#------------------------------------------------------------------------------
#$Date: 2016-03-25 17:07:58 +0200 (Fri, 25 Mar 2016) $
#$Revision: 180004 $
#$URL: svn://www.crystallography.net/cod/cif/7/02/98/7029821.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7029821
loop_
_publ_author_name
'Zhang, Lei'
'Kuang, Xiaofei'
'Wu, Xiaoyuan'
'Yang, Wenbin'
'Lu, Canzhong'
_publ_section_title
;
 Supramolecular interactions induced hinge-like motion of a metal-organic
 framework accompanied by anisotropic thermal expansion.
;
_journal_issue                   19
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              7146
_journal_page_last               7152
_journal_paper_doi               10.1039/c3dt53580k
_journal_volume                  43
_journal_year                    2014
_chemical_formula_sum            'C72 H48 Ag4 Mo8 N24 O26'
_chemical_formula_weight         2864.34
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 115.315(4)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   22.0700(7)
_cell_length_b                   16.4328(4)
_cell_length_c                   25.6173(12)
_cell_measurement_reflns_used    16591
_cell_measurement_temperature    250.01(10)
_cell_measurement_theta_max      29.0530
_cell_measurement_theta_min      3.1930
_cell_volume                     8398.5(6)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      250.01(10)
_diffrn_detector_area_resol_mean 10.3503
_diffrn_measured_fraction_theta_full 0.972
_diffrn_measured_fraction_theta_max 0.972
_diffrn_measurement_device_type  'SuperNova, Dual, Cu at zero, Atlas'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  mirror
_diffrn_radiation_source         'SuperNova (Mo) X-ray Source'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0266
_diffrn_reflns_av_sigmaI/netI    0.0294
_diffrn_reflns_limit_h_max       21
_diffrn_reflns_limit_h_min       -26
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       30
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_number            19417
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         3.06
_exptl_absorpt_coefficient_mu    2.153
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.70344
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            brown
_exptl_crystal_density_diffrn    2.265
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block-like
_exptl_crystal_F_000             5520
_exptl_crystal_size_max          0.32
_exptl_crystal_size_mid          0.12
_exptl_crystal_size_min          0.09
_refine_diff_density_max         1.479
_refine_diff_density_min         -1.499
_refine_diff_density_rms         0.122
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.017
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     605
_refine_ls_number_reflns         7203
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.017
_refine_ls_R_factor_all          0.0401
_refine_ls_R_factor_gt           0.0337
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0477P)²+52.8779P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0885
_refine_ls_wR_factor_ref         0.0932
_reflns_number_gt                6278
_reflns_number_total             7203
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c3dt53580k2.cif
_cod_data_source_block           A_250K
_cod_depositor_comments
;Adding full bibliography for
 ./tmp-cod-update-bibliographies-12899/cifs/7029821.cif.
;
_cod_original_cell_volume        8398.5(5)
_cod_original_sg_symbol_H-M      C2/c
_cod_database_code               7029821
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Mo1 Mo 0.5000 0.40586(5) 0.2500 0.03572(17) Uani 1 2 d S
Mo2 Mo 0.51013(2) 0.29143(3) 0.143517(18) 0.02315(11) Uani 1 1 d .
Mo3 Mo 0.50133(2) 0.08883(3) 0.139441(17) 0.02217(11) Uani 1 1 d .
Mo4 Mo 0.5000 -0.03830(5) 0.2500 0.04002(19) Uani 1 2 d S
Mo5 Mo 0.591628(19) 0.19330(2) 0.291024(18) 0.02183(11) Uani 1 1 d .
O1 O 0.4427(2) 0.4671(3) 0.2004(2) 0.0575(12) Uani 1 1 d .
O2 O 0.54868(19) 0.3583(2) 0.21208(17) 0.0409(9) Uani 1 1 d .
O3 O 0.5790(2) 0.2871(3) 0.12969(19) 0.0467(10) Uani 1 1 d .
O4 O 0.4588(2) 0.3561(3) 0.09325(18) 0.0463(10) Uani 1 1 d .
