#------------------------------------------------------------------------------
#$Date: 2016-03-25 17:06:09 +0200 (Fri, 25 Mar 2016) $
#$Revision: 180003 $
#$URL: svn://www.crystallography.net/cod/cif/7/02/97/7029799.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7029799
loop_
_publ_author_name
'Zhang, Lei'
'Kuang, Xiaofei'
'Wu, Xiaoyuan'
'Yang, Wenbin'
'Lu, Canzhong'
_publ_section_title
;
 Supramolecular interactions induced hinge-like motion of a metal-organic
 framework accompanied by anisotropic thermal expansion.
;
_journal_issue                   19
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              7146
_journal_page_last               7152
_journal_paper_doi               10.1039/c3dt53580k
_journal_volume                  43
_journal_year                    2014
_chemical_formula_sum            'C72 H48 Ag4 Mo8 N24 O26'
_chemical_formula_weight         2864.34
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 115.366(5)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   21.9504(7)
_cell_length_b                   16.7095(7)
_cell_length_c                   25.6128(10)
_cell_measurement_reflns_used    14017
_cell_measurement_temperature    410.01(10)
_cell_measurement_theta_max      28.7900
_cell_measurement_theta_min      3.1920
_cell_volume                     8488.6(7)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      410.01(10)
_diffrn_detector_area_resol_mean 10.3503
_diffrn_measured_fraction_theta_full 0.971
_diffrn_measured_fraction_theta_max 0.971
_diffrn_measurement_device_type  'SuperNova, Dual, Cu at zero, Atlas'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  mirror
_diffrn_radiation_source         'SuperNova (Mo) X-ray Source'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0360
_diffrn_reflns_av_sigmaI/netI    0.0451
_diffrn_reflns_limit_h_max       21
_diffrn_reflns_limit_h_min       -26
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_k_min       -19
_diffrn_reflns_limit_l_max       24
_diffrn_reflns_limit_l_min       -30
_diffrn_reflns_number            19739
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         3.06
_exptl_absorpt_coefficient_mu    2.131
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.73506
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            crimson
_exptl_crystal_density_diffrn    2.241
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block-like
_exptl_crystal_F_000             5520
_exptl_crystal_size_max          0.33
_exptl_crystal_size_mid          0.11
_exptl_crystal_size_min          0.07
_refine_diff_density_max         1.576
_refine_diff_density_min         -1.229
_refine_diff_density_rms         0.144
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.091
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     605
_refine_ls_number_reflns         7274
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.091
_refine_ls_R_factor_all          0.0559
_refine_ls_R_factor_gt           0.0447
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0742P)²+17.9769P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1293
_refine_ls_wR_factor_ref         0.1412
_reflns_number_gt                5967
_reflns_number_total             7274
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c3dt53580k2.cif
_cod_data_source_block           A_410K
_cod_depositor_comments
;Adding full bibliography for
 ./tmp-cod-update-bibliographies-12899/cifs/7029799.cif.
;
_cod_original_cell_volume        8488.6(6)
_cod_original_sg_symbol_H-M      C2/c
_cod_database_code               7029799
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Ag1 Ag 0.27363(3) 0.20879(4) -0.13206(2) 0.05384(19) Uani 1 1 d .
Ag2 Ag 0.79557(3) 0.50313(4) 0.36744(2) 0.0611(2) Uani 1 1 d .
C3 C 0.6531(3) 0.7198(3) 0.5003(3) 0.0301(13) Uani 1 1 d .
C15 C 0.4222(3) 0.8995(4) 0.3919(3) 0.0388(14) Uani 1 1 d .
H15A H 0.4014 0.9025 0.3518 0.047 Uiso 1 1 calc R
C16 C 0.6276(3) 0.5611(4) -0.0894(3) 0.0440(16) Uani 1 1 d .
H16A H 0.5849 0.5397 -0.1108 0.053 Uiso 1 1 calc R
C23 C 0.6275(3) 0.5067(4) 0.0017(3) 0.0310(13) Uani 1 1 d .
