#------------------------------------------------------------------------------
#$Date: 2016-02-13 21:28:24 +0200 (Sat, 13 Feb 2016) $
#$Revision: 176429 $
#$URL: svn://www.crystallography.net/cod/cif/7/03/48/7034870.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7034870
loop_
_publ_author_name
'Dong, Yongkwan'
'Eckert, Brian'
'Wang, Hsin'
'Zeng, Xiaoyu'
'Tritt, Terry M.'
'Nolas, George S.'
_publ_section_title
;
 Synthesis, crystal structure, and transport properties of
 Cu2.2Zn0.8SnSe4-xTex (0.1 ≤ x ≤ 0.4).
;
_journal_issue                   19
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              9014
_journal_page_last               9019
_journal_paper_doi               10.1039/c5dt00910c
_journal_volume                  44
_journal_year                    2015
_chemical_formula_sum            'Cu2.2 Se3.69 Sn Te0.31 Zn0.8'
_chemical_formula_weight         641.72
_chemical_name_systematic        ' ?'
_space_group_IT_number           121
_symmetry_cell_setting           tetragonal
_symmetry_space_group_name_Hall  'I -4 2'
_symmetry_space_group_name_H-M   'I -4 2 m'
_audit_creation_date             2014-12-15T15:06
_audit_creation_method           'from EXP file using GSAS2CIF'
_audit_update_record
' 2014-12-15T15:06  Initial CIF as created by GSAS2CIF'
_cell_angle_alpha                90.0
_cell_angle_beta                 90.0
_cell_angle_gamma                90.0
_cell_formula_units_Z            2
_cell_length_a                   5.70846(32)
_cell_length_b                   5.70846
_cell_length_c                   11.3823(8)
_cell_volume                     370.91(3)
_computing_structure_refinement  GSAS
_diffrn_radiation_polarisn_ratio 0.87
_diffrn_radiation_probe          x-ray
_exptl_absorpt_correction_T_max  1.00311
_exptl_absorpt_correction_T_min  1.00311
_exptl_absorpt_process_details
;   GSAS Absorption/surface roughness correction: function number 0
 Debye-Scherrer absorption correction
Term (= MU.r/wave) =    -0.60779E-03
Correction is refined.
;
_pd_block_id
2014-12-15T15:06|SE36TE04_1|Se36Te04.cif|Bruker_D8
_pd_calc_method                  'Rietveld Refinement'
_pd_instr_location               ' ?'
_pd_meas_2theta_range_inc        0.01998
_pd_meas_2theta_range_max        100.00214
_pd_meas_2theta_range_min        15.0
_pd_meas_number_of_points        4256
_pd_phase_name
'from E:/USF/USF data/PXRD/YD143/refinements/Se36Te04/Se36Te04.cel'
_pd_proc_2theta_range_inc        0.01998
_pd_proc_2theta_range_max        100.00214
_pd_proc_2theta_range_min        15.0
_pd_proc_info_datetime           2014-12-15T15:06:06
_pd_proc_info_excluded_regions   ' ?'
_pd_proc_ls_background_function
;   GSAS Background function number 2 with  3 terms.
 Cosine Fourier series
      1:    3423.43     2:   -823.022     3:    713.478    
;
_pd_proc_ls_peak_cutoff          0.00050
_pd_proc_ls_profile_function
;
 CW Profile function number 3 with  19 terms
 Pseudovoigt profile coefficients as parameterized in
 P. Thompson, D.E. Cox & J.B. Hastings (1987). J. Appl. Cryst.,20,79-83.
 Asymmetry correction of L.W. Finger, D.E. Cox & A. P. Jephcoat (1994).
 J. Appl. Cryst.,27,892-900.
 Peak tails are ignored  where the intensity is below 0.0005 times the peak
   Aniso. broadening axis   0.0   0.0   1.0
;
_pd_proc_ls_prof_R_factor        0.0487
_pd_proc_ls_prof_wR_expected     0.0166
_pd_proc_ls_prof_wR_factor       0.0655
_pd_proc_number_of_points        4256
_pd_spec_mounting                ' ?'