O5 O 0.46703(18) 0.1900(2) 0.10644(16) 0.0351(9) Uani 1 1 d .
O6 O 0.5513(2) 0.1859(2) 0.21418(17) 0.0440(10) Uani 1 1 d .
O7 O 0.56428(19) 0.2822(2) 0.31558(17) 0.0379(9) Uani 1 1 d .
O8 O 0.67594(18) 0.1988(2) 0.31600(19) 0.0443(11) Uani 1 1 d .
O9 O 0.5760(2) 0.1046(3) 0.32319(18) 0.0444(10) Uani 1 1 d .
O10 O 0.4481(2) 0.0253(3) 0.08710(18) 0.0463(10) Uani 1 1 d .
O11 O 0.57371(19) 0.0831(3) 0.13110(18) 0.0438(10) Uani 1 1 d .
O12 O 0.53463(19) 0.0141(2) 0.20646(16) 0.0370(9) Uani 1 1 d .
O13 O 0.4377(4) -0.1011(4) 0.2055(3) 0.112(3) Uani 1 1 d .
Ag1 Ag 0.344170(19) -0.04239(3) -0.632204(17) 0.03280(12) Uani 1 1 d .
Ag2 Ag 0.32282(2) 0.25282(3) -0.132803(17) 0.03688(13) Uani 1 1 d .
C17 C 0.1239(2) 0.2568(3) -0.49814(19) 0.0197(10) Uani 1 1 d .
C18 C 0.0332(2) 0.3123(3) -0.5891(2) 0.0258(11) Uani 1 1 d .
H18A H 0.0549 0.2914 -0.6103 0.031 Uiso 1 1 calc R
C21 C 0.4441(2) 0.3435(3) -0.0352(2) 0.0250(10) Uani 1 1 d .
H21A H 0.4241 0.3156 -0.0151 0.030 Uiso 1 1 calc R
C23 C 0.5978(2) 0.4702(3) 0.0007(2) 0.0203(10) Uani 1 1 d .
C24 C 0.7780(2) 0.6379(3) 0.0092(2) 0.0273(11) Uani 1 1 d .
H24A H 0.7989 0.6342 0.0492 0.033 Uiso 1 1 calc R
C25 C 0.0600(2) 0.3018(3) -0.5302(2) 0.0207(10) Uani 1 1 d .
C26 C 0.2352(2) 0.0646(3) -0.6116(2) 0.0265(11) Uani 1 1 d .
H26A H 0.2132 0.0575 -0.6514 0.032 Uiso 1 1 calc R
C27 C 0.5036(2) 0.3837(3) -0.0037(2) 0.0247(10) Uani 1 1 d .
H27A H 0.5232 0.3823 0.0365 0.030 Uiso 1 1 calc R
C29 C 0.7201(2) 0.6521(3) -0.1078(2) 0.0254(11) Uani 1 1 d .
H29A H 0.6999 0.6566 -0.1478 0.030 Uiso 1 1 calc R
C32 C 0.2097(2) 0.2264(3) -0.4127(2) 0.0215(10) Uani 1 1 d .
C33 C 0.2979(2) 0.0843(3) -0.4953(2) 0.0230(10) Uani 1 1 d .
H33A H 0.3202 0.0888 -0.4554 0.028 Uiso 1 1 calc R
C36 C 0.5336(2) 0.4264(3) -0.03333(19) 0.0193(9) Uani 1 1 d .
C37 C 0.0260(2) 0.3353(3) -0.5004(2) 0.0274(11) Uani 1 1 d .
H37A H 0.0434 0.3306 -0.4604 0.033 Uiso 1 1 calc R
C38 C -0.0331(2) 0.3753(3) -0.5306(2) 0.0313(12) Uani 1 1 d .
H38A H -0.0554 0.3971 -0.5102 0.038 Uiso 1 1 calc R
C39 C 0.2433(2) 0.2371(3) -0.3490(2) 0.0236(10) Uani 1 1 d .
