#------------------------------------------------------------------------------
#$Date: 2016-03-25 17:06:09 +0200 (Fri, 25 Mar 2016) $
#$Revision: 180003 $
#$URL: svn://www.crystallography.net/cod/cif/7/02/97/7029798.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7029798
loop_
_publ_author_name
'Zhang, Lei'
'Kuang, Xiaofei'
'Wu, Xiaoyuan'
'Yang, Wenbin'
'Lu, Canzhong'
_publ_section_title
;
 Supramolecular interactions induced hinge-like motion of a metal-organic
 framework accompanied by anisotropic thermal expansion.
;
_journal_issue                   19
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              7146
_journal_page_last               7152
_journal_paper_doi               10.1039/c3dt53580k
_journal_volume                  43
_journal_year                    2014
_chemical_formula_sum            'C72 H48 Ag4 Mo8 N24 O26'
_chemical_formula_weight         2864.34
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 115.344(5)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   21.9717(6)
_cell_length_b                   16.6692(6)
_cell_length_c                   25.6289(9)
_cell_measurement_reflns_used    14686
_cell_measurement_temperature    380.00(10)
_cell_measurement_theta_max      28.8470
_cell_measurement_theta_min      3.1910
_cell_volume                     8483.2(6)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      380.00(10)
_diffrn_detector_area_resol_mean 10.3503
_diffrn_measured_fraction_theta_full 0.971
_diffrn_measured_fraction_theta_max 0.971
_diffrn_measurement_device_type  'SuperNova, Dual, Cu at zero, Atlas'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  mirror
_diffrn_radiation_source         'SuperNova (Mo) X-ray Source'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0358
_diffrn_reflns_av_sigmaI/netI    0.0452
_diffrn_reflns_limit_h_max       21
_diffrn_reflns_limit_h_min       -26
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_k_min       -19
_diffrn_reflns_limit_l_max       24
_diffrn_reflns_limit_l_min       -30
_diffrn_reflns_number            19756
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         3.07
_exptl_absorpt_coefficient_mu    2.132
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.73164
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            crimson
_exptl_crystal_density_diffrn    2.243
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block-like
_exptl_crystal_F_000             5520
_exptl_crystal_size_max          0.33
_exptl_crystal_size_mid          0.12
_exptl_crystal_size_min          0.07
_refine_diff_density_max         1.775
_refine_diff_density_min         -1.233
_refine_diff_density_rms         0.139
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.090
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     605
_refine_ls_number_reflns         7272
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.090
_refine_ls_R_factor_all          0.0518
_refine_ls_R_factor_gt           0.0421
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0648P)²+21.6801P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1189
_refine_ls_wR_factor_ref         0.1291
_reflns_number_gt                6043
_reflns_number_total             7272
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c3dt53580k2.cif
_cod_data_source_block           A_380K
_cod_depositor_comments
;Adding full bibliography for
 ./tmp-cod-update-bibliographies-12899/cifs/7029798.cif.
;
_cod_original_cell_volume        8483.2(5)
_cod_original_sg_symbol_H-M      C2/c
_cod_database_code               7029798
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Ag1 Ag 0.27371(2) 0.20896(4) -0.13192(2) 0.04890(17) Uani 1 1 d .
Ag2 Ag 0.29539(3) 0.00244(4) 0.36756(2) 0.05608(19) Uani 1 1 d .
C11 C -0.0779(3) 0.3997(4) 0.3920(3) 0.0350(13) Uani 1 1 d .
H11A H -0.0983 0.4034 0.3519 0.042 Uiso 1 1 calc R
C12 C 0.1535(3) 0.2200(3) 0.5008(2) 0.0294(12) Uani 1 1 d .
C19 C 0.1276(3) 0.0614(4) -0.0891(3) 0.0399(15) Uani 1 1 d .
H19A H 0.0849 0.0401 -0.1104 0.048 Uiso 1 1 calc R
C25 C 0.1280(3) 0.0072(3) 0.0019(2) 0.0287(12) Uani 1 1 d .