_refine_ls_goodness_of_fit_all   3.95
_refine_ls_matrix_type           full
_refine_ls_number_parameters     18
_refine_ls_number_restraints     0
_refine_ls_R_Fsqd_factor         0.15988
_refine_ls_shift/su_max          1.19
_refine_ls_shift/su_mean         0.18
_reflns_d_resolution_high        1.008
_reflns_d_resolution_low         5.691
_reflns_limit_h_max              5
_reflns_limit_h_min              0
_reflns_limit_k_max              4
_reflns_limit_k_min              0
_reflns_limit_l_max              11
_reflns_limit_l_min              0
_reflns_number_total             151
_cod_data_source_file            c5dt00910c2.cif
_cod_data_source_block           SE36TE04_1_publ
_cod_depositor_comments
;
The following automatic conversions were performed:

'_geom_bond_publ_flag' value 'N' changed to 'n' according to
/usr/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26 (42
times).

'_geom_angle_publ_flag' value 'N' changed to 'n' according to
/usr/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26 (132
times).

Automatic conversion script
Id: cif_fix_values 3271 2015-04-21 07:52:19Z andrius 

 Adding full bibliography for 7034870--7034873.cif.
;
_cod_original_cell_volume        370.91(6)
_cod_original_formula_sum        'Cu2.20 Se3.69 Sn Te0.31 Zn0.80'
_cod_database_code               7034870
#BEGIN Tags that were not found in dictionaries:
_gsas_exptl_extinct_corr_t_min   1.00000
_gsas_exptl_extinct_corr_t_max   1.00000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_site_id
_symmetry_equiv_pos_as_xyz
1 +x,+y,+z
2 +y,-x,-z
3 -x,-y,+z
4 -y,+x,-z
5 -x,+y,-z
6 +y,+x,+z
7 +x,-y,-z
8 -y,-x,+z
101 +x+1/2,+y+1/2,+z+1/2
102 +y+1/2,-x+1/2,-z+1/2
103 -x+1/2,-y+1/2,+z+1/2
104 -y+1/2,+x+1/2,-z+1/2
105 -x+1/2,+y+1/2,-z+1/2
106 +y+1/2,+x+1/2,+z+1/2
107 +x+1/2,-y+1/2,-z+1/2
108 -y+1/2,-x+1/2,+z+1/2
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_thermal_displace_type
_atom_site_U_iso_or_equiv
_atom_site_symmetry_multiplicity
Cu Cu1 0.0 0.5 0.25 1.0 Uiso 0.0136(31) 4
Cu Cu2 0.0 0.0 0.0 0.19968 Uiso 0.048(4) 2
Zn Zn 0.0 0.0 0.0 0.8 Uiso 0.048(4) 2
Sn Sn 0.0 0.0 0.5 1.0 Uiso 0.0329(23) 2
Se Se 0.24255 0.24255 0.12923 0.9229 Uiso 0.0190(16) 8
Te Te 0.24255 0.24255 0.12923 0.07731 Uiso 0.0190(16) 8
loop_
_atom_type_symbol
_atom_type_number_in_cell
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_Cromer_Mann_a1
_atom_type_scat_Cromer_Mann_a2
_atom_type_scat_Cromer_Mann_a3
_atom_type_scat_Cromer_Mann_a4
_atom_type_scat_Cromer_Mann_b1