C40 C 0.6825(2) 0.5518(3) 0.0066(2) 0.0204(10) Uani 1 1 d .
C41 C 0.7155(2) 0.6015(3) -0.0225(2) 0.0220(10) Uani 1 1 d .
C42 C 0.6803(2) 0.5022(3) 0.0879(2) 0.0227(10) Uani 1 1 d .
C43 C 0.6791(3) 0.4559(4) 0.1810(2) 0.0347(13) Uani 1 1 d .
H43A H 0.6350 0.4384 0.1609 0.042 Uiso 1 1 calc R
C44 C 0.2054(2) 0.1721(3) -0.4949(2) 0.0208(10) Uani 1 1 d .
C45 C -0.0266(2) 0.3545(3) -0.6161(2) 0.0281(11) Uani 1 1 d .
H45A H -0.0438 0.3623 -0.6559 0.034 Uiso 1 1 calc R
C46 C 0.8074(3) 0.5049(3) 0.2425(2) 0.0351(13) Uani 1 1 d .
H46A H 0.8515 0.5216 0.2634 0.042 Uiso 1 1 calc R
C47 C 0.2359(2) 0.1214(3) -0.5256(2) 0.0207(10) Uani 1 1 d .
C48 C 0.3256(2) 0.0404(3) -0.5262(2) 0.0241(10) Uani 1 1 d .
H48A H 0.3676 0.0169 -0.5059 0.029 Uiso 1 1 calc R
C49 C 0.2038(2) 0.1099(3) -0.5850(2) 0.0250(10) Uani 1 1 d .
H49A H 0.1618 0.1325 -0.6066 0.030 Uiso 1 1 calc R
C50 C 0.7124(2) 0.4915(3) 0.1517(2) 0.0245(10) Uani 1 1 d .
C51 C 0.8079(3) 0.6798(3) -0.0210(2) 0.0293(11) Uani 1 1 d .
H51A H 0.8493 0.7043 0.0001 0.035 Uiso 1 1 calc R
C52 C 0.6865(2) 0.6100(3) -0.0817(2) 0.0224(10) Uani 1 1 d .
H52A H 0.6446 0.5875 -0.1038 0.027 Uiso 1 1 calc R
C53 C 0.5024(2) 0.4271(3) -0.0930(2) 0.0285(11) Uani 1 1 d .
H53A H 0.5206 0.4563 -0.1140 0.034 Uiso 1 1 calc R
C54 C 0.4436(2) 0.3835(3) -0.1210(2) 0.0297(11) Uani 1 1 d .
H54A H 0.4237 0.3827 -0.1612 0.036 Uiso 1 1 calc R
C55 C 0.7119(3) 0.4466(4) 0.2404(2) 0.0380(14) Uani 1 1 d .
H55A H 0.6890 0.4227 0.2596 0.046 Uiso 1 1 calc R
C56 C 0.2155(3) 0.2886(3) -0.3222(2) 0.0324(12) Uani 1 1 d .
H56A H 0.1770 0.3183 -0.3439 0.039 Uiso 1 1 calc R
C57 C 0.2458(3) 0.2952(4) -0.2628(2) 0.0361(13) Uani 1 1 d .
H57A H 0.2269 0.3302 -0.2453 0.043 Uiso 1 1 calc R
C58 C 0.3023(3) 0.1978(3) -0.3151(2) 0.0319(12) Uani 1 1 d .
H58A H 0.3241 0.1658 -0.3318 0.038 Uiso 1 1 calc R
C59 C 0.7783(3) 0.5167(3) 0.1833(2) 0.0323(12) Uani 1 1 d .
H59A H 0.8022 0.5409 0.1651 0.039 Uiso 1 1 calc R
C60 C 0.3284(3) 0.2072(4) -0.2559(2) 0.0402(14) Uani 1 1 d .
H60A H 0.3676 0.1792 -0.2333 0.048 Uiso 1 1 calc R
N1 N -0.06078(19) 0.3846(3) -0.58827(18) 0.0264(9) Uani 1 1 d .
