#------------------------------------------------------------------------------
#$Date: 2016-03-25 17:06:09 +0200 (Fri, 25 Mar 2016) $
#$Revision: 180003 $
#$URL: svn://www.crystallography.net/cod/cif/7/02/97/7029792.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7029792
loop_
_publ_author_name
'Zhang, Lei'
'Kuang, Xiaofei'
'Wu, Xiaoyuan'
'Yang, Wenbin'
'Lu, Canzhong'
_publ_section_title
;
 Supramolecular interactions induced hinge-like motion of a metal-organic
 framework accompanied by anisotropic thermal expansion.
;
_journal_issue                   19
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              7146
_journal_page_last               7152
_journal_paper_doi               10.1039/c3dt53580k
_journal_volume                  43
_journal_year                    2014
_chemical_formula_sum            'C72 H51 Ag4 Mo8 N24 O27.63'
_chemical_formula_weight         2893.37
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 115.397(4)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   22.0366(6)
_cell_length_b                   16.4532(6)
_cell_length_c                   25.6805(8)
_cell_measurement_reflns_used    18294
_cell_measurement_temperature    220.00(10)
_cell_measurement_theta_max      29.4340
_cell_measurement_theta_min      3.3160
_cell_volume                     8411.2(5)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      220.00(10)
_diffrn_detector_area_resol_mean 10.3503
_diffrn_measured_fraction_theta_full 0.971
_diffrn_measured_fraction_theta_max 0.971
_diffrn_measurement_device_type  'SuperNova, Dual, Cu at zero, Atlas'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  mirror
_diffrn_radiation_source         'SuperNova (Mo) X-ray Source'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0365
_diffrn_reflns_av_sigmaI/netI    0.0450
_diffrn_reflns_limit_h_max       21
_diffrn_reflns_limit_h_min       -26
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_k_min       -19
_diffrn_reflns_limit_l_max       24
_diffrn_reflns_limit_l_min       -30
_diffrn_reflns_number            19501
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         3.07
_exptl_absorpt_coefficient_mu    2.153
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.77748
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            kermesinus
_exptl_crystal_density_diffrn    2.285
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block-like
_exptl_crystal_F_000             5584
_exptl_crystal_size_max          0.31
_exptl_crystal_size_mid          0.13
_exptl_crystal_size_min          0.08
_refine_diff_density_max         1.133
_refine_diff_density_min         -1.274
_refine_diff_density_rms         0.107
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.075
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     623
_refine_ls_number_reflns         7206
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.075
_refine_ls_R_factor_all          0.0343
_refine_ls_R_factor_gt           0.0287
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0208P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0602
_refine_ls_wR_factor_ref         0.0636
_reflns_number_gt                6346
_reflns_number_total             7206
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c3dt53580k2.cif
_cod_data_source_block           A_220K
_cod_depositor_comments
;Adding full bibliography for
 ./tmp-cod-update-bibliographies-12899/cifs/7029792.cif.
;
_cod_original_sg_symbol_H-M      C2/c
_cod_database_code               7029792
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Ag1 Ag 0.274042(14) 0.70856(2) -0.131802(13) 0.02775(9) Uani 1 1 d .
Ag2 Ag 0.794645(15) 1.00021(2) 0.367683(13) 0.03200(10) Uani 1 1 d .
C18 C 0.62836(18) 1.0621(2) -0.08821(17) 0.0230(9) Uani 1 1 d .
H18A H 0.5858 1.0404 -0.1094 0.028 Uiso 1 1 calc R
C19 C 0.42295(17) 1.4000(2) 0.39285(17) 0.0222(9) Uani 1 1 d .
H19A H 0.4033 1.4043 0.3529 0.027 Uiso 1 1 calc R
C22 C 0.62842(16) 1.0075(2) 0.00282(16) 0.0167(8) Uani 1 1 d .
C24 C 0.65412(17) 1.2190(2) 0.50174(16) 0.0177(8) Uani 1 1 d .
C26 C 0.48163(18) 1.3869(2) 0.50950(17) 0.0237(9) Uani 1 1 d .