C24 C 0.5746(3) 0.8016(4) 0.5060(3) 0.0350(14) Uani 1 1 d .
C25 C 0.7707(3) 0.5935(4) 0.4646(3) 0.0388(14) Uani 1 1 d .
H25A H 0.8108 0.5659 0.4848 0.047 Uiso 1 1 calc R
C26 C 0.4819(3) 0.8873(4) 0.5087(3) 0.0442(16) Uani 1 1 d .
H26A H 0.5013 0.8842 0.5488 0.053 Uiso 1 1 calc R
C27 C 0.4029(3) 0.3159(4) -0.1112(3) 0.0430(15) Uani 1 1 d .
H27A H 0.3847 0.3095 -0.1511 0.052 Uiso 1 1 calc R
C29 C 0.7428(3) 0.6339(4) 0.4956(3) 0.0372(14) Uani 1 1 d .
H29A H 0.7634 0.6331 0.5358 0.045 Uiso 1 1 calc R
C31 C 0.6589(3) 0.5515(4) -0.0310(3) 0.0347(14) Uani 1 1 d .
C32 C 0.7224(3) 0.5851(5) -0.0018(3) 0.0452(16) Uani 1 1 d .
H32A H 0.7453 0.5804 0.0381 0.054 Uiso 1 1 calc R
C33 C 0.6836(3) 0.6759(4) 0.4663(2) 0.0313(13) Uani 1 1 d .
C35 C 0.6269(3) 0.4753(4) 0.0872(3) 0.0338(13) Uani 1 1 d .
C36 C 0.6581(3) 0.4858(4) 0.1505(3) 0.0371(14) Uani 1 1 d .
C37 C 0.4819(3) 0.8584(4) 0.4180(3) 0.0366(14) Uani 1 1 d .
H37A H 0.5016 0.8362 0.3957 0.044 Uiso 1 1 calc R
C38 C 0.5496(3) 0.4225(3) 0.0046(3) 0.0316(13) Uani 1 1 d .
C39 C 0.6899(3) 0.7420(4) 0.6515(3) 0.0399(15) Uani 1 1 d .
C40 C 0.4572(3) 0.3341(4) 0.0053(3) 0.0366(14) Uani 1 1 d .
H40A H 0.4751 0.3376 0.0454 0.044 Uiso 1 1 calc R
C41 C 0.7510(3) 0.6248(5) -0.0319(3) 0.0506(18) Uani 1 1 d .
H41A H 0.7937 0.6465 -0.0114 0.061 Uiso 1 1 calc R
C43 C 0.4607(3) 0.3609(4) -0.0851(3) 0.0397(15) Uani 1 1 d .
H43A H 0.4809 0.3833 -0.1070 0.048 Uiso 1 1 calc R
C44 C 0.7518(4) 0.7071(5) 0.6800(3) 0.0535(19) Uani 1 1 d .
H44A H 0.7758 0.6895 0.6598 0.064 Uiso 1 1 calc R
C46 C 0.6605(3) 0.6030(5) -0.1158(3) 0.0485(17) Uani 1 1 d .
H46A H 0.6382 0.6098 -0.1556 0.058 Uiso 1 1 calc R
C47 C 0.7783(4) 0.6982(5) 0.7396(3) 0.058(2) Uani 1 1 d .
H47A H 0.8202 0.6738 0.7586 0.070 Uiso 1 1 calc R
C48 C 0.3990(3) 0.2909(4) -0.0257(3) 0.0390(15) Uani 1 1 d .
H48A H 0.3777 0.2671 -0.0051 0.047 Uiso 1 1 calc R
C49 C 0.6561(4) 0.7677(5) 0.6833(3) 0.0525(19) Uani 1 1 d .
H49A H 0.6140 0.7918 0.6654 0.063 Uiso 1 1 calc R
C50 C 0.6583(3) 0.7515(4) 0.5872(3) 0.0343(13) Uani 1 1 d .
C51 C 0.5124(3) 0.8500(4) 0.4769(3) 0.0353(14) Uani 1 1 d .
