#------------------------------------------------------------------------------
#$Date: 2016-03-25 16:43:26 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179986 $
#$URL: svn://www.crystallography.net/cod/cif/7/02/80/7028023.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided the Crystal Eye server at
# http://wwmm.ch.cam.ac.uk/crystaleye/, created by Nick Day at the
# Peter Murray-Rust laboratory.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_7028023
loop_
_publ_author_name
'Kessler, Vadim G.'
'Panov, Andrei N.'
'Turova, Nataliya Ya.'
'Starikova, Zoya A.'
'Yanovsky, Alexandr I.'
'Dolgushin, Fedor M.'
'Pisarevsky, Alexandr P.'
'Struchkov, Yuri T.'
_publ_section_title
;
 Anodic oxidation of molybdenum and tungsten in alcohols: isolation and
 X-ray single-crystal study of side products
;
_journal_issue                   1
_journal_name_full
'Journal of the Chemical Society, Dalton Transactions'
_journal_page_first              21
_journal_paper_doi               10.1039/a704198e
_journal_year                    1998
_chemical_formula_moiety         'C30 H74 Li4 O24 W2 ++, O19 W6 --'
_chemical_formula_sum            'C30 H74 Li4 O43 W8'
_chemical_formula_weight         2621.5
_chemical_name_systematic
;
Tetralithium-hexakis(2-methoxyethoxy)-tetrakis(2-
-methoxyethanol)-tetraoxo-di-tungsten  hexawolframate
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL
_cell_angle_alpha                89.90(3)
_cell_angle_beta                 110.73(3)
_cell_angle_gamma                103.01(3)
_cell_formula_units_Z            1
_cell_length_a                   11.461(5)
_cell_length_b                   11.828(4)
_cell_length_c                   12.623(5)
_cell_measurement_reflns_used    24
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      12
_cell_measurement_theta_min      11
_cell_volume                     1553.6(11)
_computing_cell_refinement       'CAD4 Enraf-Nonius'
_computing_data_collection       'CAD4 Enraf-Nonius'
_computing_data_reduction        'SHELXTL PLUS 5 (gamma version)'
_computing_molecular_graphics    'SHELXTL PLUS 5 (gamma version)'
_computing_publication_material  'SHELXTL PLUS 5 (gamma version)'
_computing_structure_refinement  'SHELXTL PLUS 5 (gamma version)'
_computing_structure_solution    'SHELXTL PLUS 5 (gamma version)'
_diffrn_ambient_temperature      293(2)
_diffrn_measurement_device       'CAD4 Enraf-Nonius'
_diffrn_measurement_method       'CAD4 Enraf-Nonius'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0194
_diffrn_reflns_av_sigmaI/netI    0.0515
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_k_min       -16
_diffrn_reflns_limit_l_max       16
_diffrn_reflns_limit_l_min       -17
_diffrn_reflns_number            8628
_diffrn_reflns_theta_max         28.98
_diffrn_reflns_theta_min         1.73
_diffrn_standards_decay_%        2.0
_diffrn_standards_interval_count 97
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    14.843
_exptl_absorpt_correction_T_max  0.983
_exptl_absorpt_correction_T_min  0.246
_exptl_absorpt_correction_type   empirical
_exptl_crystal_colour            colourless
_exptl_crystal_F_000             1202
_refine_diff_density_max         7.705
_refine_diff_density_min         -5.568
_refine_diff_density_rms         0.448
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_all   0.976
_refine_ls_goodness_of_fit_obs   1.070
_refine_ls_hydrogen_treatment    noref
_refine_ls_matrix_type           full
_refine_ls_number_parameters     388
_refine_ls_number_reflns         8192
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.007
_refine_ls_restrained_S_obs      1.070
_refine_ls_R_factor_all          0.0893
_refine_ls_R_factor_obs          0.0591
_refine_ls_shift/esd_max         -0.011
_refine_ls_shift/esd_mean        0.002
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.1360P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_all         0.1761
_refine_ls_wR_factor_obs         0.1594
_reflns_number_observed          5988
_reflns_number_total             8230
_reflns_observed_criterion       >2sigma(I)
_cod_data_source_file            e704198sup1.cif
_cod_data_source_block           str_VII
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 1891 2012-01-12 08:04:46Z andrius 

The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value 'calc
w=1/[\s^2^(Fo^2^)+(0.1360P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3' was
changed to 'calc'. New tag '_refine_ls_weighting_details' was
created. The value of the new tag was set to
'w=1/[\s^2^(Fo^2^)+(0.1360P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7028023
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_thermal_displace_type
_atom_site_occupancy
_atom_site_calc_flag
_atom_site_refinement_flags
W1 W -0.35408(4) 0.47312(3) -0.00278(3) 0.02557(13) Uani 1 d .