H26A H 0.5006 1.3836 0.5495 0.028 Uiso 1 1 calc R
C29 C 0.40311(18) 0.8166(2) -0.11112(17) 0.0232(9) Uani 1 1 d .
H29A H 0.3850 0.8108 -0.1510 0.028 Uiso 1 1 calc R
C30 C 0.74388(17) 1.1331(2) 0.49673(16) 0.0213(8) Uani 1 1 d .
H30A H 0.7647 1.1328 0.5368 0.026 Uiso 1 1 calc R
C31 C 0.72318(17) 1.0864(2) 0.00014(17) 0.0229(9) Uani 1 1 d .
H31A H 0.7455 1.0821 0.0400 0.028 Uiso 1 1 calc R
C32 C 0.57523(17) 1.3009(2) 0.50731(16) 0.0171(8) Uani 1 1 d .
C33 C 0.66041(17) 1.0525(2) -0.02928(16) 0.0181(8) Uani 1 1 d .
C35 C 0.62810(17) 0.9764(2) 0.08825(16) 0.0187(8) Uani 1 1 d .
C36 C 0.77212(18) 1.0925(2) 0.46566(17) 0.0237(9) Uani 1 1 d .
H36A H 0.8125 1.0652 0.4858 0.028 Uiso 1 1 calc R
C37 C 0.46113(17) 0.8609(2) -0.08415(16) 0.0210(9) Uani 1 1 d .
H37A H 0.4818 0.8835 -0.1056 0.025 Uiso 1 1 calc R
C38 C 0.7800(2) 1.1983(3) 0.74082(18) 0.0308(10) Uani 1 1 d .
H38A H 0.8221 1.1746 0.7599 0.037 Uiso 1 1 calc R
C39 C 0.65853(17) 0.9869(2) 0.15185(16) 0.0210(9) Uani 1 1 d .
C40 C 0.69090(18) 1.2427(2) 0.65244(17) 0.0215(8) Uani 1 1 d .
C41 C 0.75254(19) 1.1271(3) -0.03035(17) 0.0285(10) Uani 1 1 d .
H41A H 0.7951 1.1494 -0.0101 0.034 Uiso 1 1 calc R
C42 C 0.55014(17) 0.9226(2) 0.00605(16) 0.0172(8) Uani 1 1 d .
C43 C 0.66106(18) 1.1051(2) -0.11533(17) 0.0255(9) Uani 1 1 d .
H43A H 0.6387 1.1127 -0.1550 0.031 Uiso 1 1 calc R
C44 C 0.71218(19) 1.0386(3) 0.17865(17) 0.0271(9) Uani 1 1 d .
H44A H 0.7280 1.0698 0.1569 0.033 Uiso 1 1 calc R
C45 C 0.48236(17) 1.3580(2) 0.41910(17) 0.0200(8) Uani 1 1 d .
H45A H 0.5021 1.3351 0.3970 0.024 Uiso 1 1 calc R
C46 C 0.68425(17) 1.1744(2) 0.46749(16) 0.0163(8) Uani 1 1 d .
C47 C 0.45688(17) 0.8341(2) 0.00548(16) 0.0193(8) Uani 1 1 d .
H47A H 0.4744 0.8379 0.0454 0.023 Uiso 1 1 calc R
C48 C 0.75343(19) 1.2073(3) 0.68173(17) 0.0283(10) Uani 1 1 d .
H48A H 0.7775 1.1896 0.6617 0.034 Uiso 1 1 calc R
C49 C 0.6869(2) 1.2569(3) 0.74328(18) 0.0304(10) Uani 1 1 d .
H49A H 0.6639 1.2742 0.7643 0.036 Uiso 1 1 calc R
C50 C 0.6563(2) 1.2683(2) 0.68386(18) 0.0274(9) Uani 1 1 d .
H50A H 0.6141 1.2923 0.6657 0.033 Uiso 1 1 calc R
C51 C 0.51278(17) 1.3500(2) 0.47833(16) 0.0190(8) Uani 1 1 d .
C52 C 0.65893(17) 1.2525(2) 0.58855(16) 0.0189(8) Uani 1 1 d .
C53 C 0.7421(2) 1.0438(3) 0.23781(18) 0.0315(10) Uani 1 1 d .