_atom_type_scat_Cromer_Mann_b2
_atom_type_scat_Cromer_Mann_b3
_atom_type_scat_Cromer_Mann_b4
_atom_type_scat_Cromer_Mann_c
_atom_type_scat_source
Cu 4.399 0.000 0.000 13.3380 3.58280 7.16760 0.24700 5.61580 11.3966 1.67350
64.8126 1.19100 International_Tables_Vol_C
Zn 1.6 0.000 0.000 14.0743 3.26550 7.03180 0.23330 5.16520 10.3163 2.41000
58.7097 1.30410 International_Tables_Vol_C
Sn 2.0 0.000 0.000 19.1889 5.83030 19.1005 0.50310 4.45850 26.8909 2.46630
83.9571 4.78210 International_Tables_Vol_C
Se 7.383 0.000 0.000 17.0006 2.40980 5.81960 0.27260 3.97310 15.2372 4.35430
43.8163 2.84090 International_Tables_Vol_C
Te 0.618 0.000 0.000 19.9644 4.81742 19.0138 0.42088 6.14487 28.5284 2.52390
70.8403 4.35200 International_Tables_Vol_C
loop_
_diffrn_radiation_wavelength
_diffrn_radiation_wavelength_wt
_diffrn_radiation_type
_diffrn_radiation_wavelength_id
1.540600 1.000 K\a~1~ 1
1.544400 0.500 K\a~2~ 2
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Se Cu1 Se 111.505(5) 1_555 3_565 n
Se Cu1 Se 108.4641(24) 1_555 102_455 n
Se Cu1 Se 108.4641(24) 1_555 104_555 n
Se Cu1 Te 0.0 1_555 1_555 n
Se Cu1 Te 111.505(5) 1_555 3_565 n
Se Cu1 Te 108.4641(24) 1_555 102_455 n
Se Cu1 Te 108.4641(24) 1_555 104_555 n
Se Cu1 Se 108.4641(24) 3_565 102_455 n
Se Cu1 Se 108.4641(24) 3_565 104_555 n
Se Cu1 Te 111.505(5) 3_565 1_555 n
Se Cu1 Te 0.0 3_565 3_565 n
Se Cu1 Te 108.4641(24) 3_565 102_455 n
Se Cu1 Te 108.4641(24) 3_565 104_555 n
Se Cu1 Se 111.505(5) 102_455 104_555 n
Se Cu1 Te 108.4641(24) 102_455 1_555 n
Se Cu1 Te 108.4641(24) 102_455 3_565 n
Se Cu1 Te 0.0 102_455 102_455 n
Se Cu1 Te 111.505(5) 102_455 104_555 n
Se Cu1 Te 108.4641(24) 104_555 1_555 n
Se Cu1 Te 108.4641(24) 104_555 3_565 n
Se Cu1 Te 111.505(5) 104_555 102_455 n
Se Cu1 Te 0.0 104_555 104_555 n
Te Cu1 Te 111.505(5) 1_555 3_565 n
Te Cu1 Te 108.4641(24) 1_555 102_455 n
Te Cu1 Te 108.4641(24) 1_555 104_555 n
Te Cu1 Te 108.4641(24) 3_565 102_455 n
Te Cu1 Te 108.4641(24) 3_565 104_555 n
Te Cu1 Te 111.505(5) 102_455 104_555 n
Se Cu2 Se 111.1453(26) 1_555 2_555 n
Se Cu2 Se 106.173(5) 1_555 3_555 n
Se Cu2 Se 111.1453(26) 1_555 4_555 n
Se Cu2 Te 0.0 1_555 1_555 n
Se Cu2 Te 111.1453(26) 1_555 2_555 n
Se Cu2 Te 106.173(5) 1_555 3_555 n
Se Cu2 Te 111.1453(26) 1_555 4_555 n
Se Cu2 Se 111.1453(26) 2_555 3_555 n
Se Cu2 Se 106.173(5) 2_555 4_555 n
Se Cu2 Te 111.1453(26) 2_555 1_555 n
Se Cu2 Te 0.0 2_555 2_555 n
Se Cu2 Te 111.1453(26) 2_555 3_555 n
Se Cu2 Te 106.173(5) 2_555 4_555 n
Se Cu2 Se 111.1453(26) 3_555 4_555 n