W2 W 0.00859(5) 0.19201(4) -0.54309(4) 0.03486(15) Uani 1 d .
W3 W -0.11775(5) -0.06318(4) -0.69044(4) 0.0373(2) Uani 1 d .
W4 W -0.18946(5) -0.00992(4) -0.46905(5) 0.0409(2) Uani 1 d .
Li1 Li -0.1887(21) 0.3192(21) -0.1263(16) 0.042(5) Uani 1 d .
Li2 Li -0.4897(21) 0.3521(16) 0.1927(17) 0.038(4) Uani 1 d .
O1 O -0.2021(8) 0.5275(8) 0.0968(7) 0.039(2) Uani 1 d .
O2 O -0.3282(8) 0.3923(7) -0.1018(8) 0.039(2) Uani 1 d .
O3 O -0.4450(6) 0.5473(6) 0.0961(6) 0.0262(14) Uani 1 d .
O4 O -0.3605(8) 0.4585(8) 0.3132(7) 0.041(2) Uani 1 d .
O5 O -0.4046(8) 0.3348(6) 0.0729(7) 0.033(2) Uani 1 d .
O6 O -0.4895(9) 0.1787(8) 0.1991(9) 0.048(2) Uani 1 d .
O7 O -0.6472(8) 0.3820(7) 0.0770(7) 0.036(2) Uani 1 d .
O8 O -0.6221(9) 0.3281(10) 0.2855(9) 0.057(3) Uani 1 d .
O9 O -0.2888(10) 0.2628(11) -0.2895(9) 0.063(3) Uani 1 d .
O10 O -0.0606(9) 0.3995(11) -0.1952(8) 0.056(3) Uani 1 d .
H10 H -0.0051(9) 0.3363(11) -0.1820(8) 0.079(59) Uiso 1 d R
O11 O -0.1871(10) 0.1609(9) -0.0632(8) 0.053(2) Uani 1 d .
O12 O -0.0560(10) 0.3684(8) 0.0405(8) 0.047(2) Uani 1 d .
H12 H -0.0271(10) 0.4484(8) 0.0971(8) 0.032(32) Uiso 1 d R
O13 O -0.3295(11) -0.0163(11) -0.4482(12) 0.071(3) Uani 1 d .
O14 O -0.0587(10) 0.0434(9) -0.3236(8) 0.049(2) Uani 1 d .
O15 O -0.1450(9) 0.1471(7) -0.5094(8) 0.041(2) Uani 1 d .
O16 O -0.2468(8) -0.0593(7) -0.6265(8) 0.042(2) Uani 1 d .
O17 O -0.1599(9) -0.1608(7) -0.4416(8) 0.044(2) Uani 1 d .
O18 O 0.0157(11) 0.3320(8) -0.5750(9) 0.057(3) Uani 1 d .
O19 O -0.2024(12) -0.1083(9) -0.8308(8) 0.064(3) Uani 1 d .
O20 O 0.1013(9) 0.2057(7) -0.3811(7) 0.041(2) Uani 1 d .
O21 O -0.0882(9) 0.1034(7) -0.6887(7) 0.042(2) Uani 1 d .