H53A H 0.7783 1.0789 0.2553 0.038 Uiso 1 1 calc R
C54 C 0.39894(18) 0.7909(2) -0.02520(17) 0.0210(9) Uani 1 1 d .
H54A H 0.3776 0.7669 -0.0048 0.025 Uiso 1 1 calc R
C55 C 0.65563(19) 1.1747(2) 0.40809(17) 0.0252(9) Uani 1 1 d .
H55A H 0.6163 1.2036 0.3873 0.030 Uiso 1 1 calc R
C56 C 0.63376(19) 0.9449(3) 0.18561(17) 0.0272(10) Uani 1 1 d .
H56A H 0.5957 0.9123 0.1689 0.033 Uiso 1 1 calc R
C57 C 0.6674(2) 0.9531(3) 0.24475(19) 0.0361(11) Uani 1 1 d .
H57A H 0.6514 0.9239 0.2673 0.043 Uiso 1 1 calc R
C58 C 0.42193(19) 1.4286(2) 0.47980(18) 0.0255(9) Uani 1 1 d .
H58A H 0.4017 1.4532 0.5009 0.031 Uiso 1 1 calc R
C59 C 0.48905(17) 0.8722(2) -0.02467(16) 0.0178(8) Uani 1 1 d .
C60 C 0.68672(19) 1.1312(3) 0.38001(18) 0.0269(9) Uani 1 1 d .
H60A H 0.6665 1.1303 0.3399 0.032 Uiso 1 1 calc R
N1 N 0.37117(14) 0.78101(18) -0.08254(14) 0.0198(7) Uani 1 1 d .
N2 N 0.72246(15) 1.1359(2) -0.08781(14) 0.0225(7) Uani 1 1 d .
N3 N 0.72127(16) 1.0001(2) 0.27168(14) 0.0294(8) Uani 1 1 d .
N4 N 0.57480(14) 0.96111(19) -0.02693(13) 0.0191(7) Uani 1 1 d .
N5 N 0.65627(14) 1.01856(19) 0.05975(13) 0.0200(7) Uani 1 1 d .
N6 N 0.57485(14) 0.92718(19) 0.06336(13) 0.0194(7) Uani 1 1 d .
N7 N 0.74459(15) 1.0901(2) 0.40779(14) 0.0238(7) Uani 1 1 d .
N8 N 0.39180(14) 1.43528(19) 0.42208(14) 0.0213(7) Uani 1 1 d .
N9 N 0.74691(16) 1.2228(2) 0.77201(14) 0.0290(8) Uani 1 1 d .
N10 N 0.59747(14) 1.26002(18) 0.47353(13) 0.0184(7) Uani 1 1 d .
N11 N 0.60422(15) 1.29900(19) 0.56492(14) 0.0216(7) Uani 1 1 d .
N12 N 0.68724(15) 1.21254(19) 0.55933(13) 0.0202(7) Uani 1 1 d .
Mo1 Mo 0.0000 0.71282(4) -0.2500 0.03807(15) Uani 1 2 d S
Mo2 Mo 0.112056(15) 0.83834(2) -0.139657(14) 0.02000(9) Uani 1 1 d .
Mo3 Mo 0.117388(15) 1.04114(2) -0.143702(14) 0.02027(9) Uani 1 1 d .
Mo4 Mo 0.0000 1.15132(3) -0.2500 0.02818(13) Uani 1 2 d S
Mo5 Mo 0.050519(15) 0.94350(2) -0.291303(14) 0.01841(9) Uani 1 1 d .
O1 O -0.01704(18) 0.6507(3) -0.2051(2) 0.0992(18) Uani 1 1 d .
O2 O 0.07901(13) 0.76471(17) -0.20686(12) 0.0308(7) Uani 1 1 d .
O3 O 0.19359(13) 0.83319(18) -0.13022(13) 0.0345(7) Uani 1 1 d .
O4 O 0.11000(14) 0.77527(18) -0.08794(13) 0.0374(7) Uani 1 1 d .
O5 O 0.00277(13) 0.85493(18) -0.32141(13) 0.0368(7) Uani 1 1 d .