C52 C 0.6550(3) 0.6751(4) 0.4070(3) 0.0441(16) Uani 1 1 d .
H52A H 0.6158 0.7039 0.3859 0.053 Uiso 1 1 calc R
C53 C 0.6864(4) 0.7567(5) 0.7419(3) 0.0562(19) Uani 1 1 d .
H53A H 0.6633 0.7740 0.7629 0.067 Uiso 1 1 calc R
C54 C 0.7124(3) 0.5370(5) 0.1773(3) 0.0531(19) Uani 1 1 d .
H54A H 0.7290 0.5667 0.1555 0.064 Uiso 1 1 calc R
C55 C 0.4885(3) 0.3725(4) -0.0255(3) 0.0341(13) Uani 1 1 d .
C56 C 0.4221(3) 0.9291(4) 0.4790(3) 0.0449(16) Uani 1 1 d .
H56A H 0.4019 0.9536 0.5002 0.054 Uiso 1 1 calc R
C57 C 0.7415(4) 0.5433(5) 0.2366(3) 0.059(2) Uani 1 1 d .
H57A H 0.7776 0.5782 0.2540 0.071 Uiso 1 1 calc R
C58 C 0.6330(4) 0.4460(5) 0.1844(3) 0.0519(19) Uani 1 1 d .
H58A H 0.5944 0.4147 0.1681 0.062 Uiso 1 1 calc R
C59 C 0.6677(4) 0.4546(6) 0.2438(3) 0.066(2) Uani 1 1 d .
H59A H 0.6526 0.4248 0.2667 0.079 Uiso 1 1 calc R
C60 C 0.6853(4) 0.6310(5) 0.3790(3) 0.0497(17) Uani 1 1 d .
H60A H 0.6642 0.6286 0.3389 0.060 Uiso 1 1 calc R
N1 N 0.3715(3) 0.2809(3) -0.0825(2) 0.0401(13) Uani 1 1 d .
N2 N 0.7216(3) 0.6345(3) -0.0889(2) 0.0425(13) Uani 1 1 d .
N3 N 0.7203(3) 0.5014(4) 0.2706(3) 0.0558(16) Uani 1 1 d .
N4 N 0.5739(2) 0.4610(3) -0.0279(2) 0.0350(11) Uani 1 1 d .
N5 N 0.6557(3) 0.5171(3) 0.0583(2) 0.0381(12) Uani 1 1 d .
N6 N 0.5749(3) 0.4272(3) 0.0626(2) 0.0369(12) Uani 1 1 d .
N7 N 0.7436(3) 0.5914(3) 0.4068(2) 0.0432(13) Uani 1 1 d .
N8 N 0.7463(3) 0.7232(4) 0.7710(3) 0.0523(15) Uani 1 1 d .
N9 N 0.3922(3) 0.9358(3) 0.4220(2) 0.0405(13) Uani 1 1 d .
N10 N 0.5973(2) 0.7611(3) 0.4729(2) 0.0337(11) Uani 1 1 d .
N11 N 0.6858(3) 0.7129(3) 0.5583(2) 0.0378(12) Uani 1 1 d .
N12 N 0.6035(3) 0.7988(3) 0.5639(2) 0.0399(12) Uani 1 1 d .
Mo1 Mo 0.0000 0.21691(6) -0.2500 0.0590(3) Uani 1 2 d S
Mo2 Mo 0.11211(3) 0.34018(3) -0.13938(2) 0.03653(17) Uani 1 1 d .
Mo3 Mo 0.11618(3) 0.54012(4) -0.14303(2) 0.03822(17) Uani 1 1 d .
Mo4 Mo 0.0000 0.65270(6) -0.2500 0.0538(3) Uani 1 2 d S
Mo5 Mo 0.05179(3) 0.44329(3) -0.29069(2) 0.03487(17) Uani 1 1 d .
O1 O -0.0199(5) 0.1561(6) -0.2063(6) 0.181(6) Uani 1 1 d .
O2 O 0.0784(3) 0.2665(3) -0.2059(2) 0.0620(14) Uani 1 1 d .