O22 O 0.0000 0.0000 -0.5000 0.027(2) Uani 1 d S
C1 C -0.3694(10) 0.6270(9) 0.1973(8) 0.029(2) Uani 1 d .
H1B H -0.3961(10) 0.6997(9) 0.1889(8) 0.034 Uiso 1 calc R
H1C H -0.2791(10) 0.6437(9) 0.2073(8) 0.034 Uiso 1 calc R
C2 C -0.3891(12) 0.5707(9) 0.3026(8) 0.033(2) Uani 1 d .
H2A H -0.3339(12) 0.6213(9) 0.3705(8) 0.040 Uiso 1 calc R
H2B H -0.4775(12) 0.5629(9) 0.2961(8) 0.040 Uiso 1 calc R
C3 C -0.2263(14) 0.4615(15) 0.3548(13) 0.058(4) Uani 1 d .
H3A H -0.2151(14) 0.3834(15) 0.3596(13) 0.086 Uiso 1 calc R
H3B H -0.1856(14) 0.5029(15) 0.4289(13) 0.086 Uiso 1 calc R
H3C H -0.1882(14) 0.5003(15) 0.3039(13) 0.086 Uiso 1 calc R
C4 C -0.4545(16) 0.2194(10) 0.0276(13) 0.050(3) Uani 1 d .
H4A H -0.4128(16) 0.2015(10) -0.0229(13) 0.060 Uiso 1 calc R
H4B H -0.5461(16) 0.2056(10) -0.0153(13) 0.060 Uiso 1 calc R
C5 C -0.4300(16) 0.1452(11) 0.1254(14) 0.054(4) Uani 1 d .
H5A H -0.4661(16) 0.0636(11) 0.0982(14) 0.065 Uiso 1 calc R
H5B H -0.3384(16) 0.1566(11) 0.1661(14) 0.065 Uiso 1 calc R
C6 C -0.4618(17) 0.1233(15) 0.3033(14) 0.065(4) Uani 1 d .
H6A H -0.5044(17) 0.1495(15) 0.3484(14) 0.097 Uiso 1 calc R
H6B H -0.3707(17) 0.1429(15) 0.3447(14) 0.097 Uiso 1 calc R
H6C H -0.4918(17) 0.0404(15) 0.2867(14) 0.097 Uiso 1 calc R
C7 C -0.7529(11) 0.3045(12) 0.0916(12) 0.045(3) Uani 1 d .
H7A H -0.7485(11) 0.2246(12) 0.0811(12) 0.054 Uiso 1 calc R
H7B H -0.8329(11) 0.3151(12) 0.0364(12) 0.054 Uiso 1 calc R
C8 C -0.7468(13) 0.3308(15) 0.2102(12) 0.055(4) Uani 1 d .
H8A H -0.7628(13) 0.4069(15) 0.2177(12) 0.066 Uiso 1 calc R
H8B H -0.8112(13) 0.2731(15) 0.2272(12) 0.066 Uiso 1 calc R
C9 C -0.6031(20) 0.3602(18) 0.3961(13) 0.081(6) Uani 1 d .
H9A H -0.5178(20) 0.3574(18) 0.4444(13) 0.121 Uiso 1 calc R
H9B H -0.6646(20) 0.3077(18) 0.4196(13) 0.121 Uiso 1 calc R
H9C H -0.6136(20) 0.4380(18) 0.4015(13) 0.121 Uiso 1 calc R
C10 C -0.1023(15) 0.3586(24) -0.3104(16) 0.097(8) Uani 1 d .
H10A H -0.0720(15) 0.4209(24) -0.3513(16) 0.116 Uiso 1 calc R
H10B H -0.0630(15) 0.2954(24) -0.3158(16) 0.116 Uiso 1 calc R
C11 C -0.2363(14) 0.3192(17) -0.3639(12) 0.062(4) Uani 1 d .
H11A H -0.2736(14) 0.3848(17) -0.3896(12) 0.075 Uiso 1 calc R
H11B H -0.2560(14) 0.2662(17) -0.4299(12) 0.075 Uiso 1 calc R
C12 C -0.4238(16) 0.2150(14) -0.3340(14) 0.061(4) Uani 1 d .