O6 O 0.10967(14) 0.94996(18) -0.31720(14) 0.0382(8) Uani 1 1 d .
O7 O 0.08966(15) 0.93580(17) -0.21427(12) 0.0353(7) Uani 1 1 d .
O8 O 0.10938(12) 0.94020(16) -0.10743(11) 0.0269(6) Uani 1 1 d .
O9 O 0.11447(13) 1.10670(18) -0.09430(13) 0.0360(7) Uani 1 1 d .
O10 O 0.20024(13) 1.03745(18) -0.12898(13) 0.0360(7) Uani 1 1 d .
O11 O -0.00128(12) 1.03253(17) -0.31366(12) 0.0292(7) Uani 1 1 d .
O12 O 0.08790(13) 1.10827(17) -0.21220(12) 0.0300(7) Uani 1 1 d .
O13 O -0.00730(16) 1.2140(2) -0.20032(14) 0.0447(8) Uani 1 1 d .
O14 O -0.0807(5) 1.3633(6) -0.2324(4) 0.095(3) Uani 0.50 1 d P
H14A H -0.0583 1.3193 -0.2232 0.143 Uiso 0.50 1 d PR
H14B H -0.0605 1.3965 -0.2448 0.143 Uiso 0.50 1 d PR
O15 O 0.0131(12) 1.4818(11) -0.2234(9) 0.128(10) Uani 0.25 1 d P
H15A H 0.0019 1.5290 -0.2174 0.192 Uiso 0.25 1 d PR
H15B H -0.0172 1.4484 -0.2252 0.192 Uiso 0.25 1 d PR
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mo Mo -1.6832 0.6857 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
N2 Ag1 N9 129.72(12) 3_445 3_444
N2 Ag1 N1 123.30(11) 3_445 .
N9 Ag1 N1 106.94(11) 3_444 .
N8 Ag2 N3 135.02(11) 3_545 .
N8 Ag2 N7 121.91(11) 3_545 .
N3 Ag2 N7 103.06(11) . .
C33 C18 C43 118.5(4) . .
N8 C19 C45 123.3(3) . .
N5 C22 N4 125.6(3) . .
N5 C22 C33 115.7(3) . .
N4 C22 C33 118.6(3) . .
N10 C24 N12 125.5(3) . .
N10 C24 C46 118.5(3) . .
N12 C24 C46 116.0(3) . .
C58 C26 C51 118.9(4) . .
N1 C29 C37 123.1(4) . .
C36 C30 C46 119.0(4) . .
C33 C31 C41 119.3(4) . .
N11 C32 N10 124.6(3) . .
N11 C32 C51 117.8(3) . .
N10 C32 C51 117.6(3) . .
C18 C33 C31 118.5(3) . .
C18 C33 C22 121.6(3) . .
C31 C33 C22 120.0(3) . .
N6 C35 N5 124.7(3) . .
N6 C35 C39 119.0(3) . .
N5 C35 C39 116.4(3) . .
N7 C36 C30 123.6(4) . .
C29 C37 C59 120.1(3) . .
N9 C38 C48 122.5(4) . .
C44 C39 C56 118.5(3) . .
C44 C39 C35 120.5(3) . .
C56 C39 C35 121.0(3) . .
C48 C40 C50 118.6(4) . .
C48 C40 C52 122.3(3) . .
C50 C40 C52 119.2(3) . .
N2 C41 C31 123.0(4) . .
N6 C42 N4 125.7(3) . .
N6 C42 C59 117.7(3) . .
N4 C42 C59 116.6(3) . .
N2 C43 C18 123.7(4) . .
C53 C44 C39 119.5(4) . .
C19 C45 C51 119.9(3) . .
C55 C46 C30 118.8(3) . .
C55 C46 C24 122.6(3) . .
C30 C46 C24 118.6(3) . .
C54 C47 C59 118.7(3) . .
C38 C48 C40 119.7(3) . .
N9 C49 C50 124.3(4) . .
C49 C50 C40 117.8(4) . .
C45 C51 C26 117.7(3) . .
C45 C51 C32 120.6(3) . .
C26 C51 C32 121.6(3) . .
