#------------------------------------------------------------------------------
#$Date: 2016-03-25 17:07:58 +0200 (Fri, 25 Mar 2016) $
#$Revision: 180004 $
#$URL: svn://www.crystallography.net/cod/cif/7/02/98/7029805.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7029805
loop_
_publ_author_name
'Zhang, Lei'
'Kuang, Xiaofei'
'Wu, Xiaoyuan'
'Yang, Wenbin'
'Lu, Canzhong'
_publ_section_title
;
 Supramolecular interactions induced hinge-like motion of a metal-organic
 framework accompanied by anisotropic thermal expansion.
;
_journal_issue                   19
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              7146
_journal_page_last               7152
_journal_paper_doi               10.1039/c3dt53580k
_journal_volume                  43
_journal_year                    2014
_chemical_formula_sum            'C72 H48 Ag4 Mo8 N24 O26'
_chemical_formula_weight         2864.34
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 115.265(5)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   22.0870(8)
_cell_length_b                   16.3172(4)
_cell_length_c                   25.6279(10)
_cell_measurement_reflns_used    15701
_cell_measurement_temperature    160.01(10)
_cell_measurement_theta_max      29.1600
_cell_measurement_theta_min      3.2270
_cell_volume                     8352.7(6)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      160.01(10)
_diffrn_detector_area_resol_mean 10.3503
_diffrn_measured_fraction_theta_full 0.958
_diffrn_measured_fraction_theta_max 0.958
_diffrn_measurement_device_type  'SuperNova, Dual, Cu at zero, Atlas'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  mirror
_diffrn_radiation_source         'SuperNova (Mo) X-ray Source'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0276
_diffrn_reflns_av_sigmaI/netI    0.0332
_diffrn_reflns_limit_h_max       26
_diffrn_reflns_limit_h_min       -26
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_k_min       -14
_diffrn_reflns_limit_l_max       30
_diffrn_reflns_limit_l_min       -27
_diffrn_reflns_number            17987
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         3.07
_exptl_absorpt_coefficient_mu    2.165
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.68046
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            brown
_exptl_crystal_density_diffrn    2.278
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block-like
_exptl_crystal_F_000             5520
_exptl_crystal_size_max          0.31
_exptl_crystal_size_mid          0.14
_exptl_crystal_size_min          0.10
_refine_diff_density_max         2.008
_refine_diff_density_min         -1.857
_refine_diff_density_rms         0.143
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.051
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     605
_refine_ls_number_reflns         7059
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.051
_refine_ls_R_factor_all          0.0416
_refine_ls_R_factor_gt           0.0348
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0438P)²+77.3691P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0898
_refine_ls_wR_factor_ref         0.0950
_reflns_number_gt                6175
_reflns_number_total             7059
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c3dt53580k2.cif
_cod_data_source_block           B_160K
_cod_depositor_comments
;Adding full bibliography for
 ./tmp-cod-update-bibliographies-12899/cifs/7029805.cif.
;
_cod_original_cell_volume        8352.7(5)
_cod_original_sg_symbol_H-M      C2/c
_cod_database_code               7029805
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Ag1 Ag -0.17704(2) 0.25212(3) -0.132771(18) 0.02484(12) Uani 1 1 d .
Ag2 Ag 0.34397(2) 0.45717(3) 0.367761(18) 0.02273(12) Uani 1 1 d .
C17 C 0.6237(2) 0.2568(3) 0.5024(2) 0.0136(11) Uani 1 1 d .
C21 C 0.7353(3) 0.0652(3) 0.3882(2) 0.0183(11) Uani 1 1 d .
H21A H 0.7134 0.0586 0.3484 0.022 Uiso 1 1 calc R
C22 C 0.2776(3) 0.6377(3) 0.0089(2) 0.0188(11) Uani 1 1 d .
H22A H 0.2985 0.6340 0.0489 0.023 Uiso 1 1 calc R
C26 C 0.0033(3) 0.3837(3) -0.0035(2) 0.0157(11) Uani 1 1 d .
