#------------------------------------------------------------------------------
#$Date: 2017-03-05 07:27:40 +0200 (Sun, 05 Mar 2017) $
#$Revision: 193879 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/05/59/7055969.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7055969
loop_
_publ_author_name
'Dodds, Christopher A.'
'Hobday, Claire L.'
'Kennedy, Alan R.'
'McKellar, Scott C.'
'Smillie, Katy'
'Walls, Aiden'
_publ_section_title
;
 Ag(i) bipyridyl coordination polymers containing functional anions
;
_journal_issue                   4
_journal_name_full               'New J. Chem.'
_journal_page_first              1574
_journal_paper_doi               10.1039/C6NJ03555H
_journal_volume                  41
_journal_year                    2017
_chemical_formula_sum            'C28 H26 Ag N7 O4 S'
_chemical_formula_weight         664.49
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_audit_update_record
;
2016-11-14 deposited with the CCDC.
2017-01-19 downloaded from the CCDC.
;
_cell_angle_alpha                109.697(4)
_cell_angle_beta                 101.688(3)
_cell_angle_gamma                98.473(3)
_cell_formula_units_Z            2
_cell_length_a                   7.1356(5)
_cell_length_b                   14.0212(11)
_cell_length_c                   15.4526(9)
_cell_measurement_reflns_used    6049
_cell_measurement_temperature    120(2)
_cell_measurement_theta_max      27.48
_cell_measurement_theta_min      1.00
_cell_volume                     1385.86(17)
_computing_cell_refinement       DENZO
_computing_data_collection       COLLLECT
_computing_data_reduction        'DENZO and SADABS'
_computing_molecular_graphics    MERCURY
_computing_publication_material  SHELXL
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    SIR92
_diffrn_ambient_temperature      120(2)
_diffrn_measured_fraction_theta_full 0.996
_diffrn_measured_fraction_theta_max 0.908
_diffrn_measurement_device_type  'Nonius Kappa CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'rotating anode'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0681
_diffrn_reflns_av_sigmaI/netI    0.0949
_diffrn_reflns_limit_h_max       9
_diffrn_reflns_limit_h_min       -9
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       19
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_number            25884
_diffrn_reflns_theta_full        27.00
_diffrn_reflns_theta_max         28.42
_diffrn_reflns_theta_min         3.40
_exptl_absorpt_coefficient_mu    0.851
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.783495
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   sadabs
_exptl_crystal_colour            orange
_exptl_crystal_density_diffrn    1.592
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       'cut block'
_exptl_crystal_F_000             676
_exptl_crystal_size_max          0.14
_exptl_crystal_size_mid          0.08
_exptl_crystal_size_min          0.05
_refine_diff_density_max         0.801
_refine_diff_density_min         -0.541
_refine_diff_density_rms         0.102
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.052
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     376
_refine_ls_number_reflns         6336
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.052
_refine_ls_R_factor_all          0.1008
_refine_ls_R_factor_gt           0.0567
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0283P)²+1.6632P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0841
_refine_ls_wR_factor_ref         0.0932
_reflns_number_gt                4638
_reflns_number_total             6336
_reflns_threshold_expression     I>\2s(I)
_cod_data_source_file            c6nj03555h2.cif
_cod_data_source_block           dw2dye
_cod_depositor_comments
'Adding full bibliography for 7055960--7055969.cif.'
_cod_original_cell_volume        1385.85(17)
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7055969
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Ag1 Ag 0.78416(4) 0.47028(2) 0.427511(18) 0.02956(10) Uani 1 1 d .
S1 S 0.05592(13) 0.24639(7) 0.38647(6) 0.0261(2) Uani 1 1 d .
O1 O -0.1063(4) 0.29310(19) 0.36394(16) 0.0341(6) Uani 1 1 d .
O2 O 0.2097(4) 0.31468(18) 0.47103(16) 0.0339(6) Uani 1 1 d .
O3 O -0.0113(4) 0.14398(18) 0.38875(16) 0.0329(6) Uani 1 1 d .
O4 O -0.6113(4) -0.0651(2) -0.37108(17) 0.0354(6) Uani 1 1 d .
N1 N 0.0128(5) 0.1355(2) 0.0221(2) 0.0321(7) Uani 1 1 d .
N2 N -0.1706(5) 0.1226(2) 0.0085(2) 0.0319(7) Uani 1 1 d .