N11 C52 N12 125.1(3) . .
N11 C52 C40 118.1(3) . .
N12 C52 C40 116.8(3) . .
N3 C53 C44 123.0(4) . .
N1 C54 C47 124.5(3) . .
C46 C55 C60 118.6(4) . .
C57 C56 C39 117.9(4) . .
N3 C57 C56 124.4(4) . .
N8 C58 C26 123.4(3) . .
C37 C59 C47 117.1(3) . .
C37 C59 C42 122.0(3) . .
C47 C59 C42 120.9(3) . .
N7 C60 C55 123.4(4) . .
C54 N1 C29 116.5(3) . .
C54 N1 Ag1 123.1(2) . .
C29 N1 Ag1 120.4(3) . .
C43 N2 C41 117.0(3) . .
C43 N2 Ag1 123.5(3) . 3
C41 N2 Ag1 119.4(2) . 3
C57 N3 C53 116.5(4) . .
C57 N3 Ag2 128.1(3) . .
C53 N3 Ag2 114.4(3) . .
C22 N4 C42 114.0(3) . .
C22 N5 C35 115.2(3) . .
C42 N6 C35 114.8(3) . .
C36 N7 C60 116.6(3) . .
C36 N7 Ag2 115.6(2) . .
C60 N7 Ag2 127.2(3) . .
C58 N8 C19 116.8(3) . .
C58 N8 Ag2 127.5(2) . 3_455
C19 N8 Ag2 115.7(2) . 3_455
C49 N9 C38 117.1(3) . .
C49 N9 Ag1 112.2(2) . 3_556
C38 N9 Ag1 130.5(3) . 3_556
C24 N10 C32 114.8(3) . .
C52 N11 C32 115.3(3) . .
C52 N12 C24 114.6(3) . .
O1 Mo1 O1 106.0(4) . 2_554
O1 Mo1 O2 107.48(18) . .
O1 Mo1 O2 105.22(15) 2_554 .
O1 Mo1 O2 105.22(15) . 2_554
O1 Mo1 O2 107.48(18) 2_554 2_554
O2 Mo1 O2 124.24(18) . 2_554
O4 Mo2 O3 103.73(14) . .
O4 Mo2 O8 100.58(13) . .
O3 Mo2 O8 102.20(12) . .
O4 Mo2 O2 100.65(13) . .
O3 Mo2 O2 93.71(12) . .
O8 Mo2 O2 149.51(12) . .
O4 Mo2 O5 91.09(12) . 2_554
O3 Mo2 O5 163.68(12) . 2_554
O8 Mo2 O5 81.34(11) . 2_554
O2 Mo2 O5 76.62(11) . 2_554
O4 Mo2 O7 166.60(12) . .
O3 Mo2 O7 89.42(12) . .
O8 Mo2 O7 73.71(10) . .
O2 Mo2 O7 80.70(11) . .
O5 Mo2 O7 76.18(10) 2_554 .
O9 Mo3 O10 103.84(14) . .
O9 Mo3 O12 102.24(14) . .
O10 Mo3 O12 97.61(12) . .
O9 Mo3 O8 98.33(13) . .
O10 Mo3 O8 99.91(13) . .
O12 Mo3 O8 148.83(11) . .
O9 Mo3 O11 90.23(11) . 2_554
O10 Mo3 O11 165.19(13) . 2_554
O12 Mo3 O11 74.53(10) . 2_554
O8 Mo3 O11 82.28(10) . 2_554
O9 Mo3 O7 162.54(11) . .
O10 Mo3 O7 92.51(13) . .
O12 Mo3 O7 81.25(11) . .
O8 Mo3 O7 72.44(10) . .
O11 Mo3 O7 74.08(10) 2_554 .
O13 Mo4 O13 105.4(2) . 2_554
O13 Mo4 O12 101.91(13) . 2_554
O13 Mo4 O12 104.32(14) 2_554 2_554
O13 Mo4 O12 104.32(14) . .
O13 Mo4 O12 101.91(13) 2_554 .
O12 Mo4 O12 136.04(17) 2_554 .
O6 Mo5 O5 107.00(14) . .