N2 N 0.29547(19) 0.0302(2) -0.58330(17) 0.0236(9) Uani 1 1 d .
N3 N 0.3008(2) 0.2539(3) -0.22911(18) 0.0339(11) Uani 1 1 d .
N4 N 0.15295(19) 0.2680(2) -0.44090(17) 0.0233(9) Uani 1 1 d .
N5 N 0.14800(19) 0.2109(2) -0.52763(17) 0.0220(8) Uani 1 1 d .
N6 N 0.23813(19) 0.1776(2) -0.43735(17) 0.0230(9) Uani 1 1 d .
N7 N 0.4135(2) 0.3423(3) -0.09317(18) 0.0265(9) Uani 1 1 d .
N8 N 0.7802(2) 0.6868(2) -0.07857(18) 0.0251(9) Uani 1 1 d .
N9 N 0.7758(2) 0.4710(3) 0.27145(18) 0.0341(10) Uani 1 1 d .
N10 N 0.62287(19) 0.4624(2) 0.05853(17) 0.0237(9) Uani 1 1 d .
N11 N 0.62625(18) 0.5115(2) -0.02705(17) 0.0210(8) Uani 1 1 d .
N12 N 0.71152(19) 0.5495(2) 0.06460(17) 0.0246(9) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mo Mo -1.6832 0.6857 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O1 Mo1 O1 106.8(3) 2_655 .
O1 Mo1 O2 105.4(2) 2_655 2_655
O1 Mo1 O2 103.0(2) . 2_655
O1 Mo1 O2 103.0(2) 2_655 .
O1 Mo1 O2 105.4(2) . .
O2 Mo1 O2 131.4(2) 2_655 .
O3 Mo2 O4 103.7(2) . .
O3 Mo2 O5 98.96(18) . .
O4 Mo2 O5 97.93(19) . .
O3 Mo2 O2 97.32(19) . .
O4 Mo2 O2 103.1(2) . .
O5 Mo2 O2 149.42(16) . .
O3 Mo2 O7 165.15(18) . 2_655
O4 Mo2 O7 90.66(16) . 2_655
O5 Mo2 O7 82.61(15) . 2_655
O2 Mo2 O7 75.29(15) . 2_655
O3 Mo2 O6 92.47(18) . .
O4 Mo2 O6 162.45(18) . .
O5 Mo2 O6 72.39(14) . .
O2 Mo2 O6 81.22(15) . .
O7 Mo2 O6 73.83(15) 2_655 .
O10 Mo3 O11 103.6(2) . .
O10 Mo3 O5 100.31(18) . .
O11 Mo3 O5 102.25(18) . .
O10 Mo3 O12 100.20(19) . .
O11 Mo3 O12 93.12(18) . .
O5 Mo3 O12 150.60(16) . .
O10 Mo3 O9 90.68(18) . 2_655
O11 Mo3 O9 164.00(17) . 2_655
O5 Mo3 O9 81.91(16) . 2_655
O12 Mo3 O9 77.01(15) . 2_655
O10 Mo3 O6 166.17(18) . .
O11 Mo3 O6 90.04(18) . .
O5 Mo3 O6 74.08(15) . .
O12 Mo3 O6 81.09(15) . .
O9 Mo3 O6 76.12(15) 2_655 .
O13 Mo4 O13 105.6(6) . 2_655
O13 Mo4 O12 105.5(2) . 2_655
O13 Mo4 O12 107.8(3) 2_655 2_655
O13 Mo4 O12 107.8(3) . .
O13 Mo4 O12 105.5(2) 2_655 .
O12 Mo4 O12 123.4(2) 2_655 .
O8 Mo5 O9 105.6(2) . .
O8 Mo5 O7 107.70(18) . .
O9 Mo5 O7 110.14(18) . .
O8 Mo5 O6 111.7(2) . .
O9 Mo5 O6 110.57(19) . .
O7 Mo5 O6 111.00(19) . .
Mo1 O2 Mo2 125.0(2) . .
Mo3 O5 Mo2 121.30(19) . .
