 . . .
C43 K4 N4 C47 -176.2(13) . . . .
K4 N4 C47 C47 -9.7(14) . . . 4_565
C54 C51 C52 C53 0.00(2) 1_655 . . 3_666
C54 C55 C56 C53 0.000(8) 3_666 . . 1_655
C54 C55 C56 C57 180.000(6) 3_666 . . .
Pb5 Pb5 Pb2 Pb2 0.000(13) . 4_575 . 4_575
Pb5 Pb2 Pb2 Pb3 0.000(7) 4_575 . 4_575 .
Pb2 Pb2 Pb3 Pb3 0.0 . 4_575 . 4_575
Pb1 Pb4 Pb2 Pb3 43.137(14) . . . 4_575