Se Cu2 Te 106.173(5) 3_555 1_555 n
Se Cu2 Te 111.1453(26) 3_555 2_555 n
Se Cu2 Te 0.0 3_555 3_555 n
Se Cu2 Te 111.1453(26) 3_555 4_555 n
Se Cu2 Te 111.1453(26) 4_555 1_555 n
Se Cu2 Te 106.173(5) 4_555 2_555 n
Se Cu2 Te 111.1453(26) 4_555 3_555 n
Se Cu2 Te 0.0 4_555 4_555 n
Te Cu2 Te 111.1453(26) 1_555 2_555 n
Te Cu2 Te 106.173(5) 1_555 3_555 n
Te Cu2 Te 111.1453(26) 1_555 4_555 n
Te Cu2 Te 111.1453(26) 2_555 3_555 n
Te Cu2 Te 106.173(5) 2_555 4_555 n
Te Cu2 Te 111.1453(26) 3_555 4_555 n
Se Zn Se 111.1453(26) 1_555 2_555 n
Se Zn Se 106.173(5) 1_555 3_555 n
Se Zn Se 111.1453(26) 1_555 4_555 n
Se Zn Te 0.0 1_555 1_555 n
Se Zn Te 111.1453(26) 1_555 2_555 n
Se Zn Te 106.173(5) 1_555 3_555 n
Se Zn Te 111.1453(26) 1_555 4_555 n
Se Zn Se 111.1453(26) 2_555 3_555 n
Se Zn Se 106.173(5) 2_555 4_555 n
Se Zn Te 111.1453(26) 2_555 1_555 n
Se Zn Te 0.0 2_555 2_555 n
Se Zn Te 111.1453(26) 2_555 3_555 n
Se Zn Te 106.173(5) 2_555 4_555 n
Se Zn Se 111.1453(26) 3_555 4_555 n
Se Zn Te 106.173(5) 3_555 1_555 n
Se Zn Te 111.1453(26) 3_555 2_555 n
Se Zn Te 0.0 3_555 3_555 n
Se Zn Te 111.1453(26) 3_555 4_555 n
Se Zn Te 111.1453(26) 4_555 1_555 n
Se Zn Te 106.173(5) 4_555 2_555 n
Se Zn Te 111.1453(26) 4_555 3_555 n
Se Zn Te 0.0 4_555 4_555 n
Te Zn Te 111.1453(26) 1_555 2_555 n
Te Zn Te 106.173(5) 1_555 3_555 n
Te Zn Te 111.1453(26) 1_555 4_555 n
Te Zn Te 111.1453(26) 2_555 3_555 n
Te Zn Te 106.173(5) 2_555 4_555 n
Te Zn Te 111.1453(26) 3_555 4_555 n
Se Sn Se 109.4944(25) 101_445 102_455 n
Se Sn Se 109.425(5) 101_445 103_555 n
Se Sn Se 109.4944(25) 101_445 104_545 n
Se Sn Te 0.0 101_445 101_445 n
Se Sn Te 109.4944(25) 101_445 102_455 n
Se Sn Te 109.425(5) 101_445 103_555 n
Se Sn Te 109.4944(25) 101_445 104_545 n
Se Sn Se 109.4944(25) 102_455 103_555 n
Se Sn Se 109.425(5) 102_455 104_545 n
Se Sn Te 109.4944(25) 102_455 101_445 n
Se Sn Te 0.0 102_455 102_455 n
Se Sn Te 109.4944(25) 102_455 103_555 n
Se Sn Te 109.425(5) 102_455 104_545 n
Se Sn Se 109.4944(25) 103_555 104_545 n
Se Sn Te 109.425(5) 103_555 101_445 n
Se Sn Te 109.4944(25) 103_555 102_455 n
Se Sn Te 0.0 103_555 103_555 n
Se Sn Te 109.4944(25) 103_555 104_545 n
Se Sn Te 109.4944(25) 104_545 101_445 n
Se Sn Te 109.425(5) 104_545 102_455 n
Se Sn Te 109.4944(25) 104_545 103_555 n
Se Sn Te 0.0 104_545 104_545 n
Te Sn Te 109.4944(25) 101_445 102_455 n
Te Sn Te 109.425(5) 101_445 103_555 n
Te Sn Te 109.4944(25) 101_445 104_545 n
Te Sn Te 109.4944(25) 102_455 103_555 n
Te Sn Te 109.425(5) 102_455 104_545 n
Te Sn Te 109.4944(25) 103_555 104_545 n