C26 C -0.0183(3) 0.3870(4) 0.5090(3) 0.0401(15) Uani 1 1 d .
H26A H 0.0009 0.3836 0.5491 0.048 Uiso 1 1 calc R
C27 C -0.0970(3) -0.1846(4) -0.1111(3) 0.0396(15) Uani 1 1 d .
H27A H -0.1147 -0.1917 -0.1509 0.048 Uiso 1 1 calc R
C28 C 0.0748(3) 0.3015(3) 0.5063(3) 0.0307(13) Uani 1 1 d .
C29 C 0.2434(3) 0.1334(4) 0.4965(3) 0.0345(13) Uani 1 1 d .
H29A H 0.2637 0.1323 0.5367 0.041 Uiso 1 1 calc R
C30 C 0.2711(3) 0.0932(4) 0.4648(3) 0.0365(14) Uani 1 1 d .
H30A H 0.3113 0.0658 0.4848 0.044 Uiso 1 1 calc R
C31 C 0.2228(3) 0.0850(4) -0.0010(3) 0.0412(15) Uani 1 1 d .
H31A H 0.2460 0.0799 0.0388 0.049 Uiso 1 1 calc R
C32 C 0.1596(3) 0.0517(3) -0.0305(3) 0.0309(13) Uani 1 1 d .
C34 C 0.1274(3) -0.0241(4) 0.0875(3) 0.0314(13) Uani 1 1 d .
C35 C 0.1583(3) -0.0144(4) 0.1512(3) 0.0350(13) Uani 1 1 d .
C37 C -0.0394(3) -0.1387(4) -0.0847(3) 0.0368(14) Uani 1 1 d .
H37A H -0.0196 -0.1156 -0.1066 0.044 Uiso 1 1 calc R
C38 C 0.1839(3) 0.1757(3) 0.4663(2) 0.0284(12) Uani 1 1 d .
C39 C 0.1900(3) 0.2424(4) 0.6514(3) 0.0380(14) Uani 1 1 d .
C40 C 0.2507(3) 0.1259(5) -0.0322(3) 0.0495(18) Uani 1 1 d .
H40A H 0.2928 0.1490 -0.0119 0.059 Uiso 1 1 calc R
C41 C -0.0179(3) 0.3580(4) 0.4183(3) 0.0349(13) Uani 1 1 d .
H41A H 0.0017 0.3355 0.3960 0.042 Uiso 1 1 calc R
C42 C -0.0428(3) -0.1662(4) 0.0051(3) 0.0350(14) Uani 1 1 d .
H42A H -0.0250 -0.1629 0.0452 0.042 Uiso 1 1 calc R
C43 C 0.2520(3) 0.2073(5) 0.6805(3) 0.0483(17) Uani 1 1 d .
H43A H 0.2759 0.1896 0.6602 0.058 Uiso 1 1 calc R
C44 C 0.0495(3) -0.0772(3) 0.0051(2) 0.0283(12) Uani 1 1 d .
C46 C 0.2791(3) 0.1982(5) 0.7399(3) 0.055(2) Uani 1 1 d .
H46A H 0.3211 0.1743 0.7589 0.066 Uiso 1 1 calc R
C47 C 0.1606(3) 0.1039(4) -0.1157(3) 0.0450(16) Uani 1 1 d .
H47A H 0.1382 0.1114 -0.1554 0.054 Uiso 1 1 calc R
C48 C 0.0126(3) 0.3499(3) 0.4770(3) 0.0315(13) Uani 1 1 d .
C49 C 0.1558(4) 0.2682(4) 0.6832(3) 0.0478(17) Uani 1 1 d .
H49A H 0.1136 0.2921 0.6654 0.057 Uiso 1 1 calc R
C50 C 0.1583(3) 0.2516(4) 0.5874(3) 0.0338(13) Uani 1 1 d .
C51 C -0.1010(3) -0.2093(4) -0.0257(3) 0.0361(14) Uani 1 1 d .