O3 O 0.1925(3) 0.3327(4) -0.1305(3) 0.0705(16) Uani 1 1 d .
O4 O 0.1104(3) 0.2797(4) -0.0866(3) 0.0798(18) Uani 1 1 d .
O5 O 0.1101(3) 0.4402(3) -0.1068(2) 0.0585(14) Uani 1 1 d .
O6 O 0.0887(3) 0.4367(3) -0.2146(2) 0.0656(15) Uani 1 1 d .
O7 O 0.0033(3) 0.3560(4) -0.3225(3) 0.0694(16) Uani 1 1 d .
O8 O 0.1094(3) 0.4481(3) -0.3177(3) 0.0689(16) Uani 1 1 d .
O9 O 0.1991(3) 0.5377(4) -0.1292(3) 0.0783(18) Uani 1 1 d .
O10 O 0.1145(3) 0.6022(4) -0.0926(3) 0.0798(19) Uani 1 1 d .
O11 O 0.0862(3) 0.6070(3) -0.2112(2) 0.0632(14) Uani 1 1 d .
O12 O -0.0004(2) 0.5314(3) -0.3149(3) 0.0621(14) Uani 1 1 d .
O13 O -0.0092(4) 0.7126(4) -0.2010(3) 0.092(2) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mo Mo -1.6832 0.6857 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
N2 Ag1 N8 129.0(2) 3_445 3_444
N2 Ag1 N1 124.1(2) 3_445 .
N8 Ag1 N1 106.8(2) 3_444 .
N9 Ag2 N3 134.5(2) 3_545 .
N9 Ag2 N7 123.0(2) 3_545 .
N3 Ag2 N7 102.3(2) . .
N10 C3 N11 124.6(5) . .
N10 C3 C33 119.5(5) . .
N11 C3 C33 115.9(5) . .
N9 C15 C37 122.8(6) . .
C31 C16 C46 118.4(6) . .
N5 C23 N4 125.6(5) . .
N5 C23 C31 115.9(5) . .
N4 C23 C31 118.5(5) . .
N10 C24 N12 123.8(6) . .
N10 C24 C51 118.1(5) . .
N12 C24 C51 118.0(5) . .
N7 C25 C29 123.8(6) . .
C56 C26 C51 118.6(6) . .
N1 C27 C43 123.8(6) . .
C25 C29 C33 119.1(6) . .
C16 C31 C32 117.6(6) . .
C16 C31 C23 122.4(5) . .
C32 C31 C23 120.0(5) . .
C41 C32 C31 119.6(6) . .
C52 C33 C29 118.2(6) . .
C52 C33 C3 122.8(5) . .
C29 C33 C3 119.0(5) . .
N6 C35 N5 124.5(5) . .
N6 C35 C36 119.8(5) . .
N5 C35 C36 115.6(5) . .
C54 C36 C58 118.4(6) . .
C54 C36 C35 120.9(6) . .
C58 C36 C35 120.7(6) . .
C15 C37 C51 120.2(6) . .
N4 C38 N6 125.1(5) . .
N4 C38 C55 117.4(5) . .
N6 C38 C55 117.5(5) . .
C44 C39 C49 118.6(6) . .
C44 C39 C50 121.2(6) . .
C49 C39 C50 120.2(6) . .
C48 C40 C55 118.0(6) . .
N2 C41 C32 123.9(6) . .
C27 C43 C55 119.3(6) . .
C39 C44 C47 119.0(6) . .
N2 C46 C16 125.0(6) . .
N8 C47 C44 123.1(7) . .
N1 C48 C40 124.7(6) . .
C53 C49 C39 118.2(7) . .
N11 C50 N12 125.5(6) . .
N11 C50 C39 117.5(5) . .
N12 C50 C39 116.9(5) . .
C37 C51 C26 117.6(6) . .
C37 C51 C24 121.2(5) . .
C26 C51 C24 121.2(6) . .
C33 C52 C60 119.1(6) . .
N8 C53 C49 124.9(7) . .