H26A H 0.0228 0.3822 0.0366 0.019 Uiso 1 1 calc R
C27 C -0.0565(3) 0.3433(3) -0.0352(2) 0.0183(11) Uani 1 1 d .
H27A H -0.0767 0.3152 -0.0152 0.022 Uiso 1 1 calc R
C28 C 0.2196(2) 0.6521(3) -0.1081(2) 0.0166(11) Uani 1 1 d .
H28A H 0.1996 0.6565 -0.1481 0.020 Uiso 1 1 calc R
C29 C 0.5332(3) 0.3121(3) 0.4112(2) 0.0193(12) Uani 1 1 d .
H29A H 0.5550 0.2912 0.3900 0.023 Uiso 1 1 calc R
C30 C 0.0977(2) 0.4699(3) 0.0010(2) 0.0148(11) Uani 1 1 d .
C31 C 0.7981(2) 0.0840(3) 0.5049(2) 0.0157(11) Uani 1 1 d .
H31A H 0.8204 0.0883 0.5449 0.019 Uiso 1 1 calc R
C33 C 0.5598(2) 0.3019(3) 0.4701(2) 0.0156(11) Uani 1 1 d .
C35 C 0.1792(3) 0.4563(4) 0.1815(2) 0.0238(13) Uani 1 1 d .
H35A H 0.1352 0.4388 0.1616 0.029 Uiso 1 1 calc R
C36 C 0.0334(2) 0.4262(3) -0.0329(2) 0.0136(10) Uani 1 1 d .
C37 C 0.7098(3) 0.2269(3) 0.5876(2) 0.0156(11) Uani 1 1 d .
C38 C 0.7433(3) 0.2373(3) 0.6514(2) 0.0172(11) Uani 1 1 d .
C39 C 0.5259(3) 0.3352(3) 0.5001(2) 0.0192(11) Uani 1 1 d .
H39A H 0.5430 0.3305 0.5400 0.023 Uiso 1 1 calc R
C40 C 0.1804(3) 0.5023(3) 0.0884(2) 0.0167(11) Uani 1 1 d .
C41 C 0.1825(2) 0.5517(3) 0.0067(2) 0.0147(11) Uani 1 1 d .
C42 C 0.8260(3) 0.0408(3) 0.4741(2) 0.0164(11) Uani 1 1 d .
H42A H 0.8680 0.0176 0.4944 0.020 Uiso 1 1 calc R
C43 C 0.2151(2) 0.6013(3) -0.0226(2) 0.0151(11) Uani 1 1 d .
C44 C 0.1855(3) 0.6098(3) -0.0818(2) 0.0151(11) Uani 1 1 d .
H44A H 0.1435 0.5875 -0.1037 0.018 Uiso 1 1 calc R
C45 C 0.7362(2) 0.1209(3) 0.4749(2) 0.0141(11) Uani 1 1 d .
C46 C 0.3079(3) 0.5048(4) 0.2427(2) 0.0252(13) Uani 1 1 d .
H46A H 0.3521 0.5212 0.2634 0.030 Uiso 1 1 calc R
C47 C 0.4666(3) 0.3753(4) 0.4693(2) 0.0222(12) Uani 1 1 d .
H47A H 0.4443 0.3976 0.4896 0.027 Uiso 1 1 calc R
C48 C 0.7056(2) 0.1721(3) 0.5052(2) 0.0147(11) Uani 1 1 d .
C49 C 0.3081(3) 0.6797(3) -0.0211(2) 0.0200(12) Uani 1 1 d .
H49A H 0.3497 0.7036 -0.0001 0.024 Uiso 1 1 calc R
C50 C 0.4728(3) 0.3544(3) 0.3840(2) 0.0193(12) Uani 1 1 d .
H50A H 0.4553 0.3621 0.3443 0.023 Uiso 1 1 calc R
C51 C -0.0564(3) 0.3835(3) -0.1204(2) 0.0217(12) Uani 1 1 d .
H51A H -0.0761 0.3824 -0.1606 0.026 Uiso 1 1 calc R
C52 C 0.0023(3) 0.4272(3) -0.0929(2) 0.0196(12) Uani 1 1 d .