H51A H -0.1223 -0.2331 -0.0051 0.043 Uiso 1 1 calc R
C52 C 0.1871(4) 0.2566(5) 0.7424(3) 0.0528(18) Uani 1 1 d .
H52A H 0.1643 0.2741 0.7637 0.063 Uiso 1 1 calc R
C53 C 0.1552(3) 0.1752(4) 0.4070(3) 0.0398(15) Uani 1 1 d .
H53A H 0.1160 0.2040 0.3860 0.048 Uiso 1 1 calc R
C54 C -0.0778(3) 0.4286(4) 0.4793(3) 0.0422(16) Uani 1 1 d .
H54A H -0.0978 0.4534 0.5005 0.051 Uiso 1 1 calc R
C55 C 0.2412(4) 0.0439(5) 0.2368(3) 0.0501(17) Uani 1 1 d .
H55A H 0.2767 0.0796 0.2542 0.060 Uiso 1 1 calc R
C56 C 0.2118(3) 0.0377(5) 0.1774(3) 0.0478(17) Uani 1 1 d .
H56A H 0.2277 0.0680 0.1554 0.057 Uiso 1 1 calc R
C57 C 0.1333(4) -0.0551(4) 0.1846(3) 0.0468(17) Uani 1 1 d .
H57A H 0.0951 -0.0872 0.1680 0.056 Uiso 1 1 calc R
C58 C -0.0112(3) -0.1273(3) -0.0253(3) 0.0309(13) Uani 1 1 d .
C59 C 0.1674(4) -0.0462(5) 0.2442(3) 0.057(2) Uani 1 1 d .
H59A H 0.1516 -0.0751 0.2670 0.068 Uiso 1 1 calc R
C60 C 0.1859(4) 0.1312(5) 0.3795(3) 0.0489(17) Uani 1 1 d .
H60A H 0.1652 0.1292 0.3394 0.059 Uiso 1 1 calc R
N1 N 0.2220(2) 0.1346(3) -0.0884(2) 0.0396(12) Uani 1 1 d .
N2 N -0.1286(2) -0.2192(3) -0.0825(2) 0.0348(11) Uani 1 1 d .
N3 N 0.2206(3) 0.0002(4) 0.2709(2) 0.0493(15) Uani 1 1 d .
N4 N 0.0740(2) -0.0393(3) -0.0279(2) 0.0323(11) Uani 1 1 d .
N5 N 0.0747(2) -0.0726(3) 0.0626(2) 0.0332(11) Uani 1 1 d .
N6 N 0.1558(2) 0.0175(3) 0.0587(2) 0.0337(11) Uani 1 1 d .
N7 N 0.2438(3) 0.0910(3) 0.4072(2) 0.0399(12) Uani 1 1 d .
N8 N -0.1080(3) 0.4352(3) 0.4220(2) 0.0391(12) Uani 1 1 d .
N9 N 0.2464(3) 0.2230(4) 0.7711(2) 0.0494(14) Uani 1 1 d .
N10 N 0.0971(2) 0.2608(3) 0.4727(2) 0.0320(11) Uani 1 1 d .
N11 N 0.1036(2) 0.2993(3) 0.5640(2) 0.0364(12) Uani 1 1 d .
N12 N 0.1861(2) 0.2126(3) 0.5584(2) 0.0334(11) Uani 1 1 d .
Mo1 Mo 0.0000 0.21623(6) -0.2500 0.0558(3) Uani 1 2 d S
Mo2 Mo 0.11203(2) 0.33998(3) -0.13945(2) 0.03325(15) Uani 1 1 d .
Mo3 Mo 0.11641(2) 0.54031(3) -0.14319(2) 0.03470(16) Uani 1 1 d .
Mo4 Mo 0.05155(2) 0.44338(3) -0.29086(2) 0.03165(15) Uani 1 1 d .
Mo5 Mo 0.0000 0.65236(6) -0.2500 0.0491(2) Uani 1 2 d S
O1 O -0.0194(4) 0.1556(6) -0.2059(5) 0.160(5) Uani 1 1 d .
O2 O 0.0785(2) 0.2662(3) -0.2063(2) 0.0532(12) Uani 1 1 d .