C36 C54 C57 119.1(7) . .
C43 C55 C40 117.5(6) . .
C43 C55 C38 121.6(5) . .
C40 C55 C38 121.0(5) . .
N9 C56 C26 123.4(6) . .
N3 C57 C54 123.3(7) . .
C59 C58 C36 117.4(7) . .
N3 C59 C58 125.5(7) . .
N7 C60 C52 123.4(6) . .
C48 N1 C27 116.6(6) . .
C48 N1 Ag1 123.2(4) . .
C27 N1 Ag1 120.2(4) . .
C46 N2 C41 115.5(5) . .
C46 N2 Ag1 124.8(5) . 3
C41 N2 Ag1 119.6(4) . 3
C59 N3 C57 116.1(6) . .
C59 N3 Ag2 129.0(5) . .
C57 N3 Ag2 113.6(5) . .
C23 N4 C38 114.5(5) . .
C23 N5 C35 115.0(5) . .
C35 N6 C38 115.3(5) . .
C60 N7 C25 116.4(5) . .
C60 N7 Ag2 127.7(4) . .
C25 N7 Ag2 115.2(4) . .
C53 N8 C47 116.2(6) . .
C53 N8 Ag1 112.8(4) . 3_556
C47 N8 Ag1 130.8(5) . 3_556
C56 N9 C15 117.3(5) . .
C56 N9 Ag2 127.5(4) . 3_455
C15 N9 Ag2 115.2(4) . 3_455
C3 N10 C24 116.2(5) . .
C50 N11 C3 115.0(5) . .
C24 N12 C50 114.7(5) . .
O1 Mo1 O1 106.6(10) 2_554 .
O1 Mo1 O2 103.9(4) 2_554 .
O1 Mo1 O2 107.9(4) . .
O1 Mo1 O2 107.9(4) 2_554 2_554
O1 Mo1 O2 103.9(4) . 2_554
O2 Mo1 O2 125.3(4) . 2_554
O3 Mo2 O4 103.1(3) . .
O3 Mo2 O5 103.2(3) . .
O4 Mo2 O5 99.4(3) . .
O3 Mo2 O2 93.1(3) . .
O4 Mo2 O2 100.8(3) . .
O5 Mo2 O2 150.3(2) . .
O3 Mo2 O7 164.3(3) . 2_554
O4 Mo2 O7 90.6(3) . 2_554
O5 Mo2 O7 81.7(2) . 2_554
O2 Mo2 O7 76.6(2) . 2_554
O3 Mo2 O6 90.5(3) . .
O4 Mo2 O6 165.9(3) . .
O5 Mo2 O6 73.7(2) . .
O2 Mo2 O6 81.6(2) . .
O7 Mo2 O6 76.4(2) 2_554 .
O10 Mo3 O9 103.4(3) . .
O10 Mo3 O11 103.2(3) . .
O9 Mo3 O11 96.9(3) . .
O10 Mo3 O5 97.8(3) . .
O9 Mo3 O5 99.6(3) . .
O11 Mo3 O5 149.4(2) . .
O10 Mo3 O12 90.9(2) . 2_554
O9 Mo3 O12 164.9(3) . 2_554
O11 Mo3 O12 74.5(2) . 2_554
O5 Mo3 O12 83.2(2) . 2_554
O10 Mo3 O6 163.0(3) . .
O9 Mo3 O6 92.2(3) . .
O11 Mo3 O6 81.3(2) . .
O5 Mo3 O6 72.5(2) . .
O12 Mo3 O6 74.4(2) 2_554 .
O13 Mo4 O13 107.0(5) . 2_554
O13 Mo4 O11 102.7(3) . 2_554
O13 Mo4 O11 105.2(3) 2_554 2_554
O13 Mo4 O11 105.2(3) . .
O13 Mo4 O11 102.7(3) 2_554 .
O11 Mo4 O11 132.1(3) 2_554 .
O8 Mo5 O6 112.7(3) . .
O8 Mo5 O7 104.9(3) . .
O6 Mo5 O7 110.8(3) . .