H12A H -0.4502(16) 0.1780(14) -0.2757(14) 0.091 Uiso 1 calc R
H12B H -0.4451(16) 0.1586(14) -0.3966(14) 0.091 Uiso 1 calc R
H12C H -0.4672(16) 0.2761(14) -0.3596(14) 0.091 Uiso 1 calc R
C13 C -0.0949(13) 0.2798(13) 0.1092(10) 0.046(3) Uani 1 d .
H13A H -0.1766(13) 0.2843(13) 0.1136(10) 0.055 Uiso 1 calc R
H13B H -0.0312(13) 0.2906(13) 0.1857(10) 0.055 Uiso 1 calc R
C14 C -0.1067(15) 0.1645(13) 0.0526(12) 0.053(3) Uani 1 d .
H14B H -0.0227(15) 0.1557(13) 0.0581(12) 0.064 Uiso 1 calc R
H14C H -0.1440(15) 0.1017(13) 0.0891(12) 0.064 Uiso 1 calc R
C15 C -0.2014(23) 0.0557(15) -0.1289(16) 0.078(6) Uani 1 d .
H15A H -0.2565(23) 0.0580(15) -0.2061(16) 0.116 Uiso 1 calc R
H15B H -0.2385(23) -0.0104(15) -0.0972(16) 0.116 Uiso 1 calc R
H15C H -0.1187(23) 0.0494(15) -0.1270(16) 0.116 Uiso 1 calc R
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
W W -0.8490 6.8722 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Li Li -0.0003 0.0001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O2 W1 O1 103.7(4) . .
O2 W1 O7 98.1(4) . 2_465
O1 W1 O7 92.5(4) . 2_465
O2 W1 O5 92.9(4) . .
O1 W1 O5 97.9(4) . .
O7 W1 O5 162.6(3) 2_465 .
O2 W1 O3 95.5(3) . 2_465
O1 W1 O3 160.1(3) . 2_465
O7 W1 O3 79.2(3) 2_465 2_465
O5 W1 O3 86.4(3) . 2_465
O2 W1 O3 163.1(3) . .
O1 W1 O3 92.7(3) . .
O7 W1 O3 85.0(3) 2_465 .
O5 W1 O3 80.7(3) . .
O3 W1 O3 68.7(3) 2_465 .
O18 W2 O15 104.1(5) . .
O18 W2 O17 103.8(5) . 2_554
O15 W2 O17 152.1(4) . 2_554
O18 W2 O20 103.6(4) . .
O15 W2 O20 86.7(4) . .
O17 W2 O20 86.4(4) 2_554 .
O18 W2 O21 103.4(4) . .
O15 W2 O21 86.9(4) . .
O17 W2 O21 87.1(4) 2_554 .
O20 W2 O21 152.9(3) . .
O18 W2 O22 179.5(4) . .
O15 W2 O22 76.3(3) . .
O17 W2 O22 75.7(3) 2_554 .
O20 W2 O22 76.5(2) . .
O21 W2 O22 76.4(2) . .
O19 W3 O21 102.9(4) . .
O19 W3 O14 103.7(5) . 2_554
O21 W3 O14 86.9(4) . 2_554
O19 W3 O20 104.0(4) . 2_554
O21 W3 O20 153.1(3) . 2_554
O14 W3 O20 86.2(4) 2_554 2_554
O19 W3 O16 104.8(5) . .
O21 W3 O16 87.2(4) . .
O14 W3 O16 151.5(4) 2_554 .
O20 W3 O16 86.5(4) 2_554 .
O19 W3 O22 179.1(4) . .
O21 W3 O22 76.6(2) . .
O14 W3 O22 75.6(3) 2_554 .
O20 W3 O22 76.5(2) 2_554 .
O16 W3 O22 76.0(2) . .
O13 W4 O17 104.2(5) . .
O13 W4 O16 102.7(5) . .
O17 W4 O16 86.3(4) . .