O3 O 0.1106(3) 0.2793(4) -0.0865(2) 0.0701(16) Uani 1 1 d .
O4 O 0.1928(3) 0.3329(4) -0.1306(2) 0.0653(15) Uani 1 1 d .
O5 O 0.0886(3) 0.4362(3) -0.2148(2) 0.0603(14) Uani 1 1 d .
O6 O 0.0032(2) 0.3561(3) -0.3222(2) 0.0629(14) Uani 1 1 d .
O7 O 0.1097(3) 0.4486(3) -0.3176(3) 0.0622(15) Uani 1 1 d .
O8 O -0.0005(2) 0.5315(3) -0.3148(2) 0.0551(13) Uani 1 1 d .
O9 O 0.1100(2) 0.4401(3) -0.1070(2) 0.0510(12) Uani 1 1 d .
O10 O 0.1992(3) 0.5376(4) -0.1293(3) 0.0702(16) Uani 1 1 d .
O11 O 0.0867(2) 0.6075(3) -0.2115(2) 0.0590(13) Uani 1 1 d .
O12 O 0.1146(3) 0.6032(4) -0.0929(2) 0.0699(16) Uani 1 1 d .
O13 O -0.0089(3) 0.7131(4) -0.2009(3) 0.0838(18) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mo Mo -1.6832 0.6857 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
N1 Ag1 N2 123.89(18) . 3
N1 Ag1 N9 129.1(2) . 1_554
N2 Ag1 N9 106.89(19) 3 1_554
N8 Ag2 N3 134.2(2) 3_545 .
N8 Ag2 N7 122.86(19) 3_545 .
N3 Ag2 N7 102.8(2) . .
N8 C11 C41 122.7(6) . .
N10 C12 N12 125.5(5) . .
N10 C12 C38 118.5(5) . .
N12 C12 C38 116.0(5) . .
C32 C19 C47 118.0(6) . .
N6 C25 N4 125.1(5) . .
N6 C25 C32 116.2(5) . .
N4 C25 C32 118.6(5) . .
C54 C26 C48 118.3(6) . .
N2 C27 C37 123.4(6) . .
N11 C28 N10 124.5(5) . .
N11 C28 C48 118.1(5) . .
N10 C28 C48 117.3(5) . .
C30 C29 C38 117.7(5) . .
N7 C30 C29 124.3(6) . .
C40 C31 C32 118.4(6) . .
C19 C32 C31 118.4(5) . .
C19 C32 C25 121.8(5) . .
C31 C32 C25 119.8(5) . .
N5 C34 N6 124.2(5) . .
N5 C34 C35 119.3(5) . .
N6 C34 C35 116.5(5) . .
C56 C35 C57 119.2(6) . .
C56 C35 C34 119.9(5) . .
C57 C35 C34 120.9(6) . .
C27 C37 C58 119.9(6) . .
C53 C38 C29 119.2(5) . .
C53 C38 C12 122.9(5) . .
C29 C38 C12 117.9(5) . .
C43 C39 C49 118.1(6) . .
C43 C39 C50 122.0(5) . .
C49 C39 C50 119.8(6) . .
N1 C40 C31 124.7(6) . .
C48 C41 C11 120.1(5) . .
C51 C42 C58 118.6(6) . .
C39 C43 C46 120.2(6) . .
N4 C44 N5 125.5(5) . .
N4 C44 C58 116.7(5) . .
N5 C44 C58 117.8(5) . .
N9 C46 C43 122.0(6) . .
N1 C47 C19 124.6(6) . .
C41 C48 C26 117.8(5) . .
C41 C48 C28 121.5(5) . .
C26 C48 C28 120.7(5) . .
C52 C49 C39 117.4(6) . .
N12 C50 N11 125.4(5) . .
N12 C50 C39 117.3(5) . .
N11 C50 C39 117.3(5) . .
N2 C51 C42 124.7(5) . .
N9 C52 C49 125.4(6) . .
C60 C53 C38 118.5(6) . .