N3 N 0.7980(4) 0.5013(2) 0.30076(18) 0.0245(6) Uani 1 1 d .
N4 N 0.7448(4) 0.4584(2) -0.03629(18) 0.0269(7) Uani 1 1 d .
N5 N 0.7365(4) 0.4728(2) -0.12246(19) 0.0265(7) Uani 1 1 d .
N6 N 0.7249(4) 0.4304(2) -0.45591(18) 0.0240(6) Uani 1 1 d .
C1 C 0.3646(5) 0.2389(3) 0.3048(2) 0.0269(8) Uani 1 1 d .
H1 H 0.4473 0.2604 0.3678 0.032 Uiso 1 1 calc R
C2 C 0.1619(5) 0.2243(3) 0.2891(2) 0.0247(8) Uani 1 1 d .
C3 C 0.0384(5) 0.1909(3) 0.1966(2) 0.0257(8) Uani 1 1 d .
H3 H -0.1003 0.1801 0.1858 0.031 Uiso 1 1 calc R
C4 C 0.1225(5) 0.1738(3) 0.1206(2) 0.0275(8) Uani 1 1 d .
C5 C 0.3246(5) 0.1902(3) 0.1370(3) 0.0319(8) Uani 1 1 d .
H5 H 0.3810 0.1793 0.0848 0.038 Uiso 1 1 calc R
C6 C 0.4454(5) 0.2222(3) 0.2284(3) 0.0313(8) Uani 1 1 d .
H6 H 0.5840 0.2327 0.2388 0.038 Uiso 1 1 calc R
C7 C -0.2760(5) 0.0800(3) -0.0900(2) 0.0289(8) Uani 1 1 d .
C8 C -0.4789(5) 0.0573(3) -0.1101(2) 0.0328(9) Uani 1 1 d .
H8 H -0.5389 0.0736 -0.0590 0.039 Uiso 1 1 calc R
C9 C -0.5973(5) 0.0110(3) -0.2039(2) 0.0321(8) Uani 1 1 d .
H9 H -0.7367 -0.0033 -0.2171 0.039 Uiso 1 1 calc R
C10 C -0.5068(5) -0.0141(3) -0.2781(2) 0.0296(8) Uani 1 1 d .
C11 C -0.3028(5) 0.0115(3) -0.2585(2) 0.0299(8) Uani 1 1 d .
H11 H -0.2425 -0.0029 -0.3095 0.036 Uiso 1 1 calc R
C12 C -0.1874(5) 0.0578(3) -0.1651(2) 0.0294(8) Uani 1 1 d .
H12 H -0.0480 0.0745 -0.1519 0.035 Uiso 1 1 calc R
C13 C 0.8088(5) 0.4243(3) 0.2222(2) 0.0268(8) Uani 1 1 d .
H13 H 0.8259 0.3600 0.2265 0.032 Uiso 1 1 calc R
C14 C 0.7960(5) 0.4352(3) 0.1358(2) 0.0284(8) Uani 1 1 d .
H14 H 0.8032 0.3788 0.0822 0.034 Uiso 1 1 calc R
C15 C 0.7727(5) 0.5286(3) 0.1273(2) 0.0244(8) Uani 1 1 d .
C16 C 0.7680(5) 0.6088(3) 0.2091(2) 0.0264(8) Uani 1 1 d .
H16 H 0.7572 0.6750 0.2074 0.032 Uiso 1 1 calc R
C17 C 0.7790(5) 0.5917(3) 0.2933(2) 0.0273(8) Uani 1 1 d .
H17 H 0.7728 0.6469 0.3481 0.033 Uiso 1 1 calc R
C18 C 0.7585(5) 0.5426(3) 0.0347(2) 0.0249(8) Uani 1 1 d .
C19 C 0.7575(7) 0.6476(3) 0.0313(3) 0.0425(10) Uani 1 1 d .
H19A H 0.8740 0.6985 0.0785 0.064 Uiso 1 1 calc R
H19B H 0.6385 0.6681 0.0458 0.064 Uiso 1 1 calc R
H19C H 0.7595 0.6452 -0.0327 0.064 Uiso 1 1 calc R
C20 C 0.7157(5) 0.3879(3) -0.1941(2) 0.0260(8) Uani 1 1 d .
C21 C 0.6964(7) 0.2809(3) -0.1931(3) 0.0418(10) Uani 1 1 d .