O8 Mo5 O12 107.4(2) . .
O6 Mo5 O12 110.7(3) . .
O7 Mo5 O12 110.1(3) . .
Mo1 O2 Mo2 137.0(3) . .
Mo2 O5 Mo3 122.3(3) . .
Mo5 O6 Mo2 140.3(3) . .
Mo5 O6 Mo3 130.1(3) . .
Mo2 O6 Mo3 88.47(18) . .
Mo5 O7 Mo2 128.3(3) . 2_554
Mo4 O11 Mo3 125.9(3) . .
Mo5 O12 Mo3 128.6(3) . 2_554
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ag1 N2 2.269(5) 3_445
Ag1 N8 2.303(6) 3_444
Ag1 N1 2.312(5) .
Ag2 N9 2.276(5) 3_545
Ag2 N3 2.317(6) .
Ag2 N7 2.341(5) .
C3 N10 1.316(7) .
C3 N11 1.349(8) .
C3 C33 1.497(8) .
C15 N9 1.351(8) .
C15 C37 1.374(9) .
C16 C31 1.361(9) .
C16 C46 1.376(9) .
C23 N5 1.323(8) .
C23 N4 1.333(8) .
C23 C31 1.495(8) .
C24 N10 1.336(8) .
C24 N12 1.343(8) .
C24 C51 1.484(9) .
C25 N7 1.337(8) .
C25 C29 1.372(9) .
C26 C56 1.392(9) .
C26 C51 1.402(9) .
C27 N1 1.339(8) .
C27 C43 1.374(9) .
C29 C33 1.381(8) .
C31 C32 1.387(8) .
C32 C41 1.357(9) .
C33 C52 1.375(9) .
C35 N6 1.315(8) .
C35 N5 1.354(8) .
C35 C36 1.476(8) .
C36 C54 1.387(9) .
C36 C58 1.382(9) .
C37 C51 1.370(9) .
C38 N4 1.331(8) .
C38 N6 1.346(8) .
C38 C55 1.485(8) .
C39 C44 1.367(9) .
C39 C49 1.384(9) .
C39 C50 1.498(9) .
C40 C48 1.383(9) .
C40 C55 1.404(8) .
C41 N2 1.329(9) .
C43 C55 1.393(9) .
C44 C47 1.389(10) .
C46 N2 1.326(8) .
C47 N8 1.342(9) .
C48 N1 1.326(8) .
C49 C53 1.369(10) .
C50 N11 1.309(8) .
C50 N12 1.347(8) .
C52 C60 1.380(9) .
C53 N8 1.325(10) .
C54 C57 1.376(10) .
C56 N9 1.324(9) .
C57 N3 1.348(10) .
C58 C59 1.387(10) .
C59 N3 1.317(10) .
C60 N7 1.343(9) .
N2 Ag1 2.269(5) 3
N8 Ag1 2.303(6) 3_556
N9 Ag2 2.276(5) 3_455
Mo1 O1 1.700(9) 2_554
Mo1 O1 1.700(9) .
Mo1 O2 1.805(5) .
Mo1 O2 1.805(5) 2_554
Mo2 O3 1.686(5) .
Mo2 O4 1.700(6) .
Mo2 O5 1.876(5) .
Mo2 O2 1.971(5) .
Mo2 O7 2.306(5) 2_554
Mo2 O6 2.394(5) .
Mo3 O10 1.669(6) .
Mo3 O9 1.699(6) .
Mo3 O11 1.936(6) .
Mo3 O5 1.942(5) .
Mo3 O12 2.301(5) 2_554
Mo3 O6 2.401(5) .
Mo4 O13 1.684(7) .
Mo4 O13 1.684(7) 2_554
Mo4 O11 1.881(5) 2_554
Mo4 O11 1.881(5) .
Mo5 O8 1.684(5) .
Mo5 O6 1.764(5) .
Mo5 O7 1.784(6) .
Mo5 O12 1.804(6) .
O7 Mo2 2.306(5) 2_554
O12 Mo3 2.301(5) 2_554