H52A H 0.0205 0.4565 -0.1139 0.023 Uiso 1 1 calc R
C53 C 0.7040(3) 0.1103(3) 0.4152(2) 0.0175(11) Uani 1 1 d .
H53A H 0.6621 0.1334 0.3939 0.021 Uiso 1 1 calc R
C54 C 0.2782(3) 0.5166(3) 0.1833(2) 0.0219(12) Uani 1 1 d .
H54A H 0.3022 0.5402 0.1648 0.026 Uiso 1 1 calc R
C55 C 0.2123(3) 0.4924(3) 0.1520(2) 0.0191(11) Uani 1 1 d .
C56 C 0.8283(3) 0.2071(4) 0.7446(2) 0.0285(14) Uani 1 1 d .
H56A H 0.8677 0.1795 0.7672 0.034 Uiso 1 1 calc R
C57 C 0.7154(3) 0.2894(4) 0.6781(2) 0.0247(13) Uani 1 1 d .
H57A H 0.6773 0.3198 0.6563 0.030 Uiso 1 1 calc R
C58 C 0.8023(3) 0.1975(3) 0.6851(2) 0.0220(12) Uani 1 1 d .
H58A H 0.8240 0.1651 0.6685 0.026 Uiso 1 1 calc R
C59 C 0.2119(3) 0.4465(4) 0.2404(2) 0.0256(13) Uani 1 1 d .
H59A H 0.1890 0.4221 0.2595 0.031 Uiso 1 1 calc R
C60 C 0.7450(3) 0.2953(4) 0.7372(3) 0.0267(13) Uani 1 1 d .
H60A H 0.7257 0.3300 0.7547 0.032 Uiso 1 1 calc R
N1 N -0.0867(2) 0.3426(3) -0.09278(19) 0.0187(10) Uani 1 1 d .
N2 N 0.2800(2) 0.6872(3) -0.0786(2) 0.0181(10) Uani 1 1 d .
N3 N 0.2759(2) 0.4709(3) 0.2717(2) 0.0255(11) Uani 1 1 d .
N4 N 0.1228(2) 0.4627(3) 0.05890(18) 0.0169(9) Uani 1 1 d .
N5 N 0.1263(2) 0.5112(3) -0.02685(18) 0.0146(9) Uani 1 1 d .
N6 N 0.2115(2) 0.5499(3) 0.06485(19) 0.0174(10) Uani 1 1 d .
N7 N 0.4390(2) 0.3843(3) 0.41210(19) 0.0199(10) Uani 1 1 d .
N8 N 0.7957(2) 0.0303(3) 0.41656(18) 0.0154(9) Uani 1 1 d .
N9 N 0.8004(2) 0.2536(3) 0.7713(2) 0.0244(11) Uani 1 1 d .
N10 N 0.6480(2) 0.2105(3) 0.47260(18) 0.0156(9) Uani 1 1 d .
N11 N 0.7382(2) 0.1775(3) 0.56314(18) 0.0161(9) Uani 1 1 d .
N12 N 0.6529(2) 0.2681(3) 0.55923(18) 0.0165(9) Uani 1 1 d .
Mo1 Mo 0.5000 0.46036(5) 0.2500 0.03136(19) Uani 1 2 d S
Mo2 Mo 0.49868(2) 0.58819(3) 0.360442(19) 0.01540(12) Uani 1 1 d .
Mo3 Mo 0.48952(2) 0.79183(3) 0.356363(19) 0.01579(12) Uani 1 1 d .
Mo4 Mo 0.5000 0.90515(5) 0.2500 0.02659(18) Uani 1 2 d S
Mo5 Mo 0.40861(2) 0.69328(3) 0.20926(2) 0.01532(12) Uani 1 1 d .
O1 O 0.5618(4) 0.3962(4) 0.2947(3) 0.091(3) Uani 1 1 d .
O2 O 0.4650(2) 0.5127(3) 0.29310(18) 0.0318(10) Uani 1 1 d .