N8 C54 C26 123.8(6) . .
N3 C55 C56 122.9(6) . .
C55 C56 C35 118.9(6) . .
C35 C57 C59 117.4(6) . .
C37 C58 C42 116.7(5) . .
C37 C58 C44 122.2(5) . .
C42 C58 C44 121.2(5) . .
N3 C59 C57 124.8(6) . .
N7 C60 C53 123.9(6) . .
C40 N1 C47 115.9(5) . .
C40 N1 Ag1 119.7(4) . .
C47 N1 Ag1 124.2(4) . .
C51 N2 C27 116.6(5) . .
C51 N2 Ag1 123.2(4) . 3_445
C27 N2 Ag1 120.2(4) . 3_445
C59 N3 C55 116.6(6) . .
C59 N3 Ag2 128.9(5) . .
C55 N3 Ag2 113.7(4) . .
C44 N4 C25 114.1(5) . .
C34 N5 C44 115.4(5) . .
C25 N6 C34 115.6(5) . .
C60 N7 C30 116.5(5) . .
C60 N7 Ag2 127.7(4) . .
C30 N7 Ag2 115.2(4) . .
C54 N8 C11 117.3(5) . .
C54 N8 Ag2 127.6(4) . 3_455
C11 N8 Ag2 115.1(4) . 3_455
C52 N9 C46 116.9(6) . .
C52 N9 Ag1 112.5(4) . 1_556
C46 N9 Ag1 130.4(5) . 1_556
C12 N10 C28 115.0(5) . .
C28 N11 C50 114.6(5) . .
C50 N12 C12 114.6(5) . .
O1 Mo1 O1 107.1(9) . 2_554
O1 Mo1 O2 107.8(4) . .
O1 Mo1 O2 104.0(3) 2_554 .
O1 Mo1 O2 104.0(3) . 2_554
O1 Mo1 O2 107.8(4) 2_554 2_554
O2 Mo1 O2 125.1(3) . 2_554
O4 Mo2 O3 103.1(3) . .
O4 Mo2 O9 103.0(2) . .
O3 Mo2 O9 99.4(2) . .
O4 Mo2 O2 93.1(2) . .
O3 Mo2 O2 101.2(3) . .
O9 Mo2 O2 150.2(2) . .
O4 Mo2 O6 164.0(2) . 2_554
O3 Mo2 O6 91.0(2) . 2_554
O9 Mo2 O6 81.6(2) . 2_554
O2 Mo2 O6 76.6(2) . 2_554
O4 Mo2 O5 90.4(2) . .
O3 Mo2 O5 166.1(2) . .
O9 Mo2 O5 73.90(19) . .
O2 Mo2 O5 81.13(19) . .
O6 Mo2 O5 76.10(19) 2_554 .
O12 Mo3 O10 103.4(3) . .
O12 Mo3 O11 102.9(3) . .
O10 Mo3 O11 97.0(3) . .
O12 Mo3 O9 98.0(3) . .
O10 Mo3 O9 99.6(3) . .
O11 Mo3 O9 149.4(2) . .
O12 Mo3 O8 90.8(2) . 2_554
O10 Mo3 O8 165.0(3) . 2_554
O11 Mo3 O8 74.77(19) . 2_554
O9 Mo3 O8 82.92(19) . 2_554
O12 Mo3 O5 162.9(2) . .
O10 Mo3 O5 92.3(3) . .
O11 Mo3 O5 81.4(2) . .
O9 Mo3 O5 72.39(19) . .
O8 Mo3 O5 74.23(19) 2_554 .
O7 Mo4 O5 112.3(3) . .
O7 Mo4 O6 105.6(3) . .
O5 Mo4 O6 110.3(3) . .
O7 Mo4 O8 107.5(2) . .
O5 Mo4 O8 110.9(2) . .
O6 Mo4 O8 110.1(2) . .
O13 Mo5 O13 106.4(5) . 2_554
O13 Mo5 O11 102.3(3) . 2_554
O13 Mo5 O11 105.2(3) 2_554 2_554
O13 Mo5 O11 105.2(3) . .