H21A H 0.6999 0.2839 -0.1284 0.063 Uiso 1 1 calc R
H21B H 0.8055 0.2525 -0.2126 0.063 Uiso 1 1 calc R
H21C H 0.5713 0.2359 -0.2375 0.063 Uiso 1 1 calc R
C22 C 0.7118(5) 0.4012(3) -0.2863(2) 0.0227(7) Uani 1 1 d .
C23 C 0.6876(5) 0.4933(3) -0.2971(2) 0.0253(8) Uani 1 1 d .
H23 H 0.6680 0.5484 -0.2462 0.030 Uiso 1 1 calc R
C24 C 0.6920(5) 0.5045(3) -0.3817(2) 0.0243(8) Uani 1 1 d .
H24 H 0.6708 0.5673 -0.3883 0.029 Uiso 1 1 calc R
C25 C 0.7438(5) 0.3406(3) -0.4463(2) 0.0258(8) Uani 1 1 d .
H25 H 0.7627 0.2867 -0.4984 0.031 Uiso 1 1 calc R
C26 C 0.7370(5) 0.3226(3) -0.3639(2) 0.0268(8) Uani 1 1 d .
H26 H 0.7494 0.2574 -0.3604 0.032 Uiso 1 1 calc R
N1S N 0.0701(7) 0.1396(3) 0.6448(3) 0.0737(13) Uani 1 1 d .
C1S C 0.3028(7) 0.0993(3) 0.5357(3) 0.0531(12) Uani 1 1 d .
H2S H 0.4058 0.0709 0.5637 0.080 Uiso 1 1 calc R
H3S H 0.3633 0.1637 0.5302 0.080 Uiso 1 1 calc R
H1S H 0.2282 0.0484 0.4722 0.080 Uiso 1 1 calc R
C2S C 0.1718(8) 0.1214(3) 0.5961(3) 0.0536(12) Uani 1 1 d .
H1H H -0.727(7) -0.088(4) -0.373(3) 0.071(17) Uiso 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
N6 Ag1 N3 171.63(10) 1_556 .
N6 Ag1 Ag1 77.06(7) 1_556 2_766
N3 Ag1 Ag1 111.30(7) . 2_766
O2 S1 O1 113.38(15) . .
O2 S1 O3 112.69(14) . .
O1 S1 O3 112.13(15) . .
O2 S1 C2 106.58(15) . .
O1 S1 C2 105.42(15) . .
O3 S1 C2 105.89(15) . .
C10 O4 H1H 108(3) . .
N2 N1 C4 114.5(3) . .
N1 N2 C7 113.2(3) . .
C17 N3 C13 117.4(3) . .
C17 N3 Ag1 122.6(2) . .
C13 N3 Ag1 119.7(2) . .
C18 N4 N5 113.6(3) . .
C20 N5 N4 113.5(3) . .
C25 N6 C24 117.0(3) . .
C25 N6 Ag1 123.7(2) . 1_554
C24 N6 Ag1 118.7(2) . 1_554
C6 C1 C2 119.6(3) . .
C6 C1 H1 120.2 . .
C2 C1 H1 120.2 . .
C1 C2 C3 120.7(3) . .
C1 C2 S1 120.2(3) . .
C3 C2 S1 119.1(3) . .
C4 C3 C2 118.8(3) . .
C4 C3 H3 120.6 . .
C2 C3 H3 120.6 . .
C5 C4 C3 120.2(3) . .
C5 C4 N1 115.3(3) . .
C3 C4 N1 124.5(3) . .
C6 C5 C4 120.8(3) . .
C6 C5 H5 119.6 . .
C4 C5 H5 119.6 . .
C5 C6 C1 119.9(3) . .
C5 C6 H6 120.0 . .
C1 C6 H6 120.0 . .
C8 C7 C12 119.4(3) . .
C8 C7 N2 116.2(3) . .
C12 C7 N2 124.3(3) . .
C7 C8 C9 121.3(3) . .
C7 C8 H8 119.4 . .
C9 C8 H8 119.4 . .
C8 C9 C10 118.7(3) . .
C8 C9 H9 120.7 . .
C10 C9 H9 120.7 . .
O4 C10 C11 117.4(3) . .
O4 C10 C9 122.3(3) . .
C11 C10 C9 120.3(3) . .
C12 C11 C10 120.2(3) . .