O6 Mo5 O7 110.44(15) . .
O5 Mo5 O7 109.80(14) . .
O6 Mo5 O11 108.23(12) . .
O5 Mo5 O11 110.81(13) . .
O7 Mo5 O11 110.49(13) . .
Mo1 O2 Mo2 135.69(14) . .
Mo5 O5 Mo2 128.60(14) . 2_554
Mo5 O7 Mo2 140.47(15) . .
Mo5 O7 Mo3 129.16(14) . .
Mo2 O7 Mo3 88.90(9) . .
Mo2 O8 Mo3 121.51(13) . .
Mo5 O11 Mo3 128.59(14) . 2_554
Mo4 O12 Mo3 123.35(12) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ag1 N2 2.258(3) 3_445
Ag1 N9 2.291(3) 3_444
Ag1 N1 2.298(3) .
Ag2 N8 2.261(3) 3_545
Ag2 N3 2.296(3) .
Ag2 N7 2.332(3) .
C18 C33 1.377(5) .
C18 C43 1.391(5) .
C19 N8 1.346(4) .
C19 C45 1.374(5) .
C22 N5 1.333(5) .
C22 N4 1.337(5) .
C22 C33 1.491(5) .
C24 N10 1.328(5) .
C24 N12 1.344(5) .
C24 C46 1.501(5) .
C26 C58 1.386(5) .
C26 C51 1.397(5) .
C29 N1 1.349(4) .
C29 C37 1.374(5) .
C30 C36 1.378(5) .
C30 C46 1.380(5) .
C31 C33 1.378(5) .
C31 C41 1.384(5) .
C32 N11 1.337(5) .
C32 N10 1.346(4) .
C32 C51 1.491(5) .
C35 N6 1.341(5) .
C35 N5 1.339(4) .
C35 C39 1.486(5) .
C36 N7 1.343(5) .
C37 C59 1.393(5) .
C38 N9 1.354(5) .
C38 C48 1.380(5) .
C39 C44 1.378(5) .
C39 C56 1.390(5) .
C40 C48 1.384(5) .
C40 C50 1.392(5) .
C40 C52 1.491(5) .
C41 N2 1.341(5) .
C42 N6 1.335(5) .
C42 N4 1.345(4) .
C42 C59 1.487(5) .
C43 N2 1.330(5) .
C44 C53 1.375(6) .
C45 C51 1.380(5) .
C46 C55 1.378(5) .
C47 C54 1.376(5) .
C47 C59 1.402(5) .
C49 N9 1.331(5) .
C49 C50 1.391(6) .
C52 N11 1.334(5) .
C52 N12 1.336(4) .
C53 N3 1.351(5) .
C54 N1 1.340(5) .
C55 C60 1.388(5) .
C56 C57 1.381(6) .
C57 N3 1.335(5) .
C58 N8 1.344(5) .
C60 N7 1.346(5) .
N2 Ag1 2.258(3) 3
N8 Ag2 2.261(3) 3_455
N9 Ag1 2.291(3) 3_556
Mo1 O1 1.700(4) .
Mo1 O1 1.700(4) 2_554
Mo1 O2 1.826(3) .
Mo1 O2 1.826(3) 2_554
Mo2 O4 1.701(3) .
Mo2 O3 1.709(2) .
Mo2 O8 1.881(3) .
Mo2 O2 1.974(3) .
Mo2 O5 2.304(3) 2_554
Mo2 O7 2.382(3) .
Mo3 O9 1.687(3) .
Mo3 O10 1.699(3) .
Mo3 O12 1.938(3) .
Mo3 O8 1.949(3) .
Mo3 O11 2.316(2) 2_554
Mo3 O7 2.390(3) .
Mo4 O13 1.701(3) .
Mo4 O13 1.701(3) 2_554
Mo4 O12 1.893(3) 2_554
Mo4 O12 1.893(3) .
Mo5 O6 1.702(2) .
Mo5 O5 1.769(3) .
Mo5 O7 1.792(3) .
Mo5 O11 1.793(3) .
O5 Mo2 2.304(3) 2_554
O11 Mo3 2.316(2) 2_554
O15 O15 1.23(4) 2_554