O3 O 0.5524(2) 0.5237(3) 0.41262(19) 0.0355(10) Uani 1 1 d .
O4 O 0.4267(2) 0.5823(3) 0.36940(18) 0.0338(10) Uani 1 1 d .
O5 O 0.5334(2) 0.6898(3) 0.39344(17) 0.0282(9) Uani 1 1 d .
O6 O 0.4484(2) 0.6851(3) 0.28598(18) 0.0360(11) Uani 1 1 d .
O7 O 0.4249(2) 0.6036(3) 0.1773(2) 0.0357(11) Uani 1 1 d .
O8 O 0.3240(2) 0.6990(3) 0.1835(2) 0.0356(11) Uani 1 1 d .
O9 O 0.4209(2) 0.7871(3) 0.37061(19) 0.0343(10) Uani 1 1 d .
O10 O 0.5407(2) 0.8573(3) 0.40609(18) 0.0343(10) Uani 1 1 d .
O11 O 0.4503(2) 0.8586(3) 0.28769(18) 0.0316(10) Uani 1 1 d .
O12 O 0.4368(2) 0.7828(3) 0.18538(18) 0.0297(10) Uani 1 1 d .
O13 O 0.5568(2) 0.9668(3) 0.3001(2) 0.0422(12) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mo Mo -1.6832 0.6857 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
N2 Ag1 N9 135.25(17) 3_445 1_454
N2 Ag1 N1 122.17(16) 3_445 .
N9 Ag1 N1 102.58(16) 1_454 .
N7 Ag2 N3 129.69(16) . .
N7 Ag2 N8 123.33(16) . 3_455
N3 Ag2 N8 106.95(16) . 3_455
N12 C17 N10 125.3(5) . .
N12 C17 C33 116.2(4) . .
N10 C17 C33 118.5(4) . .
N8 C21 C53 123.3(5) . .
C43 C22 C49 118.6(5) . .
C36 C26 C27 118.6(5) . .
N1 C27 C26 123.5(5) . .
N2 C28 C44 123.4(5) . .
C33 C29 C50 118.4(5) . .
N5 C30 N4 124.9(5) . .
N5 C30 C36 119.0(4) . .
N4 C30 C36 116.1(4) . .
C42 C31 C45 118.5(5) . .
C29 C33 C39 118.8(5) . .
C29 C33 C17 121.8(5) . .
C39 C33 C17 119.4(5) . .
C59 C35 C55 119.8(5) . .
C26 C36 C52 118.7(5) . .
C26 C36 C30 118.8(4) . .
C52 C36 C30 122.4(5) . .
N11 C37 N12 124.9(5) . .
N11 C37 C38 118.3(5) . .
N12 C37 C38 116.8(4) . .
C58 C38 C57 118.7(5) . .
C58 C38 C37 121.8(5) . .
C57 C38 C37 119.5(5) . .
C47 C39 C33 118.2(5) . .
N4 C40 N6 124.9(5) . .
N4 C40 C55 117.4(5) . .
N6 C40 C55 117.7(5) . .
N5 C41 N6 124.7(4) . .
N5 C41 C43 117.3(4) . .
N6 C41 C43 118.0(4) . .
N8 C42 C31 123.8(5) . .
C44 C43 C22 118.7(5) . .
C44 C43 C41 120.5(5) . .
C22 C43 C41 120.8(5) . .
C43 C44 C28 118.9(5) . .
C31 C45 C53 118.3(5) . .
C31 C45 C48 120.9(5) . .
C53 C45 C48 120.8(5) . .
N3 C46 C54 123.4(5) . .
N7 C47 C39 124.2(5) . .
N10 C48 N11 125.0(5) . .
N10 C48 C45 117.3(5) . .
N11 C48 C45 117.7(4) . .
N2 C49 C22 123.0(5) . .
N7 C50 C29 123.2(5) . .
N1 C51 C52 123.9(5) . .
C51 C52 C36 118.2(5) . .
C21 C53 C45 119.1(5) . .