C12 C11 H11 119.9 . .
C10 C11 H11 119.9 . .
C11 C12 C7 120.0(3) . .
C11 C12 H12 120.0 . .
C7 C12 H12 120.0 . .
N3 C13 C14 122.7(3) . .
N3 C13 H13 118.6 . .
C14 C13 H13 118.6 . .
C13 C14 C15 120.1(3) . .
C13 C14 H14 120.0 . .
C15 C14 H14 120.0 . .
C14 C15 C16 117.1(3) . .
C14 C15 C18 121.2(3) . .
C16 C15 C18 121.6(3) . .
C17 C16 C15 119.6(3) . .
C17 C16 H16 120.2 . .
C15 C16 H16 120.2 . .
N3 C17 C16 123.1(3) . .
N3 C17 H17 118.5 . .
C16 C17 H17 118.5 . .
N4 C18 C19 126.4(3) . .
N4 C18 C15 114.1(3) . .
C19 C18 C15 119.5(3) . .
C18 C19 H19A 109.5 . .
C18 C19 H19B 109.5 . .
H19A C19 H19B 109.5 . .
C18 C19 H19C 109.5 . .
H19A C19 H19C 109.5 . .
H19B C19 H19C 109.5 . .
N5 C20 C21 126.7(3) . .
N5 C20 C22 114.8(3) . .
C21 C20 C22 118.5(3) . .
C20 C21 H21A 109.5 . .
C20 C21 H21B 109.5 . .
H21A C21 H21B 109.5 . .
C20 C21 H21C 109.5 . .
H21A C21 H21C 109.5 . .
H21B C21 H21C 109.5 . .
C23 C22 C26 117.6(3) . .
C23 C22 C20 121.2(3) . .
C26 C22 C20 121.2(3) . .
C24 C23 C22 119.7(3) . .
C24 C23 H23 120.1 . .
C22 C23 H23 120.1 . .
N6 C24 C23 123.2(3) . .
N6 C24 H24 118.4 . .
C23 C24 H24 118.4 . .
N6 C25 C26 123.2(3) . .
N6 C25 H25 118.4 . .
C26 C25 H25 118.4 . .
C25 C26 C22 119.3(3) . .
C25 C26 H26 120.4 . .
C22 C26 H26 120.4 . .
C2S C1S H2S 109.5 . .
C2S C1S H3S 109.5 . .
H2S C1S H3S 109.5 . .
C2S C1S H1S 109.5 . .
H2S C1S H1S 109.5 . .
H3S C1S H1S 109.5 . .
N1S C2S C1S 179.1(6) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ag1 N6 2.158(3) 1_556
Ag1 N3 2.162(3) .
Ag1 Ag1 3.2235(6) 2_766
S1 O2 1.447(2) .
S1 O1 1.451(3) .
S1 O3 1.460(2) .
S1 C2 1.775(3) .
O4 C10 1.359(4) .
O4 H1H 0.83(5) .
N1 N2 1.258(4) .
N1 C4 1.435(4) .
N2 C7 1.425(4) .
N3 C17 1.335(4) .
N3 C13 1.351(4) .
N4 C18 1.287(4) .
N4 N5 1.404(4) .
N5 C20 1.288(4) .
N6 C25 1.339(4) .
N6 C24 1.352(4) .
N6 Ag1 2.158(3) 1_554
C1 C6 1.382(5) .
C1 C2 1.389(5) .
C1 H1 0.9500 .
C2 C3 1.399(4) .
C3 C4 1.390(5) .
C3 H3 0.9500 .
C4 C5 1.383(5) .
C5 C6 1.380(5) .
C5 H5 0.9500 .
C6 H6 0.9500 .
C7 C8 1.382(5) .
C7 C12 1.398(5) .
C8 C9 1.394(5) .
C8 H8 0.9500 .
C9 C10 1.397(5) .
C9 H9 0.9500 .
C10 C11 1.390(5) .
C11 C12 1.384(5) .
C11 H11 0.9500 .
C12 H12 0.9500 .
C13 C14 1.380(4) .
C13 H13 0.9500 .
C14 C15 1.389(5) .
C14 H14 0.9500 .
C15 C16 1.391(5) .
C15 C18 1.495(4) .
C16 C17 1.390(4) .
C16 H16 0.9500 .
C17 H17 0.9500 .
C18 C19 1.492(5) .