Cu1 Se Cu1 111.430(5) 1_555 6_555 n
Cu1 Se Cu2 110.9588(24) 1_555 1_555 n
Cu1 Se Zn 110.9588(24) 1_555 1_555 n
Cu1 Se Sn 107.7582(25) 1_555 101_554 n
Cu1 Se Cu2 110.9588(24) 6_555 1_555 n
Cu1 Se Zn 110.9588(24) 6_555 1_555 n
Cu1 Se Sn 107.7582(25) 6_555 101_554 n
Cu2 Se Zn 0.0 1_555 1_555 n
Cu2 Se Sn 107.799(5) 1_555 101_554 n
Zn Se Sn 107.799(5) 1_555 101_554 n
Cu1 Te Cu1 111.430(5) 1_555 6_555 n
Cu1 Te Cu2 110.9588(24) 1_555 1_555 n
Cu1 Te Zn 110.9588(24) 1_555 1_555 n
Cu1 Te Sn 107.7582(25) 1_555 101_554 n
Cu1 Te Cu2 110.9588(24) 6_555 1_555 n
Cu1 Te Zn 110.9588(24) 6_555 1_555 n
Cu1 Te Sn 107.7582(25) 6_555 101_554 n
Cu2 Te Zn 0.0 1_555 1_555 n
Cu2 Te Sn 107.799(5) 1_555 101_554 n
Zn Te Sn 107.799(5) 1_555 101_554 n
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Cu1 Se 2.44267(11) 1_555 n
Cu1 Se 2.44267(11) 3_565 n
Cu1 Se 2.44267(11) 102_455 n
Cu1 Se 2.44267(11) 104_555 n
Cu1 Te 2.44267(11) 1_555 n
Cu1 Te 2.44267(11) 3_565 n
Cu1 Te 2.44267(11) 102_455 n
Cu1 Te 2.44267(11) 104_555 n
Cu2 Se 2.44902(11) 1_555 n
Cu2 Se 2.44902(11) 2_555 n
Cu2 Se 2.44902(11) 3_555 n
Cu2 Se 2.44902(11) 4_555 n
Cu2 Te 2.44902(11) 1_555 n
Cu2 Te 2.44902(11) 2_555 n
Cu2 Te 2.44902(11) 3_555 n
Cu2 Te 2.44902(11) 4_555 n
Zn Se 2.44902(11) 1_555 n
Zn Se 2.44902(11) 2_555 n
Zn Se 2.44902(11) 3_555 n
Zn Se 2.44902(11) 4_555 n
Zn Te 2.44902(11) 1_555 n
Zn Te 2.44902(11) 2_555 n
Zn Te 2.44902(11) 3_555 n
Zn Te 2.44902(11) 4_555 n
Sn Se 2.54623(11) 101_445 n
Sn Se 2.54623(11) 102_455 n
Sn Se 2.54623(11) 103_555 n
Sn Se 2.54623(11) 104_545 n
Sn Te 2.54623(11) 101_445 n
Sn Te 2.54623(11) 102_455 n
Sn Te 2.54623(11) 103_555 n
Sn Te 2.54623(11) 104_545 n
Se Cu1 2.44267(11) 1_555 n
Se Cu1 2.44267(11) 6_555 n
Se Cu2 2.44902(11) 1_555 n
Se Zn 2.44902(11) 1_555 n
Se Sn 2.54623(11) 101_554 n
Te Cu1 2.44267(11) 1_555 n
Te Cu1 2.44267(11) 6_555 n
Te Cu2 2.44902(11) 1_555 n
Te Zn 2.44902(11) 1_555 n
Te Sn 2.54623(11) 101_554 n
loop_
_pd_meas_counts_total
_pd_proc_ls_weight
_pd_proc_intensity_bkg_calc
_pd_calc_intensity_total
4170.0 0.0002398 3246.34180 3251.52246
4219.0 0.0002370 3246.16724 3251.70801
4159.0 0.0002404 3245.99268 3251.93237
4137.0 0.0002417 3245.81738 3252.20215
4182.0 0.0002391 3245.64209 3252.52295
4240.0 0.0002358 3245.46680 3252.90503
4289.0 0.0002332 3245.29126 3253.35693
4316.0 0.0002317 3245.11548 3253.89185
4241.0 0.0002358 3244.93945 3254.52417
4181.0 0.0002392 3244.76318 3255.27344
4204.0 0.0002379 3244.58667 3256.16260
4235.0 0.0002361 3244.41016 3257.22095