C55 C54 C46 118.7(5) . .
C54 C55 C35 118.3(5) . .
C54 C55 C40 119.5(5) . .
C35 C55 C40 122.2(5) . .
N9 C56 C58 124.1(5) . .
C60 C57 C38 118.8(5) . .
C38 C58 C56 118.1(5) . .
N3 C59 C35 122.7(5) . .
N9 C60 C57 123.6(5) . .
C27 N1 C51 117.0(5) . .
C27 N1 Ag1 114.8(3) . .
C51 N1 Ag1 127.4(4) . .
C49 N2 C28 117.4(4) . .
C49 N2 Ag1 127.0(3) . 3
C28 N2 Ag1 115.5(3) . 3
C46 N3 C59 117.1(5) . .
C46 N3 Ag2 112.2(4) . .
C59 N3 Ag2 130.5(4) . .
C40 N4 C30 115.1(4) . .
C30 N5 C41 115.4(4) . .
C40 N6 C41 114.8(4) . .
C50 N7 C47 117.1(5) . .
C50 N7 Ag2 122.5(4) . .
C47 N7 Ag2 120.2(3) . .
C21 N8 C42 117.0(4) . .
C21 N8 Ag2 120.7(3) . 3_545
C42 N8 Ag2 122.3(3) . 3_545
C56 N9 C60 116.5(5) . .
C56 N9 Ag1 127.4(4) . 1_656
C60 N9 Ag1 115.0(4) . 1_656
C17 N10 C48 114.4(4) . .
C37 N11 C48 114.9(4) . .
C17 N12 C37 115.5(4) . .
O1 Mo1 O1 104.7(6) . 2_655
O1 Mo1 O2 105.7(2) . 2_655
O1 Mo1 O2 107.8(3) 2_655 2_655
O1 Mo1 O2 107.8(3) . .
O1 Mo1 O2 105.7(2) 2_655 .
O2 Mo1 O2 123.7(3) 2_655 .
O4 Mo2 O3 103.6(2) . .
O4 Mo2 O5 102.42(19) . .
O3 Mo2 O5 100.2(2) . .
O4 Mo2 O2 93.29(19) . .
O3 Mo2 O2 100.0(2) . .
O5 Mo2 O2 150.58(17) . .
O4 Mo2 O7 164.17(19) . 2_655
O3 Mo2 O7 90.43(18) . 2_655
O5 Mo2 O7 81.97(17) . 2_655
O2 Mo2 O7 76.76(17) . 2_655
O4 Mo2 O6 90.14(19) . .
O3 Mo2 O6 166.17(19) . .
O5 Mo2 O6 74.48(16) . .
O2 Mo2 O6 80.84(16) . .
O7 Mo2 O6 76.27(16) 2_655 .
O10 Mo3 O9 103.8(2) . .
O10 Mo3 O11 103.1(2) . .
O9 Mo3 O11 97.26(19) . .
O10 Mo3 O5 98.0(2) . .
O9 Mo3 O5 99.10(19) . .
O11 Mo3 O5 149.20(17) . .
O10 Mo3 O12 90.70(17) . 2_655
O9 Mo3 O12 164.92(19) . 2_655
O11 Mo3 O12 75.18(16) . 2_655
O5 Mo3 O12 82.52(16) . 2_655
O10 Mo3 O6 162.40(19) . .
O9 Mo3 O6 92.40(19) . .
O11 Mo3 O6 81.11(16) . .
O5 Mo3 O6 72.31(16) . .
O12 Mo3 O6 73.71(16) 2_655 .
O13 Mo4 O13 107.0(3) . 2_655
O13 Mo4 O11 104.7(2) . .
O13 Mo4 O11 102.7(2) 2_655 .
O13 Mo4 O11 102.7(2) . 2_655
O13 Mo4 O11 104.7(2) 2_655 2_655
O11 Mo4 O11 133.0(3) . 2_655
O8 Mo5 O6 112.0(2) . .
O8 Mo5 O7 105.7(2) . .
O6 Mo5 O7 110.1(2) . .