O13 W4 O14 104.5(5) . .
O17 W4 O14 87.4(4) . .
O16 W4 O14 152.8(4) . .
O13 W4 O15 103.2(5) . .
O17 W4 O15 152.6(4) . .
O16 W4 O15 87.4(4) . .
O14 W4 O15 86.2(4) . .
O13 W4 O22 179.1(5) . .
O17 W4 O22 76.4(3) . .
O16 W4 O22 76.6(3) . .
O14 W4 O22 76.1(3) . .
O15 W4 O22 76.2(3) . .
O9 Li1 O10 80.7(9) . .
O9 Li1 O11 97.8(11) . .
O10 Li1 O11 122.9(11) . .
O9 Li1 O2 96.0(9) . .
O10 Li1 O2 124.5(12) . .
O11 Li1 O2 112.5(12) . .
O9 Li1 O12 169.5(12) . .
O10 Li1 O12 92.5(10) . .
O11 Li1 O12 79.2(8) . .
O2 Li1 O12 94.4(9) . .
O4 Li2 O7 127.7(11) . .
O4 Li2 O6 117.6(11) . .
O7 Li2 O6 113.5(10) . .
O4 Li2 O5 105.3(11) . .
O7 Li2 O5 93.4(9) . .
O6 Li2 O5 80.3(8) . .
O4 Li2 O8 91.3(9) . .
O7 Li2 O8 78.1(9) . .
O6 Li2 O8 89.9(9) . .
O5 Li2 O8 163.3(11) . .
O4 Li2 O3 75.5(7) . .
O7 Li2 O3 67.0(6) . .
O6 Li2 O3 148.1(11) . .
O5 Li2 O3 68.0(6) . .
O8 Li2 O3 120.0(9) . .
O4 Li2 C2 29.7(5) . .
O7 Li2 C2 98.0(8) . .
O6 Li2 C2 146.8(10) . .
O5 Li2 C2 109.1(9) . .
O8 Li2 C2 86.5(8) . .
O3 Li2 C2 54.3(4) . .
O4 Li2 C7 136.0(11) . .
O7 Li2 C7 29.5(5) . .
O6 Li2 C7 92.6(8) . .
O5 Li2 C7 111.2(9) . .
O8 Li2 C7 55.4(6) . .
O3 Li2 C7 95.8(7) . .
C2 Li2 C7 111.9(8) . .
W1 O2 Li1 141.9(7) . .
C1 O3 W1 125.1(6) . 2_465
C1 O3 W1 121.5(5) . .
W1 O3 W1 111.3(3) 2_465 .
C1 O3 Li2 99.7(7) . .
W1 O3 Li2 91.4(5) 2_465 .
W1 O3 Li2 92.6(5) . .
C3 O4 C2 114.4(10) . .
C3 O4 Li2 125.0(11) . .
C2 O4 Li2 108.8(9) . .
C4 O5 W1 128.5(8) . .
C4 O5 Li2 104.9(9) . .
W1 O5 Li2 118.5(6) . .
C6 O6 C5 113.8(11) . .
C6 O6 Li2 122.5(11) . .
C5 O6 Li2 110.7(10) . .
C7 O7 W1 127.8(8) . 2_465
C7 O7 Li2 106.8(9) . .
W1 O7 Li2 121.9(7) 2_465 .
C9 O8 C8 111.9(13) . .
C9 O8 Li2 131.5(11) . .
C8 O8 Li2 109.8(9) . .
C11 O9 C12 116.2(12) . .
C11 O9 Li1 113.9(11) . .
C12 O9 Li1 123.7(12) . .
C10 O10 Li1 110.0(12) . .
C14 O11 C15 113.1(12) . .
C14 O11 Li1 114.9(10) . .
C15 O11 Li1 124.4(11) . .
C13 O12 Li1 105.6(10) . .
W4 O14 W3 118.1(5) . 2_554
W2 O15 W4 117.3(4) . .
W4 O16 W3 117.6(4) . .