Mo5 O6 Mo2 129.5(2) . .
Mo5 O6 Mo3 141.0(2) . .
Mo2 O6 Mo3 88.94(13) . .
Mo5 O7 Mo2 128.7(2) . 2_655
Mo5 O9 Mo3 127.6(2) . 2_655
Mo4 O12 Mo3 136.8(2) . .
N1 Ag1 N2 123.72(15) 3_545 .
N1 Ag1 N9 129.27(16) 3_545 3_444
N2 Ag1 N9 106.96(15) . 3_444
N8 Ag2 N7 122.62(15) 3_445 .
N8 Ag2 N3 135.23(16) 3_445 .
N7 Ag2 N3 102.12(15) . .
N4 C17 N5 125.5(4) . .
N4 C17 C25 115.7(4) . .
N5 C17 C25 118.9(4) . .
C45 C18 C25 118.8(4) . .
N7 C21 C27 123.8(4) . .
N10 C23 N11 125.1(4) . .
N10 C23 C36 116.0(4) . .
N11 C23 C36 118.9(4) . .
C51 C24 C41 118.2(5) . .
C37 C25 C18 118.3(4) . .
C37 C25 C17 119.9(4) . .
C18 C25 C17 121.8(4) . .
N2 C26 C49 123.7(5) . .
C21 C27 C36 118.5(4) . .
N8 C29 C52 123.5(5) . .
N6 C32 N4 125.0(4) . .
N6 C32 C39 118.5(4) . .
N4 C32 C39 116.5(4) . .
C48 C33 C47 118.5(4) . .
C27 C36 C53 118.7(4) . .
C27 C36 C23 118.5(4) . .
C53 C36 C23 122.7(4) . .
C38 C37 C25 119.0(5) . .
C37 C38 N1 123.5(4) . .
C58 C39 C56 118.2(5) . .
C58 C39 C32 122.0(4) . .
C56 C39 C32 119.9(4) . .
N11 C40 N12 124.7(4) . .
N11 C40 C41 117.6(4) . .
N12 C40 C41 117.7(4) . .
C24 C41 C52 118.3(4) . .
C24 C41 C40 121.0(4) . .
C52 C41 C40 120.7(4) . .
N10 C42 N12 125.4(4) . .
N10 C42 C50 116.9(4) . .
N12 C42 C50 117.7(4) . .
C55 C43 C50 119.4(5) . .
N6 C44 N5 125.1(4) . .
N6 C44 C47 117.8(4) . .
N5 C44 C47 117.1(4) . .
N1 C45 C18 123.6(5) . .
N9 C46 C59 124.0(5) . .
C33 C47 C49 118.0(4) . .
C33 C47 C44 120.6(4) . .
C49 C47 C44 121.3(4) . .
C33 C48 N2 123.7(4) . .
C26 C49 C47 119.0(4) . .
C59 C50 C43 118.4(5) . .
C59 C50 C42 119.5(4) . .
C43 C50 C42 122.0(4) . .
C24 C51 N8 123.5(5) . .
C29 C52 C41 119.5(4) . .
C36 C53 C54 118.7(5) . .
N7 C54 C53 123.5(5) . .
N9 C55 C43 122.6(5) . .
C57 C56 C39 119.1(5) . .
C56 C57 N3 123.4(5) . .
C60 C58 C39 118.5(5) . .
C46 C59 C50 118.4(5) . .
N3 C60 C58 124.0(5) . .
C45 N1 C38 116.8(4) . .
C45 N1 Ag1 123.2(3) . 3_455
C38 N1 Ag1 119.8(3) . 3_455
C26 N2 C48 117.0(4) . .
C26 N2 Ag1 120.8(3) . .
C48 N2 Ag1 122.1(3) . .
C60 N3 C57 116.6(5) . .
C60 N3 Ag2 127.8(4) . .
C57 N3 Ag2 114.4(3) . .
C17 N4 C32 115.0(4) . .
C17 N5 C44 114.5(4) . .
C32 N6 C44 115.0(4) . .