4165.0 0.0002401 3244.23315 3258.48682
4128.0 0.0002422 3244.05640 3260.01196
4212.0 0.0002374 3243.87891 3261.87183
4258.0 0.0002349 3243.70166 3264.18677
4224.0 0.0002367 3243.52393 3267.17407
4186.0 0.0002389 3243.34595 3271.25049
4300.0 0.0002326 3243.16797 3277.21216
4142.0 0.0002414 3242.98975 3286.52075
4248.0 0.0002354 3242.81152 3301.62988
4262.0 0.0002346 3242.63281 3327.25732
4326.0 0.0002312 3242.45386 3366.13135
4173.0 0.0002396 3242.27490 3424.78857
4275.0 0.0002339 3242.09546 3505.82397
4325.0 0.0002312 3241.91602 3609.57495
4355.0 0.0002296 3241.73657 3729.69263
4391.0 0.0002277 3241.55664 3851.37769
4350.0 0.0002299 3241.37646 3951.07007
4456.0 0.0002244 3241.19629 4002.64380
4507.0 0.0002219 3241.01587 3991.51367
4411.0 0.0002267 3240.83521 3922.59937
4394.0 0.0002276 3240.65430 3815.17090
4414.0 0.0002266 3240.47339 3693.46948
4330.0 0.0002309 3240.29199 3577.92480
4118.0 0.0002428 3240.11060 3480.75049
4200.0 0.0002381 3239.92871 3406.34961
4095.0 0.0002442 3239.74707 3353.67456
4047.0 0.0002471 3239.56494 3318.67212
4169.0 0.0002399 3239.38257 3296.44751
4101.0 0.0002438 3239.20020 3282.60693
4068.0 0.0002458 3239.01758 3273.86768
4151.0 0.0002409 3238.83472 3268.08228
4157.0 0.0002406 3238.65161 3263.97949
4010.0 0.0002494 3238.46826 3260.86743
4085.0 0.0002448 3238.28491 3258.37744
4004.0 0.0002498 3238.10132 3256.31689
4021.0 0.0002487 3237.91748 3254.57471
4162.0 0.0002403 3237.73340 3253.08154
4090.0 0.0002445 3237.54907 3251.78882
4034.0 0.0002479 3237.36475 3250.66138
4082.0 0.0002450 3237.18018 3249.67090
4055.0 0.0002466 3236.99536 3248.79565
4013.0 0.0002492 3236.81030 3248.01880
4060.0 0.0002463 3236.62500 3247.32544
3981.0 0.0002512 3236.43970 3246.70459
4075.0 0.0002454 3236.25391 3246.14673
4040.0 0.0002475 3236.06812 3245.64404
4134.0 0.0002419 3235.88208 3245.19019
3961.0 0.0002525 3235.69604 3244.78027
4142.0 0.0002414 3235.50928 3244.40967
3881.0 0.0002577 3235.32275 3244.07446
4015.0 0.0002491 3235.13599 3243.77222
4064.0 0.0002461 3234.94897 3243.50073
3970.0 0.0002519 3234.76172 3243.25757
3863.0 0.0002589 3234.57446 3243.04053
4047.0 0.0002471 3234.38696 3242.84961
4059.0 0.0002464 3234.19897 3242.68311
3999.0 0.0002501 3234.01099 3242.54053
3980.0 0.0002513 3233.82275 3242.42163
4000.0 0.0002500 3233.63452 3242.32593
3993.0 0.0002504 3233.44580 3242.25366
4016.0 0.0002490 3233.25708 3242.20557
3925.0 0.0002548 3233.06812 3242.18140
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4248.0 . . .