O8 Mo5 O12 107.86(19) . .
O6 Mo5 O12 111.0(2) . .
O7 Mo5 O12 110.14(19) . .
Mo1 O2 Mo2 136.3(2) . .
Mo2 O5 Mo3 120.8(2) . .
Mo5 O6 Mo2 141.5(2) . .
Mo5 O6 Mo3 128.8(2) . .
Mo2 O6 Mo3 88.96(14) . .
Mo5 O7 Mo2 127.7(2) . 2_655
Mo4 O11 Mo3 123.7(2) . .
Mo5 O12 Mo3 128.8(2) . 2_655
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ag1 N2 2.252(4) 3_445
Ag1 N9 2.292(5) 1_454
Ag1 N1 2.338(4) .
Ag2 N7 2.253(4) .
Ag2 N3 2.282(5) .
Ag2 N8 2.294(4) 3_455
C17 N12 1.330(7) .
C17 N10 1.338(6) .
C17 C33 1.491(7) .
C21 N8 1.343(7) .
C21 C53 1.380(7) .
C22 C43 1.400(7) .
C22 C49 1.398(7) .
C26 C36 1.385(7) .
C26 C27 1.387(7) .
C27 N1 1.336(7) .
C28 N2 1.349(7) .
C28 C44 1.389(7) .
C29 C33 1.377(7) .
C29 C50 1.397(8) .
C30 N5 1.321(6) .
C30 N4 1.350(7) .
C30 C36 1.493(7) .
C31 C42 1.383(7) .
C31 C45 1.389(7) .
C33 C39 1.393(7) .
C35 C59 1.376(8) .
C35 C55 1.387(8) .
C36 C52 1.391(7) .
C37 N11 1.330(7) .
C37 N12 1.335(7) .
C37 C38 1.490(7) .
C38 C58 1.380(8) .
C38 C57 1.390(8) .
C39 C47 1.372(8) .
C40 N4 1.337(7) .
C40 N6 1.339(7) .
C40 C55 1.482(7) .
C41 N5 1.345(7) .
C41 N6 1.347(7) .
C41 C43 1.483(7) .
C42 N8 1.345(7) .
C43 C44 1.378(7) .
C45 C53 1.395(7) .
C45 C48 1.484(7) .
C46 N3 1.342(7) .
C46 C54 1.391(8) .
C47 N7 1.334(7) .
C48 N10 1.343(7) .
C48 N11 1.349(7) .
C49 N2 1.339(7) .
C50 N7 1.331(7) .
C51 N1 1.342(7) .
C51 C52 1.380(8) .
C54 C55 1.387(8) .
C56 N9 1.335(7) .
C56 C58 1.389(8) .
C57 C60 1.373(8) .
C59 N3 1.355(7) .
C60 N9 1.345(8) .
N2 Ag1 2.252(4) 3
N8 Ag2 2.294(4) 3_545
N9 Ag1 2.292(5) 1_656
Mo1 O1 1.714(6) .
Mo1 O1 1.714(6) 2_655
Mo1 O2 1.809(4) 2_655
Mo1 O2 1.809(4) .
Mo2 O4 1.703(4) .
Mo2 O3 1.717(4) .
Mo2 O5 1.870(4) .
Mo2 O2 1.989(4) .
Mo2 O7 2.290(4) 2_655
Mo2 O6 2.359(4) .
Mo3 O10 1.678(4) .
Mo3 O9 1.707(4) .
Mo3 O11 1.932(4) .
Mo3 O5 1.957(4) .
Mo3 O12 2.303(4) 2_655
Mo3 O6 2.391(4) .
Mo4 O13 1.690(5) .
Mo4 O13 1.690(5) 2_655
Mo4 O11 1.903(4) .
Mo4 O11 1.903(4) 2_655
Mo5 O8 1.698(4) .
Mo5 O6 1.784(4) .
Mo5 O7 1.787(4) .
Mo5 O12 1.795(4) .
O7 Mo2 2.290(4) 2_655
O12 Mo3 2.303(4) 2_655