C54 N7 C21 116.7(4) . .
C54 N7 Ag2 127.7(3) . .
C21 N7 Ag2 115.0(3) . .
C29 N8 C51 117.1(4) . .
C29 N8 Ag2 115.7(3) . 3
C51 N8 Ag2 127.2(3) . 3
C55 N9 C46 117.2(4) . .
C55 N9 Ag1 130.4(4) . 3_556
C46 N9 Ag1 112.3(3) . 3_556
C23 N10 C42 114.7(4) . .
C40 N11 C23 115.3(4) . .
C42 N12 C40 114.6(4) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Mo1 O1 1.689(5) 2_655
Mo1 O1 1.689(5) .
Mo1 O2 1.898(4) 2_655
Mo1 O2 1.898(4) .
Mo2 O3 1.703(4) .
Mo2 O4 1.680(4) .
Mo2 O5 1.952(4) .
Mo2 O2 1.934(4) .
Mo2 O7 2.300(4) 2_655
Mo2 O6 2.388(4) .
Mo3 O10 1.709(4) .
Mo3 O11 1.702(4) .
Mo3 O5 1.872(4) .
Mo3 O12 1.979(4) .
Mo3 O9 2.301(4) 2_655
Mo3 O6 2.371(4) .
Mo4 O13 1.708(6) .
Mo4 O13 1.708(6) 2_655
Mo4 O12 1.816(4) 2_655
Mo4 O12 1.816(4) .
Mo5 O8 1.692(4) .
Mo5 O9 1.779(4) .
Mo5 O7 1.795(4) .
Mo5 O6 1.784(4) .
O7 Mo2 2.300(4) 2_655
O9 Mo3 2.301(4) 2_655
Ag1 N1 2.256(4) 3_545
Ag1 N2 2.302(4) .
Ag1 N9 2.287(4) 3_444
Ag2 N8 2.260(4) 3_445
Ag2 N7 2.337(4) .
Ag2 N3 2.302(4) .
C17 N4 1.338(6) .
C17 N5 1.329(6) .
C17 C25 1.491(6) .
C18 C45 1.386(7) .
C18 C25 1.375(7) .
C21 N7 1.344(6) .
C21 C27 1.380(7) .
C23 N10 1.346(6) .
C23 N11 1.321(6) .
C23 C36 1.494(6) .
C24 C51 1.395(7) .
C24 C41 1.400(7) .
C25 C37 1.392(7) .
C26 N2 1.338(6) .
C26 C49 1.378(7) .
C27 C36 1.392(7) .
C29 N8 1.341(6) .
C29 C52 1.379(7) .
C32 N6 1.333(6) .
C32 N4 1.336(6) .
C32 C39 1.485(7) .
C33 C48 1.392(7) .
C33 C47 1.391(7) .
C36 C53 1.383(7) .
C37 C38 1.368(7) .
C38 N1 1.343(6) .
C39 C58 1.379(7) .
C39 C56 1.387(7) .
C40 N11 1.344(6) .
C40 N12 1.343(6) .
C40 C41 1.490(6) .
C41 C52 1.376(7) .
C42 N10 1.335(6) .
C42 N12 1.336(6) .
C42 C50 1.488(7) .
C43 C55 1.386(7) .
C43 C50 1.384(7) .
C44 N6 1.339(6) .
C44 N5 1.344(6) .
C44 C47 1.489(6) .
C45 N1 1.336(6) .
C46 N9 1.336(7) .
C46 C59 1.385(8) .
C47 C49 1.390(7) .
C48 N2 1.333(6) .
C50 C59 1.390(7) .
C51 N8 1.339(7) .
C53 C54 1.384(7) .
C54 N7 1.346(6) .
C55 N9 1.351(7) .
C56 C57 1.380(7) .
C57 N3 1.336(7) .
C58 C60 1.382(8) .
C60 N3 1.338(7) .
N1 Ag1 2.256(4) 3_455
N8 Ag2 2.260(4) 3
N9 Ag1 2.287(4) 3_556