O13 Mo5 O11 102.3(3) 2_554 .
O11 Mo5 O11 133.2(3) 2_554 .
Mo1 O2 Mo2 136.6(3) . .
Mo4 O5 Mo2 140.8(3) . .
Mo4 O5 Mo3 129.7(3) . .
Mo2 O5 Mo3 88.36(17) . .
Mo4 O6 Mo2 128.5(3) . 2_554
Mo4 O8 Mo3 128.7(3) . 2_554
Mo2 O9 Mo3 122.2(2) . .
Mo5 O11 Mo3 125.1(3) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ag1 N1 2.269(5) .
Ag1 N2 2.307(5) 3
Ag1 N9 2.307(5) 1_554
Ag2 N8 2.275(5) 3_545
Ag2 N3 2.315(6) .
Ag2 N7 2.341(5) .
C11 N8 1.346(8) .
C11 C41 1.383(8) .
C12 N10 1.324(7) .
C12 N12 1.342(7) .
C12 C38 1.508(8) .
C19 C32 1.369(9) .
C19 C47 1.384(9) .
C25 N6 1.328(7) .
C25 N4 1.347(7) .
C25 C32 1.488(8) .
C26 C54 1.386(8) .
C26 C48 1.411(8) .
C27 N2 1.337(8) .
C27 C37 1.381(8) .
C28 N11 1.337(8) .
C28 N10 1.345(7) .
C28 C48 1.485(8) .
C29 C30 1.381(8) .
C29 C38 1.393(8) .
C30 N7 1.335(8) .
C31 C40 1.378(9) .
C31 C32 1.381(8) .
C34 N5 1.330(7) .
C34 N6 1.345(7) .
C34 C35 1.482(8) .
C35 C56 1.382(9) .
C35 C57 1.379(9) .
C37 C58 1.389(8) .
C38 C53 1.374(8) .
C39 C43 1.372(9) .
C39 C49 1.393(9) .
C39 C50 1.489(8) .
C40 N1 1.310(8) .
C41 C48 1.366(8) .
C42 C51 1.381(8) .
C42 C58 1.406(8) .
C43 C46 1.387(9) .
C44 N4 1.337(7) .
C44 N5 1.337(7) .
C44 C58 1.481(8) .
C46 N9 1.347(9) .
C47 N1 1.329(8) .
C49 C52 1.386(10) .
C50 N12 1.319(7) .
C50 N11 1.349(7) .
C51 N2 1.326(8) .
C52 N9 1.315(9) .
C53 C60 1.377(9) .
C54 N8 1.331(8) .
C55 N3 1.355(9) .
C55 C56 1.378(9) .
C57 C59 1.391(10) .
C59 N3 1.322(9) .
C60 N7 1.341(8) .
N2 Ag1 2.307(5) 3_445
N8 Ag2 2.275(5) 3_455
N9 Ag1 2.307(5) 1_556
Mo1 O1 1.701(8) .
Mo1 O1 1.701(8) 2_554
Mo1 O2 1.808(5) .
Mo1 O2 1.808(5) 2_554
Mo2 O4 1.693(5) .
Mo2 O3 1.703(5) .
Mo2 O9 1.874(5) .
Mo2 O2 1.977(5) .
Mo2 O6 2.305(5) 2_554
Mo2 O5 2.390(5) .
Mo3 O12 1.674(5) .
Mo3 O10 1.699(5) .
Mo3 O11 1.941(5) .
Mo3 O9 1.944(5) .
Mo3 O8 2.306(5) 2_554
Mo3 O5 2.407(5) .
Mo4 O7 1.690(4) .
Mo4 O5 1.766(5) .
Mo4 O6 1.778(5) .
Mo4 O8 1.800(5) .
Mo5 O13 1.692(6) .
Mo5 O13 1.692(6) 2_554
Mo5 O11 1.885(5) 2_554
Mo5 O11 1.885(5) .
O6 Mo2 2.305(5) 2_554
O8 Mo3 2.306(5) 2_554