C19 H19A 0.9800 .
C19 H19B 0.9800 .
C19 H19C 0.9800 .
C20 C21 1.492(5) .
C20 C22 1.494(4) .
C21 H21A 0.9800 .
C21 H21B 0.9800 .
C21 H21C 0.9800 .
C22 C23 1.387(5) .
C22 C26 1.392(5) .
C23 C24 1.373(4) .
C23 H23 0.9500 .
C24 H24 0.9500 .
C25 C26 1.388(4) .
C25 H25 0.9500 .
C26 H26 0.9500 .
N1S C2S 1.143(6) .
C1S C2S 1.444(7) .
C1S H2S 0.9800 .
C1S H3S 0.9800 .
C1S H1S 0.9800 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
C4 N1 N2 C7 -177.2(3) .
N6 Ag1 N3 C17 91.3(8) 1_556
Ag1 Ag1 N3 C17 -92.2(2) 2_766
N6 Ag1 N3 C13 -82.7(8) 1_556
Ag1 Ag1 N3 C13 93.9(2) 2_766
C18 N4 N5 C20 -177.6(3) .
C6 C1 C2 C3 1.2(5) .
C6 C1 C2 S1 -179.5(3) .
O2 S1 C2 C1 21.6(3) .
O1 S1 C2 C1 142.4(3) .
O3 S1 C2 C1 -98.6(3) .
O2 S1 C2 C3 -159.1(3) .
O1 S1 C2 C3 -38.3(3) .
O3 S1 C2 C3 80.7(3) .
C1 C2 C3 C4 -0.7(5) .
S1 C2 C3 C4 180.0(3) .
C2 C3 C4 C5 -0.3(5) .
C2 C3 C4 N1 177.4(3) .
N2 N1 C4 C5 -178.9(3) .
N2 N1 C4 C3 3.2(5) .
C3 C4 C5 C6 1.0(5) .
N1 C4 C5 C6 -177.0(3) .
C4 C5 C6 C1 -0.5(5) .
C2 C1 C6 C5 -0.6(5) .
N1 N2 C7 C8 175.9(3) .
N1 N2 C7 C12 -2.2(5) .
C12 C7 C8 C9 1.1(5) .
N2 C7 C8 C9 -177.0(3) .
C7 C8 C9 C10 1.1(5) .
C8 C9 C10 O4 175.9(3) .
C8 C9 C10 C11 -3.1(5) .
O4 C10 C11 C12 -176.1(3) .
C9 C10 C11 C12 2.9(5) .
C10 C11 C12 C7 -0.7(5) .
C8 C7 C12 C11 -1.3(5) .
N2 C7 C12 C11 176.6(3) .
C17 N3 C13 C14 -1.7(5) .
Ag1 N3 C13 C14 172.6(3) .
N3 C13 C14 C15 0.6(5) .
C13 C14 C15 C16 1.5(5) .
C13 C14 C15 C18 180.0(3) .
C14 C15 C16 C17 -2.3(5) .
C18 C15 C16 C17 179.1(3) .
C13 N3 C17 C16 0.7(5) .
Ag1 N3 C17 C16 -173.4(2) .
C15 C16 C17 N3 1.3(5) .
N5 N4 C18 C19 2.6(5) .
N5 N4 C18 C15 -178.5(3) .
C14 C15 C18 N4 8.3(5) .
C16 C15 C18 N4 -173.3(3) .
C14 C15 C18 C19 -172.8(3) .
C16 C15 C18 C19 5.7(5) .
N4 N5 C20 C21 1.4(5) .
N4 N5 C20 C22 -178.4(3) .
N5 C20 C22 C23 -13.8(5) .
C21 C20 C22 C23 166.4(3) .
N5 C20 C22 C26 164.7(3) .
C21 C20 C22 C26 -15.2(5) .
C26 C22 C23 C24 -0.9(5) .
C20 C22 C23 C24 177.6(3) .
C25 N6 C24 C23 3.4(5) .
Ag1 N6 C24 C23 -168.1(2) 1_554
C22 C23 C24 N6 -2.0(5) .
C24 N6 C25 C26 -2.0(5) .
Ag1 N6 C25 C26 169.1(2) 1_554
N6 C25 C26 C22 -0.8(5) .
C23 C22 C26 C25 2.2(5) .
C20 C22 C26 C25 -176.3(3) .