W4 O17 W2 118.0(4) . 2_554
W3 O20 W2 117.0(4) 2_554 .
W3 O21 W2 117.0(4) . .
W4 O22 W4 180.0 . 2_554
W4 O22 W2 89.89(3) . 2_554
W4 O22 W2 90.11(3) 2_554 2_554
W4 O22 W2 90.11(3) . .
W4 O22 W2 89.89(3) 2_554 .
W2 O22 W2 180.0 2_554 .
W4 O22 W3 89.82(4) . .
W4 O22 W3 90.18(4) 2_554 .
W2 O22 W3 89.99(4) 2_554 .
W2 O22 W3 90.01(4) . .
W4 O22 W3 90.18(4) . 2_554
W4 O22 W3 89.82(4) 2_554 2_554
W2 O22 W3 90.01(4) 2_554 2_554
W2 O22 W3 89.99(4) . 2_554
W3 O22 W3 180.0 . 2_554
O3 C1 C2 109.3(8) . .
O4 C2 C1 111.8(9) . .
O4 C2 Li2 41.5(6) . .
C1 C2 Li2 93.6(7) . .
O5 C4 C5 107.0(12) . .
O6 C5 C4 107.8(11) . .
O7 C7 C8 107.6(10) . .
O7 C7 Li2 43.7(6) . .
C8 C7 Li2 83.8(9) . .
O8 C8 C7 107.3(11) . .
C11 C10 O10 114.5(14) . .
O9 C11 C10 110.3(15) . .
O12 C13 C14 106.8(10) . .
O11 C14 C13 107.6(11) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
W1 O2 1.720(8) .
W1 O1 1.725(8) .
W1 O7 1.952(8) 2_465
W1 O5 1.971(8) .
W1 O3 2.140(7) 2_465
W1 O3 2.179(7) .
W2 O18 1.695(9) .
W2 O15 1.916(9) .
W2 O17 1.925(10) 2_554
W2 O20 1.929(8) .
W2 O21 1.935(8) .
W2 O22 2.3230(9) .
W3 O19 1.708(9) .
W3 O21 1.922(8) .
W3 O14 1.926(10) 2_554
W3 O20 1.926(8) 2_554
W3 O16 1.929(10) .
W3 O22 2.3268(12) .
W4 O13 1.701(11) .
W4 O17 1.899(9) .
W4 O16 1.904(9) .
W4 O14 1.909(10) .
W4 O15 1.929(9) .
W4 O22 2.3167(11) .
Li1 O9 2.00(2) .
Li1 O10 2.02(3) .
Li1 O11 2.04(2) .
Li1 O2 2.09(2) .
Li1 O12 2.10(2) .
Li2 O4 1.91(2) .
Li2 O7 1.98(2) .
Li2 O6 2.05(2) .
Li2 O5 2.10(2) .
Li2 O8 2.19(2) .
Li2 O3 2.64(2) .
Li2 C2 2.73(2) .
Li2 C7 2.75(3) .
O3 C1 1.458(11) .
O3 W1 2.140(7) 2_465
O4 C3 1.43(2) .
O4 C2 1.432(14) .
O5 C4 1.391(14) .
O6 C6 1.43(2) .
O6 C5 1.44(2) .
O7 C7 1.414(13) .
O7 W1 1.952(8) 2_465
O8 C9 1.38(2) .
O8 C8 1.42(2) .
O9 C11 1.38(2) .
O9 C12 1.42(2) .
O10 C10 1.41(2) .
O11 C14 1.42(2) .
O11 C15 1.44(2) .
O12 C13 1.45(2) .
O14 W3 1.926(10) 2_554
O17 W2 1.925(10) 2_554
O20 W3 1.926(8) 2_554
O22 W4 2.3167(11) 2_554
O22 W2 2.3230(9) 2_554
O22 W3 2.3268(12) 2_554
C1 C2 1.549(14) .
C4 C5 1.50(2) .
C7 C8 1.50(2) .
C10 C11 1.41(2) .
C13 C14 1.50(2) .
